CN110846158A - Preparation method of amino acid soap and amino acid soap - Google Patents
Preparation method of amino acid soap and amino acid soap Download PDFInfo
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- CN110846158A CN110846158A CN201911191077.0A CN201911191077A CN110846158A CN 110846158 A CN110846158 A CN 110846158A CN 201911191077 A CN201911191077 A CN 201911191077A CN 110846158 A CN110846158 A CN 110846158A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/002—Non alkali-metal soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/267—Organic compounds, e.g. vitamins containing oxygen containing free fatty acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a preparation method of amino acid soap, which comprises the following steps: providing a material A and a material B; stirring and cooking the material A at a first set temperature to enable the material A to be in a clear state; adding the material B into the material A in a clear state, and heating under the stirring condition to ensure that the material A and the material B completely react to prepare a mixed material; when the temperature of the mixed materials is raised to a first set temperature, reducing the stirring speed, then discharging and pouring a film to prepare the amino acid soap; wherein, the material A comprises lauric acid, sorbitol, propylene glycol, glycerol, water, stearic acid and urea; the material B comprises alkali and a humectant; the first set temperature is 88-93 ℃. The pH value of the amino acid soap is 5-6, is very close to human skin, and is very stable. The amino acid soap has good skin cleaning effect, is mild and non-irritant, and has no tight skin feeling after being used. The amino acid soap has strong degradation performance, and the discharged waste water after use can not cause pollution to the environment.
Description
Technical Field
The invention relates to the technical field of soaps, in particular to a preparation method of an amino acid soap and the amino acid soap prepared by the method.
Background
As is well known, the skin pH value of human body is 4.0 at the lowest and can reach 9.6 at the highest, especially the skin pH value of infants is lower, and the average pH value is between 5.0 and 7.0.
The outermost layer of the skin is a leather lipid film which is thinner than the preservative film, and the toilet soap with high pH value can damage the leather lipid film of the skin, so that the skin loses the protective capability, cannot store enough moisture, and is easy to cause skin aging, dryness, itch and allergy. Therefore, the use of a product with too strong alkalinity can cause a great loss of sebum, reduce the alkali neutralization capacity of the skin and cause skin damage.
The pH value of the prior toilet soap product for bathing is as high as 10.57 and is far higher than the pH value of skin, the toilet soap has the advantage of strong cleaning capability, but has the technical problems of high alkalinity, dry and tight feeling after cleaning, insufficient moisture retention and moistening degree and the like, and aiming at the technical problems, the invention develops a milder and non-irritant facial and skin-moistening soap with the pH value being attached to a human body.
Disclosure of Invention
The invention aims to provide a preparation method of an amino acid soap, wherein the pH value of the amino acid soap prepared by the method is 5-6, and the amino acid soap has the most basic skin cleaning function, and also has the effects of water locking, moisture retention, mildness, no stimulation and the like.
In order to achieve the purpose, the invention adopts the following technical scheme:
in one aspect, a method for preparing an amino acid soap is provided, which comprises the following steps:
s10, providing a material A and a material B;
s20, stirring and cooking the material A at a first set temperature to enable the material A to be in a clear state;
s30, adding the material B into the material A in a clear state, and heating under the stirring condition to enable the material A and the material B to completely react to obtain a mixed material;
s40, when the temperature of the mixed material is raised to the first set temperature, reducing the stirring speed, and then discharging and pouring a film to obtain the amino acid soap;
wherein the material A comprises lauric acid, sorbitol, propylene glycol, glycerol, water, stearic acid and urea; the material B comprises alkali and a humectant; the first set temperature is 88-93 ℃.
The invention takes the mixed material of lauric acid, sorbitol, propylene glycol, glycerin, water, stearic acid and urea as the material A, at 88-93 deg.C, lauric acid can be completely dissolved and dispersed in the mixture of sorbitol, propylene glycol, glycerin, water, stearic acid and urea, so that the material A is in a clear state, the alkali and the humectant are taken as the material B and added into the material A in the clear state, heating under stirring to make alkali dissolved in humectant in material B and lauric acid produce neutralization reaction to produce amino acid, uniformly dispersing the produced amino acid in the mixed material under stirring condition, the pH value of the mixed material is 5-6, then the temperature is raised to 88-93 ℃, the stirring speed is reduced, the pH value of the mixed material can be stably maintained at 5-6 and is very close to that of Asian skin, and the moisture retention and moistening degree of the amino acid soap is greatly improved compared with that of the existing soap. The amino acid soap prepared by the method has the most basic skin cleaning function, has the effects of water locking, moisture retention, mildness, no stimulation and the like, is clean and not tight after the skin is cleaned, and can enable the skin to be moisturized and people to feel wet after long-term use; the amino acid soap does not contain chemical preservatives, has strong degradation performance, and can not cause any pollution to the environment by the waste water discharged after the human body is cleaned.
In the technical scheme, the material A comprises the following components in parts by weight:
25 to 35 parts of lauric acid, for example, 25.3 parts, 25.5 parts, 25.8 parts, 26 parts, 26.5 parts, 27 parts, 27.5 parts, 28 parts, 28.5 parts, 29 parts, 29.5 parts, 30 parts, 30.5 parts, 31 parts, 32 parts, 33 parts or 34 parts, etc.;
3 to 7 parts of sorbitol, for example, 3.2 parts, 3.3 parts, 3.5 parts, 3.7 parts, 3.9 parts, 4 parts, 4.1 parts, 4.3 parts, 4.5 parts, 4.8 parts, 5 parts, 5.3 parts, 5.5 parts, 5.8 parts, 6 parts, 6.5 parts, or 6.8 parts, etc.;
3 to 7 parts of propylene glycol, such as 3.2 parts, 3.3 parts, 3.5 parts, 3.7 parts, 3.9 parts, 4 parts, 4.1 parts, 4.3 parts, 4.5 parts, 4.8 parts, 5 parts, 5.3 parts, 5.5 parts, 5.8 parts, 6 parts, 6.5 parts, or 6.8 parts, etc.;
9 to 15 parts of glycerin, such as 9.1 parts, 9.3 parts, 9.5 parts, 9.8 parts, 10 parts, 10.5 parts, 10.8 parts, 11 parts, 11.5 parts, 12 parts, 12.5 parts, 13 parts, 13.5 parts, 14 parts or 14.5 parts, etc.;
15 to 25 parts of water, for example, 15.1 parts, 15.3 parts, 5.5 parts, 15.8 parts, 16 parts, 16.2 parts, 16.5 parts, 16.8 parts, 17 parts, 17.5 parts, 18 parts, 18.5 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts or the like;
0.25 to 0.75 parts of stearic acid, for example, 0.255 part, 0.26 part, 0.27 part, 0.28 part, 0.29 part, 0.3 part, 0.32 part, 0.35 part, 0.38 part, 0.4 part, 0.45 part, 0.5 part, 0.55 part, 0.6 part, 0.65 part, or 0.7 part;
3 to 7 parts of urea, for example, 3.2 parts, 3.3 parts, 3.5 parts, 3.7 parts, 3.9 parts, 4 parts, 4.1 parts, 4.3 parts, 4.5 parts, 4.8 parts, 5 parts, 5.3 parts, 5.5 parts, 5.8 parts, 6 parts, 6.5 parts, or 6.8 parts.
Preferably, the material A comprises the following components in parts by weight:
in the technical scheme, the material B comprises 0.1-0.3 part of humectant and 15-22 parts of alkali by weight, wherein the humectant comprises, for example, 0.11 part, 0.13 part, 0.15 part, 0.17 part, 0.18 part, 0.2 part, 0.22 part, 0.24 part, 0.26 part or 0.28 part by weight, and the alkali comprises, for example, 15.2 parts, 15.5 parts, 15.8 parts, 16 parts, 16.5 parts, 17 parts, 17.5 parts, 18 parts, 18.5 parts, 9 parts, 19.5 parts, 20 parts, 20.5 parts, 21 parts or 21.5 parts by weight.
Preferably, the material B comprises 0.2 part of humectant and 18 parts of alkali.
Preferably, the humectant is sucrose and the base is triethanolamine. The humectant is only limited to sucrose, the alkali is only limited to triethanolamine, and the pH value of the prepared amino acid soap cannot be stably maintained at 5-6 by adopting other humectants except sucrose or alkalis except triethanolamine as the material B.
Preferably, the first set temperature is 90 ℃, which can further improve the stability of the pH of the amino acid soap.
Wherein the stirring speed in step S20 is 22-28 r/min, such as 22.5r/min, 23r/min, 23.5r/min, 24r/min or 24.5r/min, preferably 25 r/min.
Wherein the stirring speed in the step S30 is 28-33 r/min, such as 28.5r/min, 29r/min, 29.5r/min, 30r/min, 31r/min or 32r/min, preferably 30 r/min;
preferably, the stirring speed in the step S40 is not more than 10r/min, discharging and film casting are carried out after stirring for 18-25 min, and the stirring time is preferably 20 min.
In another aspect, the invention provides an amino acid soap which is prepared by the preparation method.
The invention has the beneficial effects that: by adopting the preparation method disclosed by the invention, the pH value of the prepared amino acid soap can be stably maintained at 5-6, and is very close to the pH value of Asian skin. The amino acid soap has the most basic skin cleaning function, also has strong effects of water locking, moisture retention, mildness, no stimulation and the like, is clean and not tight after the skin is cleaned, and can make the skin moist after long-term use; the amino acid soap does not contain chemical preservatives, has strong degradation performance, and can not cause any pollution to the environment by the waste water discharged after the human body is cleaned.
Detailed Description
The technical solution of the present invention is further explained by the following embodiments.
Unless otherwise specified, various starting materials of the present invention are commercially available or prepared according to conventional methods in the art.
Example 1
Putting the material A into a pot according to the material components shown in the table 1, cooking at 90 ℃ and 25r/min, adjusting the rotating speed to 30r/min when the material A in the pot is clear, then adding the material B, and continuing to heat; regulating the rotation speed to below 10r/min after the temperature in the pot rises to 90 deg.C, and standing the soap liquid for about 20min to obtain the final product (the temperature in the pot is not lower than 90 deg.C) with color matching.
Example 2
Putting the material A into a pot according to the material components shown in the table 1, cooking at 88 ℃ and 23r/min, adjusting the rotating speed to 28r/min when the material A in the pot is clear, then adding the material B, and continuing to heat; regulating the rotation speed to below 10r/min after the temperature in the pot rises to 88 deg.C, and standing the soap liquid for about 20min to obtain the final product (the temperature in the pot is below 88 deg.C during soap pouring period).
Example 3
Putting the material A into a pot according to the material components shown in the table 1, cooking at 92 ℃ at 27r/min, adjusting the rotating speed to 33r/min when the material A in the pot is clear, then adding the material B, and continuing to heat; regulating the rotation speed to below 10r/min after the temperature in the pot is raised to 902 deg.C, and standing the soap liquid for about 20min to obtain the final product (the temperature in the pot is not lower than 92 deg.C) with color matching.
TABLE 1 compositions (in parts by weight) of the materials used in examples 1-3
The amino acid soap is developed by further researching and developing the problems of strong cleaning capacity, high alkalinity, dry and tight feeling after washing, insufficient moisture retention and moistening degree and the like of the soap, and the amino acid soap is finally developed by optimizing and adjusting the formula and the preparation steps, wherein the pH value of the amino acid soap prepared according to the embodiments 1-3 of the invention is close to that of human skin, is between 5 and 6 and is very stable.
The amino acid soap prepared by the embodiment is used for cleaning skin, has small irritation to the skin of a human body during cleaning, avoids side effects on the skin on the basis of keeping high-efficiency cleaning, can be used by pregnant women and children, and is particularly suitable for acne muscles and sensitive muscles.
The amino acid soap prepared by the embodiment has strong degradation performance, and the discharged wastewater after the human body is cleaned does not cause any pollution to the environment.
The above examples are only intended to illustrate the detailed process of the present invention, and the present invention is not limited to the above detailed process, i.e., it is not intended that the present invention necessarily depends on the above detailed process for its implementation. It is understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention and the addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (10)
1. The preparation method of the amino acid soap is characterized by comprising the following steps:
s10, providing a material A and a material B;
s20, stirring and cooking the material A at a first set temperature to enable the material A to be in a clear state;
s30, adding the material B into the material A in a clear state, and heating under the stirring condition to enable the material A and the material B to completely react to obtain a mixed material;
s40, when the temperature of the mixed material is raised to the first set temperature, reducing the stirring speed, and then discharging and pouring a film to obtain the amino acid soap;
wherein the material A comprises lauric acid, sorbitol, propylene glycol, glycerol, water, stearic acid and urea; the material B comprises alkali and a humectant; the first set temperature is 88-93 ℃.
2. The method for preparing the amino acid soap as claimed in claim 1, wherein the material A comprises the following components in parts by weight:
3. the method for preparing the amino acid soap as claimed in claim 2, wherein the material A comprises the following components in parts by weight:
4. the method for preparing the amino acid soap according to claim 1, wherein the material B comprises 0.1-0.3 part of humectant and 15-22 parts of alkali by weight.
5. The method according to claim 4, wherein said material B comprises 0.2 part by weight of humectant and 18 parts by weight of alkali.
6. The method according to claim 1, wherein the humectant is sucrose and the alkali is triethanolamine.
7. The method according to claim 1, wherein the first set temperature is 90 ℃.
8. The method for producing an amino acid soap according to claim 1, wherein the stirring speed in step S20 is 22 to 28r/min, preferably 25 r/min.
9. The method for producing an amino acid soap according to claim 1, wherein the stirring speed in step S30 is 28 to 33r/min, preferably 30 r/min;
preferably, the stirring speed in the step S40 is not more than 10r/min, and discharging and film casting are carried out after stirring for 18-25 min.
10. An amino acid soap, characterized by being produced by the production method according to any one of claims 1 to 9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911191077.0A CN110846158A (en) | 2019-11-28 | 2019-11-28 | Preparation method of amino acid soap and amino acid soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911191077.0A CN110846158A (en) | 2019-11-28 | 2019-11-28 | Preparation method of amino acid soap and amino acid soap |
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| Publication Number | Publication Date |
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| CN110846158A true CN110846158A (en) | 2020-02-28 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201911191077.0A Pending CN110846158A (en) | 2019-11-28 | 2019-11-28 | Preparation method of amino acid soap and amino acid soap |
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Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199091A (en) * | 1997-05-14 | 1998-11-18 | 王大龙 | Transparent skin moistening toilet soap |
| CN1213398A (en) * | 1996-01-25 | 1999-04-07 | 庄臣及庄臣株式会社 | Body soap composition |
| CN1519305A (en) * | 2003-02-07 | 2004-08-11 | 花王株式会社 | Formed soap compsn. |
| CN101497849A (en) * | 2009-01-20 | 2009-08-05 | 佛山市美心美容保健用品有限公司 | Transparent perfumed soap and preparation thereof |
| CN102776085A (en) * | 2012-06-30 | 2012-11-14 | 澳宝化妆品（惠州）有限公司 | Novel transparent soap |
| CN102787037A (en) * | 2012-08-28 | 2012-11-21 | 广西奥奇丽股份有限公司 | Transparent soap |
| CN102796634B (en) * | 2012-08-28 | 2013-08-21 | 广西奥奇丽股份有限公司 | Production process for transparent soap |
| CN103301051A (en) * | 2012-03-07 | 2013-09-18 | 南京华狮化工有限公司 | Transparent beauty treatment soap composition |
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
-
2019
- 2019-11-28 CN CN201911191077.0A patent/CN110846158A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1213398A (en) * | 1996-01-25 | 1999-04-07 | 庄臣及庄臣株式会社 | Body soap composition |
| CN1199091A (en) * | 1997-05-14 | 1998-11-18 | 王大龙 | Transparent skin moistening toilet soap |
| CN1519305A (en) * | 2003-02-07 | 2004-08-11 | 花王株式会社 | Formed soap compsn. |
| CN101497849A (en) * | 2009-01-20 | 2009-08-05 | 佛山市美心美容保健用品有限公司 | Transparent perfumed soap and preparation thereof |
| CN103301051A (en) * | 2012-03-07 | 2013-09-18 | 南京华狮化工有限公司 | Transparent beauty treatment soap composition |
| CN102776085A (en) * | 2012-06-30 | 2012-11-14 | 澳宝化妆品（惠州）有限公司 | Novel transparent soap |
| CN102787037A (en) * | 2012-08-28 | 2012-11-21 | 广西奥奇丽股份有限公司 | Transparent soap |
| CN102796634B (en) * | 2012-08-28 | 2013-08-21 | 广西奥奇丽股份有限公司 | Production process for transparent soap |
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
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