CN112022780B - Multifunctional wet tissue and preparation method thereof - Google Patents
Multifunctional wet tissue and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the technical field of wet tissues and provides a multifunctional wet tissue and a preparation method thereof, wherein the multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, and the wet tissue compound liquid comprises the following components in parts by weight: 0.01 to 0.1 portion of aloe extract, 0.1 to 0.5 portion of cucumber juice, 1 to 5 portions of mint essential oil, 0.2 to 0.4 portion of pine needle oil, 0.3 to 0.6 portion of orange peel essential oil, 1.5 to 3 portions of borneol, 0.4 to 0.8 portion of polyhexamethylene biguanide hydrochloride, 1.2 to 3.6 portions of propylene glycol, 1.5 to 3 portions of polyoxyethylene lauryl ether, 0.2 to 0.4 portion of solubilizer and 85 to 95 portions of deionized water. The problem of the wet tissue function of the prior art comparatively single is solved, and the wet tissue of preparation collects cleanness, moisturizes, antibiotic, refreshing effect in an organic whole.
Description
Technical Field
The invention relates to the technical field of wet tissues, in particular to a multifunctional wet tissue and a preparation method thereof.
Background
The wet tissue is a disposable cleaning sanitary article prepared by selecting a wet-strength soft-fiber high-permeability base material, folding, humidifying and packaging, and becomes an essential cleaning article in daily life of people due to the characteristics of basic functions of cleaning and moisturizing skin, convenience in carrying and the like. However, the current commercially available wet tissue has a single function, and with the improvement of the hygiene and cleanliness awareness of people, the wet tissue with a cleaning function is gradually unable to meet the demand, and the wet tissue with the functions of cleaning, antibiosis and the like is gradually favored.
For example, chinese patent No.: 202010224735.8 discloses a wet tissue for infants, which comprises a wet tissue base material and a wet tissue immersion liquid, wherein the wet tissue immersion liquid comprises the following components in percentage by weight: 1,3-bis
4-8% of [3- (dimethylamine) propyl ] urea/2,5-bischloromethyl-1,3,4-oxadiazole ionic polycondensate, 1-3% of plant polysaccharide, 0.1-0.2% of butyl ethyl levulinate, 1-3% of dodecanoic acid 2-epoxy ethyl methyl ester modified methoxy polyethylene glycol amine, 0.2-0.4% of transdermal agent, 0.5-1.5% of Chinese herbal medicine extract, 3-5% of glycerol and the balance of deionized water. The wet tissue for infants prepared by the invention has multiple functions of cleaning, sterilizing, disinfecting, repelling mosquitoes, relieving itching and protecting skin, has small irritation to the skin of infants, good biocompatibility, sanitary, safe and effective use, convenient carrying and simple use.
In order to meet different requirements of people, the applicant adopts different technical schemes and takes natural plant extracts as main raw materials to prepare the multifunctional wet tissue.
Disclosure of Invention
Therefore, aiming at the above, the invention provides a multifunctional wet tissue and a preparation method thereof, which solve the problem that the wet tissue in the prior art has single function.
In order to achieve the purpose, the invention is realized by the following technical scheme:
the multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the wet tissue compound liquid comprises the following components in parts by weight: 0.01 to 0.1 portion of aloe extract, 0.1 to 0.5 portion of cucumber juice, 1 to 5 portions of mint essential oil, 0.2 to 0.4 portion of pine needle oil, 0.3 to 0.6 portion of orange peel essential oil, 1.5 to 3 portions of borneol, 0.4 to 0.8 portion of polyhexamethylene biguanide hydrochloride, 1.2 to 3.6 portions of propylene glycol, 1.5 to 3 portions of polyoxyethylene lauryl ether, 0.2 to 0.4 portion of solubilizer and 85 to 95 portions of deionized water.
The further improvement is that: the base material is spunlace non-woven fabric.
The further improvement is that: the base material takes viscose fiber and polyester fiber as raw materials, and the mass ratio of the viscose fiber to the polyester fiber is 3:1-2.
The further improvement is that: the mass ratio of the viscose fibers to the polyester fibers is 3:2.
The further improvement is that: the solubilizer is PEG-60 hydrogenated castor oil or Tween-80.
The invention also provides a preparation method of the multifunctional wet tissue, which comprises the following steps:
(1) Adding lauryl alcohol polyoxyethylene ether and propylene glycol into deionized water, heating to 60-65 ℃, uniformly stirring, adding a solubilizer, borneol and polyhexamethylene biguanide hydrochloride, and uniformly stirring and dissolving;
(2) Cooling the solution obtained in the step (1) to below 40-45 ℃, adding aloe extract, cucumber juice, mint essential oil, pine needle oil and orange peel essential oil, stirring and mixing uniformly to prepare a wet tissue compound solution, adding an acid-base regulator, and regulating the pH value of the wet tissue compound solution to 5.0-7.0;
(3) Soaking the sterilized base material in the wet tissue compound liquid for 20-30 min to prepare the multifunctional wet tissue;
(4) And (4) folding, sealing and packaging the multifunctional wet tissue prepared in the step (3).
The further improvement is that: and (3) synchronously carrying out ultrasonic treatment in the stirring process in the step (2).
The further improvement is that: the ultrasonic treatment time is 8-15 min, and the frequency is 20kHz.
The aloe extract contains anthraquinone derivative, aloe rhubarb, saponin, amino acid, polysaccharide and other matters, has excellent moisture keeping and water locking effects, can form one smooth moisture absorbing film on the skin surface, and is rich in polysaccharide to relieve skin fatigue. Meanwhile, because of containing biological enzyme, the skin-care product can play a role in diminishing inflammation and sterilizing by slowly hydrolyzing with the skin, and can play a role in healing wounds by acting with collagen in the stratum corneum under the action of amino acid.
The cucumber juice has good moisturizing and whitening effects, can improve the water content of the horny layer, and has the moisturizing effect.
The mint essential oil is extracted from mint by a method such as hydro-distillation and the like, is fresh and cool, and is pleasant, contains substances stimulating the central nerve of a human body, and the substances can bring burning pain and cold feeling to people when acting on the skin surface of the human body, thereby achieving the effects of refreshing and restoring consciousness and relaxing the body and mind. Meanwhile, the mint essential oil has the function of purifying air, and is beneficial to keeping the surrounding air fresh.
The pine needle oil is plant essential oil obtained by purifying and processing pine needle leaves, can promote blood circulation, diminish inflammation and sterilize when being applied to skin, can provide rich vitamins and minerals, nourish delicate skin, improve skin elasticity and delay skin aging. The pine needle oil powder emits fragrance to regulate nerves and play a role in tranquilizing and allaying excitement. When people are tired, the pine needle oil is smeared on the temple and other parts and is gently massaged, so that the symptoms of dizziness and mental weakness can be relieved, and the pine needle oil has the functions of refreshing and restoring consciousness, and keeps people energetic.
The pericarpium Citri Junoris essential oil is aromatic mixture extracted from fresh and sweet pericarpium Citri Junoris, pericarpium Citri Tangerinae, and pericarpium Citri Grandis, and mainly contains D-limonene, linalool, citral, citronella oil, etc. The orange peel essential oil is moisture-retaining and skin-moistening, has no irritation to human body, and has good antibacterial property, and strong permeability and spreadability.
Borneol is pungent in flavor and cool in nature, and has the effects of inducing resuscitation, refreshing mind, clearing away heat and toxic materials, diminishing inflammation, relieving pain and the like.
The polyhexamethylene biguanide hydrochloride belongs to a cationic polymer, is colorless, odorless, nonirritant to skin, nontoxic and the like, has the advantages of broad-spectrum antibacterial property, high action speed, stable property and the like, and has an antibacterial mechanism that the permeability of bacterial cell membranes is changed by dissolving lipid to cause the metabolism in bacteria to be obstructed so as to kill the bacteria.
By adopting the technical scheme, the invention has the beneficial effects that:
the invention fully researches the effects of various raw materials of the wet tissue compound liquid, eliminates the possibility of mutual restriction or incompatibility among the raw materials, optimizes the weight ratio of the raw materials, ensures that the raw materials are mutually promoted in a synergistic way while exerting the self-action of the raw materials, and the prepared wet tissue has the effects of cleaning, moisturizing, antibiosis and refreshing. The wet tissue compound liquid mainly takes natural plant components as raw materials, is safe and low in irritation to skin, has different effects on various natural plant components, can promote rapid permeation and absorption of other natural plant components due to the strong permeability of the orange peel essential oil, and is quicker in action time and more remarkable in effect. The aloe extract has certain sterilization effect while playing the effects of moisturizing and locking water; similarly, the pine needle oil and the orange peel essential oil also have antibacterial properties, the three plant extracts belong to natural bactericides, a synergistic promotion effect is generated after the three plant extracts are compounded with the synthetic bactericide polyhexamethylene biguanide hydrochloride, and the antibacterial effect is superior to that of the natural bactericide or the synthetic bactericide which is singly used. The invention can relieve various fatigue symptoms such as mental weakness, dizziness and the like through the combined action of cool skin stimulation, respiration and osmotic absorption, and has the functions of refreshing, restoring consciousness and relaxing the body and mind. The wet tissue compound liquid does not contain DMDM hydantoin and paraben common preservatives, does not generate side effects on the skin, and reduces the possibility of generating adverse symptoms such as allergy, contact dermatitis and the like.
The base material of the invention adopts spunlace non-woven fabrics, the spunlace non-woven fabrics are made of viscose fiber and polyester fiber, and a large number of experimental researches show that: when the proportion of the viscose fiber and the polyester fiber is 3:2, the comfortable feeling of the non-woven fabric is optimal, and the non-woven fabric is skin-friendly and non-irritating when in use.
Detailed Description
The following detailed description will be given with reference to specific embodiments, so that how to apply the technical means to solve the technical problems and achieve the technical effects can be fully understood and implemented.
Unless otherwise indicated, the techniques employed in the examples are conventional and well known to those skilled in the art, and the reagents and products employed are also commercially available. The source, trade name and if necessary the constituents of the reagents used are indicated at the first appearance.
Example one
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.01 part of aloe extract, 0.1 part of cucumber juice, 1 part of mint essential oil, 0.2 part of pine needle oil, 0.3 part of orange peel essential oil, 1.5 parts of borneol, 0.4 part of polyhexamethylene biguanide hydrochloride, 1.2 parts of propylene glycol, 1.5 parts of polyoxyethylene lauryl ether, 0.2 part of PEG-60 hydrogenated castor oil and 85 parts of deionized water. The cucumber juice is obtained by peeling and cleaning cucumber, squeezing and filtering.
The preparation method of the multifunctional wet tissue comprises the following steps:
(1) Adding polyoxyethylene lauryl ether and propylene glycol into deionized water, heating to 60 ℃, uniformly stirring, adding PEG-60 hydrogenated castor oil, borneol and polyhexamethylene biguanide hydrochloride, and uniformly stirring and dissolving;
(2) Cooling the solution obtained in the step (1) to 40 ℃, adding aloe extract, cucumber juice, mint essential oil, pine needle oil and orange peel essential oil, stirring and mixing uniformly to obtain a wet tissue compound liquid, adding an acid-base regulator, and regulating the pH value of the wet tissue compound liquid to 5.0-7.0;
ultrasonic treatment is synchronously carried out in the stirring process, the ultrasonic treatment time is 8min, and the frequency is 20kHz.
(3) Soaking the sterilized and disinfected substrate in the wet tissue compound liquid for 20min to obtain the multifunctional wet tissue;
(4) And (4) folding and hermetically packaging the multifunctional wet tissue prepared in the step (3).
Example two
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.05 part of aloe extract, 0.3 part of cucumber juice, 3 parts of peppermint essential oil, 0.3 part of pine needle oil, 0.35 part of orange peel essential oil, 2 parts of borneol, 0.6 part of polyhexamethylene biguanide hydrochloride, 2.4 parts of propylene glycol, 2.2 parts of polyoxyethylene lauryl ether, 0.3 part of tween-80 and 90 parts of deionized water.
The preparation method of the multifunctional wet tissue comprises the following steps:
(1) Adding polyoxyethylene lauryl ether and propylene glycol into deionized water, heating to 63 ℃, uniformly stirring, adding Tween-80, borneol and polyhexamethylene biguanide hydrochloride, and uniformly stirring and dissolving;
(2) Cooling the solution obtained in the step (1) to 42 ℃, adding aloe extract, cucumber juice, mint essential oil, pine needle oil and orange peel essential oil, stirring and mixing uniformly to obtain a wet tissue compound solution, adding an acid-base regulator, and regulating the pH value of the wet tissue compound solution to 5.0-7.0;
ultrasonic treatment is synchronously carried out in the stirring process, the ultrasonic treatment time is 12min, and the frequency is 20kHz.
(3) Soaking the sterilized and disinfected base material in the wet tissue compound liquid for 25min to obtain the multifunctional wet tissue;
(4) And (4) folding, sealing and packaging the multifunctional wet tissue prepared in the step (3).
EXAMPLE III
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.1 part of aloe extract, 0.5 part of cucumber juice, 5 parts of peppermint essential oil, 0.4 part of pine needle oil, 0.6 part of orange peel essential oil, 3 parts of borneol, 0.8 part of polyhexamethylene biguanide hydrochloride, 3.6 parts of propylene glycol, 3 parts of polyoxyethylene lauryl ether, 0.4 part of PEG-60 hydrogenated castor oil and 95 parts of deionized water.
The preparation method of the multifunctional wet tissue comprises the following steps:
(1) Adding polyoxyethylene lauryl ether and propylene glycol into deionized water, heating to 65 ℃, uniformly stirring, adding PEG-60 hydrogenated castor oil, borneol and polyhexamethylene biguanide hydrochloride, and uniformly stirring and dissolving;
(2) Cooling the solution obtained in the step (1) to 45 ℃, adding aloe extract, cucumber juice, mint essential oil, pine needle oil and orange peel essential oil, stirring and mixing uniformly to obtain a wet tissue compound solution, adding an acid-base regulator, and regulating the pH value of the wet tissue compound solution to 5.0-7.0;
ultrasonic treatment is synchronously carried out in the stirring process, the ultrasonic treatment time is 15min, and the frequency is 20kHz.
(3) Soaking the sterilized and disinfected substrate in the wet tissue compound liquid for 30min to obtain the multifunctional wet tissue;
(4) And (4) folding, sealing and packaging the multifunctional wet tissue prepared in the step (3).
Comparative example 1
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.5 part of cucumber juice, 5 parts of mint essential oil, 3 parts of borneol, 1.9 parts of polyhexamethylene biguanide hydrochloride, 3.6 parts of propylene glycol, 3 parts of polyoxyethylene lauryl ether, 0.4 part of PEG-60 hydrogenated castor oil and 95 parts of deionized water. The preparation method of the multifunctional wet tissue is consistent with the three phases of the embodiment.
Comparative example No. two
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.9 part of aloe extract, 0.5 part of cucumber juice, 5 parts of peppermint essential oil, 0.4 part of pine needle oil, 0.6 part of orange peel essential oil, 3 parts of borneol, 3.6 parts of propylene glycol, 3 parts of polyoxyethylene lauryl ether, 0.4 part of PEG-60 hydrogenated castor oil and 95 parts of deionized water. The preparation method of the multifunctional wet tissue is consistent with the three phases of the embodiment.
Comparative example No. three
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.1 part of aloe extract, 0.5 part of cucumber juice, 5 parts of peppermint essential oil, 1.2 parts of pine needle oil, 0.6 part of orange peel essential oil, 3 parts of borneol, 3.6 parts of propylene glycol, 3 parts of polyoxyethylene lauryl ether, 0.4 part of PEG-60 hydrogenated castor oil and 95 parts of deionized water. The preparation method of the multifunctional wet tissue is consistent with the three phases of the embodiment.
Comparative example No. four
The multifunctional wet tissue comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the base material is spunlace non-woven fabric, the spunlace non-woven fabric is prepared from viscose fibers and polyester fibers according to the mass ratio of 3:2, and the wet tissue compound liquid comprises the following components in parts by weight: 0.1 part of aloe extract, 0.5 part of cucumber juice, 5 parts of peppermint essential oil, 0.4 part of pine needle oil, 1.4 parts of orange peel essential oil, 3 parts of borneol, 3.6 parts of propylene glycol, 3 parts of polyoxyethylene lauryl ether, 0.4 part of PEG-60 hydrogenated castor oil and 95 parts of deionized water. The preparation method of the multifunctional wet tissue is consistent with the three phases of the embodiment.
Performance testing
The wet wipes prepared in the examples were tested for antibacterial property and skin irritation.
Antibacterial property test
According to GB15979-2002 hygienic Standard for Disposable sanitary articles, the action time is 5min, the test strains are Staphylococcus aureus ATCC6538, escherichia coli ATCC 25922 and Candida albicans ATCC10231, and the test results are shown in Table 1.
TABLE 1
As can be seen from Table 1, the wet tissue prepared by the embodiment of the invention has good antibacterial effect, and the antibacterial rate reaches more than 98%. The comparison of example three with the respective comparative examples shows that: the natural plant extracts such as the aloe extract, the pine needle oil and the orange peel essential oil and the chemically synthesized polyhexamethylene biguanide hydrochloride have antibacterial property, a synergistic effect is generated after compounding, and under the same condition of the total adding amount, the antibacterial effect of the compounded wet tissue is superior to that of the singly used natural plant extracts or polyhexamethylene biguanide hydrochloride.
Skin irritation test
15 healthy white rabbits without skin damage were used as test animals and divided into 3 groups. 24h before the test, the hair on both sides of the dorsal spine of each group of test animals was cut off, and the skin with an area of 3cmx3cm was exposed. In the test, the wet tissues prepared in the first to third examples were cut into pieces of 2.5cm × 2.5cm and applied to the exposed skin on the back side of the rabbit, and the skin on the other side was used as a control. The application was removed 4h after application and the skin reaction at the application site was observed and recorded at lh, 24h, 48h and 72h, respectively. The scoring criteria were as follows: (1) erythema formation: 0 is nothing; 1 is barely visible; 2 is significant; 3 is severe; 4 purple red erythema with eschar. (2) edema formation: 0 is nothing; 1 is barely visible; 2, the skin is raised, and the outline is clear; 3 edema swelling of about 1mm; edema swelling of more than 1mm was indicated by 4. The test results are shown in Table 2.
TABLE 2
As can be seen from Table 2, no erythema or edema appeared on the skin of each group of test animals within 72 hours, which indicates that the wet wipes prepared in examples one to three are non-irritating to the skin.
The above description is only an embodiment utilizing the technical content of the present disclosure, and any modification and variation made by those skilled in the art can be covered by the claims of the present disclosure, and not limited to the embodiments disclosed.
Claims (7)
1. A multifunctional wet tissue is characterized in that: the wet tissue compound liquid comprises a base material and a wet tissue compound liquid soaked on the base material, wherein the wet tissue compound liquid comprises the following components in parts by weight: 0.01 to 0.1 portion of aloe extract, 0.1 to 0.5 portion of cucumber juice, 1 to 5 portions of mint essential oil, 0.2 to 0.4 portion of pine needle oil, 0.3 to 0.6 portion of orange peel essential oil, 1.5 to 3 portions of borneol, 0.4 to 0.8 portion of polyhexamethylene biguanide hydrochloride, 1.2 to 3.6 portions of propylene glycol, 1.5 to 3 portions of polyoxyethylene lauryl ether, 0.2 to 0.4 portion of solubilizer and 85 to 95 portions of deionized water, wherein the solubilizer is PEG-60 hydrogenated castor oil or Tween-80.
2. The multifunctional wet wipe as set forth in claim 1, wherein: the base material is spunlace non-woven fabric.
3. The multifunctional wet wipe as set forth in claim 2, wherein: the base material takes viscose and polyester fiber as raw materials, and the mass ratio of the viscose to the polyester fiber is 3:1-2.
4. The multifunctional wet wipe as set forth in claim 3, wherein: the mass ratio of the viscose fiber to the polyester fiber is 3:2.
5. The method for preparing the multifunctional wet wipe as set forth in claim 1, wherein the method comprises the steps of: the method comprises the following steps:
(1) Adding lauryl alcohol polyoxyethylene ether and propylene glycol into deionized water, heating to 60-65 ℃, uniformly stirring, adding a solubilizer, borneol and polyhexamethylene biguanide hydrochloride, and uniformly stirring and dissolving;
(2) Cooling the solution obtained in the step (1) to 40-45 ℃, adding aloe extract, cucumber juice, mint essential oil, pine needle oil and orange peel essential oil, stirring and mixing uniformly to obtain a wet tissue compound solution, adding an acid-base regulator, and regulating the pH value of the wet tissue compound solution to 5.0-7.0;
(3) Soaking the sterilized and disinfected base material in the wet tissue compound liquid for 20-30 min to prepare the multifunctional wet tissue;
(4) And (4) folding, sealing and packaging the multifunctional wet tissue prepared in the step (3).
6. The method for preparing a multifunctional wet wipe as claimed in claim 5, wherein the method comprises the following steps: and (3) synchronously carrying out ultrasonic treatment in the stirring process in the step (2).
7. The method for preparing a multifunctional wet wipe as set forth in claim 5, wherein: the ultrasonic treatment time is 8-15 min, and the frequency is 20kHz.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113116772A (en) * | 2021-03-07 | 2021-07-16 | 张殿荣 | Traditional Chinese medicine wet tissue with sterilizing and inflammation diminishing functions and preparation method thereof |
| CN114010550A (en) * | 2021-10-22 | 2022-02-08 | 江苏天佑医用科技有限公司 | High-water-locking type disinfection wet tissue and production process thereof |
| CN115054553B (en) * | 2022-07-19 | 2023-05-26 | 橙的(福建)卫生用品有限责任公司 | Mosquito-repellent wet tissue |
| CN115040450B (en) * | 2022-07-19 | 2023-05-16 | 橙的(福建)卫生用品有限责任公司 | Female private wet tissue and preparation method thereof |
| CN115869223B (en) * | 2022-12-30 | 2024-07-26 | 福建恒安集团有限公司 | Deodorization and mite-removal cleaning agent and cleaning wet tissue using same |
| CN116509781B (en) * | 2023-05-08 | 2024-02-06 | 厦门耀健纸业股份有限公司 | Sanitary wipes and preparation method thereof |
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| CN103040688A (en) * | 2013-01-10 | 2013-04-17 | 林建广 | Hand-mouth baby wet tissue and preparation method thereof |
| CN104042558B (en) * | 2014-06-13 | 2017-12-05 | 云南白药清逸堂实业有限公司 | A kind of feature feminine care wet tissue and preparation method |
| CN104436261A (en) * | 2014-11-19 | 2015-03-25 | 铜陵麟安生物科技有限公司 | Wet tissue for refrigerator |
| CN106212551B (en) * | 2016-07-29 | 2018-11-30 | 腾科宝迪（厦门）生物科技有限公司 | Daily non-stimulated disinfectant of one kind and preparation method thereof |
| US10456437B1 (en) * | 2018-05-22 | 2019-10-29 | Shulan Jiang | Antibacterial wet wipe for skin care |
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