CN112442919A - Connecting agent suitable for tipping paper containing acid composite flavor and preparation method thereof - Google Patents
Connecting agent suitable for tipping paper containing acid composite flavor and preparation method thereof Download PDFInfo
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- CN112442919A CN112442919A CN202011433695.4A CN202011433695A CN112442919A CN 112442919 A CN112442919 A CN 112442919A CN 202011433695 A CN202011433695 A CN 202011433695A CN 112442919 A CN112442919 A CN 112442919A
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- tipping paper
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/20—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/20—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H19/22—Polyalkenes, e.g. polystyrene
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/34—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising cellulose or derivatives thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/10—Packing paper
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paper (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a connecting agent suitable for acid-containing composite flavor tipping paper and a preparation method thereof, wherein the connecting agent is prepared from the following raw materials in parts by weight: 5-20 parts of polyvinyl alcohol, 1-10 parts of polyvinylpyrrolidone, 1-10 parts of hydroxyethyl cellulose, 1-10 parts of alcohol-soluble rosin modified resin, 0.1-0.5 part of edible polyethylene wax, 10-50 parts of ethanol and 30-70 parts of purified water. The linking agent is weakly acidic, does not react with sour substances, and special components in the linking agent can generate complexation with acidic groups, so that the decay period of the acidic substances is prolonged, and the sour taste is kept for a longer time. Meanwhile, the bonding agent also has the characteristics of transparent paint film, no influence on the color of the ground color, firm adhesion with the ground color ink layer, wear resistance, environmental protection, safety, simple and easily controlled production process and the like.
Description
Technical Field
The invention relates to a coating composition, in particular to a connecting agent suitable for tipping paper containing acid composite flavor and a preparation method thereof.
Background
The tipping paper is a special paper which takes base paper (white base paper, aluminized transfer paper and the like) as a base material and is used for rolling and jointing a cigarette branch section and a filter stick section through processes such as prepress design, printing processing, post-printing treatment and the like. With the progress of the technology of the cigarette industry, the promotion of related products and technologies is promoted, and the tipping paper is used as an important element in cigarettes and has great innovation in functions and purposes. The application of the tipping paper in cigarette enterprises is not limited to simple packaging any more, the decoration and printing aesthetic property of the tipping paper are more important, and the tipping paper with a single connecting function can not meet the design requirement of cigarettes. The tipping paper is in direct contact with the oral cavity of a consumer, so that developers and the consumer are prompted to expect that the tipping paper has certain special mouthfeel, different mouthfeel such as sweet, sour, cool, sweet and cool taste is given to the tipping paper through technical innovation, the consumer obtains special taste experience of the mouth and the lip in the smoking process, and special taste experience coordinated with the cigarette fragrance is captured. As a complement to the traditional type, tipping papers with a certain mouth feel have gained wide acceptance and favor in the market once they are launched.
The tipping paper containing acid and acid-containing composite flavor is an important one, and is prepared by adding a single sour substance or a sour substance and other taste substances through a certain production process. Due to the special physicochemical properties of the sour substances, such as faintly acid, water solubility and the like, the processing process of the sour substances is more special than other taste types such as sweet, cool and the like. By using the conventional solvent-type connecting agent, the sour substance cannot be dissolved, a homogeneous system cannot be formed with the solvent-type connecting agent, the quality of the production process is difficult to control, and meanwhile, the sour substance can migrate to the surface of the tipping paper and be attenuated quickly, the sour taste can disappear quickly, and the storage period is short. The aqueous connecting agent generally contains alkaline amines, which can generate acid-base neutralization reaction with sour substances, directly destroy the chemical structure of the sour substances, and cannot achieve the designed acidic taste.
Disclosure of Invention
In order to solve the defects of the prior art, the invention aims to provide a connecting agent suitable for tipping paper containing acid composite flavor and a preparation method thereof. The connecting agent is weakly acidic, does not react with sour substances, and special components in the connecting agent can generate complexation with acidic groups to prolong the decay period of the sour substances, so that the sour is kept for a longer time.
In order to achieve the purpose, the invention adopts the following technical means: a connecting agent suitable for tipping paper with sour taste is prepared from the following raw materials in parts by weight: 5-20 parts of polyvinyl alcohol, 1-10 parts of polyvinylpyrrolidone, 1-10 parts of hydroxyethyl cellulose, 1-10 parts of alcohol-soluble rosin modified resin, 0.1-0.5 part of edible polyethylene wax, 10-50 parts of ethanol and 30-70 parts of purified water.
Preferably, the connecting agent suitable for the sour taste tipping paper comprises the following raw materials in parts by weight: 8-12 parts of polyvinyl alcohol, 3-4 parts of polyvinylpyrrolidone, 1-3 parts of hydroxyethyl cellulose, 2-6 parts of alcohol-soluble rosin modified resin, 0.1-0.3 part of edible polyethylene wax, 20-40 parts of ethanol and 40-60 parts of purified water.
The polyvinyl alcohol (PVA) is prepared by vinyl acetate through polymerization reaction and alcoholysis, is a white, stable and nontoxic water-soluble high polymer, can be quickly dissolved in water to form a stable colloid, and the water is a good solvent of the polyvinyl alcohol. The resulting film has excellent adhesion, solvent resistance, abrasion resistance, tensile strength and oxygen barrier properties. Since polyvinyl alcohol (PVA) has both hydrophilic and hydrophobic functional groups, it is a substance having interfacial activity and therefore can be used as a protective colloid in the case of emulsion or suspension polymerization of a polymer. PVA is hardly affected by weak acids, weak bases or organic solvents, and has high oil resistance. The method is mainly used for producing products such as synthetic fibers, plastics, adhesives, coatings, novel building materials and the like, and is widely applied to the industries and fields such as chemical industry, textile industry, printing and papermaking, leather making industry, building industry and the like.
Polyvinylpyrrolidone (PVP) is a nonionic aqueous high molecular compound, is the most distinctive of N-vinyl amide polymers, and is the most deeply and widely researched fine chemical varieties. Has the general properties of water-soluble high molecular compounds, such as colloid protection, film-forming property, caking property, hygroscopicity, solubilization or coacervation. PVP can form solid-state complexes with many materials, particularly compounds containing hydroxyl, carboxyl, amino, and other active hydrogen atoms. The thermodynamic activity of the micromolecular substances is reduced after the micromolecular substances are complexed by PVP, so that the stability is improved; PVP is dissolved in most organic solvents, so that the toxicity is low and the biocompatibility is good. Can be used as a thickening agent, a stabilizing agent and a particle size regulator in high-molecular emulsion polymerization and suspension polymerization and can be added into ink and ink as a surface coating agent of organic azo pigments.
Hydroxyethyl cellulose (HEC), formula (C)2H6O2)nIs a white or light yellow, tasteless and nontoxic fibrous or powdery solid, is prepared by etherification reaction of alkali cellulose and ethylene oxide (or chloroethanol), belongs to nonionic soluble cellulose ether, and has the softening temperature: 135 ℃ and 140 ℃. HEC has been widely used in the fields of oil extraction, paints, construction, medical food, textile, paper making, and polymer polymerization because it has properties of good thickening, suspending, dispersing, emulsifying, binding, film forming, moisture protecting, and protective colloid providing.
The alcohol-soluble rosin modified resin is light-colored resin formed by modifying rosin, dibasic acid and polybasic acid. Color (iron cobalt color number): 4-8; acid value: 180-; softening point (ring and ball method): 90-150 ℃. The application is as follows: the alcohol-soluble rosin resin is partially esterified by unsaturated acid modified rosin and polyhydric alcohol, can be dissolved in solvents such as ethanol, methanol, gasoline and the like, and can be dissolved in alcohol-soluble gravure printing ink, varnish, water-based ink, paint and the like.
The food-grade polyethylene wax is superfine polyethylene wax micropowder, and the product is white powder, and has the special properties of low viscosity, high softening point, white color, high glossiness, good lubricity, higher hardness, good wear resistance, adhesion resistance, stain resistance, precipitation resistance, scratch resistance, smooth hand feeling, excellent dispersibility and the like. It has good light resistance and chemical property, can be used as a carrier of pigment, can improve the wear resistance of paint and ink, improves the dispersibility of pigment and filler, and prevents pigment from sinking. No toxicity and corrosion, high softening point, high hardness and moderate viscosity. Compared with resins, the polyethylene hydrocarbon resin has low melt viscosity, similar chemical resistance, excellent electrical properties and excellent heat resistance. Has excellent compatibility with various plastics, resins, paraffin and the like. Has special dissolving behavior for the solvent. The ink is applied to the fields of woodenware paint, industrial paint, powder coating, inner printing, surface printing, silk screen, relief printing, intaglio printing and the like.
Ethanol is an organic substance, commonly called alcohol, is saturated monohydric alcohol with a hydroxyl group, is flammable and volatile colorless transparent liquid at normal temperature and normal pressure, and has the smell of bouquet and slight irritation in an aqueous solution. Has the smell of wine and pungent taste, and is slightly sweet. The ethanol has wide application range, and can be used for preparing acetic acid, beverages, essence, paint, ink and the like.
The preparation method of the connecting agent suitable for the tipping paper with sour taste comprises the following steps:
a. adding purified water weighed according to the proportion into a dispersion machine, and gradually adding polyvinyl alcohol, polyvinylpyrrolidone and hydroxyethyl cellulose weighed according to the proportion under the condition that the stirring speed is 100-;
b. adjusting the stirring speed of the dispersion machine to 600-;
c. adding ethanol weighed according to the proportion into a container, gradually adding the alcohol-soluble rosin modified resin weighed according to the proportion under the condition that the stirring speed is 100-one-step at 300 r/min, adjusting the stirring speed to be 600-one-step at 1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain a mixed solution B;
d. under the condition that the stirring speed is 100-300 r/min, adding food-grade polyethylene wax weighed according to the proportion into the mixed solution B, adjusting the stirring speed to be 600-1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain mixed solution C;
e. adding the mixed solution C into the mixed solution A, stirring at the stirring speed of 600-1000 r/min for 0.5h at normal temperature until the mixture is completely and uniformly dispersed, complementing the mixture to 100 parts by using ethanol, and filtering by using a 180-200-mesh screen to obtain the connecting agent suitable for the sour taste tipping paper.
The invention has the following beneficial effects:
the connecting agent is weakly acidic, does not react with acidic substances, and can complex with acidic groups to prolong the decay period of the acidic substances, so that the acidity is kept for a longer time.
The connecting agent suitable for the sour taste tipping paper has the characteristics of transparent paint film, firm adhesion with a ground color ink layer and wear resistance, and does not influence the ground color.
The connecting agent suitable for the tipping paper with sour taste prepared by the invention is green, environment-friendly, safe, and simple and easy to control in production process.
Detailed Description
Example 1
The specific formula of the embodiment comprises the following components in parts by weight: 12 parts of polyvinyl alcohol, 4 parts of polyvinylpyrrolidone, 1 part of hydroxyethyl cellulose, 2.9 parts of alcohol-soluble rosin modified resin, 0.1 part of edible polyethylene wax, 20 parts of ethanol and 60 parts of purified water.
The production is carried out according to the following steps:
a. adding purified water weighed according to the proportion into a dispersion machine, and gradually adding polyvinyl alcohol, polyvinylpyrrolidone and hydroxyethyl cellulose weighed according to the proportion under the condition that the stirring speed is 100-;
b. adjusting the stirring speed of the dispersion machine to 600-;
c. adding ethanol weighed according to the proportion into a container, gradually adding the alcohol-soluble rosin modified resin weighed according to the proportion under the condition that the stirring speed is 100-one-step at 300 r/min, adjusting the stirring speed to be 600-one-step at 1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain a mixed solution B;
d. under the condition that the stirring speed is 100-300 r/min, adding food-grade polyethylene wax weighed according to the proportion into the mixed solution B, adjusting the stirring speed to be 600-1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain mixed solution C;
e. adding the mixed solution C into the mixed solution A, stirring at the stirring speed of 600-1000 r/min for 0.5h at normal temperature until the mixture is completely and uniformly dispersed, complementing the mixture to 100 parts by using ethanol, and filtering by using a 180-200-mesh screen to obtain the connecting agent suitable for the sour taste tipping paper.
Adding a proper amount of citric acid into the prepared connecting agent, and adopting a printing plate with 110 lines/cm, drying temperature of 130-2Printing process with dry coating amount of 32-45g/m2The surface of the tipping paper is printed, dried and rolled to obtain the sour taste tipping paper product. The tipping paper has light sour taste, and is firmly adhered to the bottom color ink layer and is wear-resistant.
Example 2
The specific formula of the embodiment comprises the following components in parts by weight: 10 parts of polyvinyl alcohol, 3.5 parts of polyvinylpyrrolidone, 2 parts of hydroxyethyl cellulose, 4.3 parts of alcohol-soluble rosin modified resin, 0.2 part of edible polyethylene wax, 30 parts of ethanol and 50 parts of purified water.
The production is carried out according to the following steps:
a. adding purified water weighed according to the proportion into a dispersion machine, and gradually adding polyvinyl alcohol, polyvinylpyrrolidone and hydroxyethyl cellulose weighed according to the proportion under the condition that the stirring speed is 100-;
b. adjusting the stirring speed of the dispersion machine to 600-;
c. adding ethanol weighed according to the proportion into a container, gradually adding the alcohol-soluble rosin modified resin weighed according to the proportion under the condition that the stirring speed is 100-one-step at 300 r/min, adjusting the stirring speed to be 600-one-step at 1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain a mixed solution B;
d. under the condition that the stirring speed is 100-300 r/min, adding food-grade polyethylene wax weighed according to the proportion into the mixed solution B, adjusting the stirring speed to be 600-1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain mixed solution C;
e. adding the mixed solution C into the mixed solution A, stirring at the stirring speed of 600-1000 r/min for 0.5h at normal temperature until the mixture is completely and uniformly dispersed, complementing the mixture to 100 parts by using ethanol, and filtering by using a 180-200-mesh screen to obtain the connecting agent suitable for the sour taste tipping paper.
Adding a proper amount of malic acid into the prepared connecting agent, and adopting a printing plate with 110 lines/cm at a drying temperature of 130-2Printing process with dry coating amount of 32-45g/m2The surface of the tipping paper is printed, dried and rolled to obtain the sour taste tipping paper product. The tipping paper has light sour taste, and is firmly adhered to the bottom color ink layer and is wear-resistant.
Example 3
The specific formula of the embodiment comprises the following components in parts by weight: 8 parts of polyvinyl alcohol, 3 parts of polyvinylpyrrolidone, 3 parts of hydroxyethyl cellulose, 5.7 parts of alcohol-soluble rosin modified resin, 0.3 part of edible polyethylene wax, 40 parts of ethanol and 40 parts of purified water.
The production is carried out according to the following steps:
a. adding purified water weighed according to the proportion into a dispersion machine, and gradually adding polyvinyl alcohol, polyvinylpyrrolidone and hydroxyethyl cellulose weighed according to the proportion under the condition that the stirring speed is 100-;
b. adjusting the stirring speed of the dispersion machine to 600-;
c. adding ethanol weighed according to the proportion into a container, gradually adding the alcohol-soluble rosin modified resin weighed according to the proportion under the condition that the stirring speed is 100-one-step at 300 r/min, adjusting the stirring speed to be 600-one-step at 1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain a mixed solution B;
d. under the condition that the stirring speed is 100-300 r/min, adding food-grade polyethylene wax weighed according to the proportion into the mixed solution B, adjusting the stirring speed to be 600-1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain mixed solution C;
e. adding the mixed solution C into the mixed solution A, stirring at the stirring speed of 600-1000 r/min for 0.5h at normal temperature until the mixture is completely and uniformly dispersed, complementing the mixture to 100 parts by using ethanol, and filtering by using a 180-200-mesh screen to obtain the connecting agent suitable for the sour taste tipping paper.
Adding a proper amount of the neotame and malic acid compound into the prepared connecting agent, and adopting a printing plate with the temperature of 20-30 ℃ and the relative humidity of 50-70 percent to dry the printing plate at the temperature of 130-2Printing process with dry coating amount of 32-45g/m2The surface of the tipping paper is printed, dried and rolled to obtain the sour and sweet taste tipping paper product. The tipping paper has light sour and sweet taste, and is firmly adhered to the base color ink layer and is wear-resistant.
Example 4
A connecting agent suitable for tipping paper with sour taste is prepared from the following raw materials in parts by weight: 5 parts of polyvinyl alcohol, 10 parts of polyvinylpyrrolidone, 4 parts of hydroxyethyl cellulose, 5.5 parts of alcohol-soluble rosin modified resin, 0.5 part of edible polyethylene wax, 45 parts of ethanol and 30 parts of purified water.
The procedure was as in example 1.
Adding a proper amount of the Neotame and citric acid compound into the prepared connecting agent, and adopting a printing plate with 110 lines/cm at the drying temperature of 130 ℃ and the printing speed of 180 DEG/min of 0.5-0.8g/m in the environment with the temperature of 20-30 ℃ and the relative humidity of 50-70 percent2Printing process with dry coating amount of 32-45g/m2The surface of the tipping paper is printed, dried and rolled to obtain the sour and sweet taste tipping paper product. The tipping paper has light sour and sweet taste, and is firmly adhered to the base color ink layer and is wear-resistant.
Example 5
A connecting agent suitable for tipping paper with sour taste is prepared from the following raw materials in parts by weight: 15 parts of polyvinyl alcohol, 1 part of polyvinylpyrrolidone, 2 parts of hydroxyethyl cellulose, 1.9 parts of alcohol-soluble rosin modified resin, 0.1 part of edible polyethylene wax, 10 parts of ethanol and 70 parts of purified water.
The procedure was as in example 1.
Adding a proper amount of the neotame and malic acid compound into the prepared connecting agent, and adopting a printing plate with the temperature of 20-30 ℃ and the relative humidity of 50-70 percent to dry the printing plate at the temperature of 130-2Printing process with dry coating amount of 32-45g/m2The surface of the tipping paper is printed, dried and rolled to obtain the sour and sweet taste tipping paper product. The tipping paper has light sour and sweet taste, and is firmly adhered to the base color ink layer and is wear-resistant.
Claims (3)
1. The connecting agent suitable for the tipping paper containing the acid composite flavor is characterized by comprising the following raw materials in parts by weight: 5-20 parts of polyvinyl alcohol, 1-10 parts of polyvinylpyrrolidone, 1-10 parts of hydroxyethyl cellulose, 1-10 parts of alcohol-soluble rosin modified resin, 0.1-0.5 part of edible polyethylene wax, 10-50 parts of ethanol and 30-70 parts of purified water.
2. The connecting agent suitable for the tipping paper containing the acid composite flavor according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 8-12 parts of polyvinyl alcohol, 3-4 parts of polyvinylpyrrolidone, 1-3 parts of hydroxyethyl cellulose, 2-6 parts of alcohol-soluble rosin modified resin, 0.1-0.3 part of edible polyethylene wax, 20-40 parts of ethanol and 40-60 parts of purified water.
3. The method for preparing the binding agent suitable for the sour taste tipping paper according to any one of claims 1 to 2, characterized by comprising the following steps:
a. adding purified water weighed according to the proportion into a dispersion machine, and gradually adding polyvinyl alcohol, polyvinylpyrrolidone and hydroxyethyl cellulose weighed according to the proportion under the condition that the stirring speed is 100-;
b. adjusting the stirring speed of the dispersion machine to 600-;
c. adding ethanol weighed according to the proportion into a container, gradually adding the alcohol-soluble rosin modified resin weighed according to the proportion under the condition that the stirring speed is 100-one-step at 300 r/min, adjusting the stirring speed to be 600-one-step at 1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain a mixed solution B;
d. under the condition that the stirring speed is 100-300 r/min, adding food-grade polyethylene wax weighed according to the proportion into the mixed solution B, adjusting the stirring speed to be 600-1000 r/min after the addition is finished, and stirring at normal temperature for 1-2 h to obtain mixed solution C;
e. adding the mixed solution C into the mixed solution A, stirring at the stirring speed of 600-1000 r/min for 0.5h at normal temperature until the mixture is completely and uniformly dispersed, complementing the mixture to 100 parts by using ethanol, and filtering by using a 180-200-mesh screen to obtain the binder suitable for the sour taste tipping paper.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202011433695.4A CN112442919B (en) | 2020-12-10 | 2020-12-10 | Connecting agent suitable for acid-containing composite-flavor tipping paper and preparation method thereof |
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| CN202011433695.4A CN112442919B (en) | 2020-12-10 | 2020-12-10 | Connecting agent suitable for acid-containing composite-flavor tipping paper and preparation method thereof |
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| CN112442919B CN112442919B (en) | 2023-05-05 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114438826A (en) * | 2022-02-14 | 2022-05-06 | 河南中烟工业有限责任公司 | Sweet-taste-profile-modified neotame sweetener suitable for tipping paper for cigarettes and preparation method and application thereof |
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| CN109294328A (en) * | 2018-10-10 | 2019-02-01 | 玉溪接装纸制造有限公司 | A kind of gravure ink binder and preparation method thereof suitable for tipping paper of aluminizing |
| CN110747691A (en) * | 2019-09-25 | 2020-02-04 | 云南中烟工业有限责任公司 | Anti-lip adhesion tipping paper for cigarettes |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102732098A (en) * | 2012-07-23 | 2012-10-17 | 玉溪市星源油墨厂 | Ink for low-heavy metal tipping paper, and preparation method thereof |
| CN108264797A (en) * | 2018-02-08 | 2018-07-10 | 玉溪接装纸制造有限公司 | It is a kind of for gravure pearly-lustre varnish of tipping paper and preparation method thereof |
| CN108576922A (en) * | 2018-03-21 | 2018-09-28 | 云南中烟工业有限责任公司 | The complex additive and its preparation method and application of phenol release amount in a kind of reduction flue gas |
| CN109294328A (en) * | 2018-10-10 | 2019-02-01 | 玉溪接装纸制造有限公司 | A kind of gravure ink binder and preparation method thereof suitable for tipping paper of aluminizing |
| CN110747691A (en) * | 2019-09-25 | 2020-02-04 | 云南中烟工业有限责任公司 | Anti-lip adhesion tipping paper for cigarettes |
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| CN114438826A (en) * | 2022-02-14 | 2022-05-06 | 河南中烟工业有限责任公司 | Sweet-taste-profile-modified neotame sweetener suitable for tipping paper for cigarettes and preparation method and application thereof |
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|---|---|
| CN112442919B (en) | 2023-05-05 |
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