CN1643664A - Plasma processing method, detecting method of completion of seasoning, plasma processing apparatus - Google Patents
Plasma processing method, detecting method of completion of seasoning, plasma processing apparatus Download PDFInfo
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- CN1643664A CN1643664A CN 03805861 CN03805861A CN1643664A CN 1643664 A CN1643664 A CN 1643664A CN 03805861 CN03805861 CN 03805861 CN 03805861 A CN03805861 A CN 03805861A CN 1643664 A CN1643664 A CN 1643664A
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- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/67—Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
- H01L21/67005—Apparatus not specifically provided for elsewhere
- H01L21/67242—Apparatus for monitoring, sorting or marking
- H01L21/67276—Production flow monitoring, e.g. for increasing throughput
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/67—Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
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Abstract
With analysis data in the prior art, it is difficult to find out if a change regarded as a judgmental standard of the completion of seasoning has come from a change due to the seasoning, namely, change in condition of the interior of a processing container or come from another change based on a temperature change among respective dummy wafers and furthermore, it is difficult to judge whether the seasoning has been completed or not. Therefore, a plasma processing method of the present invention, which is a method for detecting the completion of seasoning in performing the seasoning by loading dummy wafers W into a processing container 2 of a plasma processing apparatus 1, includes a process of creating a predictive formula for predicting the completion of seasoning and another process of detecting the completion of seasoning in performing the seasoning, based on the predictive formula.
Description
Technical field
The present invention relates to employed method of plasma processing and aging detection of end method and plasma processing apparatus in a kind of etch processes device etc.
Background technology
For example, processing unit such as etch processes device has: the container handling of air tight construction; That in this container handling, dispose and keep the maintenance body of handled object, be constructed such that in container handling, to produce plasma, handled object is carried out predetermined process.Then, if continue the processing of handled object, polluted by secondary product etc. in the container handling, internal part is depleted.For this reason, temporarily stop processing unit, just carry out the interior cleaning of container handling or the maintenance works such as replacing of loss product.Then, after safeguarding end, restart processing unit.
For example under the situation of etch processes device, puppet (dummy) wafer to the regulation number is provided in the container handling when restarting repeats etching cycle, adjusts to desired state when producing in the container handling, carries out so-called aging (seasoning).Etch uniformity in aging end " Invest, Then Investigate " etch-rate and wafer face etc.The measurement data of the luminescent spectrum that use the measurement data that obtains from a plurality of dummy wafers when aging, is for example obtained by endpoint detector is carried out data analysis.Then, aging whether the end judged in the variation of observing these analysis data.
But in existing analysis data, the variation that becomes the aging judgment standard that finishes changes because of aging, promptly is difficult to judge whether to change according to the state variation in the container handling, is difficult to judge whether to change according to the variations in temperature between each dummy wafer.Therefore, have to be difficult to judge wear out whether finish such problem.
That is, the present inventor for example uses a kind of main component analysis as multi-variables analysis, as described later measurement data is carried out data analysis, but in this analysis result, the big peak value that expression changes confirms there are two, is difficult to judge aging whether the end.Here, this main component analysis is described.By the method same, gather measurement data in this case with prior art.For example, 130 dummy wafers were provided, entered production process and provide 30 dummy wafers to carry out etching in second day in first day.The measurement data of the luminescent spectrum that use obtains respectively from the 51st～60 dummy wafer of first day and the 121st～130 dummy wafer is carried out principal component analysis, and Fig. 8 A, Fig. 8 B and Fig. 9 A, Fig. 9 B represent the analysis result that obtains.In this principal component analysis, use the wavelength that is in 297 kinds in 193nm～419nm short wavelength zone in the luminescent spectrum, for a dummy wafer, measured 18 each Wavelength strengths in per 3 seconds at 1 minute, carry out principal component analysis according to these measurement data.Then, principal component test statistics (invocation point) and residual error when obtaining each measurement respectively, with HOTELLINGS TSQUARE (quadratic sum of principal component test statistics) curve plotting is Fig. 8 A, Fig. 9 A, is Fig. 8 B, Fig. 9 B with quadratic sum (residual test statistic) curve plotting of residual error.Know that from these analysis results the data of first day data and second day have big peak value simultaneously in any curve, are difficult to judge aging end.In addition, the transverse axis of each curve represents to measure number of times.
The present invention makes in order to address the above problem, and its purpose is, provides a kind of and can clearly judge aging method of plasma processing and aging detection of end method and the plasma processing apparatus that finishes.
Present inventors etc. carry out various discussions to the reason of confirming these two kinds of peak values, and its result is judged as the acquisition method that reason is present in employed measurement data in the data analysis.So, by in container handling, carrying out specific processing when the image data, obtain promptly getting rid of the influence that causes by the variations in temperature between dummy wafer to draw a conclusion, reliably grasp the variation that causes by aging, just can judge aging end reliably.
Summary of the invention
The present invention is based on that above-mentioned opinion makes, the described method of plasma processing of claim 1 of the present invention, the test handled object is provided in the container handling to processing unit, above-mentioned aging end when detection is worn out, it is characterized in that, comprise: the step that forms prediction type, to above-mentioned test handled object is provided in the above-mentioned container handling, after in the above-mentioned container handling of cooling, a plurality of measurement data that use obtains when a plurality of above-mentioned tests are provided once more in to above-mentioned container handling with handled object, carry out multi-variables analysis, form the prediction type of the described aging end of prediction; Based on above-mentioned prediction type, detect the step carry out above-mentioned aging end when aging.
The described method of plasma processing of claim 2 of the present invention is characterized in that, in the described invention of claim 1, uses principal component analysis as above-mentioned multi-variables analysis.
The described method of plasma processing of claim 3 of the present invention is characterized in that, in claim 1 or 2 described inventions, uses luminescence of plasma spectrum to be used as above-mentioned measurement data.
The described method of plasma processing of claim 4 of the present invention is characterized in that, in the described invention of claim 3, uses wavelength high to the influence degree of residual error in the wavelength of above-mentioned luminescent spectrum.
The described method of plasma processing of claim 5 of the present invention is characterized in that, in claim 1 or 2 described inventions, uses by electricity and calculates the resulting high frequency voltage of measurement mechanism as above-mentioned measurement data.
The described method of plasma processing of claim 6 of the present invention is characterized in that, in claim 1 or 2 described inventions, uses the high-frequency current that is obtained by electricity calculating measurement mechanism as above-mentioned measurement data.
The described method of plasma processing of claim 7 of the present invention is characterized in that, in claim 1 or 2 described inventions, uses by electricity and calculates high frequency voltage that measurement mechanism obtains and the phase difference of high-frequency current is used as above-mentioned measurement data.
The described aging detection of end method of claim 8 of the present invention, the test handled object is provided in the container handling to processing unit, above-mentioned aging end when detection is worn out, it is characterized in that, comprise: the step that forms prediction type, to above-mentioned test handled object is provided in the above-mentioned container handling, after in the above-mentioned container handling of cooling, a plurality of measurement data that use obtains when a plurality of above-mentioned tests are provided once more in the above-mentioned container handling with handled object, carry out multi-variables analysis, form the prediction type of the described aging end of prediction; Detect the step of carrying out above-mentioned aging end when aging based on above-mentioned prediction type.
The described plasma processing apparatus of claim 9 of the present invention is characterized in that having: the container handling of accommodating handled object; Measure the detector of the luminescence of plasma spectrum in this container handling; Be connected with this detector, input is from the control device of the measurement data of this detector, when it provides test to wear out with handled object in to above-mentioned container handling, to above-mentioned test handled object is provided in the above-mentioned container handling, after in the above-mentioned container handling of cooling, when in to above-mentioned container handling, providing a plurality of above-mentioned tests to use handled object once more, based on a plurality of measurement data by above-mentioned detectors measure, use the multi-variables analysis program to carry out multi-variables analysis, form the prediction type of the above-mentioned aging end of prediction, detect based on this prediction type and carry out above-mentioned aging end when aging.
The described plasma processing apparatus of claim 10 of the present invention is characterized in that having: the container handling of accommodating handled object; The electricity that is provided with in this container handling calculates measurement mechanism; Calculating measurement mechanism with this electricity is connected, the control device of the measurement data of measurement mechanism is calculated in input from this electricity, when it provides test to wear out with handled object in to above-mentioned container handling, to above-mentioned test handled object is provided in the above-mentioned container handling, after in the above-mentioned container handling of cooling, when in to above-mentioned container handling, providing a plurality of above-mentioned tests to use handled object once more, based on a plurality of measurement data by above-mentioned detectors measure, use the multi-variables analysis program to carry out multi-variables analysis, form the prediction type of the above-mentioned aging end of prediction, based on this prediction type, detect and to carry out above-mentioned aging end when aging.
Description of drawings
Fig. 1 is the pie graph of an example of the expression plasma processing apparatus that uses the analytical method of aging data of the present invention and method of plasma processing and aging detection of end method.
Fig. 2 A, Fig. 2 B are the figure about the analysis result of the measurement data of plasma processing apparatus shown in Figure 1 that is obtained by one embodiment of the present invention, Fig. 2 A is the curve chart of change of quadratic sum of the principal component test statistics of expression measurement data, and Fig. 2 B is the curve chart of change of the residual test statistic of expression measurement data.
Fig. 3 A, Fig. 3 B are the figure of the analysis result that obtained by other execution mode of the present invention of expression, are respectively the curve charts that is equivalent to Fig. 2 A, Fig. 2 B.
Fig. 4 is to the curve chart of the influence degree of the residual error of the measurement data of the luminescent spectrum that uses in expression other execution mode of the present invention.
Fig. 5 A, Fig. 5 B are the figure that the analysis result that wavelength mean value shown in Figure 4 obtains is used in expression, are respectively the curve charts that is equivalent to Fig. 2 A, Fig. 2 B.
Fig. 6 A, Fig. 6 B are the figure that the analysis result that wavelength shown in Figure 4 obtains is used in expression, are respectively the curve charts that is equivalent to Fig. 2 A, Fig. 2 B.
Fig. 7 is the pie graph of other example of the expression plasma processing apparatus that uses the analytical method of aging data of the present invention and aging detection of end method.
Fig. 8 A, Fig. 8 B are the figure of the analysis result that obtained by existing analytical method of expression, the curve chart that is equivalent to Fig. 2 A, Fig. 2 B respectively when using the 51st～60 dummy wafer of aging first day.
Fig. 9 A, Fig. 9 B are the figure of other analysis result of being obtained by existing analytical method of expression, the curve chart that is equivalent to Fig. 2 A, Fig. 2 B respectively when using the 121st～130 dummy wafer of aging first day.
Embodiment
Below, to execution mode shown in Figure 7 the present invention is described based on Fig. 1.
The plasma apparatus 1 of present embodiment for example as shown in Figure 1, has: can keep the condition of high vacuum degree of wishing, surface to carry out alunite processing and container handling electrical ground 2; Be configured in bottom surface central authorities in this container handling 2 and the lower electrode 3 of mounting handled object (for example wafer) W; Support this lower electrode 3 from the below and be configured in the support 4 of the bottom surface of container handling 2 by insulating element 2A; With lower electrode 3 gapped settings and be formed with the upper electrode 5 of hollow shape.On lower electrode 3, connect for example high frequency electric source 6 of 2MHz, on upper electrode 5, connect the high frequency electric source 7 of for example 60MHz higher than the frequency of lower electrode 3 by adaptation 7A by adaptation 6A.On lower electrode 3, connect high pass filter 8, on upper electrode 5, connect low pass filter 9.In addition, on the exhaust outlet 2B of the bottom surface of container handling 2, connect exhaust apparatus 11, carry out vacuum exhaust in 11 pairs of container handlings 2 of this exhaust apparatus, keep the vacuum degree of hope by gas exhaust pipe 11A.And, below, as required lower electrode 3 and support 4 summarized and be called mounting table 10 and describe.
Upper central at upper electrode 5 forms gas introduction tube 5A, and this gas introduction tube 5A connects the upper central of container handling 2 by insulating element 2C.And this gas introduction tube 5A provides etching gas by gas supply pipe 13 connection processing gas supply sources 12 from this processing gas supply source 12.That is, handle gas supply source 12 and have C
5F
8 Gas supply source 12A, O
2 Gas supply source 12B and Ar gas supply source 12C, these each gas supply sources 12A, 12B, 12C are connected with branched pipe 13A, 13B, the 13C of gas supply pipe 13 respectively.On each branched pipe 13A, 13B, 13C, from upstream side downstream side be provided with in proper order and C
5F
8 Gas supply source 12A, O
2 Gas supply source 12B and the pairing volume control device 12D of Ar gas supply source 12C, 12E, 12F and valve 12G, 12H, 12I control to the regulation flow by these volume control devices 12D, 12E, 12F and valve 12G, 12H, 12I with the etching gas that provides in container handling 2.
Even dispersion forms a plurality of hole 5B below upper electrode 5, disperses equably to supply with in container handling 2 to handle gas from each hole 5B.Therefore, when vacuumizing in container handling 2, provide the state of the etching gas of regulation with the regulation flow from handling gas supply source 12 by exhaust apparatus 11, lower electrode 3 and upper electrode 5 are applied High frequency power respectively, in container handling 2, produce the plasma of etching gas, the etching that the wafer W on the lower electrode 3 is stipulated.Mounting temperature sensor (not shown) on this lower electrode 3 monitors the temperature of the wafer W on the lower electrode 3 all the time by temperature sensor.
In mounting table 10, form the coolant stream 10A of circulation regulation coolant (for example existing known fluorine class fluid, water etc.), in coolant stream 10A, cool off lower electrode 3 between flow periods at coolant, by lower electrode 3 cooling wafer W, wafer W is controlled to the temperature of hope.In addition, the electrostatic chuck 14 that configuration is made of insulating material on lower electrode 3 connects high-voltage DC power supply 15 on the battery lead plate 14A in electrostatic chuck 14.The static of electrostatic chuck 14 by being taken place on the surface by the high voltage that applies from 15 couples of battery lead plate 14A of high-voltage DC power supply comes the Electrostatic Absorption wafer W.Outer peripheral edges at lower electrode 3 dispose the focusing ring 16 that surrounds electrostatic chuck 14, and by focusing ring 16, plasma is pooled on the wafer W.
Form the gas flow path 10B that heat conductivity gases such as He gas are provided as backside gas on mounting table 10, gas flow path 10B is a plurality of positions opening on mounting table 10.These peristomes are consistent with formed through hole on the electrostatic chuck on the mounting table 10 14.Therefore, if provide backside gas to the gas flow path 10B of mounting table 10, backside gas flows out from the through hole of electrostatic chuck 13 through gas flow 10B, and the gap integral body of asking in electrostatic chuck 14 and wafer W spreads equably, improves the heat conductivity in gap.And, in Fig. 1, the 17th, open and close the family of power and influence that taking out of of the wafer W that forms moved into mouthful in container handling 2.
For example endpoint detector 18 is installed in plasma processing apparatus 1, is used this endpoint detector 18 to measure luminescence of plasma spectrum in the container handling 2, this measured value is input in the control device 19.These control device 19 stored for example principal component analysis with program as the multi-variables analysis program, make and to carry out principal component analysis by this program.This principal component analysis when burin-in process container 2, is used for analyzing the aging data of using with program.As the data analysis data, use the measurement data of the luminescent spectrum of endpoint detector 18.Use 1024 kinds of wavelength that for example are in 193nm～950nm scope as measurement data.
Here, the aging data analysing method of present embodiment is described, the taking of the promptly so-called measurement data of in forming the aging prediction type that finishes of prediction, using.That is, behind cleaning in container handling 2 and the replacing focusing ring running stores such as (not shown), for the stabilisation that realizes container handling 2 wears out in the following sequence.At first, after starting plasma processing apparatus 1 in first day, in container handling 2, provide dummy wafer (naked silicon chip) W.Afterwards, in container handling 2, provide etching gas,, apply for example High frequency power of 60MHz and 2MHz, carry out etching from high frequency electric source 6,7 at the state that keeps the specified vacuum degree from gas supply pipe 16.Repeat this processing for for example 130 dummy wafer W.The processing of 130 dummy wafer W finishes first day processing.
Afterwards, the processing that temporarily stops etching, the input power supply is promptly placed container handling 2 more than the several hrs at the state that can restart at once.Then, the container handling 2 itself and lower electrode 12 internal parts such as grade that will be become high temperature by etch processes are cooled to design temperature.
Then, in each container handling 2, providing for example 30 dummy wafer W under the production process condition once more, each dummy wafer W is being repeated etching cycle at second day.Owing to cool off in the container handling 2, so during carrying out etching from 30 of first dummy wafer W to the, the temperature of parts such as the interior lower electrode 12 of container handling 2 itself and container handling 2, focusing ring slowly rises in the zero hour of etching cycle.For in the present embodiment from 30 at first to the dummy wafer in moment that has variations in temperature of the 20th, measured 18 luminescent spectrums at about 1 minute, the luminous intensity of the wavelength of above-mentioned 297 kinds is used as the measurement data of principal component analysis.Therefore, these measurement data have reflected the variations in temperature in the container handling 2.
And, use above-mentioned measurement data to carry out principal component analysis.For example, if carry out the measurement of m time (being 18 * 20=360 time in the present embodiment) for 20 dummy wafers, in the measurement data that has n (luminous intensity of 297 wavelength in the present embodiment) of each time measurement at every turn, the matrix of measurement data input is by formula 1 expression so.The measurement data of the measurement wavelength that one-shot measurement obtains in the row of this matrix is its composition, and the measurement data that changes according to time of each wavelength in these row is its composition.And, in control device 19, obtain mean value, dispersion value, standard deviation based on each measurement data after, come standardization by mean value and standard deviation value.Use is carried out the principal component analysis of a plurality of measurement data based on the correlation matrix of these standardized values, obtains eigenvalue and its inherent vector.Eigenvalue is represented the size of the dispersion of each measurement data, according to the size order of eigenvalue, be defined as first principal component, Second principal component, ... the n principal component.In addition, there is the inherent vector (weight) that belongs to separately in each eigenvalue.Usually, the number of times of principal component is high more, and low more to the influence degree of the evaluation of data, its value is little.
Formula
In the present embodiment, 20 dummy wafers are carried out m time measurement, to each time measurement get n measurement data respectively at every turn, j the principal component corresponding with i j eigenvalue of measuring represented by formula 2.And, will be by concrete i measurement data (X that measures
I1, X
I2..., X
In) this j principal component t of substitution
IjThe value that obtains is j the principal component test statistics that i is measured.Therefore, the test statistics t of j principal component
jDefine the inherent vector P of j principal component by formula 3
jDefine by formula 4.And, with the test statistics t of j principal component
jUse matrix X and inherent vector P
jRepresent by formula 5.In addition, use principal component test statistics and inherent vector separately to represent matrix X by formula 6.
t
ij＝x
i1P
j1+x
i2P
j2+…+x
inP
jn
t
j＝xp
j
x＝t
1p
1 T+t
2p
2 T+…+t
np
n T
Wherein, Pn
TIt is the transposed matrix of Pn.
Therefore, in principal component analysis, both made multiple measurement data, for example first principal component and Second principal component, had both made manyly to be summarised as the statistics of minority to the 3rd principal component, only investigated the minority statistics, can grasp aging state, judge aging end.If for example the accumulative total influence degree of the eigenvalue of first, second principal component surpasses 90% usually, based on its reliability height of evaluation of first, second principal component.First principal component resembles the dispersion direction of representing the measurement data maximum above-mentioned, be suitable for grasping container handling 2 aging over time, the aging judgement that finishes.Can grasp by the residual test statistic by the variation that first, second principal component can not be grasped.Obtain first principal component in the present embodiment.
Thus, in the present embodiment, under the following conditions dummy wafer W is carried out etching, by the principal component analysis of measurement data at this moment, eigenvalue can use the correlation matrix of measurement data to obtain, and maximum eigenvalue is the dispersion of first principal component test statistics.The inherent vector of first principal component can use eigenvalue and correlation matrix to obtain.And, calculating the principal component test statistics of each measurement data, quadratic sum (HOTELLINGS TSQUARE) curve plotting with each principal component test statistics is the curve shown in Fig. 2 A.Indicated as this curve, only first day measurement data is seen big peak value, does not see big peak value second day measurement data, can reliably judge aging end.In addition, the quadratic sum curve plotting with the residual error of each measurement data is the curve shown in Fig. 2 B.In the figure, also only first day measurement data is seen big peak value, can reliably judge aging the end.And the transverse axis of each curve represents to measure number of times.In the present embodiment, a dummy wafer W is carried out 18 times measurement, and handled 160 dummy wafer W in the daytime, so have scale up to 18 * 160=2880 two.
Treatment conditions
Processing unit: capacitive coupling type parallel flat plasma processing apparatus
Dummy wafer (naked silicon chip): 300mm
The power supply high-frequency and the electric power of lower electrode: 2MHz, 3800W
The power supply high-frequency and the electric power of upper electrode: 60MHz, 3300W
Processing pressure: 25mTorr
Etching gas: C
5F
8=29sccm, Ar=750sccm, O
2=47sccm
Backside gas: He=15Torr (electrode central portion)
40Torr (electrode edge portion)
Treatment temperature: upper electrode=60 ℃, sidewall=60 ℃, lower electrode=20 ℃
In the present embodiment of above explanation, promptly as method according to the prediction type that forms the aging end of prediction, use dummy wafer W, after the stage that enters production process temporarily stops plasma processing apparatus 1 midway, container handling 2 is placed several hrs, after container handling 2 itself and cooling such as its inner lower electrode 12 parts such as grade, enter production process once more, during handling 20 dummy wafer W, collection is used to judge the aging measurement data that finishes, the measurement data of the variations in temperature of reflection container handling 2 itself and lower electrode 3 parts such as grade can be accessed, peak value can be got rid of based on variations in temperature by this analysis result.In addition, by when aging, using this analysis result, can reliable Detection, judge aging end.Therefore, after reliable Detection is aging,, can carry out stable etch processes to wafer by carrying out plasma treatment.
Fig. 3 A, Fig. 3 B are the figure of the data analysing method of expression other execution mode of the present invention.In the present embodiment, different from the embodiment described above, behind the mean value of obtaining 18 measurement data (297 kinds of wavelength) that obtain for each dummy wafer W, use these mean values to carry out principal component analysis, obtain eigenvalue and inherent vector.Then, with the quadratic sum of the principal component test statistics of each dummy wafer W and the quadratic sum curve plotting of residual error, be the curve shown in Fig. 3 A, Fig. 3 B.Indicated as Fig. 3 A, Fig. 3 B, can similarly judge aging end with the curve of the above-mentioned execution mode shown in Fig. 2 A, Fig. 2 B.And, the number of the numeric representation dummy wafer of transverse axis.
In addition, Fig. 4, Fig. 5 A, Fig. 5 B are the figure of the data analysing method of expression other execution mode of the present invention.In the present embodiment, as shown in Figure 4, (for example for example select 10 kinds of influential big wavelength of the residual error to measurement data, Fig. 4 by zero wavelength that is surrounded), for these 10 kinds of wavelength, the same with above-mentioned execution mode, each dummy wafer W obtained mean value after, use these mean values to carry out principal component analysis, obtain eigenvalue and inherent vector.And, with first principal component test statistics and the residual test statistic curve plotting of each dummy wafer W, be the curve shown in Fig. 5 A, Fig. 5 B.Indicated as Fig. 5 A, Fig. 5 B, with the execution mode shown in Fig. 2 A, Fig. 2 B relatively, the sawtooth of curve reduces, and is level and smooth curve, can judge aging end more simply.
In addition, Fig. 6 A, Fig. 6 B are the figure of the data analysing method of expression other execution mode of the present invention.In the present embodiment, identical with the execution mode shown in Fig. 5 A, Fig. 5 B, select the 10 kind wavelength high to the influence degree of residual error.And, in the execution mode shown in Fig. 5 A, Fig. 5 B, dummy wafer W is adopted the time average of the measurement data of each wavelength, but in the present embodiment, use the measurement data aspect identical with the situation shown in Fig. 2 A, Fig. 2 B.But, under the situation of Fig. 2 A, Fig. 2 B, the measurement data of the measurement wavelength that is obtained by one-shot measurement in the row of matrix is its composition, the measurement data that changes according to time of each wavelength in these row is its composition, but in the present embodiment, each of each dummy wafer W and each wavelength, the row and column transposition.Delegation is about 10 wavelength measurements 16 times, so have 10 * 16=160 kind composition.One row are included 20 of wafers in the training set, and the training set with principal component analysis of 20 kinds of compositions is the matrix of 20 row, 160 row.Based on this matrix, carry out principal component analysis equally with above-mentioned each execution mode, to the quadratic sum curve plotting of the quadratic sum and the residual error of principal component test statistics, be the curve shown in Fig. 6 A and Fig. 6 B.Indicated as Fig. 6 A, Fig. 6 B, with the curve ratio shown in Fig. 5 A, Fig. 5 B, for having reduced the more level and smooth curve of sawtooth, can judge aging end more simply.
In addition, plasma processing apparatus 20 shown in Figure 7 also can equally with above-mentioned plasma processing apparatus 1 use the present invention, can expect the action effect same with above-mentioned plasma processing apparatus 1.This plasma processing unit 20 has as shown in Figure 7: the container handling 21 that is made of conductive materials such as aluminium; The lower electrode 22 of that be provided with and mounting table double as mounting wafer W in bottom surface in this container handling 21; Above this lower electrode 22 at interval the interval of regulation be provided with and the double as etching gas upper electrode 23 of ground connection of the hollow form of portion is provided; The magnetic field that forms rotating magnetic field forms parts 24, under the control of control device 25, the electric field action that is taken place between two electrodes up and down to container handling 21 forms the rotating magnetic field B that parts 24 form by magnetic field, by high-density plasma wafer W is carried out uniform plasma treatment.
The gas supply pipe 26 that connection is communicated with upper electrode 23 on container handling 21 is supplied with etching gas by gas supply pipe 26 and upper electrode 23 from gas supply source (not shown) in container handling 21.Side at container handling 21 connects the gas outlet pipe 27 that is connected with not shown vacuum pumping hardware, by vacuum pumping hardware and gas outlet pipe 27, to decompression in the container handling 21, keeps the specified vacuum degree.Connect high frequency electric source 28 at lower electrode 22, apply High frequency power from high frequency electric source 28 to lower electrode 22, between two electrodes 22,23, produce the plasma of etching gas, the etch processes of on the semiconductor wafer W surface on the lower electrode 22, for example stipulating.
For example endpoint detector 29 is installed on plasma processing apparatus 20, is used this endpoint detector 29 to measure luminescence of plasma spectrum in the container handling 21, in this measured value input control device 25.These control device 25 stored for example the program used of principal component analysis make and carry out principal component analysis as the multi-variables analysis program by this program.This principal component analysis when burin-in process container 21, is used to analyze the data of aging usefulness with program.As the data analysis data, use the measurement data of the luminescent spectrum of endpoint detector 29.Use 1024 kinds the wavelength that for example is in 193nm～950nm scope as measurement data.
And in above-mentioned each execution mode, the analytical method as judging the aging data that finish is that example is illustrated with the principal component analysis, but also can uses other multi-variables analysis.In addition, in the respective embodiments described above, the situation of using luminescence of plasma spectrum has been described, but can use other measurement data, for example, the phase difference etc. that calculates high frequency voltage, high-frequency current, high frequency voltage and high-frequency current that measurement mechanism (VI probe) detect by the electricity that is provided with in plasma processing apparatus is subjected to the measurement data of the influence of temperature variation in the container handling easily.In addition, in the respective embodiments described above, be that example is illustrated with the etch processes device, but also the present invention can be used in other plasma processing apparatus.
As the described invention of claim 1 to 7 according to the present invention, can provide a kind of and can clearly judge aging method of plasma processing and aging detection of end method and the plasma processing apparatus that finishes.
Claims (10)
1. a method of plasma processing provides the test handled object in the container handling to processing unit, detects the described aging end when wearing out, and it is characterized in that, comprising:
Form the step of prediction type, to described test handled object is provided in the described container handling, after in the described container handling of cooling, a plurality of measurement data that use obtains when a plurality of described tests are provided once more in to described container handling with handled object, carry out multi-variables analysis, form the prediction type of the described aging end of prediction;
Based on described prediction type, detect the step carry out described aging end when aging.
2. method of plasma processing according to claim 1 is characterized in that, uses principal component analysis as described multi-variables analysis.
3. method of plasma processing according to claim 1 and 2 is characterized in that,
Use luminescence of plasma spectrum to be used as described measurement data.
4. method of plasma processing according to claim 3 is characterized in that,
Use wavelength high in the wavelength of described luminescent spectrum to the influence degree of residual error.
5. method of plasma processing according to claim 1 and 2 is characterized in that,
Use is calculated the resulting high frequency voltage of measurement mechanism as described measurement data by electricity.
6. method of plasma processing according to claim 1 and 2 is characterized in that,
Use is calculated high-frequency current that measurement mechanism obtains as described measurement data by electricity.
7. method of plasma processing according to claim 1 and 2 is characterized in that,
Use calculates high frequency voltage that measurement mechanism obtains by electricity and the phase difference of high-frequency current is used as described measurement data.
8. an aging detection of end method provides the test handled object in the container handling to processing unit, detects the described aging end when wearing out, and it is characterized in that, comprising:
Form the step of prediction type, to described test handled object is provided in the described container handling, after in the described container handling of cooling, a plurality of measurement data that use obtains when a plurality of described tests are provided once more in to described container handling with handled object, carry out multi-variables analysis, form the prediction type of the described aging end of prediction;
Based on described prediction type, detect the step carry out described aging end when aging.
9. a plasma processing apparatus is characterized in that, comprising:
Accommodate the container handling of handled object;
Measure the detector of the luminescence of plasma spectrum in this container handling;
Be connected with this detector, input is from the control device of the measurement data of this detector, when it provides test to wear out with handled object in to described container handling, to described test handled object is provided in the described container handling, after in the described container handling of cooling, when in to described container handling, providing a plurality of described tests to use handled object once more, based on a plurality of measurement data by described detectors measure, use the multi-variables analysis program to carry out multi-variables analysis, form the prediction type of the described aging end of prediction, detect based on this prediction type and carry out described aging end when aging.
10. plasma processing apparatus is characterized in that having:
Accommodate the container handling of handled object;
The electricity that is provided with in this container handling calculates measurement mechanism;
Calculating measurement mechanism with this electricity is connected, the control device of the measurement data of measurement mechanism is calculated in input from this electricity, when in to described container handling, providing test to wear out with handled object, to described test handled object is provided in the described container handling, after in the described container handling of cooling, when in to described container handling, providing a plurality of described tests to use handled object once more, based on a plurality of measurement data by described detectors measure, use the multi-variables analysis program to carry out multi-variables analysis, form the prediction type of the described aging end of prediction, based on this prediction type, detect and to carry out described aging end when aging.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP66369/2002 | 2002-03-12 | ||
| JP2002066369A JP4173311B2 (en) | 2002-03-12 | 2002-03-12 | Seasoning completion detection method, plasma processing method, and plasma processing apparatus |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1643664A true CN1643664A (en) | 2005-07-20 |
| CN100355040C CN100355040C (en) | 2007-12-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB038058618A Expired - Fee Related CN100355040C (en) | 2002-03-12 | 2003-03-12 | Plasma processing method, detecting method of completion of seasoning, plasma processing apparatus |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JP4173311B2 (en) |
| CN (1) | CN100355040C (en) |
| AU (1) | AU2003221362A1 (en) |
| TW (1) | TW200421411A (en) |
| WO (1) | WO2003077303A1 (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7313451B2 (en) | 2002-03-12 | 2007-12-25 | Tokyo Electron Limited | Plasma processing method, detecting method of completion of seasoning, plasma processing apparatus and storage medium |
| KR100557673B1 (en) * | 2003-12-22 | 2006-03-06 | 어댑티브프라즈마테크놀로지 주식회사 | Method for seasoning plasma equipment |
| US7393459B2 (en) * | 2004-08-06 | 2008-07-01 | Applied Materials, Inc. | Method for automatic determination of substrates states in plasma processing chambers |
| JP4640828B2 (en) * | 2006-03-17 | 2011-03-02 | 東京エレクトロン株式会社 | Plasma processing method and plasma processing apparatus |
| CN102315112B (en) * | 2011-09-28 | 2016-03-09 | 上海华虹宏力半导体制造有限公司 | The lithographic method of stacked metal gate |
| US10896833B2 (en) * | 2018-05-09 | 2021-01-19 | Applied Materials, Inc. | Methods and apparatus for detecting an endpoint of a seasoning process |
| US12032355B2 (en) * | 2022-03-31 | 2024-07-09 | Tokyo Electron Limited | Virtual metrology model based seasoning optimization |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1131599A (en) * | 1997-07-08 | 1999-02-02 | Sumitomo Metal Ind Ltd | Preheating method for plasma-processing device, and plasma-processing device |
| US6368975B1 (en) * | 1999-07-07 | 2002-04-09 | Applied Materials, Inc. | Method and apparatus for monitoring a process by employing principal component analysis |
| JP4570736B2 (en) * | 2000-07-04 | 2010-10-27 | 東京エレクトロン株式会社 | How to monitor operating conditions |
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2002
- 2002-03-12 JP JP2002066369A patent/JP4173311B2/en not_active Expired - Fee Related
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2003
- 2003-03-12 TW TW92105530A patent/TW200421411A/en not_active IP Right Cessation
- 2003-03-12 CN CNB038058618A patent/CN100355040C/en not_active Expired - Fee Related
- 2003-03-12 AU AU2003221362A patent/AU2003221362A1/en not_active Abandoned
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Also Published As
| Publication number | Publication date |
|---|---|
| WO2003077303A1 (en) | 2003-09-18 |
| AU2003221362A1 (en) | 2003-09-22 |
| JP4173311B2 (en) | 2008-10-29 |
| CN100355040C (en) | 2007-12-12 |
| JP2003264179A (en) | 2003-09-19 |
| TW200421411A (en) | 2004-10-16 |
| TWI297904B (en) | 2008-06-11 |
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