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CN117225355B - Soaping agent high-precision proportion blending configuration equipment - Google Patents

Soaping agent high-precision proportion blending configuration equipment Download PDF

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Publication number
CN117225355B
CN117225355B CN202311503119.6A CN202311503119A CN117225355B CN 117225355 B CN117225355 B CN 117225355B CN 202311503119 A CN202311503119 A CN 202311503119A CN 117225355 B CN117225355 B CN 117225355B
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China
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plate
interface
reaction
storage tank
temporary storage
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Application number
CN202311503119.6A
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Chinese (zh)
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CN117225355A (en
Inventor
王艾德
梁丽丽
刘德铭
段红英
谢瑞丽
齐鹏举
周振红
刘庆润
田琪
刘冬冬
董科学
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Zibo Lurui Fine Chemical Co ltd
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Zibo Lurui Fine Chemical Co ltd
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Priority to CN202311503119.6A priority Critical patent/CN117225355B/en
Publication of CN117225355A publication Critical patent/CN117225355A/en
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Abstract

The application discloses soaping agent high accuracy proportion mediation configuration equipment relates to soaping agent production facility technical field, includes: a first temporary storage tank, one side of which is adjacently provided with a second temporary storage tank; the conveying pump is communicated with the temporary storage tank I and the temporary storage tank II; the reaction assembly is provided with a shunt interface, the shunt interface is connected with the output end of the conveying pump through a pipeline, and an additional switching end is reserved on the shunt interface; the motor box is fixedly arranged at the upper end of the reaction assembly, and a heat source box is further arranged on the side surface of the reaction assembly; the output valve is arranged below the reaction assembly and is communicated with the interior of the reaction assembly; the invention continuously controls the reactant to flow from bottom to top under the action of the inclined plate and the scraping plate, and the stirring components are axially arranged in a plurality of groups on the rotating shaft, so that compared with direct dripping stirring, the invention can effectively improve the mixing efficiency and reduce the occurrence of side reaction.

Description

Soaping agent high-precision proportion blending configuration equipment
Technical Field
The application relates to the technical field of soaping agent production equipment, in particular to soaping agent high-precision proportion blending configuration equipment.
Background
The soaping process mainly comprises the steps of placing dyed fabrics in soaping liquid, washing away dyes which are not combined with fibers and hydrolytic dyes through chemical combination of the soaping liquid and the dyes, and ensuring that the washed-away dyes and hydrolytic dyes are not returned to the fabrics.
Wherein the terpolymer P (MA-AA-NVP) synthesized by taking Maleic Anhydride (MA), acrylic Acid (AA) and N-vinyl pyrrolidone (NVP) as monomers has good colloid property and dispersion and solubilization, can form a complex with dye, but during the synthesis, the Maleic Anhydride (MA), the Acrylic Acid (AA) and the N-vinyl pyrrolidone (NVP) are subjected to copolymerization reaction under the action of free radicals, the charge density and the molecular weight of the copolymer are reduced along with self-polymerization side reaction, and the shuttle content (namely charge density) in the polymer is reduced to CaCO in water 3 Crystallization inhibition is weakened, molecular weight is reduced, and dispersing ability of the copolymer is impaired, and side reaction is currently inhibited by adding Maleic Anhydride (MA) at one time and dripping and stirring Acrylic Acid (AA) and N-vinyl pyrrolidone (NVP), but in the mass production process, the quality of the configured soaping agent is influenced because the amount of materials becomes large, the uniformity of mixing after dripping is difficult to ensure.
It is therefore desirable to provide a soaping agent high precision proportioning and dispensing apparatus that addresses the problems set forth in the background art discussed above.
Disclosure of Invention
In order to achieve the above purpose, the present application provides the following technical solutions: a soaping agent high precision proportioning and blending configuration device, comprising:
a first temporary storage tank, one side of which is adjacently provided with a second temporary storage tank;
the conveying pump is communicated with the temporary storage tank I and the temporary storage tank II;
the reaction assembly is provided with a shunt interface, the shunt interface is connected with the output end of the conveying pump through a pipeline, and an additional switching end is reserved on the shunt interface;
the motor box is fixedly arranged at the upper end of the reaction assembly, and a heat source box is further arranged on the side surface of the reaction assembly;
the output valve is arranged below the reaction assembly and is communicated with the inside of the reaction assembly.
Further, as an optimization, a motor composite part is arranged inside the motor box, a slow-conveying interface is arranged on the motor composite part, and the slow-conveying interface is communicated with the temporary storage tank I and the temporary storage tank II through a shunt interface.
Further, preferably, the reaction module includes:
the lower end of the reaction bin is provided with a heating component;
the scraping plate is rotatably arranged on the heating assembly and is positioned in the reaction bin;
the rotating shaft is rotatably arranged in the reaction bin, the upper end of the rotating shaft is connected to the motor composite part, the lower end of the rotating shaft is connected with the scraping plate, and the rotating shaft is controlled and driven to rotate by the motor composite part;
the stirring assemblies are arranged into a plurality of groups and are uniformly arranged on the rotating shaft;
and the canning interface is fixedly arranged on the reaction bin and communicated with the inside and the outside of the reaction bin through the shunt interface.
Further, preferably, the heating assembly includes:
the heating plate is fixed at the lower end of the reaction bin;
the heat source interface is arranged on the side surface of the heating disc and is externally connected with the heat source box for providing energy;
the heating wire is spirally wound in the heating disc and is connected with the heat source interface;
and the supporting plate is fixedly arranged between the heating plate and the reaction bin.
Further, preferably, the heating assembly further includes an output interface, the output interface is fixedly disposed on the heating plate, and the output interface penetrates through the heating plate and the supporting plate.
Further, preferably, the scraping plate is rotatably disposed on the supporting plate, and a plurality of fan blades are uniformly disposed on the circumference of the scraping plate, and the mounting position of the output interface corresponds to the fan blades.
Further, as the preference, evenly set up a plurality of clamping grooves that are used for installing in the pivot stirring subassembly, just the pivot is hollow tube, just inside interlude of pivot has the defeated pipe slowly, it passes through to slow the defeated pipe the interface intercommunication temporary storage jar one with temporary storage jar two, just it follows in the pivot the synchronous rotation of pivot to slow the defeated pipe.
Further, preferably, the stirring assembly includes a stirring plate group and an impact plate group symmetrically disposed about the rotation axis.
Further, as an preference, the impact plate group comprises a first drainage plate, a second drainage plate and a scraping plate, wherein the first drainage plate and the second drainage plate are arranged in parallel, the scraping plate is vertically arranged between the first drainage plate and the second drainage plate, and an included angle exists between a projection line formed on the first drainage plate by the long side of the scraping plate and the long side of the first drainage plate.
Further, as an preference, the stirring plate set includes an inclined plate, a third drainage plate and a drip-adding interface, wherein the lower surface of the inclined plate is parallel to the third drainage plate, an inclined plane is provided on the upper surface of the inclined plate, the drip-adding interface is fixedly provided on the upper surface of the third drainage plate, and the drip-adding interface is connected with the buffer pipe.
Compared with the prior art, the application provides a soaping agent high-precision proportion blending configuration device, which has the following beneficial effects: in the stirring process of the stirring plate set, the Acrylic Acid (AA), the N-vinyl pyrrolidone (NVP) and the Maleic Anhydride (MA) are added at the dripping interface to promote local mixing of the Acrylic Acid (AA), the N-vinyl pyrrolidone (NVP) and the Maleic Anhydride (MA) by means of turbulence, meanwhile, the Acrylic Acid (AA), the N-vinyl pyrrolidone (NVP) and the Maleic Anhydride (MA) are fully mixed between layers by means of circumferential impact of the impact plate set, in addition, the reactant flow from bottom to top is continuously controlled under the action of the inclined plate and the scraping plate, and a plurality of groups of stirring components are axially arranged on the rotating shaft, so that compared with direct dripping stirring, the mixing efficiency can be effectively improved, and the occurrence of side reaction is reduced.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a high-precision proportional tempering configuration device for soaping agent;
FIG. 2 is a schematic structural diagram of a reaction component in a high-precision proportioning and blending configuration device for soaping agent;
FIG. 3 is an enlarged schematic view of the structure of FIG. 2 at A;
FIG. 4 is a schematic diagram of the structure of a spindle in a high-precision proportional tempering configuration device for soaping agent;
FIG. 5 is a schematic diagram of the structure of an impingement plate group in a high-precision proportional tempering arrangement of a soaping agent;
FIG. 6 is an enlarged schematic view of the structure at B in FIG. 5;
in the figure: 1. a temporary storage tank I; 2. a temporary storage tank II; 3. a transfer pump; 4. a reaction assembly; 41. a reaction bin; 42. a heating assembly; 421. a heating plate; 422. a heat source interface; 423. a heating wire; 424. a supporting plate; 425. an output interface; 43. scraping a disc; 44. a rotating shaft; 441. a clamping groove; 442. a slow conveying pipe; 45. a stirring assembly; 451. a stirring plate group; 452. an impingement plate set; 453. a drainage plate I; 454. a drainage plate II; 455. a scraper; 456. an inclined plate; 457. a drainage plate III; 458. dropwise adding an interface; 46. a canning interface; 5. a shunt interface; 6. a motor case; 61. a motor composite; 62. a slow-transmission interface; 7. a heat source box; 8. and an output valve.
Detailed Description
Referring to fig. 1-6, in an embodiment of the present application, a high-precision proportioning and blending device for soaping agent includes:
a first temporary storage tank 1, one side of which is adjacently provided with a second temporary storage tank 2, wherein the first temporary storage tank 1 is used for transferring and storing Acrylic Acid (AA), and the second temporary storage tank 2 is used for transferring and storing N-vinyl pyrrolidone (NVP);
a delivery pump 3, which is communicated with the temporary storage tank 1 and the temporary storage tank 2, wherein the delivery pump 3 provides power for the internal solution transmission of the temporary storage tank 1 and the temporary storage tank 2;
the reaction assembly 4 is provided with a split-flow interface 5, the split-flow interface 5 is connected with the output end of the delivery pump 3 through a pipeline, an additional switching end is reserved on the split-flow interface 5, and canned Maleic Anhydride (MA) and deionized water are delivered through the switching end;
the motor box 6 is fixedly arranged at the upper end of the reaction assembly 4, and a heat source box 7 is also arranged on the side surface of the reaction assembly 4;
an output valve 8 is disposed below the reaction module 4, and the output valve 8 communicates with the inside of the reaction module 4, and the synthesized terpolymer P (MA-AA-NVP) is discharged through the output valve 8.
As a preferred embodiment, the motor box 6 is internally provided with a motor composite part 61, and the motor composite part 61 is provided with a buffer port 62, the buffer port 62 is communicated with the temporary storage tank 1 and the temporary storage tank 2 through a shunt port 5, and Acrylic Acid (AA) and N-vinyl pyrrolidone (NVP) are conveyed through the buffer port 62.
In this embodiment, as shown in fig. 2, the reaction module 4 includes:
a reaction chamber 41, the lower end of which is provided with a heating assembly 42;
a scraping plate 43 rotatably disposed on the heating assembly 42, and the scraping plate 43 is positioned inside the reaction chamber 41;
the rotating shaft 44 is rotatably arranged in the reaction bin 41, the upper end of the rotating shaft 44 is connected to the motor composite part 61, the lower end of the rotating shaft is connected to the scraping plate 43, and the motor composite part 61 controls the driving to rotate;
the stirring assemblies 45 are arranged in a plurality of groups and uniformly distributed on the rotating shaft 44, and the stirring assemblies 45 rotate along with the rotating shaft 44 to stir reactants in the reaction bin 41;
and a canning interface 46, which is fixedly arranged on the reaction bin 41, wherein the canning interface 46 is communicated with the inside and the outside of the reaction bin 41 through the shunt interface 5, and specifically, maleic Anhydride (MA), deionized water and an initiator are conveyed through the canning interface 46.
In this embodiment, as shown in fig. 3, the heating assembly 42 includes:
a heating plate 421 fixed to the lower end of the reaction chamber 41;
a heat source interface 422 disposed on a side surface of the heating plate 421, and the heat source interface 422 is externally connected to the heat source box 7 for providing energy;
the heating wire 423 is spirally wound in the heating disc 421, and the heating wire 423 is connected with the heat source interface 422 to heat the bottom of the reaction bin 41 through the heating wire 423;
the supporting plate 424 is fixedly arranged between the heating plate 421 and the reaction chamber 41, and separates the internal space of the reaction chamber 41 from the heating wires 423 by the supporting plate 424.
As a preferred embodiment, the heating assembly 42 further includes an output interface 425, the output interface 425 is fixedly disposed on the heating plate 421, and the output interface 425 penetrates through the heating plate 421 and the supporting plate 424, and the output interface 425 communicates with the interior of the reaction chamber 41 and the output valve 8.
As a preferred embodiment, the scraping plate 43 is rotatably disposed on the supporting plate 424, and a plurality of fan blades are uniformly disposed on the circumference of the scraping plate 43, specifically, the scraping plate 43 can effectively promote the reactant to flow from bottom to top in the reaction chamber 41 through the fan blades in the rotation process, and the mounting position of the output interface 425 corresponds to the fan blades, so that the terpolymer P (MA-AA-NVP) can be effectively promoted to be discharged by controlling the rotation direction of the scraping plate 43 after the reaction is completed.
As a preferred embodiment, the rotating shaft 44 is uniformly provided with a plurality of clamping grooves 441 for mounting the stirring assembly 45, the rotating shaft 44 is a hollow tube, a slow conveying tube 442 is inserted inside the rotating shaft 44, the slow conveying tube 442 is communicated with the temporary storage tank 1 and the temporary storage tank 2 through the slow conveying interface 62, and the slow conveying tube 442 rotates in the rotating shaft 44 along with the rotating shaft 44 synchronously.
In a preferred embodiment, the stirring assembly 45 includes a stirring plate set 451 and an impact plate set 452 symmetrically disposed about the rotation axis 44.
It should be noted that, as illustrated in the three-axis coordinate system of the X-axis, the Y-axis and the Z-axis established in fig. 4, the stirring plate set 451 can effectively promote the reactant to flow upward in the Y-axis and the Z-axis planes during the rotation of the rotating shaft 44, which is shown as promoting the reactant to flow downward in the reaction chamber 41, and the impact plate set 452 can effectively promote the reactant to flow circumferentially in the Y-axis and the Z-axis planes toward the rotating shaft 44 during the rotation of the rotating shaft 44.
As a preferred embodiment, the impact plate set 452 includes a first drainage plate 453, a second drainage plate 454 and a scraper 455, where the first drainage plate 453 and the second drainage plate 454 are arranged in parallel, the scraper 455 is vertically disposed between the first drainage plate 453 and the second drainage plate 454, and an included angle exists between a projection line formed by a long side of the scraper 455 on the first drainage plate 453 and a long side of the first drainage plate 453, specifically, a reactant passing through the space between the first drainage plate 453 and the second drainage plate 454 flows horizontally and circumferentially under the action of the scraper 455, and the reactant located on the same horizontal plane is impacted and mixed.
As a preferred embodiment, the stirring plate set 451 includes an inclined plate 456, a three drainage plate 457 and a drip interface 458, wherein the lower surface of the inclined plate 456 is parallel to the three drainage plate 457, the upper surface of the inclined plate 456 is provided with an inclined surface, specifically, the reactant flowing upward through the upper surface of the inclined plate 456, and the drip interface 458 is fixedly disposed on the upper surface of the three drainage plate 457, the reactant limited by the inclined plate 456 and the three drainage plate 457 passes through the drip interface 458, and a turbulent flow is formed at the drip interface 458, and the drip interface 458 is connected with the buffer tube 442, and the mixing can be effectively promoted by means of the turbulent flow by outputting the Acrylic Acid (AA) and the N-vinyl-pyrrolidone (NVP) through the drip interface 458.
It should be explained that, during the agitation of the agitation plate assembly 451, the Acrylic Acid (AA) and the N-vinyl pyrrolidone (NVP) are locally mixed by turbulence promotion by the addition of the Acrylic Acid (AA), the N-vinyl pyrrolidone (NVP) and the Maleic Anhydride (MA) at the drop-in interface 458, while the Acrylic Acid (AA), the N-vinyl pyrrolidone (NVP) and the Maleic Anhydride (MA) are sufficiently mixed between the layers by the circumferential impact by the impact plate assembly 452, and further the flow of the reactants from bottom to top is continuously controlled by the action of the inclined plate 456 and the scraping plate 43, and the agitation assembly 45 is arranged in plural groups in the axial direction of the rotating shaft 44, which is effective in improving the mixing efficiency as compared to the direct drop-in agitation, reducing the occurrence of side reactions.
In specific implementation, maleic Anhydride (MA) and deionized water are conveyed into the reaction component 4 through the transfer end of the shunt interface 5, the Maleic Anhydride (MA) and the deionized water in the reaction component 4 are preheated to 70 ℃ for 15min by heating through the heat source box 7, meanwhile, stirring is carried out in the reaction component 4 at the speed of 170r/min, the interior of the reaction component 4 is gradually heated to 80 ℃, an initiator is added into the interior of the reaction component 4 through the transfer end of the shunt interface 5 for continuous heat preservation for 5min, then, the continuous conveying of Acrylic Acid (AA) and N-vinyl pyrrolidone (NVP) into the reaction component 4 is controlled by the conveying pump 3, the temperature is gradually increased to 95 ℃ for promoting the completion of the copolymerization reaction, and then, cooling is carried out, and the terpolymer P (MA-AA-NVP) is discharged through the output valve 8.
The foregoing description is only a preferred embodiment of the present application, but the scope of the present application is not limited thereto, and any person skilled in the art, within the scope of the present application, should be covered by the protection scope of the present application, since all the technical solutions and the application concepts of the present application are equivalent and changed.

Claims (4)

1. A soaping agent high-precision proportion blending configuration device is characterized in that: comprising the following steps:
a temporary storage tank I (1), one side of which is adjacently provided with a temporary storage tank II (2);
a conveying pump (3) which is communicated with the temporary storage tank I (1) and the temporary storage tank II (2);
the reaction assembly (4) is provided with a shunt interface (5), the shunt interface (5) is connected with the output end of the conveying pump (3) through a pipeline, and an additional switching end is reserved on the shunt interface (5);
the motor box (6) is fixedly arranged at the upper end of the reaction assembly (4), and a heat source box (7) is also arranged at the side of the reaction assembly (4);
the output valve (8) is arranged below the reaction assembly (4), and the output valve (8) is communicated with the inside of the reaction assembly (4);
a motor composite part (61) is arranged in the motor box (6), a slow conveying interface (62) is arranged on the motor composite part (61), and the slow conveying interface (62) is communicated with the temporary storage tank I (1) and the temporary storage tank II (2) through a shunt interface (5);
the reaction module (4) comprises:
a reaction bin (41), the lower end of which is provided with a heating component (42);
a scraping plate (43) which is rotatably arranged on the heating component (42), and the scraping plate (43) is positioned in the reaction bin (41);
the rotating shaft (44) is rotatably arranged in the reaction bin (41), the upper end of the rotating shaft (44) is connected to the motor composite part (61), the lower end of the rotating shaft is connected to the scraping plate (43), and the motor composite part (61) controls the motor to drive the scraping plate to rotate;
the stirring assemblies (45) are arranged in a plurality of groups and uniformly distributed on the rotating shaft (44);
the canning interface (46) is fixedly arranged on the reaction bin (41), and the canning interface (46) is communicated with the inside and the outside of the reaction bin (41) through the shunt interface (5);
a plurality of clamping grooves (441) for installing the stirring assembly (45) are uniformly distributed on the rotating shaft (44), the rotating shaft (44) is a hollow tube, a slow conveying pipe (442) is inserted into the rotating shaft (44), the slow conveying pipe (442) is communicated with the temporary storage tank I (1) and the temporary storage tank II (2) through the slow conveying interface (62), and the slow conveying pipe (442) synchronously rotates in the rotating shaft (44) along with the rotating shaft (44);
the stirring assembly (45) comprises a stirring plate group (451) and an impact plate group (452) which are symmetrically arranged about the rotating shaft (44);
the impact plate group (452) comprises a first drainage plate (453), a second drainage plate (454) and a scraping plate (455), wherein the first drainage plate (453) and the second drainage plate (454) are arranged in parallel, the scraping plate (455) is vertically arranged between the first drainage plate (453) and the second drainage plate (454), and the plane of the scraping plate (455) is not parallel to the edge of the first drainage plate (453) or the edge of the second drainage plate (454);
stirring board group (451) are including hang plate (456), drainage board three (457) and dropwise add interface (458), wherein hang plate (456) lower surface with drainage board three (457) are parallel, the inclined plane has been seted up above hang plate (456), just drip add interface (458) are fixed to be set up drainage board three (457) upper surface, just drip add interface (458) are connected defeated pipe (442) slowly.
2. The soaping agent high precision proportioning and blending apparatus as defined in claim 1, wherein: the heating assembly (42) includes:
a heating plate (421) fixed at the lower end of the reaction chamber (41);
a heat source interface (422) arranged on the side surface of the heating plate (421), wherein the heat source interface (422) is externally connected with the heat source box (7) for providing energy;
the heating wire (423) is spirally wound inside the heating disc (421), and the heating wire (423) is connected with the heat source interface (422);
and the supporting plate (424) is fixedly arranged between the heating plate (421) and the reaction bin (41).
3. The soaping agent high precision proportioning and blending apparatus as claimed in claim 2, wherein: the heating assembly (42) further comprises an output interface (425), the output interface (425) is fixedly arranged on the heating plate (421), and the output interface (425) penetrates through the heating plate (421) and the supporting plate (424).
4. A soaping agent high precision proportioning and blending apparatus as defined in claim 3, wherein: the scraping plate (43) is rotatably arranged on the supporting plate (424), a plurality of fan blades are uniformly distributed on the circumference of the scraping plate (43), and the installation position of the output interface (425) corresponds to the fan blades.
CN202311503119.6A 2023-11-13 2023-11-13 Soaping agent high-precision proportion blending configuration equipment Active CN117225355B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202311503119.6A CN117225355B (en) 2023-11-13 2023-11-13 Soaping agent high-precision proportion blending configuration equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202311503119.6A CN117225355B (en) 2023-11-13 2023-11-13 Soaping agent high-precision proportion blending configuration equipment

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CN117225355A CN117225355A (en) 2023-12-15
CN117225355B true CN117225355B (en) 2024-01-09

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4721391A (en) * 1985-04-01 1988-01-26 Krauss-Maffei A.G. Impingement mixing device with auxiliary input and process for producing plastic parts
CN109052808A (en) * 2018-07-23 2018-12-21 徐州工程学院 A kind of ancillary equipment in more milk with probiotics production
CN112405865A (en) * 2020-11-12 2021-02-26 肖景雄 Waste scraping equipment for concrete mixer truck
CN217323502U (en) * 2022-04-28 2022-08-30 泸州山水秀美环保科技有限公司 Calcium removing device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4721391A (en) * 1985-04-01 1988-01-26 Krauss-Maffei A.G. Impingement mixing device with auxiliary input and process for producing plastic parts
CN109052808A (en) * 2018-07-23 2018-12-21 徐州工程学院 A kind of ancillary equipment in more milk with probiotics production
CN112405865A (en) * 2020-11-12 2021-02-26 肖景雄 Waste scraping equipment for concrete mixer truck
CN217323502U (en) * 2022-04-28 2022-08-30 泸州山水秀美环保科技有限公司 Calcium removing device

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