CN113208953A - Seaweed hair dye cream and preparation process thereof - Google Patents
Seaweed hair dye cream and preparation process thereof Download PDFInfo
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- CN113208953A CN113208953A CN202110409196.XA CN202110409196A CN113208953A CN 113208953 A CN113208953 A CN 113208953A CN 202110409196 A CN202110409196 A CN 202110409196A CN 113208953 A CN113208953 A CN 113208953A
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- 239000000118 hair dye Substances 0.000 title claims abstract description 48
- 241001474374 Blennius Species 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000006071 cream Substances 0.000 title claims description 21
- 241000199919 Phaeophyceae Species 0.000 claims description 34
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 30
- 239000002994 raw material Substances 0.000 claims description 29
- 239000000661 sodium alginate Substances 0.000 claims description 23
- 235000010413 sodium alginate Nutrition 0.000 claims description 23
- 229940005550 sodium alginate Drugs 0.000 claims description 23
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 15
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 10
- 235000010443 alginic acid Nutrition 0.000 claims description 10
- 229920000615 alginic acid Polymers 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 10
- WQABCVAJNWAXTE-UHFFFAOYSA-N dimercaprol Chemical compound OCC(S)CS WQABCVAJNWAXTE-UHFFFAOYSA-N 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- LSRUBRSFDNKORM-UHFFFAOYSA-N 1,1-diaminopropan-1-ol Chemical compound CCC(N)(N)O LSRUBRSFDNKORM-UHFFFAOYSA-N 0.000 claims description 5
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- 229940072056 alginate Drugs 0.000 claims description 5
- 229960001126 alginic acid Drugs 0.000 claims description 5
- 239000000783 alginic acid Substances 0.000 claims description 5
- 150000004781 alginic acids Chemical class 0.000 claims description 5
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 239000012528 membrane Substances 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 239000003755 preservative agent Substances 0.000 claims description 5
- 230000002335 preservative effect Effects 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 239000004094 surface-active agent Substances 0.000 claims description 4
- 239000000975 dye Substances 0.000 abstract description 3
- 230000004048 modification Effects 0.000 abstract description 3
- 238000012986 modification Methods 0.000 abstract description 3
- 238000005406 washing Methods 0.000 abstract description 2
- 239000000049 pigment Substances 0.000 description 12
- 241000196324 Embryophyta Species 0.000 description 10
- -1 sulfhydryl sodium alginate Chemical compound 0.000 description 10
- 239000000126 substance Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 238000004043 dyeing Methods 0.000 description 3
- 241000195493 Cryptophyta Species 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 230000004054 inflammatory process Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- AEUVIXACNOXTBX-UHFFFAOYSA-N 1-sulfanylpropan-1-ol Chemical compound CCC(O)S AEUVIXACNOXTBX-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 1
- 229920000855 Fucoidan Polymers 0.000 description 1
- 229930195725 Mannitol Natural products 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 241001260874 Sargassum horneri Species 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 241000196252 Ulva Species 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000033115 angiogenesis Effects 0.000 description 1
- 239000000981 basic dye Substances 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- GRWZHXKQBITJKP-UHFFFAOYSA-L dithionite(2-) Chemical compound [O-]S(=O)S([O-])=O GRWZHXKQBITJKP-UHFFFAOYSA-L 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 108010025899 gelatin film Proteins 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 239000000594 mannitol Substances 0.000 description 1
- 235000010355 mannitol Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- JVKAWJASTRPFQY-UHFFFAOYSA-N n-(2-aminoethyl)hydroxylamine Chemical compound NCCNO JVKAWJASTRPFQY-UHFFFAOYSA-N 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000004804 polysaccharides Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 210000004761 scalp Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/006—Heteroglycans, i.e. polysaccharides having more than one sugar residue in the main chain in either alternating or less regular sequence; Gellans; Succinoglycans; Arabinogalactans; Tragacanth or gum tragacanth or traganth from Astragalus; Gum Karaya from Sterculia urens; Gum Ghatti from Anogeissus latifolia; Derivatives thereof
- C08B37/0084—Guluromannuronans, e.g. alginic acid, i.e. D-mannuronic acid and D-guluronic acid units linked with alternating alpha- and beta-1,4-glycosidic bonds; Derivatives thereof, e.g. alginates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Birds (AREA)
- Biotechnology (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Botany (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of hair dye paste, in particular to seaweed hair dye paste, and also discloses a preparation process of the seaweed hair dye paste. After modification, dye molecules are firmly fixed in the hair cortex, so that the washing times are increased, and the hair is not damaged.
Description
Technical Field
The invention relates to the technical field of hair dye cream, in particular to seaweed hair dye cream and a preparation process thereof.
Background
Algae, which grow in the sea, are cryptophytes of the plant kingdom and include several different classes of organisms that produce energy by photosynthesis, which are generally considered to be simple plants.
The method for extracting pigment from thallus Porphyrae, Enteromorpha and Sargassum horneri has been disclosed, and the natural pigment is a colorant extracted and refined from plant, microorganism and animal material by various methods, and has high safety. The extraction and application of natural pigments is the main direction of current and future development, especially in the food, pharmaceutical and cosmetic industries. The marine area of China is vast, the seaweed resources are rich, generally speaking, the pigment content in marine plants is far higher than that of terrestrial plants, the pigment extracted from the seaweed has various beneficial biological activities such as oxidation resistance, tumor resistance, inflammation resistance, obesity resistance, angiogenesis resistance, nerve protection and the like, and the application of a plurality of activities of the seaweed pigment to the field of hair dyeing not only provides a novel hair dye and a hair dyeing method, but also is a component for comprehensive utilization of the seaweed, and is favorable for improving the additional value of the seaweed.
If a pure plant hair dye can be invented, the pure plant hair dye is extracted from seaweed, organic substances such as benzene and the like are not added, the pure plant hair dye is safe and non-irritant, and is different from chemical hair dye, the chemical hair dye is that hair scales are forcibly opened to drive pigments into hair, so that hair can be damaged, hair is withered, scalp inflammation is caused, even cancer is caused, and the problem can be solved by pure plant hair dye.
Disclosure of Invention
The invention aims to provide a seaweed hair dye cream and a preparation process thereof, which aim to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: a seaweed hair dye cream comprises 15-58 parts of modified polyhydroxy sulfhydryl sodium alginate and 44-90 parts of hair dye.
Preferably, 35 parts of modified polyhydroxy sodium alginate and 72 parts of hair dye.
Preferably, the modified polyhydroxy sodium alginate hydrosulfite comprises 2-10 parts of sodium carbonate, 5-20 parts of acid, 6-24 parts of diaminopropanol, 6-26 parts of tetrahydroxypropyl ethylenediamine and water.
Preferably, the hair dye comprises 30-60 parts of brown algae raw materials, 5-15 parts of propylene glycol and water.
Preferably, the brown algae raw material has wide sources, can be artificially cultured and can be collected from a water area.
A preparation process of seaweed hair dye cream comprises the following steps:
the method comprises the following steps: adding soda into the brown algae raw material, boiling by microwave, and filtering by a membrane to obtain a brown algae raw material filtrate with a certain molecular weight;
step two: putting the brown algae raw material filtrate into a reaction kettle, and adding acid to adjust the pH to 3-4 to obtain alginic acid;
step three: adding 5-10% of 2-amino-2-methyl-propanol serving as a catalyst into a reaction kettle;
step four: preparing sodium alginate, according to a catalyst, filtering a brown algae raw material: tetrahydroxypropyl ethylenediamine: adding the mixed solution of 2, 3-dimercaptopropanol with the weight ratio of 0.1-0.5:6-8:1-3 into a reaction kettle, preserving the heat at the temperature of 30-50 ℃ for 1-3 hours, and reacting to obtain modified polyhydroxy sodium hydrosulfo alginate;
step five: wherein tetrahydroxypropylethylenediamine: 2, 3-dimercaptopropanol in the weight ratio of 1-5 to 5-9, propylene glycol, preservative, etc.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention utilizes brown algae to prepare the hair dye cream, has the advantages that the brown algae contains a large amount of hydrophilic substances such as mannitol, fucoidan sulfate and the like, can effectively open hydrogen bonds in hair scales of hair, enables pigment to enter hair cortex more easily, and does not hurt the hair.
2. The brown algae contains a large amount of natural pigments, can directly dye the hair into brown without adding any additional pigment, and forms a gel film on the surface of the hair by utilizing polysaccharide substances contained in the brown algae, so that the hair is more healthy and bright;
3. adding hydroxy ethylenediamine and mercaptopropanol into sodium alginate molecules, combining the sodium alginate molecules with basic dye through chemical bonds, and then crosslinking the sodium alginate molecules with protein in hair through sulfydryl to form stable dimercapto bonds. After modification, dye molecules are firmly fixed in the hair cortex, so that the washing times are increased, and the hair is not damaged;
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. Based on the technical solutions in the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the invention provides a technical scheme that: a seaweed hair dye cream comprises 15-58 parts of modified polyhydroxy sulfhydryl sodium alginate, 44-90 parts of hair dye, more specifically 35 parts of modified polyhydroxy sulfhydryl sodium alginate and 72 parts of hair dye, wherein the modified polyhydroxy sulfhydryl sodium alginate comprises 8 parts of sodium carbonate, 17 parts of acid, 13 parts of diaminopropanol, 22 parts of tetrahydroxypropyl ethylenediamine and water, the hair dye comprises 35 parts of brown algae raw materials, 12 parts of propylene glycol, 9 parts of surfactant and water, the brown algae raw materials are wide in source and can be artificially cultured and collected from a water area.
A preparation process of seaweed hair dye cream comprises the following steps:
the method comprises the following steps: adding soda into the brown algae raw material, boiling by microwave, and filtering by a membrane to obtain a brown algae raw material filtrate with a certain molecular weight;
step two: putting the brown algae raw material filtrate into a reaction kettle, and adding acid to adjust the pH to 3-4 to obtain alginic acid;
step three: adding 5-10% of 2-amino-2-methyl-propanol serving as a catalyst into a reaction kettle;
step four: preparing sodium alginate, according to a catalyst, filtering a brown algae raw material: tetrahydroxypropyl ethylenediamine: adding the mixed solution of 2, 3-dimercaptopropanol with the weight ratio of 0.1-0.5:6-8:1-3 into a reaction kettle, preserving the heat at the temperature of 30-50 ℃ for 1-3 hours, and reacting to obtain modified polyhydroxy sodium hydrosulfo alginate;
step five: wherein tetrahydroxypropylethylenediamine: 2, 3-dimercaptopropanol in the weight ratio of 1-5 to 5-9, propylene glycol, preservative, etc.
Example two:
the invention provides a technical scheme that: a seaweed hair dye cream comprises 15-58 parts of modified polyhydroxy sulfhydryl sodium alginate, 44-90 parts of hair dye, more specifically 35 parts of modified polyhydroxy sulfhydryl sodium alginate and 72 parts of hair dye, wherein the modified polyhydroxy sulfhydryl sodium alginate comprises 6 parts of sodium carbonate, 14 parts of acid, 17 parts of diaminopropanol, 18 parts of tetrahydroxypropyl ethylenediamine and water, the hair dye comprises 45 parts of brown algae raw materials, 10 parts of propylene glycol, 7 parts of surfactant and water, and the brown algae raw materials are wide in source and can be artificially cultured and collected from a water area.
A preparation process of seaweed hair dye cream comprises the following steps:
the method comprises the following steps: adding soda into the brown algae raw material, boiling by microwave, and filtering by a membrane to obtain a brown algae raw material filtrate with a certain molecular weight;
step two: putting the brown algae raw material filtrate into a reaction kettle, and adding acid to adjust the pH to 3-4 to obtain alginic acid;
step three: adding 5-10% of 2-amino-2-methyl-propanol serving as a catalyst into a reaction kettle;
step four: preparing sodium alginate, according to a catalyst, filtering a brown algae raw material: tetrahydroxypropyl ethylenediamine: adding the mixed solution of 2, 3-dimercaptopropanol with the weight ratio of 0.1-0.5:6-8:1-3 into a reaction kettle, preserving the heat at the temperature of 30-50 ℃ for 1-3 hours, and reacting to obtain modified polyhydroxy sodium hydrosulfo alginate;
step five: wherein tetrahydroxypropylethylenediamine: 2, 3-dimercaptopropanol in the weight ratio of 1-5 to 5-9, propylene glycol, preservative, etc.
Example three:
the invention provides a technical scheme that: a seaweed hair dye cream comprises 15-58 parts of modified polyhydroxy sulfhydryl sodium alginate, 44-90 parts of hair dye, more specifically 35 parts of modified polyhydroxy sulfhydryl sodium alginate and 72 parts of hair dye, wherein the modified polyhydroxy sulfhydryl sodium alginate comprises 4 parts of sodium carbonate, 13 parts of acid, 20 parts of diaminopropanol, 14 parts of tetrahydroxypropyl ethylenediamine and water, the hair dye comprises 55 parts of brown algae raw materials, 8 parts of propylene glycol, 5 parts of surfactant and water, and the brown algae raw materials are wide in source and can be artificially cultured and collected from a water area.
A preparation process of seaweed hair dye cream comprises the following steps:
the method comprises the following steps: adding soda into the brown algae raw material, boiling by microwave, and filtering by a membrane to obtain a brown algae raw material filtrate with a certain molecular weight;
step two: putting the brown algae raw material filtrate into a reaction kettle, and adding acid to adjust the pH to 3-4 to obtain alginic acid;
step three: adding 5-10% of 2-amino-2-methyl-propanol serving as a catalyst into a reaction kettle;
step four: preparing sodium alginate, according to a catalyst, filtering a brown algae raw material: tetrahydroxypropyl ethylenediamine: adding the mixed solution of 2, 3-dimercaptopropanol with the weight ratio of 0.1-0.5:6-8:1-3 into a reaction kettle, preserving the heat at the temperature of 30-50 ℃ for 1-3 hours, and reacting to obtain modified polyhydroxy sodium hydrosulfo alginate;
step five: wherein tetrahydroxypropylethylenediamine: 2, 3-dimercaptopropanol in the weight ratio of 1-5 to 5-9, propylene glycol, preservative, etc.
The hair dye cream product of the second embodiment has better effect, ensures the stability of fat-soluble seaweed pigment in a hair dye system, has good safety and nutrition effect on hair quality due to pure plant hair dye, and has good dyeing effect and strong color fastness due to the colorant obtained by extracting and refining the pigment from the seaweed by the method.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A seaweed hair dye cream is characterized in that: comprises 15-58 parts of modified polyhydroxy sodium alginate and 44-90 parts of hair dye.
2. The seaweed hair dye cream according to claim 1, characterized in that: 35 parts of modified polyhydroxy sodium alginate and 72 parts of hair dye.
3. The seaweed hair dye cream according to claim 1, characterized in that: the modified polyhydroxy sodium alginate hydrosulphonate comprises 2-10 parts of sodium carbonate, 5-20 parts of acid, 6-24 parts of diaminopropanol, 6-26 parts of tetrahydroxypropyl ethylenediamine and water.
4. The seaweed hair dye cream according to claim 1, characterized in that: the hair dye comprises 30-60 parts of brown algae raw materials, 5-15 parts of propylene glycol, 3-10 parts of surfactant and water.
5. The seaweed hair dye cream according to claim 1, characterized in that: the brown algae has wide source, can be artificially cultured and can be collected from a water area.
6. The preparation process of the seaweed hair dye cream as claimed in claim 1, which is characterized by comprising the following steps:
the method comprises the following steps: adding soda into the brown algae raw material, boiling by microwave, and filtering by a membrane to obtain a brown algae raw material filtrate with a certain molecular weight;
step two: putting the brown algae raw material filtrate into a reaction kettle, and adding acid to adjust the pH value to 3-4 to obtain alginic acid;
step three: adding 5-10% of 2-amino-2-methyl-propanol serving as a catalyst into a reaction kettle;
step four: preparing sodium alginate, according to a catalyst, filtering a brown algae raw material: tetrahydroxypropyl ethylenediamine: adding the mixed solution of 2, 3-dimercaptopropanol with the weight ratio of 0.1-0.5:6-8:1-3 into a reaction kettle, preserving the heat at the temperature of 30-50 ℃ for 1-3 hours, and reacting to obtain modified polyhydroxy sodium hydrosulfo alginate;
step five: wherein tetrahydroxypropylethylenediamine: 2, 3-dimercaptopropanol in the weight ratio of 1-5 to 5-9, propylene glycol, preservative, etc.
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| CN202110409196.XA CN113208953A (en) | 2021-04-16 | 2021-04-16 | Seaweed hair dye cream and preparation process thereof |
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| CN202110409196.XA CN113208953A (en) | 2021-04-16 | 2021-04-16 | Seaweed hair dye cream and preparation process thereof |
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Citations (7)
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| US5336668A (en) * | 1986-06-30 | 1994-08-09 | Fidia, S.P.A. | Esters of alginic acid |
| WO2004099259A1 (en) * | 2003-05-09 | 2004-11-18 | Toho Chemical Industry Co., Ltd. | Cation-modified alginic acid derivative and cosmetic preparation composition containing the substance |
| CN1813662A (en) * | 2005-11-16 | 2006-08-09 | 江南大学 | Sulfhydryl modified dye and its preparing method for sulfhydryl modified hair dye |
| KR20100070911A (en) * | 2008-12-18 | 2010-06-28 | (주)이지코스 | Cosmetic composition with superior coloring and hair tension |
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