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CN110314407A - A kind of fat rapidly extracting device - Google Patents

A kind of fat rapidly extracting device Download PDF

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Publication number
CN110314407A
CN110314407A CN201910705584.5A CN201910705584A CN110314407A CN 110314407 A CN110314407 A CN 110314407A CN 201910705584 A CN201910705584 A CN 201910705584A CN 110314407 A CN110314407 A CN 110314407A
Authority
CN
China
Prior art keywords
tube
pipe
condenser pipe
flask
reservoir
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910705584.5A
Other languages
Chinese (zh)
Inventor
杨红伟
郭吉原
孙春华
隋莉
罗福星
谢庚楠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong New Hope Liuhe Group Co Ltd
New Hope Liuhe Co Ltd
Original Assignee
Shandong New Hope Liuhe Group Co Ltd
New Hope Liuhe Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong New Hope Liuhe Group Co Ltd, New Hope Liuhe Co Ltd filed Critical Shandong New Hope Liuhe Group Co Ltd
Priority to CN201910705584.5A priority Critical patent/CN110314407A/en
Publication of CN110314407A publication Critical patent/CN110314407A/en
Priority to PCT/CN2020/091681 priority patent/WO2021017591A1/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0292Treatment of the solvent
    • B01D11/0296Condensation of solvent vapours
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14Suction devices, e.g. pumps; Ejector devices

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

The present invention provides a kind of fatty rapidly extracting devices, water-bath including bottom, flask is placed in water-bath, flask top movable is connected with condenser pipe, condenser pipe outer tube is provided with interlayer, inner tube is coiled pipe, coiled pipe one end is connected with water inlet pipe, the other end is connected to outer tube interlayer, and interlayer is connected with outlet pipe, is provided with reservoir in condenser pipe, reservoir and it is externally connected to inlet tube and outlet tube, it is connected with circulation pipe in outlet tube and condenser pipe tube body, sample is placed in specimen holder, and specimen holder is connected at the top of condenser pipe by lifting rope.The invention has the benefit that design is rationally, structure is simple, securely and reliably, extraction of lipid stability can be improved and extract timeliness and can save water resource.

Description

A kind of fat rapidly extracting device
Technical field
The present invention relates to fat-extraction equipment technical field more particularly to a kind of fatty rapidly extracting devices.
Background technique
Current main extraction of lipid equipment mainly has traditional soxhlet type equipment and some other Milko-Tester. Soxhlet type apparatus mainly utilizes solvent refluxing and siphon principle, reaches solid matter continuously by pure solvent extraction To the purpose of effective component extracting.But to extract the fatty time long for Soxhlet extraction equipment, needs 6 more than hour, it is only a kind of Immersion mode, time can not shorten;And waste condensed water, no water circle device, clean tap water are directly exhausted, especially When summer temperature is high, even if condensate pipe is led to maximum, good condensation effect is not had yet, and after water is opened to the maximum, Usually because water flow is excessive, and condensate pipe connector is caused to be rushed to open, drainage occurs;And meticulous sample can leak out, Influence testing result.
Although having occurred many novel extraction equipment for fat on the market, generally existing following deficiency: poor sealing, After a period of use, the case where gas leakage is occurred as soon as, experiment does not terminate also, and petroleum ether is just evaporated completely, if twining unsintered tape also still It can not so settle the matter once and for all;Heating is uneven, and at 60 DEG C of temperature setting, the effect of intermediate reflux is preferable, but both sides are returned The effect of stream is bad, and intermediate and both sides testing result is caused to differ greatly, and increases temperature, and both sides reflux can be with, but it is intermediate because It is excessively high for temperature, there is boiling explosion phenomenon, petroleum ether loss is big, and grease has loss;Because extracting tank is too small, detection fat content is high Sample, often there is the phenomenon that bumping.
How to solve above-mentioned technical problem is the project that the present invention faces.
Summary of the invention
In order to solve the deficiencies in the prior art, the present invention provides a kind of designs rationally, easy to operate, securely and reliably, can It improves extraction of lipid stability and extracts the fatty rapidly extracting device of timeliness.
The technical solution adopted by the present invention to solve the technical problems is: the present invention provides a kind of fatty rapidly extractings to fill It sets, including flask, the flask is located in water-bath, is connected with the condenser pipe being vertically arranged, the condensation at the top of the flask Pipe includes outer tube and inner tube, and inner tube setting is provided with reservoir in the outer tube, around the rinse condenser pipe inwall lower part;
The outer tube wall offers liquid in-out mouth, and liquid in-out mouth is separately connected inlet tube and outlet tube, the inlet tube and goes out Liquid pipe is respectively communicated with outside the condenser pipe and inside reservoir;
Outlet tube valve is provided on the pipeline of the outlet tube;
Outer tube tube body lower part is connected with circulation pipe, and described circulation pipe one end is connected to outlet tube valve on the outlet tube tube body With the part between the condensation pipe outer wall, the other end is connected to inside the condenser pipe, and the circulation pipe tube body is provided with circulation Tube valve;
The condenser pipe is internally provided with specimen holder, lifting rope is fixedly connected at the top of the specimen holder, the lifting rope is through described It at the top of condenser pipe and extends to outside the condenser pipe, is placed with sample in the specimen holder.
It is divided into the condensation segment on top and the elution section of lower part inside the condenser pipe, the internal diameter of the elution section is less than described The internal diameter of condensation segment, the elution section bottom are flexibly connected with the flask bottleneck.
The tube wall of the outer tube of the condensing tube condensation section is provided with two layers, is interlayer between two layers of outer tube wall, described The top of interlayer is closed with bottom end, is connected to outside the condenser pipe inside the interlayer by outlet pipe.
Said inner tube is hollow helix tube, and one end of said inner tube is connected to the water inlet pipe, described in other end connection Inside interlayer.
The reservoir is located at the condensation segment, the reservoir bottom closure, top opening;
The end that the inlet tube is located on the outside of the condenser pipe is connected with funnel, is provided with feed liquor on the pipeline of the inlet tube Tube valve, the inlet tube extend to inside the reservoir through the interlayer.
The outlet tube is connected to the trench bottom of the reservoir;
The circulation pipe is connected to the elution section of the condenser pipe.
Sealing-plug is provided at the top of the condenser pipe, the lifting rope runs through the sealing-plug, and the lifting rope rope body is overhang In the middle part of the condenser pipe, the lifting rope bottom end is flexibly connected the specimen holder by hook, and the specimen holder is the frame body of hollow out.
The water-bath is arranged on bracket, and the bracket side is vertically arranged with strut, and the strut is flexibly connected institute State the outer wall of condenser pipe.
The bottleneck inner wall of the flask is frosted layer.
The present invention is in actual use: device being assembled, is located at condenser pipe at the top of flask, is connected by frosted layer tight It is close, and fixed condenser pipe by strut, sample is ground, to increase the area of solid-liquid contact, sample is put into filter paper, It is put into inside specimen holder after being wrapped up by filter paper, and lifting rope end is connected to by Removable hook, then manually at the top of device By the height of the length adjustment specimen holder of lifting rope, specimen holder is put to flask;Then it is passed through condensed water toward water inlet pipe, condensed Water is first into coiled inner tube, subsequently into interlayer, is finally discharged from outlet pipe, to realize the circulation of condensed water, to mention High condensation efficiency;Then confirmation outlet tube valve is in off state, and circulation pipe valve and feed liquor tube valve are opening state, so The reaction reagents such as petroleum ether are poured into from funnel afterwards, petroleum ether enters outlet tube after entering reservoir, since outlet tube valve closes It closes, petroleum ether flows into condenser pipe elution section through circulation pipe and enters eventually into flask, when petroleum ether reaches certain altitude, just Stop adding petroleum ether, and close feed liquor tube valve, specimen holder is located at flask interior and is impregnated by petroleum ether at this time;Then water is opened Bath, the heating of water-bath contact petroleum ether with sample to be extracted, while petroleum ether boils, and steam rises, and steam enters It into condenser pipe, is flowed into reservoir, and is extracted along outer tube wall after the condensation water condensation in the interlayer of coiled inner tube and outer tube Petroleum ether solvent after taking is re-introduced into flask through circulation pipe to be heated, and sample, can be by sample after repeatedly impregnating extraction Product frame is pulled to the elution section of condenser pipe by lifting rope, and specimen holder is made to be located at the lower part of circulation pipe nozzle, outflow in circulation pipe at this time Petroleum ether solvent sample can be eluted after be again introduced into flask and carry out heating extraction, and the steam of solvent passes through sample When circulation pipe valve can also be closed after or so about 4 hours with example reaction, outlet tube valve is opened, and in liquid out Tube end places receiving flask, and after solvent extracted is heated at this time, steam ascends into reservoir, can directly flow along outlet tube Enter in receiving flask out, no longer flow into flask from circulation pipe, when solvent by all extraction is collected after, without solvent in flask, Water-bath can be closed, the extraction of solvent is completed.
The invention has the benefit that structure is simple, design rationally, extraction of lipid stability can be improved and extract timeliness and Water resource can be saved;Sample is placed in condenser pipe and flask by the present apparatus by lifting rope, is operated, be may be implemented using lift Sample is impregnated and eluted in petroleum ether solvent, to shorten detection time;The present apparatus uses heating water bath, solves heating not The problem too fast with heat dissipation;It is connected between flask and condenser pipe using ground, solves the problems, such as gas leakage, good airproof performance;It is cold Solidifying pipe is provided with interlayer and coiled inner tube, and uses condensate water circulatory condensing plant, has saved and has used water, while condensation efficiency is able to It improves;The present apparatus is fixed the sample package filter paper after grinding using the specimen holder of hollow out, and is connected to and is hung by Removable hook Rope will not expose sample is meticulous convenient for operation;The present apparatus is provided with reservoir, can be into reservoir by inlet tube Petroleum ether solvent is added, inlet tube is provided with feed liquor tube valve, can control frame liquid measure, and be configured with funnel in end, facilitates molten The addition of agent;Reservoir is also communicated with outlet tube, and circulation pipe, and outlet tube and circulation pipe are connected between outlet tube and condenser pipe On be provided with valve, to realize solvent-extracted circulation and the collection of solvent.
Detailed description of the invention
Fig. 1 is front view of the invention.
Fig. 2 is partial cutaway view of the invention.
Fig. 3 is sectional view of the invention.
Wherein, appended drawing reference are as follows: 1, flask;2, water-bath;3, condenser pipe;301, outer tube;302, inner tube;303, interlayer; 304, outlet pipe;305, water inlet pipe;306, sealing-plug;4, reservoir;5, inlet tube;501, funnel;502, feed liquor tube valve;6, Outlet tube;601, outlet tube valve;7, circulation pipe;701, circulation pipe valve;8, specimen holder;801, lifting rope;9, bracket;901, Strut.
Specific embodiment
It can understand and illustrate that the technical characterstic of this programme is illustrated this programme below by specific embodiment.
Referring to shown in Fig. 1 to Fig. 3, the present embodiment is a kind of fatty rapidly extracting device, including flask 1, the bottleneck of flask 1 Inner wall is frosted layer, and flask 1 is located in water-bath 2, is connected with the condenser pipe 3 being vertically arranged at the top of flask 1, inside condenser pipe 3 It is divided into the condensation segment on top and the elution section of lower part, the internal diameter for eluting section is less than the internal diameter of condensation segment, elution section bottom and flask 1 Bottleneck is flexibly connected;Condenser pipe 3 includes outer tube 301 and inner tube 302, and inner tube 302 is arranged inside outer tube 301, around condenser pipe 3 Inner wall lower is provided with reservoir 4, and reservoir 4 is located at condensation segment, 4 bottom closure of reservoir, top opening;
301 tube wall of outer tube offers liquid in-out mouth, and liquid in-out mouth is separately connected inlet tube 5 and outlet tube 6, and outlet tube 6 is connected to The trench bottom of reservoir 4 is provided with outlet tube valve 601 on the pipeline of outlet tube 6;Inlet tube 5 and outlet tube 6 are respectively communicated with cold Inside solidifying 3 outside of pipe and reservoir 4;
The tube wall of the outer tube 301 of 3 condensation segment of condenser pipe is provided with two layers, is interlayer 303 between two layers of outer tube wall, interlayer 303 Top is closed with bottom end, is connected to outside condenser pipe 3 inside interlayer 303 by outlet pipe 304, and inner tube 302 is hollow spiral Pipe, one end of inner tube 302 are connected to water inlet pipe 305, and the other end is connected to inside interlayer 303.
301 tube body lower part of outer tube is connected with circulation pipe 7, and circulation pipe 7 is connected to the elution section of condenser pipe 3, and 7 one end of circulation pipe connects Part on 6 tube body of pass-out liquid pipe between 3 outer wall of outlet tube valve 601 and condenser pipe, the other end are connected to inside condenser pipe 3, follow 7 tube body of endless tube is provided with circulation pipe valve 701;
The end that inlet tube 5 is located at 3 outside of condenser pipe is connected with funnel 501, and feed liquor tube valve is provided on the pipeline of inlet tube 5 502, inlet tube 5 extends to inside reservoir 4 through interlayer 303.
Condenser pipe 3 is internally provided with specimen holder 8, lifting rope 801 is fixedly connected at the top of specimen holder 8, lifting rope 801 is through condensation 3 top of pipe simultaneously extends to outside condenser pipe 3, is placed with sample in specimen holder 8.
Sealing-plug 306 is provided at the top of condenser pipe 3, lifting rope 801 runs through sealing-plug 306, and the rope body of lifting rope 801 overhangs condensation 3 middle part of pipe, 801 bottom end of lifting rope are flexibly connected specimen holder 8 by hook, and specimen holder 8 is the frame body of hollow out.
Water-bath 2 is arranged on bracket 9, and 9 side of bracket is vertically arranged with strut 901, and strut 901 is flexibly connected condenser pipe 3 outer wall.
The present invention is in actual use: device being assembled, so that condenser pipe 3 is located at 1 top of flask, is connected by frosted layer tight It is close, and fixed condenser pipe 3 by strut 901, sample is ground, to increase the area of solid-liquid contact, sample is put into filter It in paper, is put into after being wrapped up by filter paper inside specimen holder 8, and 801 end of lifting rope is connected to by Removable hook, then existed manually By the height of the length adjustment specimen holder 8 of lifting rope 801 at the top of device, specimen holder 8 is put to flask;Then toward water inlet pipe 305 are passed through condensed water, and condensed water is first into coiled inner tube 302, subsequently into interlayer 303, finally from 304 row of outlet pipe Out, to realize the circulation of condensed water, to improve condensation efficiency;Then confirmation outlet tube valve 601 is in off state, cycle tube valve Door 701 is in an open state with feed liquor tube valve 502, then pours into the reaction reagents such as petroleum ether from funnel 501, and petroleum ether enters Enter outlet tube 6 after to reservoir 4, since outlet tube valve 601 is closed, petroleum ether flows into condenser pipe 3 through circulation pipe 7 and elutes section And enter eventually into flask 1, when petroleum ether reaches certain altitude, just stop adding petroleum ether, and close feed liquor tube valve 502, specimen holder 8 is located at 1 inside of flask and is impregnated by petroleum ether at this time;Then water-bath 2 is opened, the heating of water-bath 2 makes stone Oily ether is contacted with sample to be extracted, while petroleum ether boils, and steam rises, and steam enters in condenser pipe 3, by coiled inner tube 302 flow into reservoir 4 with after the condensation water condensation in the interlayer 303 of outer tube 301 along 301 inner wall of outer tube, and stone extracted Oily ether solvents are re-introduced into flask 1 through circulation pipe 7 and are heated, and sample can lead to specimen holder 8 after repeatedly impregnating extraction The elution section that lifting rope 801 is pulled to condenser pipe 3 is crossed, specimen holder 8 is made to be located at the lower part of 7 nozzle of circulation pipe, outflow in circulation pipe 7 at this time Petroleum ether solvent sample can be eluted after be again introduced into flask 1 and carry out heating extraction, and the steam of solvent passes through sample Circulation pipe valve 701 can also be closed after or so about 4 hours with example reaction when product, open outlet tube valve 601, And receiving flask is placed in 6 end of outlet tube, after solvent extracted is heated at this time, steam ascends into reservoir 4, can be along out Liquid pipe 6 flows out directly into receiving flask, no longer flows into flask 1 from circulation pipe 7, after solvent is by all extraction collections, burns Without solvent in bottle 1, water-bath 2 can be closed, the extraction of solvent is completed.
Technical characteristic of the present invention without description can realize that details are not described herein by or using the prior art, certainly, The above description is not a limitation of the present invention, and the present invention is also not limited to the example above, the ordinary skill of the art The variations, modifications, additions or substitutions that personnel are made within the essential scope of the present invention also should belong to protection model of the invention It encloses.

Claims (9)

1. a kind of fat rapidly extracting device, including flask (1), the flask (1) are located in water-bath (2), the flask (1) Top is connected with the condenser pipe (3) being vertically arranged, which is characterized in that
The condenser pipe (3) includes outer tube (301) and inner tube (302), and inner tube (302) setting is internal in the outer tube (301), ring Around the condenser pipe (3), inner wall lower is provided with reservoir (4);
Outer tube (301) tube wall offers liquid in-out mouth, and liquid in-out mouth is separately connected inlet tube (5) and outlet tube (6), described It is external internal with reservoir (4) that inlet tube (5) and outlet tube (6) are respectively communicated with the condenser pipe (3);
Outlet tube valve (601) are provided on the pipeline of the outlet tube (6);
Outer tube (301) the tube body lower part is connected with circulation pipe (7), and described circulation pipe (7) one end is connected to outlet tube (6) pipe Part on body between outlet tube valve (601) and the condenser pipe (3) outer wall, the other end are connected to condenser pipe (3) inside, Circulation pipe (7) tube body is provided with circulation pipe valve (701);
The condenser pipe (3) is internally provided with specimen holder (8), is fixedly connected with lifting rope (801), institute at the top of the specimen holder (8) Lifting rope (801) are stated at the top of the condenser pipe (3) and extend to the condenser pipe (3) outside, are placed in the specimen holder (8) There is sample.
2. fat rapidly extracting device according to claim 1, which is characterized in that be divided into inside the condenser pipe (3) The internal diameter of the condensation segment in portion and the elution section of lower part, the elution section is less than the internal diameter of the condensation segment, the elution section bottom It is flexibly connected with the flask (1) bottleneck.
3. fat rapidly extracting device according to claim 2, which is characterized in that the institute of condenser pipe (3) condensation segment The tube wall for stating outer tube (301) is provided with two layers, is interlayer (303), the top and bottom of the interlayer (303) between two layers of outer tube wall End is closed, and is connected to condenser pipe (3) outside by outlet pipe (304) inside the interlayer (303).
4. fat rapidly extracting device according to claim 3, which is characterized in that said inner tube (302) is hollow spiral shell One end of coil, said inner tube (302) is connected to the water inlet pipe (305), and it is internal that the other end is connected to the interlayer (303).
5. fat rapidly extracting device according to claim 3, which is characterized in that the reservoir (4) is located at described cold Solidifying section, reservoir (4) bottom closure, top opening;
The end that the inlet tube (5) is located on the outside of the condenser pipe (3) is connected with funnel (501), the pipe of the inlet tube (5) Road is provided with feed liquor tube valve (502), and the inlet tube (5) extends in the reservoir (4) through the interlayer (303) Portion.
6. fat rapidly extracting device according to claim 1, which is characterized in that the outlet tube (6) is connected to described The trench bottom of reservoir (4);
The circulation pipe (7) is connected to the elution section of the condenser pipe (3).
7. fat rapidly extracting device according to claim 1, which is characterized in that be provided at the top of the condenser pipe (3) Sealing-plug (306), the lifting rope (801) run through the sealing-plug (306), and lifting rope (801) the rope body overhangs the condensation It manages in the middle part of (3), lifting rope (801) bottom end is flexibly connected the specimen holder (8) by hook, and the specimen holder (8) is hollow out Frame body.
8. fat rapidly extracting device according to claim 1, which is characterized in that the water-bath (2) is arranged in bracket (9) on, bracket (9) side is vertically arranged with strut (901), and the strut (901) is flexibly connected the condenser pipe (3) Outer wall.
9. fat rapidly extracting device according to claim 1, which is characterized in that the bottleneck inner wall of the flask (1) is Frosted layer.
CN201910705584.5A 2019-08-01 2019-08-01 A kind of fat rapidly extracting device Pending CN110314407A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201910705584.5A CN110314407A (en) 2019-08-01 2019-08-01 A kind of fat rapidly extracting device
PCT/CN2020/091681 WO2021017591A1 (en) 2019-08-01 2020-05-22 Quick extraction device for fat

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910705584.5A CN110314407A (en) 2019-08-01 2019-08-01 A kind of fat rapidly extracting device

Publications (1)

Publication Number Publication Date
CN110314407A true CN110314407A (en) 2019-10-11

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Application Number Title Priority Date Filing Date
CN201910705584.5A Pending CN110314407A (en) 2019-08-01 2019-08-01 A kind of fat rapidly extracting device

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CN (1) CN110314407A (en)
WO (1) WO2021017591A1 (en)

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CN112067492A (en) * 2020-07-13 2020-12-11 内蒙古沙漠之神生物科技有限公司 Camel milk component detection method
WO2021017591A1 (en) * 2019-08-01 2021-02-04 山东新希望六和集团有限公司 Quick extraction device for fat

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CN112067492A (en) * 2020-07-13 2020-12-11 内蒙古沙漠之神生物科技有限公司 Camel milk component detection method

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