CN111111576A - Integrated chemical equipment - Google Patents
Integrated chemical equipment Download PDFInfo
- Publication number
- CN111111576A CN111111576A CN201911389900.9A CN201911389900A CN111111576A CN 111111576 A CN111111576 A CN 111111576A CN 201911389900 A CN201911389900 A CN 201911389900A CN 111111576 A CN111111576 A CN 111111576A
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- cooling
- chamber
- liquid storage
- integrated chemical
- cooling chamber
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- 239000000126 substance Substances 0.000 title claims abstract description 26
- 238000001816 cooling Methods 0.000 claims abstract description 60
- 239000007788 liquid Substances 0.000 claims abstract description 40
- 238000003860 storage Methods 0.000 claims abstract description 28
- 239000000110 cooling liquid Substances 0.000 claims description 18
- 239000011550 stock solution Substances 0.000 claims description 13
- 238000005057 refrigeration Methods 0.000 claims description 11
- 239000011261 inert gas Substances 0.000 claims description 7
- 230000010354 integration Effects 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 abstract description 40
- 239000002994 raw material Substances 0.000 abstract description 30
- 238000005265 energy consumption Methods 0.000 abstract description 13
- 239000002699 waste material Substances 0.000 abstract description 4
- 239000002826 coolant Substances 0.000 description 9
- 238000012824 chemical production Methods 0.000 description 5
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000008676 import Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses integrated chemical equipment, which comprises a refrigerating system, a cooling chamber cooled by the refrigerating system, and an upper liquid storage chamber arranged above the cooling chamber, wherein the cooling chamber is communicated with the upper liquid storage chamber through a feeding pipe, and a first reactor interface is arranged on the cooling chamber. The cooling chamber cooled by the refrigerating system is arranged, so that the required amount of reaction raw materials can be cooled in batches, and the problem of energy consumption waste caused by the fact that all the reaction raw materials are cooled at one time and are not used is solved; equipment such as a reaction kettle and the like does not need to be cooled, and energy consumption required by cooling the equipment such as the reaction kettle and the like can be reduced; the cooling chamber is integrated on a refrigerating system, is an integrated structure, can effectively solve the problem of space occupation, ensures that the space occupation is small, does not need to lead out a connecting pipeline during cooling, particularly an overlong pipeline, and can effectively reduce energy consumption.
Description
Technical Field
The invention relates to the technical field of chemical production equipment, in particular to integrated chemical equipment.
Background
In chemical production, chemical raw materials are often cooled and then reacted, and the existing equipment usually needs to use a circulating condensation system (a refrigeration system) to integrally cool all reaction raw materials in a reaction kettle and then introduce the reaction raw materials into a reactor for reaction or directly react in the reaction kettle. Because of the circulating flow of the cooling liquid, large-batch reaction raw materials with larger temperature difference with the environment, and the quick heat exchange effect of the reaction kettle and the like with the environment, a large amount of effective power of a cooling system is consumed; meanwhile, the circulating condensation system and a container to be cooled (such as a reaction kettle and the like) are basically arranged separately and are combined when in use, and a plurality of factory buildings or laboratory spaces can be occupied. Therefore, the energy consumption and cost of production are increased, and the waste of energy and production resources is caused.
Disclosure of Invention
Aiming at the defects, the invention provides the integrated chemical equipment with low energy consumption and cost and small occupied space.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides a chemical industry equipment of integration, including refrigerating system, still including by the cooling chamber of refrigerating system cooling, and set up the last stock solution room of cooling chamber top, the cooling chamber pass through the inlet pipe with it is linked together to go up the stock solution room, the first reactor interface has been seted up on the cooling chamber.
Furthermore, the integrated chemical equipment also comprises a lower liquid storage chamber arranged below the cooling chamber, and a second reactor interface is arranged on the lower liquid storage chamber.
As an optimization or improvement of the invention, an air pressure balance pipe is arranged between the upper liquid storage chamber and the lower liquid storage chamber.
Furthermore, the integrated chemical equipment also comprises a cooling liquid chamber cooled by the refrigerating system, and a cooling liquid inlet and a cooling liquid outlet are arranged on the cooling liquid chamber.
Preferably, the cooling liquid chamber is further provided with a filling opening.
Furthermore, the top of the upper liquid storage chamber is provided with a feed inlet and an inert gas interface.
Further, a discharge hole is formed in the bottom of the lower liquid storage chamber.
As an optimization or improvement of the invention, the integrated chemical equipment also comprises a movable support used for supporting all parts on the integrated chemical equipment, and the bottom of the movable support is provided with universal wheels.
Preferably, the universal wheel is a self-locking universal wheel.
Compared with the prior art, the invention has the beneficial effects that:
1. the cooling chamber cooled by the refrigerating system is arranged, so that the required amount of reaction raw materials can be cooled in batches, and the problem of energy consumption waste caused by the fact that all the reaction raw materials are cooled at one time and are not used is solved;
2. the invention does not need to cool the reaction kettle and other equipment, and can reduce the energy consumption required by cooling the reaction kettle and other equipment;
3. the cooling chamber is integrated on a refrigerating system, is an integrated structure, can effectively solve the problem of space occupation, ensures that the space occupation is small, does not need to lead out a connecting pipeline during cooling, particularly an overlong pipeline, and can effectively reduce the energy consumption;
4. the natural flow of reaction raw materials in the continuous flow reactor can be realized by utilizing the height difference of the upper liquid storage chamber and the lower liquid storage chamber, and a plunger pump is not required to be used for driving;
5. the invention has the advantages of integrated arrangement, compact structure, flexible use, convenient movement, high cooling efficiency and effective saving of space and energy consumption, and can realize position movement by arranging the universal wheels.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below.
FIG. 1 is a schematic view of a viewing angle of the present invention;
fig. 2 is a schematic view of a viewing angle according to the present invention.
Detailed Description
The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1 and 2, a preferred embodiment of the present invention provides an integrated chemical plant, which mainly includes a refrigeration system 1, a cooling chamber 2 cooled by the refrigeration system 1, and an upper liquid storage chamber 3 disposed above the cooling chamber. Wherein, cooling chamber 2 is a appearance chamber, and cooling chamber 2 is installed on refrigerating system 1's refrigeration part, and refrigerating system 1 can realize the inside cooling of cooling chamber 2 to cooling chamber 2 effect, goes up stock solution room 3 and is a container for reaction raw materials such as splendid attire reaction liquid. Cooling chamber 2 is linked together through inlet pipe 16 and last stock solution room 3, is equipped with the valve on the inlet pipe 16, and reaction raw materials can't get into the cooling chamber through inlet pipe 16 from last stock solution room 3 when the valve is closed, has seted up first reactor interface 4 on the cooling chamber 2, is equipped with the valve on the first reactor interface 4, and reaction raw materials after the cooling can't go out from first reactor interface 4 when the valve is closed. It is worth noting that refrigerating system 1 adopts refrigerating system for the chemical production commonly used or for the experimental facilities, and concrete structure is no longer detailed, can select according to the in-service use, and refrigerating system 1 can realize cooling treatment to cooling chamber 2 for cooling chamber 2 can be in an ideal temperature, in order to realize cooling, cooling to getting into the inside reaction raw materials of cooling chamber 2.
During the implementation, the inside reaction raw materials that adds the capacity of upward stock solution room 3, cool down in order to realize the reaction to a certain amount of reaction raw materials when needs, open the valve on the inlet pipe 16 so that a certain amount of reaction raw materials gets into cooling chamber 2, and simultaneously, refrigerating system 1 starts, make the inside cooling of 2 inside cooling in cooling chamber, thereby realize the cooling to the reaction raw materials in cooling chamber 2, reaction raw materials after the cooling reaches required temperature after, open the valve on first reactor interface 4, the outside reactor of first reactor interface 4 connection, reaction raw materials then can follow first reactor interface 4 and get into outside reactor and react. By the mode, the required amount of reaction raw materials can be cooled in batches, so that the problem of energy consumption waste caused by the condition that all the reaction raw materials are not used at one time while all the reaction raw materials are cooled at one time is solved. Only need cool off cooling chamber 2 and inside reaction raw materials during cooling down, need not to cool off equipment such as reation kettle, can subtract because of cooling required energy consumption of equipment such as reation kettle. Go up stock solution room 3, cooling chamber 2 and refrigerating system 1 and collect as an organic whole mutually, the integration sets up, can effectual solution space occupy the problem for the space occupies for a short time, and need not to draw forth connecting tube during the cooling, especially the pipeline of overlength, can effectively reduce the energy consumption.
In the preferred embodiment, the top of the upper liquid storage chamber 3 is provided with a feed inlet 12 and an inert gas interface 13, and the feed inlet 12 and the inert gas interface 13 are respectively provided with a valve. The reaction raw materials are added from the feed port 12. The inert gas port 13 may be connected to an external cylinder containing an inert gas, which serves to prevent the reaction raw materials from being oxidized, and the reaction raw materials are introduced into the upper reservoir 3 together with the inert gas when they are fed.
In a preferred embodiment, referring to fig. 1 and fig. 2, a lower liquid storage chamber 6 is disposed below the cooling chamber 2, a second reactor interface 5 is disposed on the lower liquid storage chamber 6, and a valve is disposed on the second reactor interface 5. In practice, the reaction chamber used in combination with the outside may be connected to the second reactor interface 5, and the reacted reaction raw material may enter the lower liquid storage chamber 6 through the second reactor interface 5. In a preferred embodiment, the lower liquid storage chamber 6 is installed on a refrigeration part of the refrigeration system 1, the refrigeration system 1 cools down, and the reacted reaction raw materials entering the lower liquid storage chamber 6 can be stored and preserved at a low temperature.
Go up and be equipped with atmospheric pressure balance tube 7 between stock solution room 3 and the stock solution room 6 down, set up atmospheric pressure balance tube 7 and can realize going up the inside atmospheric pressure balance of stock solution room 3 and stock solution room 6 down. The preferred embodiment can utilize the height difference between the upper liquid chamber 3 and the lower liquid chamber 6 to realize the natural flow of the reaction raw materials in the continuous flow reactor without using a plunger pump for driving.
The bottom of the lower liquid storage chamber 6 is provided with a discharge port 14, a valve is arranged on the discharge port 14, and the reacted reaction raw materials can be discharged from the lower liquid storage chamber 6 through the discharge port 14.
The preferred embodiment further comprises a cooling liquid chamber 8 cooled by the refrigerating system 1, and the cooling liquid chamber 8 is provided with a cooling liquid inlet 9 and a cooling liquid outlet 10. During the implementation, 8 inside packings in coolant liquid room have the coolant liquid, when external equipment need use the coolant liquid to carry out the cooling of circulative cooling, external equipment passes through the pipeline and is linked together with coolant liquid import 9 and coolant liquid export 10, and the coolant liquid after the cooling gets into external equipment from coolant liquid import 9 and then after external equipment cooled down, returns coolant liquid room 8 from coolant liquid export 10 again. The cooling liquid chamber 8 is also provided with a filling opening 11 for facilitating the addition of cooling liquid.
In a preferred embodiment, the integrated chemical equipment further comprises a movable support 15 for supporting all the components on the integrated chemical equipment, the refrigeration system 1, the cooling chamber 2, the upper liquid storage chamber 3, the lower liquid storage chamber 6, the cooling liquid chamber 8 and the like are all mounted on the movable support 15, and the movable support 15 comprises a multi-layer flat plate structure and a vertical rod-shaped structure for supporting the flat plate structure, so that a stand is formed, and all the components can be mounted on the movable support 15 from top to bottom by means of a certain height difference. The bottom of the movable support 15 is provided with four universal wheels 17, and the four universal wheels 17 are respectively arranged on four bottom corners of the movable support. The movable support 15 is arranged so as to realize integration of integration, the position of the integrated chemical equipment can be conveniently moved, and the movable support is flexible to use and convenient to move. The universal wheel 17 is a self-locking universal wheel, the self-locking universal wheel can realize self-locking, and the self-locking universal wheel cannot move during self-locking so that the movable support 15 can be fixed at a certain position, and the movable support 15 is prevented from moving accidentally.
The preferred embodiment provides a chemical equipment which integrates refrigeration, liquid storage and circulating condensation into a whole and is convenient to move, and the use of the equipment can obviously reduce the energy consumption of certain chemical production processes and the requirements on plant areas, especially continuous flow chemical production processes which need to be carried out below room temperature.
The above description is only for the specific embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (9)
1. The utility model provides a chemical industry equipment of integration, including refrigerating system (1), its characterized in that: still including by cooling chamber (2) of refrigerating system (1) cooling, and set up and be in last stock solution room (3) of cooling chamber top, cooling chamber (2) through inlet pipe (16) with it is linked together to go up stock solution room (3), first reactor interface (4) have been seted up on cooling chamber (2).
2. The integrated chemical plant according to claim 1, characterized in that: the reactor is characterized by further comprising a lower liquid storage chamber (6) arranged below the cooling chamber (2), wherein a second reactor interface (5) is arranged on the lower liquid storage chamber (6).
3. The integrated chemical plant according to claim 2, characterized in that: an air pressure balance pipe (7) is arranged between the upper liquid storage chamber (3) and the lower liquid storage chamber (6).
4. The integrated chemical plant according to claim 1, characterized in that: the refrigeration system is characterized by further comprising a cooling liquid chamber (8) cooled by the refrigeration system (1), wherein a cooling liquid inlet (9) and a cooling liquid outlet (10) are formed in the cooling liquid chamber (8).
5. The integrated chemical plant according to claim 4, characterized in that: the cooling liquid chamber (8) is also provided with a liquid filling opening (11).
6. The integrated chemical plant according to claim 1, characterized in that: the top of the upper liquid storage chamber (3) is provided with a feed inlet (12) and an inert gas interface (13).
7. The integrated chemical plant according to claim 2, characterized in that: and a discharge hole (14) is formed in the bottom of the lower liquid storage chamber (6).
8. The integrated chemical plant according to any one of claims 1 to 7, characterized in that: the device is characterized by further comprising a movable support (15) used for supporting all parts on the integrated chemical equipment, and universal wheels (17) are arranged at the bottom of the movable support (15).
9. The integrated chemical plant according to claim 8, characterized in that: the universal wheel (17) is a self-locking universal wheel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911389900.9A CN111111576B (en) | 2019-12-30 | 2019-12-30 | Integrated chemical equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911389900.9A CN111111576B (en) | 2019-12-30 | 2019-12-30 | Integrated chemical equipment |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111111576A true CN111111576A (en) | 2020-05-08 |
| CN111111576B CN111111576B (en) | 2024-08-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911389900.9A Active CN111111576B (en) | 2019-12-30 | 2019-12-30 | Integrated chemical equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111111576B (en) |
Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06211905A (en) * | 1992-12-30 | 1994-08-02 | Shin Etsu Chem Co Ltd | Polymerization equipment |
| US5970729A (en) * | 1995-03-01 | 1999-10-26 | Sts Corporation | Cooling apparatus |
| US6017460A (en) * | 1996-06-07 | 2000-01-25 | Chematur Engineering Ab | Heating and reaction system and method using recycle reactor |
| CN1386109A (en) * | 2000-08-02 | 2002-12-18 | 奥斯卡·罗尔·洛佩兹·奥岱兹 | Liquid cooling system |
| CN103234368A (en) * | 2013-04-27 | 2013-08-07 | 昆山良昕环保节能有限公司 | Heat exchanger module |
| CN103294078A (en) * | 2012-02-22 | 2013-09-11 | 上海微电子装备有限公司 | Modularized temperature control device |
| CN106809829A (en) * | 2017-02-17 | 2017-06-09 | 黑龙江工业学院 | A kind of heater and heating means of graphite raw material |
| CN107138123A (en) * | 2017-07-13 | 2017-09-08 | 王东红 | A kind of concrete chain extender production line |
| CN206793678U (en) * | 2017-04-28 | 2017-12-26 | 江苏欣宝科技股份有限公司 | A kind of polyester resin production reactor with automatic feeder |
| US20180142935A1 (en) * | 2016-07-25 | 2018-05-24 | Robert W. Jacobi | Modular system for heating and/or cooling requirements |
| CN209618019U (en) * | 2019-02-24 | 2019-11-12 | 嘉兴市南湖高分子材料有限公司 | A kind of heat preservation storage tank |
| CN209791493U (en) * | 2019-01-11 | 2019-12-17 | 多氟多（昆明）科技开发有限公司 | Feeding device for producing ammonium fluoride |
| CN212068684U (en) * | 2019-12-30 | 2020-12-04 | 广西师范大学 | Integrated chemical equipment |
| CN218107686U (en) * | 2022-10-14 | 2022-12-23 | 四川盛年同缔实业有限公司 | Environment-friendly energy-saving reaction kettle for producing petrochemical engineering auxiliary agent |
-
2019
- 2019-12-30 CN CN201911389900.9A patent/CN111111576B/en active Active
Patent Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06211905A (en) * | 1992-12-30 | 1994-08-02 | Shin Etsu Chem Co Ltd | Polymerization equipment |
| US5970729A (en) * | 1995-03-01 | 1999-10-26 | Sts Corporation | Cooling apparatus |
| US6017460A (en) * | 1996-06-07 | 2000-01-25 | Chematur Engineering Ab | Heating and reaction system and method using recycle reactor |
| CN1386109A (en) * | 2000-08-02 | 2002-12-18 | 奥斯卡·罗尔·洛佩兹·奥岱兹 | Liquid cooling system |
| CN103294078A (en) * | 2012-02-22 | 2013-09-11 | 上海微电子装备有限公司 | Modularized temperature control device |
| CN103234368A (en) * | 2013-04-27 | 2013-08-07 | 昆山良昕环保节能有限公司 | Heat exchanger module |
| US20180142935A1 (en) * | 2016-07-25 | 2018-05-24 | Robert W. Jacobi | Modular system for heating and/or cooling requirements |
| CN106809829A (en) * | 2017-02-17 | 2017-06-09 | 黑龙江工业学院 | A kind of heater and heating means of graphite raw material |
| CN206793678U (en) * | 2017-04-28 | 2017-12-26 | 江苏欣宝科技股份有限公司 | A kind of polyester resin production reactor with automatic feeder |
| CN107138123A (en) * | 2017-07-13 | 2017-09-08 | 王东红 | A kind of concrete chain extender production line |
| CN209791493U (en) * | 2019-01-11 | 2019-12-17 | 多氟多（昆明）科技开发有限公司 | Feeding device for producing ammonium fluoride |
| CN209618019U (en) * | 2019-02-24 | 2019-11-12 | 嘉兴市南湖高分子材料有限公司 | A kind of heat preservation storage tank |
| CN212068684U (en) * | 2019-12-30 | 2020-12-04 | 广西师范大学 | Integrated chemical equipment |
| CN218107686U (en) * | 2022-10-14 | 2022-12-23 | 四川盛年同缔实业有限公司 | Environment-friendly energy-saving reaction kettle for producing petrochemical engineering auxiliary agent |
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| Publication number | Publication date |
|---|---|
| CN111111576B (en) | 2024-08-06 |
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