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CN113191616B - Polypropylene product quality abnormity detection method based on double-layer correlation characteristic analysis - Google Patents

Polypropylene product quality abnormity detection method based on double-layer correlation characteristic analysis Download PDF

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CN113191616B
CN113191616B CN202110440195.1A CN202110440195A CN113191616B CN 113191616 B CN113191616 B CN 113191616B CN 202110440195 A CN202110440195 A CN 202110440195A CN 113191616 B CN113191616 B CN 113191616B
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赵炜涛
陈杨
虞飞宇
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Jiangsu Hongjiahua New Material Technology Co ltd
Shenzhen Weiqing Intellectual Property Services Co.,Ltd.
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Abstract

The invention discloses a polypropylene product quality abnormity detection method based on double-layer correlation characteristic analysis, and aims to achieve the purpose of indirectly detecting whether the quality of a polypropylene product is abnormal. Specifically, the method of the invention obtains characteristic variables and components related to the quality of polypropylene products by a double-layer related characteristic analysis technology, and indirectly implements anomaly detection. When the method is used for detecting the quality abnormity of the polypropylene product, the method does not depend on a technical means of directly measuring the melt index of the polypropylene, namely a long and serious hysteresis measuring period, and indirectly detects the abnormity through a double-layer correlation characteristic analysis of a neighbor component analysis algorithm and a typical correlation analysis algorithm, so that the most relevant characteristic variable or component with the melt index of the polypropylene is obtained. Therefore, the method can detect whether the quality of the polypropylene product is abnormal in real time according to the sampling frequency of the measurement variable, and overcomes the problem of hysteresis of the traditional method.

Description

Polypropylene product quality abnormity detection method based on double-layer correlation characteristic analysis
Technical Field
The invention relates to an anomaly detection method, in particular to a polypropylene product quality anomaly detection method based on double-layer correlation characteristic analysis.
Background
Polypropylene is a thermoplastic resin polymerized from propylene as a monomer, has the advantages of low density, low production cost, high transparency, good chemical stability, no toxicity, easy processing, high impact strength, good flexibility resistance, good electrical insulation property and the like, is one of five most widely used plastics, and has been widely applied to the aspects of plastic containers, office supplies, electronics and the like. The grades of polypropylene products in industry are often divided by the melt index value, and polypropylene products of different grades have different uses. In this regard, polypropylene product quality is directly related to polypropylene melt index. The real-time monitoring of the quality of the polypropylene product is the real-time monitoring of the melt index of the polypropylene. Thus, the simplest and most direct monitoring method is more than directly measuring the melt index of polypropylene in real time.
The current methods for measuring the melt index of polypropylene all use on-line sampling and off-line testing, i.e. the polypropylene sample to be soft-measured and controlled is directly sampled at the production site, and then the required melt index value is obtained after testing for 2-4 hours in a laboratory. In fact, from the production flow of polypropylene, four production steps are needed from raw materials to final products. Each production link can ensure the stability of the quality of the final product only when running in an expected state. Therefore, the real-time monitoring of the polypropylene product quality is indirectly realized by monitoring the running states of the four production units.
However, indirect monitoring of polypropylene product quality anomalies requires attention to distinguish quality-related anomalies from those that are not. This is mainly because: the quality of the final polypropylene product is not necessarily affected by the abnormalities in the four production links. In some cases, the four stages of polypropylene production present some unusual problems, but do not affect the final polypropylene melt index. Therefore, the indirect detection of the polypropylene product quality abnormality by monitoring the running states of four production links from the raw materials to the final product also needs to effectively distinguish the characteristics related to the product quality from those unrelated to the product quality.
Disclosure of Invention
The invention aims to solve the main technical problems that: how to distinguish the characteristic variables and the characteristic components related to the polypropylene product in four production units from raw materials to final products in the production process of the polypropylene, thereby achieving the aim of indirectly detecting whether the quality of the polypropylene product is abnormal. Specifically, the method obtains characteristic variables and components related to the quality of the polypropylene product through a double-layer related characteristic analysis technology, and indirectly implements anomaly detection. The so-called double-layer characteristic analysis is to firstly distinguish characteristic variables directly related to the melt index of the polypropylene by means of neighbor component analysis and then distinguish characteristic components indirectly related to the melt index of the polypropylene by means of typical correlation analysis.
The technical scheme adopted by the method for solving the problems is as follows: a polypropylene product quality anomaly detection method based on double-layer correlation characteristic analysis comprises the following steps:
step (1): determining the measurement variables of the polypropylene production process, specifically comprising 28 measurement variables of four reactors; wherein the first reactor and the second reactor are liquid phase continuous stirred reactors, the third reactor and the fourth reactor are gas phase fluidized bed reactors, and the 7 measurement variables related to each reactor are sequentially: reactor temperature, reactor pressure, reactor liquid level, hydrogen feed flow, propylene feed flow, catalyst feed flow, and reflux flow.
Step (2): continuously collecting sample data at N sampling moments according to the determined measurement variable; meanwhile, sampling and analyzing every 2 hours to obtain the melt index of the polypropylene product in the fourth reactor; and then storing the sample data corresponding to the measurement variable into an Nx 28-dimensional data matrix X, and storing N data corresponding to the melt index into an N X1-dimensional data vector y.
And (3): element filling is carried out on the data vector Y according to the formula shown below, and then the column vector Y epsilon R is obtained N×1
Figure BSA0000240431240000021
Wherein, y 1 ,y 2 ,…,y n Representing the first to nth elements of a data vector y, f being equal to the ratio of the sampling frequency of the measured variable to the melt index, R N×1 Representing a vector of real numbers of dimension N × 1, R representing a set of real numbers, and the upper index T representing a transpose of a matrix or vector.
And (4): respectively aligning column vectors X in X according to the formula 1 ,x 2 ,…,x 28 And standardizing the column vector Y to obtain an input matrix
Figure BSA0000240431240000022
And outputting the vector
Figure BSA0000240431240000023
Figure BSA0000240431240000024
Wherein x is k And
Figure BSA0000240431240000025
respectively represent X and
Figure BSA0000240431240000026
column vector of the kth column, k ∈ {1,2, \8230;, 28}, μ k And delta k Respectively represent column vectors x k ∈R N×1 Mean and standard deviation of all elements in (u) Y And delta Y Respectively representing the mean and standard deviation of all elements in the column vector Y.
And (5): the weight vector w is obtained by optimizing the steps (5.1) to (5.6) as shown below 0 ∈R 28×1 Thereby obtaining a direct correlation feature matrix X 1 ∈R N×m And uncorrelated feature matrix X 2 ∈R N×(28-m) (ii) a Wherein m represents the number of directly related characteristic variables, R N×(28-m) A matrix of real numbers representing dimensions N x (28-m), R N×m A matrix of real numbers in dimension N × m is represented.
Step (5.1): initializing iteration times g =1, and determining parameters of a differential evolution algorithm, specifically including: population number H, scaling factor c 1 Cross probability c 2 The maximum number of iterations G.
Step (5.2): randomly generating H weight vectors w of 1 x 28 dimensions 1 ,w 2 ,…,w H The elements in each weight vector are randomly distributed according to a uniform distributionValue in the interval [ -1,1]。
Step (5.3): separately calculating weight vectors w 1 ,w 2 ,…,w H Corresponding objective function value F 1 ,F 2 ,…,F H (ii) a Wherein the h-th weight vector w is calculated h Corresponding objective function F h Is carried out as shown in steps (A) to (D), and H is ∈ {1,2, \8230;, H }.
Step (A): calculating an input matrix according to the formula
Figure BSA0000240431240000027
Middle ith row vector beta i And the jth row vector beta j Weighted distance D therebetween hi ,β j ):
D hi ,β j )=||(β ij )diag{w h }|| ③
Wherein i belongs to {1,2, \8230;, N }, j belongs to {1,2, \8230;, N }, diag { w;) h Denotes weighting vector w h And transforming the vector into a diagonal matrix, wherein the symbol | | | | represents the length of a calculation vector, and H belongs to {1,2, \8230;, H }.
Step (B): beta is calculated according to the formula shown below i And beta j The close probability p between ij
Figure BSA0000240431240000031
In the above equation, exp () represents an exponential function with a natural constant e as a base.
Step (C): the output probability error p is calculated according to the formula shown below 1 ,p 2 ,…,p N
Figure BSA0000240431240000032
In the above-mentioned formula, the compound has the following structure,
Figure BSA0000240431240000033
and
Figure BSA0000240431240000034
respectively representing output vectors
Figure BSA0000240431240000035
The ith element and the jth element in (c).
A step (D): computing the h-th weight vector w h Corresponding objective function value F h =p 1 +p 2 +…+p N
Step (5.4): f is to be 1 ,F 2 ,…,F H The weight vector corresponding to the minimum value in (1) is recorded as w 0 Then, executing the updating operation of the differential evolution algorithm to obtain H updated weight vectors w 1 ,w 2 ,…,w H And its corresponding objective function value F 1 ,F 2 ,…,F H (ii) a The specific implementation process of the updating operation of the differential evolution algorithm is shown in the steps (5.4-1) to (5.4-4).
Step (5.4-1): as a weight vector w according to the formula shown below h Generating a corresponding variation vector v h
v h =w h +c 1 ×(w 0 -w h )+c 1 ×(w a -w b ) ⑥
In the above formula, subscripts a and b are 2 mutually unequal integers randomly generated from the interval [1, H ];
step (5.4-2): for the variation vector v according to the formula shown below h And (5) correcting:
Figure BSA0000240431240000036
in the above formula, v h (k) Representing a variation vector v h The kth element of (1), k ∈ {1,2, \8230;, 28};
step (5.4-3): the H trial vectors u are generated according to the formula shown below 1 ,u 2 ,…,u H
Figure BSA0000240431240000037
Wherein u is h (k) And w h (k) Are each u h And w h The k-th element of (1), r k Represents a random number between 0 and 1;
step (5.4-4): respectively make u 1 ,u 2 ,…,u H As weight vector, and executing the same implementation process as the steps (A) to (D), thereby calculating the corresponding objective function value
Figure BSA0000240431240000038
Step (5.4-5): the H weight vectors w are updated respectively according to the formula shown below 1 ,w 2 ,…,w H And its corresponding objective function value F 1 ,F 2 ,…,F H
Figure BSA0000240431240000039
Step (5.5): judging whether the condition G is satisfied; if not, returning to the step (5.4) after setting g = g + 1; if yes, obtaining the optimal weight vector w 0
Step (5.6): determining a weight vector w 0 ∈R 1×28 M elements with the maximum number, and correspondingly inputting the m elements into the matrix according to the columns where the m elements are positioned
Figure BSA00002404312400000310
The column vectors of the same column are constructed into a direct correlation characteristic matrix X 1 ∈R N×m To do so
Figure BSA00002404312400000311
The column vectors of the other 28-m columns are constructed into an uncorrelated feature matrix X 2 ∈R N×(28-m)
And (6): firstly solving the problem of generalized eigenvalue
Figure BSA0000240431240000041
The feature vector beta corresponding to the middle maximum feature value eta is calculated according to
Figure BSA0000240431240000042
Calculating the related projection vector q ∈ R (28-m)×1 Then according to the formula
Figure BSA0000240431240000043
Computing indirect correlation feature vectors
Figure BSA0000240431240000044
Step (7) of converting X 1 And
Figure BSA00002404312400000417
combined into an input correlation feature matrix
Figure BSA0000240431240000045
Thereafter, the determination of the upper limit D of the control of the abnormality detection index is performed as shown in the following steps (7.1) to (7.4) lim
Step (7.1): initialization i =1.
Step (7.2): solving generalized eigenvalue problem
Figure BSA0000240431240000046
After the feature vector a corresponding to the medium maximum feature value lambda, performing normalization processing on a according to a formula a = a/| a |; wherein z is i A row vector representing the ith row in Z, Z i Is obtained by dividing Z by Z i The outer row vectors form a matrix.
Step (7.3): according to the formula D (i) = (z) i a) 2 The i-th element D (i) in the abnormality detection index vector D is calculated.
Step (7.4): judging whether the conditions are met: i is less than N; if yes, setting i = i +1 and returning to the step (7.2); if not, then D is carried out lim Is arranged asEqual to the maximum of the elements in the anomaly detection index vector D.
And (8): at the latest sampling time t, sample data x corresponding to the measured variable is collected t (1),x t (2),…,x t (28) And respectively carrying out standardization processing on the input vectors according to the following formulas to obtain input vectors
Figure BSA0000240431240000047
Figure BSA0000240431240000048
Wherein k ∈ {1,2, \8230;, 28},
Figure BSA0000240431240000049
representing input vectors
Figure BSA00002404312400000410
The kth element in (1).
And (9): according to the weight vector w 0 ∈R 1×28 The column where the maximum m elements are located corresponds to the input vector
Figure BSA00002404312400000411
Elements in the same column constitute the directly related feature vector y 1 ∈R 1×m Then will be
Figure BSA00002404312400000412
The remaining 28-m elements in the set constitute the uncorrelated feature vectors y 2 ∈R 1×(28-m)
Step (10): according to the formula s t =y 2 q calculating an indirect correlation feature s t Then, add y 1 And s t Combined into an input-dependent feature vector
Figure BSA00002404312400000413
Step (11): according to the steps (11.1) to (11) shown below2) calculating an abnormality detection index D corresponding to the latest sampling time t t
Step (11.1): solving generalized eigenvalue problem
Figure BSA00002404312400000414
Medium maximum eigenvalue lambda t Corresponding feature vector epsilon t Then, according to the formula ∈ t =ε t /||ε t I to ε t Carrying out normalization processing; wherein,
Figure BSA00002404312400000415
means for calculating ε t Length of (d).
Step (11.2): calculating the abnormal detection index corresponding to the latest sampling time t
Figure BSA00002404312400000416
Step (12): judging whether the conditions are met: d t ≤D lim (ii) a If yes, the quality of the polypropylene product at the current sampling moment is not abnormal, and the step (8) is returned; if not, executing step (13) to decide whether to trigger an abnormal alarm.
Step (13): returning to the step (8) to continue to carry out the quality abnormity detection of the polypropylene product at the latest sampling time, if the abnormity detection indexes of the continuous 6 latest sampling times are all larger than D lim Triggering an abnormal alarm of the quality of the polypropylene product; otherwise, no exception alarm is triggered.
The implementation step (5) of the method is to optimize and solve the objective function of the neighbor component analysis algorithm by using a differential evolution algorithm. Consider that the nearest neighbor component analysis algorithm aims at finding the weight vector w 0 Thereby outputting a probability error p 1 ,p 2 ,…,p N The sum is minimized, and the effective solution of the optimization problem can be realized through a differential evolution algorithm. Compared with the traditional method of solving the minimization problem of the analysis of the neighboring components by using a gradient descent method, the global optimization can be better ensured by using a differential evolution algorithm.
The generalized characteristics are solved in the implementation step (6) of the methodValue problem
Figure BSA0000240431240000051
Is actually performing a typical Correlation Analysis (CCA) algorithm. The idea of the CCA algorithm is to do so by respectively
Figure BSA0000240431240000052
And
Figure BSA0000240431240000053
finding the corresponding projection vectors beta and sigma to make the correlation coefficient
Figure BSA0000240431240000054
Maximization; wherein, beta and sigma need to satisfy the condition:
Figure BSA0000240431240000055
and
Figure BSA0000240431240000056
the CCA maximization problem can be transformed into a typical generalized eigenvalue problem by the lagrange multiplier method:
Figure BSA0000240431240000057
due to the fact that
Figure BSA0000240431240000058
Is a real number vector whose corresponding projection vector σ is a real number of 1 × 1 dimension. Thus, the generalized eigenvalue problem is equivalent to:
Figure BSA0000240431240000059
if λ = λ/σ is set 2 And (5) obtaining the generalized eigenvalue problem in the step (6).
The implementation step (7) of the method is a specific implementation process of an online discriminant feature analysis algorithm. The algorithm starts from the angle of abnormal detection, and enables z to be detected by searching a transformation vector a on line in real time i a to allPossible distance from Z i a point in a. Thus, the problem can be quantified as an optimization problem as follows:
Figure BSA00002404312400000510
in the above formula, by
Figure BSA00002404312400000511
To limit Z i a distance of the point from the origin of coordinate axis and simultaneously maximizing z i a is the distance from the origin of the coordinate axes. Due to the fact that
Figure BSA00002404312400000512
The optimization problem can be directly converted into a typical generalized eigenvalue problem through a Lagrange multiplier method:
Figure BSA00002404312400000513
further, the feature vector is further constrained to be a unit length by a = a/| a | |, so that the feature vector or the transform vector a represents only a direction. It is worth noting that the algorithm used in step (11) of the method of the present invention is the same as that used in step (7).
By carrying out the steps described above, the advantages of the method of the invention are presented below.
When the method is used for detecting the quality abnormity of the polypropylene product, the technical means of directly measuring the melt index of the polypropylene, namely long and serious hysteresis, is not relied on, and the characteristic variable or component which is most relevant to the melt index of the polypropylene and is obtained by double-layer relevant characteristic analysis of a neighbor component analysis algorithm and a typical relevant analysis algorithm is used for indirectly detecting the abnormity. The method can detect whether the quality of the polypropylene product is abnormal in real time according to the sampling frequency of the measured variable, and overcomes the problem of hysteresis of the traditional method.
Drawings
FIG. 1 is a schematic flow chart of the method of the present invention.
FIG. 2 is a schematic flow diagram of a polypropylene process
Detailed Description
The present invention will be described in detail below with reference to the accompanying drawings and specific embodiments.
Referring to fig. 1, the present invention discloses a method for detecting quality abnormality of polypropylene product based on double-layer correlation characteristic analysis, and the following describes a specific embodiment of the method according to a specific application example.
As shown in fig. 2, the production flow of a polypropylene process object comprises four reactors, respectively referred to as a first reactor, a second reactor, a third reactor, and a fourth reactor; wherein the first reactor and the second reactor are liquid phase continuous stirred reactors, and the third reactor and the fourth reactor are gas phase fluidized bed reactors. Each reactor had a feed of propylene and hydrogen and a feed of catalyst. In addition, the product at the outlet of the fourth reactor is a polypropylene product.
Step (1): the measured variables of the polypropylene production process are determined, and specifically comprise 28 measured variables of four reactors.
Step (2): continuously collecting sample data of N sampling moments by using a measuring instrument installed in the production process of polypropylene; meanwhile, the melt index of the polypropylene product in the fourth reactor is obtained by sampling and analyzing every 2 hours; and storing the sample data corresponding to the measurement variable into an Nx 28-dimensional data matrix X, and storing N data corresponding to the melt index into an N X1-dimensional data vector y.
And (3): element filling is carried out on the data vector Y according to the formula (1) so as to obtain a column vector Y epsilon R N×1 . In the present embodiment, the sampling period of the measured variable is 6 minutes, i.e. the sampling frequency is equal to 1/(6 × 60), while the sampling frequency of the melt index is equal to 1/(120 × 60). Therefore, f = (120 × 60)/(6 × 60) =20 in formula (1).
And (4): respectively aligning column vectors z in X according to the formula (2) 1 ,z 2 ,…,z 28 And in the column directionThe quantity Y is subjected to standardization processing, and an input matrix is obtained correspondingly
Figure BSA0000240431240000061
And outputting the vector
Figure BSA0000240431240000062
And (5): obtaining the weight vector w according to the optimization of the steps (5.1) to (5.6) 0 ∈R 28×1 To obtain a direct correlation characteristic matrix X 1 ∈R N×m And uncorrelated feature matrix X 2 ∈R N×(28-m)
And (6): firstly solving the problem of generalized eigenvalue
Figure BSA0000240431240000063
The feature vector beta corresponding to the middle maximum feature value eta is calculated according to
Figure BSA0000240431240000064
Calculating a correlation projection vector q ∈ R (28-m)×1 Then according to the formula
Figure BSA0000240431240000065
Computing indirect correlation feature vectors
Figure BSA0000240431240000066
And (7): mixing X 1 And
Figure BSA00002404312400000612
are combined into an input correlation feature matrix
Figure BSA0000240431240000067
Then, the above steps (7.1) to (7.4) are executed to determine the upper limit D of the abnormality detection index lim
And (8): at the latest sampling time t, sample data x corresponding to the measured variable is collected t (1),x t (2),…,x t (28) And are respectively paired according to the above-mentioned formulaIt performs normalization processing to obtain an input vector
Figure BSA0000240431240000068
And (9): according to the weight vector w 0 ∈R 1×28 The column where the maximum m elements are located corresponds to the input vector
Figure BSA0000240431240000069
Elements of the same column constitute a directly related feature vector y 1 ∈R 1×m Then will be
Figure BSA00002404312400000610
The remaining 28-m elements form an uncorrelated feature vector y 2 ∈R 1×(28-m)
Step (10): according to the formula s t =y 2 q calculating the indirectly related features s t Then, y is added 1 And s t Combined into an input-dependent feature vector
Figure BSA00002404312400000611
Step (11): calculating an abnormality detection index D according to the aforementioned steps (11.1) to (11.2) t
Step (12): judging whether the conditions are met: d t ≤D lim (ii) a If yes, the quality of the polypropylene product at the current sampling moment is not abnormal, and the step (8) is returned; if not, executing step (13) to decide whether to trigger an abnormal alarm.
Step (13): returning to the step (8) to continue to carry out the quality abnormity detection of the polypropylene product at the latest sampling time, if the abnormity detection indexes of the continuous 6 latest sampling times are all larger than D lim Triggering an abnormal alarm of the quality of the polypropylene product; otherwise, no abnormal alarm is triggered.
The above embodiments are merely illustrative of specific implementations of the present invention and are not intended to limit the present invention. Any modification of the present invention within the spirit of the present invention and the scope of the claims will fall within the scope of the present invention.

Claims (3)

1. A polypropylene product quality abnormity detection method based on double-layer correlation characteristic analysis is characterized by comprising the following steps:
step (1): determining the measurement variables of the polypropylene production process, specifically comprising 28 measurement variables of four reactors; wherein the first reactor and the second reactor are liquid phase continuous stirred reactors, the third reactor and the fourth reactor are gas phase fluidized bed reactors, and the 7 measurement variables related to each reactor are sequentially: reactor temperature, reactor pressure, reactor liquid level, hydrogen feed flow, propylene feed flow, catalyst feed flow, and reflux flow;
step (2): continuously collecting sample data at N sampling moments according to the determined measurement variable; meanwhile, sampling and analyzing every 2 hours to obtain the melt index of the polypropylene product in the fourth reactor; then storing sample data corresponding to the measurement variable into an Nx 28-dimensional data matrix X, and storing N data corresponding to the melt index into an N X1-dimensional data vector y; and (3): element filling is carried out on the data vector Y according to the formula shown below, and then a column vector Y epsilon R is obtained N×1
Figure FSB0000199235290000011
Wherein, y 1 ,y 2 ,…,y n Representing the first to nth elements of a data vector y, f being equal to the ratio of the sampling frequency of the measured variable to the melt index, R N×1 Real number vectors of dimension Nx 1 are represented, R represents a real number set, and the upper label T represents a matrix or a transpose of the vectors;
and (4): respectively aligning column vectors X in X according to the formula shown below 1 ,x 2 ,…,x 28 And standardizing the column vector Y to obtain an input matrix
Figure FSB0000199235290000012
And outputting the vector
Figure FSB0000199235290000013
Figure FSB0000199235290000014
Wherein x is k And
Figure FSB0000199235290000015
respectively represent X and
Figure FSB0000199235290000016
column vector of the kth column, k ∈ {1,2, \8230;, 28}, μ ∈ {1,2, \\ 8230;, 28}, a k And delta k Respectively represent column vectors x k ∈R N×1 Mean and standard deviation of all elements in (u) Y And delta Y Respectively representing the mean value and the standard deviation of all elements in the column vector Y;
and (5): the weight vector w is obtained by optimizing the steps (5.1) to (5.6) as shown below 0 ∈R 28×1 Thereby obtaining a direct correlation feature matrix X 1 ∈R N×m And uncorrelated feature matrix X 2 ∈R N×(28-m) (ii) a Wherein m represents the number of directly related characteristic variables, R N×(28-m) A matrix of real numbers representing dimensions N x (28-m), R N×m A real number matrix representing dimensions N × m, R representing a real number set;
step (5.1): initializing iteration times g =1, and determining parameters of a differential evolution algorithm, specifically including: population number H, scaling factor c 1 Cross probability c 2 Maximum iteration number G;
step (5.2): randomly generating H weight vectors w of 1 x 28 dimensions 1 ,w 2 ,…,w H The elements in each weight vector are randomly valued in the interval [ -1,1 ] according to uniform distribution];
Step (5.3): separately calculating weight vectors w 1 ,w 2 ,…,w H Corresponding objective function value F 1 ,F 2 ,…,F H
Step (5.4): f is to be 1 ,F 2 ,…,F H The weight vector corresponding to the minimum value in (1) is recorded as w 0 Then, executing the updating operation of the differential evolution algorithm to obtain H updated weight vectors w 1 ,w 2 ,…,w H And its corresponding objective function value F 1 ,F 2 ,…,F H
Step (5.5): judging whether the condition G is satisfied; if not, returning to the step (5.4) after setting g = g + 1; if yes, obtaining the optimal weight vector w 0
Step (5.6): determining a weight vector w 0 ∈R 1×28 M elements with the maximum number, and correspondingly inputting the m elements into the matrix according to the columns of the m elements
Figure FSB0000199235290000021
The column vectors of the same column constitute a direct correlation feature matrix X 1 ∈R N×m To is that
Figure FSB0000199235290000022
The column vectors of the other 28-m columns are constructed into an uncorrelated feature matrix X 2 ∈R N×(28-m)
And (6): firstly solving the problem of generalized eigenvalue
Figure FSB0000199235290000023
The feature vector beta corresponding to the middle maximum feature value eta is obtained according to
Figure FSB0000199235290000024
Calculating a correlation projection vector q ∈ R (28-m)×1 Then according to the formula
Figure FSB0000199235290000025
Computing indirect correlation feature vectors
Figure FSB0000199235290000026
Step (7) of converting X 1 And
Figure FSB0000199235290000027
are combined into an input correlation feature matrix
Figure FSB0000199235290000028
Thereafter, steps (7.1) to (7.4) shown below are performed to determine the upper limit D of control of the abnormality detection index lim
Step (7.1): initializing i =1;
step (7.2): solving generalized eigenvalue problem
Figure FSB0000199235290000029
After the eigenvector alpha corresponding to the medium and maximum eigenvalue lambda is obtained, the formula is used
Figure FSB00001992352900000210
Carrying out normalization processing on alpha; wherein z is i A row vector representing the ith row in Z, Z i Is obtained by dividing Z by Z i A matrix composed of the other row vectors;
step (7.3): according to the formula D (i) = (z) i α) 2 Calculating the ith element D (i) in the abnormal detection index vector D;
step (7.4): judging whether the conditions are met: i is less than N; if yes, returning to the step (7.2) after setting i = i + 1; if not, then D is added lim Set equal to the maximum of the elements in the anomaly detection index vector D;
and (8): at the latest sampling time t, sample data x corresponding to the measured variable is collected t (1),x t (2),…,x t (28) And respectively carrying out standardization processing on the input vectors according to the following formulas to obtain input vectors
Figure FSB00001992352900000211
Figure FSB00001992352900000212
Wherein k ∈ {1,2, \8230;, 28},
Figure FSB00001992352900000213
representing input vectors
Figure FSB00001992352900000214
The kth element in (1);
and (9): according to the weight vector w 0 ∈R 1×28 The column where the maximum m elements are located corresponds to the input vector
Figure FSB00001992352900000215
Elements in the same column constitute the directly related feature vector y 1 ∈R 1×m Then will be
Figure FSB00001992352900000216
The remaining 28-m elements in the set constitute the uncorrelated feature vectors y 2 ∈R 1×(28-m)
Step (10): according to the formula s t =y 2 q calculating an indirect correlation feature s t Then, y is added 1 And s t Combined into an input-dependent feature vector
Figure FSB00001992352900000217
Step (11): the abnormality detection index D corresponding to the latest sampling time t is calculated from the steps (11.1) to (11.2) shown below t
Step (11.1): solving generalized eigenvalue problem
Figure FSB00001992352900000218
Medium maximum eigenvalue lambda t Corresponding feature vector epsilon t Then according to the formula
Figure FSB00001992352900000219
For epsilon t Carrying out normalization processing;
step (11.2): calculating an abnormality detection index corresponding to the latest sampling time t
Figure FSB00001992352900000220
Step (12): judging whether the conditions are met: d t ≤D lim (ii) a If yes, the quality of the polypropylene product at the current sampling moment is not abnormal, and the step (8) is returned; if not, executing the step (13) to decide whether to trigger an abnormal alarm;
step (13): returning to the step (8) to continue to carry out the quality abnormity detection of the polypropylene product at the latest sampling time, if the abnormity detection indexes of the continuous 6 latest sampling times are all larger than D lim Triggering an abnormal alarm of the quality of the polypropylene product; otherwise, no exception alarm is triggered.
2. The method for detecting the quality abnormality of the polypropylene product based on the double-layer correlation characteristic analysis as claimed in claim 1, wherein the h weight vector w is calculated in the step (5.3) h Corresponding objective function F h The specific implementation process of (a) to (D) is as follows:
step (A): calculating an input matrix according to the formula
Figure FSB0000199235290000031
Middle ith row vector beta i And the jth row vector beta j Weighted distance D between hi ,β j ):
D hi ,β j )=||(β ij )diag{w h }|| ④
Wherein i belongs to {1,2, \8230;, N }, j belongs to {1,2, \8230;, N }, diag { w;) h Denotes weighting vector w h Converted into a diagonal matrix, the symbol | | | | represents the length of the calculated vector,h∈{1,2,…,H};
step (B): beta is calculated according to the formula shown below i And beta j The close probability p between ij
Figure FSB0000199235290000032
In the above equation, exp () represents an exponential function with a natural constant e as a base;
a step (C): calculating the output probability error p according to the formula 1 ,p 2 ,…,p N
Figure FSB0000199235290000033
In the above formula, the first and second carbon atoms are,
Figure FSB0000199235290000034
and
Figure FSB0000199235290000035
respectively representing output vectors
Figure FSB0000199235290000036
The ith element and the jth element in (c);
a step (D): computing the h-th weight vector w h Corresponding objective function value F h =p 1 +p 2 +…+p N
3. The method for detecting the quality abnormality of the polypropylene product based on the two-layer correlation characteristic analysis according to claim 2, wherein the step (5.4) of updating the differential evolution algorithm is implemented as shown in the steps (5.4-1) to (5.4-4):
step (5.4-1): as a weight vector w according to the formula shown below h Generating a corresponding variation vector v h
v h =w h +c 1 ×(w 0 -w h )+c t ×(w a -w b ) ⑦
In the above formula, subscripts a and b are 2 mutually unequal integers randomly generated from the interval [1, H ];
step (5.4-2): for the variation vector v according to the formula shown below h And (5) correcting:
Figure FSB0000199235290000037
in the above formula, v h (k) Representing a variation vector v h The kth element of (1), k ∈ {1,2, \8230;, 28};
step (5.4-3): the H trial vectors u are generated according to the formula shown below 1 ,u 2 ,…,u H
Figure FSB0000199235290000038
Wherein u is h (k) And w h (k) Are each u h And w h The k-th element of (1), r k Represents a random number between 0 and 1;
step (5.4-4): respectively make u 1 ,u 2 ,…,u H As weight vector, and according to the steps (A) to (D), calculating to obtain corresponding objective function value
Figure FSB0000199235290000041
Step (5.4-5): the H weight vectors w are updated separately according to the formula shown below 1 ,w 2 ,…,w H And its corresponding objective function value F 1 ,F 2 ,…,F H
Figure FSB0000199235290000042
Wherein H belongs to {1,2, \8230;, H }.
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105116726A (en) * 2015-07-20 2015-12-02 宁波大学 Parameter design method for nonlinear predictive controller based on mechanism model
CN108446735A (en) * 2018-03-06 2018-08-24 宁波大学 A kind of feature selection approach optimizing neighbour's constituent analysis based on differential evolution
CN109389314A (en) * 2018-10-09 2019-02-26 宁波大学 A kind of quality hard measurement and monitoring method based on optimal neighbour's constituent analysis
CN111915121A (en) * 2019-09-07 2020-11-10 宁波大学 Chemical process fault detection method based on generalized typical variable analysis

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011145846A (en) * 2010-01-14 2011-07-28 Hitachi Ltd Anomaly detection method, anomaly detection system and anomaly detection program
JP2013257251A (en) * 2012-06-14 2013-12-26 Internatl Business Mach Corp <Ibm> Anomaly detection method, program, and system

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105116726A (en) * 2015-07-20 2015-12-02 宁波大学 Parameter design method for nonlinear predictive controller based on mechanism model
CN108446735A (en) * 2018-03-06 2018-08-24 宁波大学 A kind of feature selection approach optimizing neighbour's constituent analysis based on differential evolution
CN109389314A (en) * 2018-10-09 2019-02-26 宁波大学 A kind of quality hard measurement and monitoring method based on optimal neighbour's constituent analysis
CN111915121A (en) * 2019-09-07 2020-11-10 宁波大学 Chemical process fault detection method based on generalized typical variable analysis

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
"JADE:Adaptive Differential Evolution With Optional External Archive";Jingqiao Zhang等;《IEEE Transcations on Evolutionary Computation》;20091031;全文 *
基于多元统计分析的轧钢过程故障诊断与质量预报研究;石怀涛;《中国优秀硕士论文数据库 工程科技Ⅰ辑 》;20150715;全文 *
基于粒子群优化算法的熔融指数预报;赵成业等;《控制工程》;20090720;全文 *

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