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CN112076134A - Noni plant essence shampoo and preparation method thereof - Google Patents

Noni plant essence shampoo and preparation method thereof Download PDF

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Publication number
CN112076134A
CN112076134A CN202011181965.7A CN202011181965A CN112076134A CN 112076134 A CN112076134 A CN 112076134A CN 202011181965 A CN202011181965 A CN 202011181965A CN 112076134 A CN112076134 A CN 112076134A
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parts
extract
phase
shampoo
noni
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麦钧策
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Wanning Fengshou Nuoli Biotechnology Co ltd
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Wanning Fengshou Nuoli Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/737Galactomannans, e.g. guar; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9755Gymnosperms [Coniferophyta]
    • A61K8/9761Cupressaceae [Cypress family], e.g. juniper or cypress
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Biotechnology (AREA)
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  • Mycology (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention provides noni plant essence shampoo, which can moisturize and care scalp by adding noni extract into the shampoo, and achieves the effects of mildly repairing damaged and withered hair. In a preferable embodiment of the invention, the shampoo can generate more foams and has strong foam endurance by adding 3 surfactants including DMDM hydantoin, methylchloroisothiazolinone and methylisothiazolinone to the shampoo. The invention also provides a preparation method of the shampoo.

Description

Noni plant essence shampoo and preparation method thereof
Technical Field
The invention relates to the technical field of lightening industry, in particular to noni plant essence shampoo and a preparation method thereof.
Background
Shampoo, also known as shampoo, shampoo or shampoo, is the most widely used hair washing product and one of the most commonly used hair cosmetics. It can be used for cleaning human body secreted oil, sweat scale, cells detached from scalp, foreign dust, microorganism, and residue and unpleasant odor of styling product, etc. attached to scalp and hair, and keeping scalp and hair clean and beautiful.
Foreign shampoos began to emerge in the early 30's of the 20 th century. Before the shampoo, people mainly use soap, perfumed soap, washing powder and the like to clean scalp and hair, and then use coconut oil soap to prepare liquid shampoo, but the shampoo products taking soap as base material have many disadvantages, especially in hard water, the soap taking potassium fatty acid as raw material can form sticky precipitate when meeting calcium and magnesium ions in hard water, and residue which is difficult to clean is left on hair; moreover, after washing hair with soap, the hair becomes sticky, non-glossy and not easy to comb.
Liquid emulsified shampoo and cream emulsified shampoo made of sodium lauryl sulfate as base material are available in the early 40 th century. Compared with soap and soap, the shampoo has several advantages: the foaming and cleaning capability is strong, and abundant foam can be generated even under the condition of hard water quality; easy to clean, does not leave unnecessary sediment residues, and is milder than soap products.
The shampoo in China is published in the early 60 s of the 20 th century, and is developed to the present, so that the shampoo becomes an indispensable shampoo product in the life of people. However, how to care the scalp and hair while cleaning, so as to moisturize the scalp and improve the quality of the hair, is a problem to be further solved in the industry.
In view of this, the invention is particularly proposed.
Disclosure of Invention
The first purpose of the invention is to provide noni plant essence shampoo.
The second purpose of the invention is to provide a preparation method of the shampoo.
In order to achieve the purpose, the technical scheme of the invention is as follows:
the invention relates to noni plant essence shampoo which comprises the following raw materials in parts by weight: 40-60 parts of pure water, 12-30 parts of surfactant, 5-10 parts of noni extract, 0.1-0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 0.05-0.2 part of citric acid, 0.01-0.1 part of EDTA disodium and 0.5-1 part of preservative.
Preferably, the surfactant is selected from at least one of sodium laureth sulfate, sodium lauroyl sarcosinate, lauramidopropyl hydroxysultaine, cocamide DEA.
Preferably, the surfactant comprises 3-5 parts of sodium laureth sulfate, 3-5 parts of sodium lauroyl sarcosinate, 4-10 parts of lauramidopropyl hydroxysultaine and 2-8 parts of cocamide DEA.
Preferably, the shampoo further comprises the following active substances: 1-5 parts of polygonum multiflorum extract, 1-5 parts of ginseng extract, 1-5 parts of platycladus orientalis extract, 1-5 parts of safflower extract and 1-5 parts of glycyrrhiza glabra extract.
Preferably, the shampoo further comprises 0.01-0.5 part of sodium chloride, 100.01-0.5 part of polyquaternium, 0.01-0.5 part of magnesium nitrate and 0.01-0.5 part of magnesium chloride.
Preferably, the preservative is selected from at least one of DMDM hydantoin, methylchloroisothiazolinone, methylisothiazolinone.
Preferably, the preservative comprises 0.1-0.4 part of DMDM hydantoin, 0.2-0.4 part of methyl chloroisothiazolinone and 0.2-0.4 part of methyl isothiazolinone.
Preferably, the shampoo further comprises essence and pigment, wherein the essence is 0.01-0.1 part, the pigment is 0.01-0.1 part, and the pigment is selected from at least one of CI 19140, CI 16255 and CI 42090.
Preferably, the shampoo comprises the following raw materials in parts by weight: 40-60 parts of pure water, 3-5 parts of sodium laureth sulfate, 3-5 parts of sodium lauroyl sarcosinate, 4-10 parts of lauramidopropyl hydroxysulfobetaine, 2-8 parts of cocamide DEA, 5-10 parts of noni fruit extract, 1-5 parts of polygonum multiflorum extract, 1-5 parts of ginseng extract, 1-5 parts of platycladus orientalis extract, 1-5 parts of safflower extract, 1-5 parts of glycyrrhiza glabra extract, 0.01-0.5 part of sodium chloride, 100.01-0.5 part of polyquaternium, 0.01-0.5 part of magnesium nitrate, 0.01-0.5 part of magnesium chloride, 0.1-0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 0.05-0.2 part of citric acid, 0.01-0.1 part of EDTA disodium, 0.1-0.4 part of DMDM hydantoin, 0.2-0.4 part of methyl chloro isothiazolinone, 0.2-0.4 part of methyl isothiazolinone, 0.2-0.4 part of essence and 0.01-0.1 part of pigment.
The invention also relates to a preparation method of the shampoo, which comprises the following steps:
(1) uniformly mixing 35-55 parts of pure water, disodium EDTA (ethylene diamine tetraacetic acid), sodium laureth sulfate, sodium lauroyl sarcosinate, lauramidopropyl hydroxysultaine and cocamide DEA to obtain a phase A for later use;
5 parts of pure water and guar gum hydroxypropyl trimethyl ammonium chloride are uniformly mixed to obtain a phase B for later use;
uniformly mixing the noni extract, the polygonum multiflorum extract, the ginseng extract, the platycladus orientalis extract, the safflower extract and the glycyrrhiza glabra extract to obtain a phase C for later use;
uniformly mixing the sodium chloride, the polyquaternium-10, the magnesium nitrate and the magnesium chloride to obtain a phase D for later use;
uniformly mixing the DMDM hydantoin, the methyl chloroisothiazolinone and the methyl isothiazolinone to obtain an E phase for later use;
uniformly mixing the essence and the pigment to obtain an F phase for later use;
(2) heating the phase A to 75-80 ℃ in a stirring pot under the stirring condition;
(3) adding the phase B into a stirring pot, stirring, keeping the temperature until the phase B is uniformly mixed, and cooling;
(4) adding the phase C into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 50-60 ℃;
(5) adding the phase D into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 40-45 ℃;
(6) stopping heating, adding the phase E and the phase F components into the stirring pot, stirring until the phase E and the phase F components are uniformly dissolved, adjusting the pH value to 6-6.5 by using citric acid, and discharging.
The invention has the beneficial effects that:
the invention provides noni plant essence shampoo, which can moisturize and care scalp by adding noni extract into the shampoo, and achieves the effects of mildly repairing damaged and withered hair.
In a preferable embodiment of the invention, the shampoo can generate more foams and has strong foam endurance by adding 3 surfactants including DMDM hydantoin, methylchloroisothiazolinone and methylisothiazolinone to the shampoo.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
The embodiment of the invention relates to noni plant essence shampoo which comprises the following raw materials in parts by weight: 40-60 parts of pure water, 12-30 parts of surfactant, 5-10 parts of noni extract, 0.1-0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 0.05-0.2 part of citric acid, 0.01-0.1 part of EDTA disodium and 0.5-1 part of preservative.
Wherein the Morinda citrifolia (Morinda citrifolia) extract is obtained from the fruit of Morinda citrifolia. It contains high content of alkaloid, vitamins and flavonoids, has strong antioxidant effect, and has scalp nourishing effect. The EDTA disodium is fully called as ethylene diamine tetraacetic acid disodium, is used as a chelating agent, plays a stabilizing role in the shampoo, and has a certain synergistic effect on an antiseptic system and an antioxidant system. Guar hydroxypropyl trimethyl ammonium chloride is used as a conditioner and has an antistatic effect. Citric acid is a pH regulator.
In one embodiment of the invention, the surfactant is selected from at least one of sodium laureth sulfate, sodium lauroyl sarcosinate, lauramidopropyl hydroxysultaine, cocamide DEA. Further, the surfactant comprises 3-5 parts of sodium laureth sulfate, 3-5 parts of sodium lauroyl sarcosine, 4-10 parts of lauramidopropyl hydroxysultaine and 2-8 parts of cocamide DEA.
Among them, lauramidopropyl hydroxysultaine is a zwitterionic surfactant, has excellent stability under acidic and alkaline conditions, and is often used in combination with anionic, cationic and nonionic surfactants as a main surfactant in a shampoo. Sodium laureth sulfate, sodium lauroyl sarcosinate and cocamide DEA are used as auxiliary surfactants in shampoo, and have foam-increasing and thickening effects. Especially, cocamide DEA has water solubility and oil solubility, so that water and oil can be uniformly dispersed in the solution, and oily dirt in hair can be caught to be easily washed off.
In one embodiment of the invention, the shampoo further comprises the following active substances: 1-5 parts of polygonum multiflorum extract, 1-5 parts of ginseng extract, 1-5 parts of platycladus orientalis extract, 1-5 parts of safflower extract and 1-5 parts of glycyrrhiza glabra extract.
Wherein the Polygoni Multiflori radix extract is extracted from dried root tuber of Polygoni Multiflori radix of Polygonaceae, and contains lecithin, emodin, and rhein. Radix Polygoni Multiflori has effects of nourishing liver and kidney, and replenishing essence and blood, and can be used for preventing and treating premature gray hair. The Ginseng radix extract is extracted from root, stem and leaf of Panax ginseng C.A. Meyer of Araliaceae, is rich in ginsenoside, and has effects of enhancing activity of human surface cell, and inhibiting aging. The product can be used in daily chemical products for removing speckle, reducing wrinkle, activating skin cells, and improving skin elasticity. The folium Platycladi extract is extracted from branch tip and leaf of Thuja orientalis of Cupressaceae, and has effects of cooling blood, stopping bleeding, promoting hair growth, and blackening hair. The Carthami flos extract contains carthamin and safflower yellow. The main function of safflower is to promote blood circulation and remove blood stasis, and it is used for scalp to dilate epidermal capillary, increase blood supply and promote hair growth. The Glycyrrhiza glabra extract is extracted from the stem of Glycyrrhiza glabra and has effects of preventing pachylosis, relieving inflammation, and inhibiting bacteria.
In one embodiment of the invention, the shampoo further comprises 0.01-0.5 part of sodium chloride, 100.01-0.5 part of polyquaternium, 0.01-0.5 part of magnesium nitrate and 0.01-0.5 part of magnesium chloride.
The addition of the above salts can balance electrolyte of scalp, reduce irritation of androgen to hair follicle, and inhibit metabolism disorder. In addition, it can inhibit local bacterial reproduction of scalp, and reduce oil secretion and dandruff.
In one embodiment of the invention, the preservative is selected from at least one of DMDM hydantoin, methylchloroisothiazolinone, methylisothiazolinone. Further, the preservative comprises 0.1-0.4 part of DMDM hydantoin, 0.2-0.4 part of methyl chloroisothiazolinone and 0.2-0.4 part of methyl isothiazolinone.
The DMDM hydantoin is a broad-spectrum and efficient antibacterial preservative, resists gram-positive bacteria, gram-negative bacteria, mold, yeast and the like by releasing formaldehyde, has good compatibility with various emulsifiers and surfactants, can be used in cosmetics and personal care, and has the maximum use concentration of 0.6%. Methylisothiazolinone (MIT) is a highly effective bactericide, has good effect in inhibiting the growth of microorganisms, and can inhibit the growth of bacteria, fungi, mold and mildew, and the product can be directly added into the fields of personal care products, cosmetics, coatings, paper pulp and the like.
In one embodiment of the invention, the shampoo further comprises essence and pigment, wherein the essence is 0.01-0.1 part, the pigment is 0.01-0.1 part, and the pigment is at least one selected from CI 19140, CI 16255 and CI 42090.
In one specific embodiment of the invention, the shampoo comprises the following raw materials in parts by weight: 40-60 parts of pure water, 3-5 parts of sodium laureth sulfate, 3-5 parts of sodium lauroyl sarcosinate, 4-10 parts of lauramidopropyl hydroxysulfobetaine, 2-8 parts of cocamide DEA, 5-10 parts of noni fruit extract, 1-5 parts of polygonum multiflorum extract, 1-5 parts of ginseng extract, 1-5 parts of platycladus orientalis extract, 1-5 parts of safflower extract, 1-5 parts of glycyrrhiza glabra extract, 0.01-0.5 part of sodium chloride, 100.01-0.5 part of polyquaternium, 0.01-0.5 part of magnesium nitrate, 0.01-0.5 part of magnesium chloride, 0.1-0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 0.05-0.2 part of citric acid, 0.01-0.1 part of EDTA disodium, 0.1-0.4 part of DMDM hydantoin, 0.2-0.4 part of methyl chloro isothiazolinone, 0.2-0.4 part of methyl isothiazolinone, 0.2-0.4 part of essence and 0.01-0.1 part of pigment.
The invention also relates to a preparation method of the shampoo, which comprises the following steps:
(1) uniformly mixing 35-55 parts of pure water, disodium EDTA (ethylene diamine tetraacetic acid), sodium laureth sulfate, sodium lauroyl sarcosinate, lauramidopropyl hydroxysultaine and cocamide DEA to obtain a phase A for later use;
5 parts of pure water and guar gum hydroxypropyl trimethyl ammonium chloride are uniformly mixed to obtain a phase B for later use;
mixing Morinda citrifolia extract, Polygoni Multiflori radix extract, Ginseng radix extract, Chinese arborvitae extract, Carthami flos extract and Glycyrrhiza glabra extract uniformly to obtain phase C;
uniformly mixing sodium chloride, polyquaternium-10, magnesium nitrate and magnesium chloride to obtain a D phase for later use;
uniformly mixing DMDM hydantoin, methylchloroisothiazolinone and methylisothiazolinone to obtain an E phase for later use;
uniformly mixing the essence and the pigment to obtain an F phase for later use;
(2) heating the phase A to 75-80 ℃ in a stirring pot under the stirring condition;
(3) adding the phase B into a stirring pot, stirring, keeping the temperature until the phase B is uniformly mixed, and cooling;
(4) adding the phase C into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 50-60 ℃;
(5) adding the phase D into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 40-45 ℃;
(6) stopping heating, adding the phase E and the phase F components into the stirring pot, stirring until the phase E and the phase F components are uniformly dissolved, adjusting the pH value to 6-6.5 by using citric acid, and discharging.
The mechanism of the preparation process is explained as follows: 1) the phases A to D are all water-soluble substances. The phase A and the phase B can be dissolved at a high temperature of 75-80 ℃ due to the characteristics of raw materials. And guar hydroxypropyl trimonium chloride of phase B is a conditioning agent, as powdery substance, is easy to agglomerate when being added into preheated water phase independently, and is difficult to be fully dissolved when being added as A, so phase B is added after phase A. 2) The components of the phase C are all biologically active substances and need to be added after the temperature is reduced, otherwise the activity is lost. 3) Phase D is a salt that needs to be added after further cooling to prevent binding with the active. 4) Phase E is preservative, phase F is essence and pigment, and is weighed separately and added finally.
The application method of the shampoo comprises: after the hair is moistened, 5-10 mL of shampoo is uniformly smeared on the hair. Rub the lather and gently massage the hair and scalp with the finger abdomen. Gently kneading for 2-5 minutes, and washing with clear water. If the eye drops are carelessly dropped into the eye, the eye drops should be immediately washed clean with clear water.
Example 1
(1) 40 parts of pure water, 0.05 part of disodium EDTA, 4 parts of sodium laureth sulfate, 4 parts of sodium lauroyl sarcosinate, 6 parts of lauramidopropyl hydroxysultaine and 5 parts of cocamide DEA are uniformly mixed to obtain a phase A for later use.
5 parts of pure water and 0.3 part of guar gum hydroxypropyl trimethyl ammonium chloride are uniformly mixed to obtain a phase B for later use.
Mixing 8 parts of noni extract, 3 parts of polygonum multiflorum extract, 3 parts of ginseng extract, 3 parts of platycladus orientalis extract, 3 parts of safflower extract and 3 parts of glycyrrhiza glabra extract uniformly to obtain phase C for later use. Wherein the noni fruit extract is obtained from Shanghai Hepu industries, Inc., and is sold as noni fruit organic powder. Ginseng radix extract was obtained from Xianchang Yue Biotech Co., Ltd. The Polygoni Multiflori radix extract and Carthami flos extract were obtained from Hibiscus sp.37025. The extract of Chinese arborvitae is obtained from Cheng biological development Co., Ltd. Glycyrrhiza glabra extract was purchased from seiran excelo biotechnology, ltd.
And uniformly mixing 0.1 part of sodium chloride, 100.1 parts of polyquaternium, 0.1 part of magnesium nitrate and 0.1 part of magnesium chloride to obtain a phase D for later use.
And uniformly mixing 0.2 part of DMDM hydantoin, 0.3 part of methylchloroisothiazolinone and 0.3 part of methylisothiazolinone to obtain an E phase for later use.
(2) Heating the phase A to 75-80 ℃ in a stirring pot under the stirring condition;
(3) adding the phase B into a stirring pot, stirring, keeping the temperature until the phase B is uniformly mixed, and cooling;
(4) adding the phase C into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 50-60 ℃;
(5) adding the phase D into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 40-45 ℃;
(6) stopping heating, adding the phase E component into the stirring pot, stirring until the phase E component is dissolved uniformly, adjusting the pH value to 6-6.5 by using citric acid, and discharging.
In the embodiments 2-5, a certain experimental parameter is changed, other operation steps and test processes are the same as those in the embodiment 1, and specific setting modes are shown in table 1.
TABLE 1
Figure BDA0002750431180000081
Figure BDA0002750431180000091
Shampoo foam height test
(1) Foam height was measured using a rockwell foam 211 model 2151 instrument. The thermostat was first opened to stabilize the temperature of the pipe clamp sleeve water bath at 40 ℃. + -. 0.5 ℃.
(2) 2.5g of one of the shampoos prepared in the above examples was weighed, and dissolved in 1000mL of water to obtain a test solution. The inner wall of the graduated tube is firstly washed by distilled water, and then the tube wall is washed by test solution.
(3) The graduated tube piston was closed and a further dropper was used to inject 50ml of the test solution to the 50ml graduation, which had been preheated to 40 ℃.
(4) The dropping tube was filled with 200ml of a test solution, which was previously heated to 40 ℃. Then the dropping liquid tube is arranged on a prepared tube frame and is vertical to the section of the graduated tube, so that the test solution flows to the center of the graduated tube, and the outlet of the dropping liquid tube is arranged on the 900mm graduation line.
(5) The piston of the dropping tube is opened to allow the sample solution to flow down. When the test solution in the drip tube was run out, a stopwatch was started immediately and the well measured the foam height, which was then recorded over a 5 minute period. The results are retained to integer numbers and are reported in table 2.
TABLE 2
0min foam height (mm) 5min foam height (mm)
Example 1 157 140
Example 2 145 135
Example 3 160 145
Example 4 142 108
Example 5 155 138
As can be seen from the data in Table 2, the addition of 3 auxiliary surfactants (including sodium laureth sulfate, sodium lauroyl sarcosinate, and cocamide DEA) in examples 1 to 3 resulted in a large amount of foam, and the foam durability was strong, and the foam height after 5min was maintained at 135mm or more.
Example 4, which removed a co-surfactant, produced no significant difference in foam amount compared to example 1, but the foam durability was not strong.
Example 5 the noni fruit extract was not added and its ability to produce foam was similar to that of example 1. The main factor influencing the foam height is the kind of surfactant added, which is not very relevant to the active substance.
Scalp use test
Selecting 40 volunteers with the age range of 18-40 years, and selecting male and female. The volunteers were randomly divided into 4 groups of 10 persons each. Wherein 1 to 3 groups were experimental groups using the shampoos prepared in examples 1, 4 and 5, respectively; group 4 was blank and used a common commercial shampoo. The shampoo is used every day or every other day according to the habit of the user, and the experimental time is 30 days.
The using method of the shampoo comprises the following steps: fully moistening the whole scalp, rubbing 5-10 mL of shampoo to obtain foam, and then applying the foam on the hair of the scalp. The finger abdomen is kneaded for 2-5 minutes and then cleaned with clear water.
The center of the vertex of the head is selected as a test part, and the moisture content of the stratum corneum of the scalp is tested by a moisture test probe Corneometer CM825 of a skin moisture tester on the 0 th day and the 30 th day of the experiment. The results are shown in Table 3, as averaged over three tests.
TABLE 3
Moisture content (C.U.) Day 0 Day 30
Example 1 19.39±1.35 23.05±1.17
Example 4 19.04±1.21 20.23±1.11
Example 5 17.65±1.08 21.85±1.36
Blank group 18.55±1.25 19.01±1.15
As is clear from Table 3, in each of examples 1, 4 and 5, the water content of the stratum corneum of the scalp was increased after 30 days of use. Example 5 the moisturizing ability was inferior to examples 1 and 2 because no Morinda citrifolia extract was added. The shampoo has the effect of moistening scalp, and can increase the water content of scalp stratum corneum and enhance the scalp barrier function.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.

Claims (10)

1. The noni plant essence shampoo is characterized by comprising the following raw materials in parts by weight: 40-60 parts of pure water, 12-30 parts of surfactant, 5-10 parts of noni extract, 0.1-0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 0.05-0.2 part of citric acid, 0.01-0.1 part of EDTA disodium and 0.5-1 part of preservative.
2. The noni plant essence shampoo of claim 1 wherein the surfactant is selected from at least one of sodium laureth sulfate, sodium lauroyl sarcosinate, lauramidopropyl hydroxysultaine, and cocamide DEA.
3. The noni plant essence shampoo of claim 2, wherein the surfactant comprises 3-5 parts of sodium laureth sulfate, 3-5 parts of sodium lauroyl sarcosinate, 4-10 parts of lauramidopropyl hydroxysultaine, and 2-8 parts of cocamide DEA.
4. The noni plant essence shampoo of claim 1 further comprising the following active ingredients: 1-5 parts of polygonum multiflorum extract, 1-5 parts of ginseng extract, 1-5 parts of platycladus orientalis extract, 1-5 parts of safflower extract and 1-5 parts of glycyrrhiza glabra extract.
5. The noni plant essence shampoo according to claim 1, further comprising 0.01 to 0.5 parts of sodium chloride, 100.01 to 0.5 parts of polyquaternium, 0.01 to 0.5 parts of magnesium nitrate, and 0.01 to 0.5 parts of magnesium chloride.
6. The noni plant essence shampoo of claim 1 wherein the preservative is selected from at least one of DMDM hydantoin, methylchloroisothiazolinone, methylisothiazolinone.
7. The noni fruit plant essence shampoo of claim 6, wherein the preservative comprises DMDM hydantoin 0.1-0.4 parts, methylchloroisothiazolinone 0.2-0.4 parts, methylisothiazolinone 0.2-0.4 parts.
8. The noni plant essence shampoo of claim 1, further comprising 0.01-0.1 part of essence and 0.01-0.1 part of pigment, wherein the pigment is at least one selected from the group consisting of CI 19140, CI 16255 and CI 42090.
9. The noni plant essence shampoo according to any one of claims 1 to 8, wherein the shampoo comprises the following raw materials in parts by weight: 40-60 parts of pure water, 3-5 parts of sodium laureth sulfate, 3-5 parts of sodium lauroyl sarcosinate, 4-10 parts of lauramidopropyl hydroxysulfobetaine, 2-8 parts of cocamide DEA, 5-10 parts of noni fruit extract, 1-5 parts of polygonum multiflorum extract, 1-5 parts of ginseng extract, 1-5 parts of platycladus orientalis extract, 1-5 parts of safflower extract, 1-5 parts of glycyrrhiza glabra extract, 0.01-0.5 part of sodium chloride, 100.01-0.5 part of polyquaternium, 0.01-0.5 part of magnesium nitrate, 0.01-0.5 part of magnesium chloride, 0.1-0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 0.05-0.2 part of citric acid, 0.01-0.1 part of EDTA disodium, 0.1-0.4 part of DMDM hydantoin, 0.2-0.4 part of methyl chloro isothiazolinone, 0.2-0.4 part of methyl isothiazolinone, 0.2-0.4 part of essence and 0.01-0.1 part of pigment.
10. The method of preparing the shampoo of any of claims 1 to 9, comprising the steps of:
(1) uniformly mixing 35-55 parts of pure water, disodium EDTA (ethylene diamine tetraacetic acid), sodium laureth sulfate, sodium lauroyl sarcosinate, lauramidopropyl hydroxysultaine and cocamide DEA to obtain a phase A for later use;
5 parts of pure water and guar gum hydroxypropyl trimethyl ammonium chloride are uniformly mixed to obtain a phase B for later use;
uniformly mixing the noni extract, the polygonum multiflorum extract, the ginseng extract, the platycladus orientalis extract, the safflower extract and the glycyrrhiza glabra extract to obtain a phase C for later use;
uniformly mixing the sodium chloride, the polyquaternium-10, the magnesium nitrate and the magnesium chloride to obtain a phase D for later use;
uniformly mixing the DMDM hydantoin, the methyl chloroisothiazolinone and the methyl isothiazolinone to obtain an E phase for later use;
uniformly mixing the essence and the pigment to obtain an F phase for later use;
(2) heating the phase A to 75-80 ℃ in a stirring pot under the stirring condition;
(3) adding the phase B into a stirring pot, stirring, keeping the temperature until the phase B is uniformly mixed, and cooling;
(4) adding the phase C into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 50-60 ℃;
(5) adding the phase D into the stirring pot and uniformly stirring when the temperature in the stirring pot is reduced to 40-45 ℃;
(6) stopping heating, adding the phase E and the phase F components into the stirring pot, stirring until the phase E and the phase F components are uniformly dissolved, adjusting the pH value to 6-6.5 by using citric acid, and discharging.
CN202011181965.7A 2020-10-29 2020-10-29 Noni plant essence shampoo and preparation method thereof Pending CN112076134A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113633597A (en) * 2021-03-31 2021-11-12 广州市百爱神生物科技有限公司 Shampoo with plant fermentation extracted components and preparation method thereof
CN115813797A (en) * 2022-10-26 2023-03-21 海南丰席树诺丽日化有限责任公司 Application of natural noni peptide extract in shampoo and preparation method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113633597A (en) * 2021-03-31 2021-11-12 广州市百爱神生物科技有限公司 Shampoo with plant fermentation extracted components and preparation method thereof
CN115813797A (en) * 2022-10-26 2023-03-21 海南丰席树诺丽日化有限责任公司 Application of natural noni peptide extract in shampoo and preparation method

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Application publication date: 20201215