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CN1167609A - Filling material for dental root-canals - Google Patents

Filling material for dental root-canals Download PDF

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Publication number
CN1167609A
CN1167609A CN 96106367 CN96106367A CN1167609A CN 1167609 A CN1167609 A CN 1167609A CN 96106367 CN96106367 CN 96106367 CN 96106367 A CN96106367 A CN 96106367A CN 1167609 A CN1167609 A CN 1167609A
Authority
CN
China
Prior art keywords
root canal
filling material
filler
millimeter
tooth root
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 96106367
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Chinese (zh)
Other versions
CN1060034C (en
Inventor
刘克付
杨凤芝
秦葵庆
曹继红
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Youyan Yijin New Material Co., Ltd.
Original Assignee
Beijing General Research Institute for Non Ferrous Metals
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing General Research Institute for Non Ferrous Metals filed Critical Beijing General Research Institute for Non Ferrous Metals
Priority to CN96106367A priority Critical patent/CN1060034C/en
Publication of CN1167609A publication Critical patent/CN1167609A/en
Application granted granted Critical
Publication of CN1060034C publication Critical patent/CN1060034C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

An alloy material used as filler of dental root canal is a Ni-Ti alloy including Ni (54.5-56.7Wt%) and Ti (the rest) and has a shape that is one of conic needle and cylinder. Its advantages are excellent anticorrosion nature and compatibility, super elasticity, and low brittleness.

Description

A kind of filler that is used for root canal
The present invention relates to a kind of root canal alloy filling material that is used for.
Current, the filler of filling root canal is commercially available gutta percha point or acupuncture needle through what use always.Gutta percha point is to be added materials such as zinc oxide, calcium oxide, white beeswax to make by Malaysia red ferrum section resin.
Chinese patent literature CN1040920A (application number 89105193.7) has introduced a kind of dental Magnetic-resin filling material.It is to make the water solublity base fluid by formaldehyde and cresols or resorcinol and sodium hydroxide, in the mixed liquor of above-mentioned any base fluid or two kinds of base fluids, adds the ferromagnetism Fe that is enclosed with activator 3O 4Minuteness particle is made root canal filling liquid.This root canal filling liquid has ferromagnetism, flowability and polymerization.
Another piece Chinese patent literature CN1062835A (application number 91107542.9) has introduced a kind of high magnetical solid filling material for periodontal duct.This is to be main body by pure Malaya natural gum and high magnetic material SmCo magnetic powder, is equipped with composite oxide powder and zinc, lithopone and paraffin, through mix homogeneously repeatedly in mixing roll, is processed into circular cone needle-like glue point.Drying technology such as magnetize is made into normalized magnetic gutta percha point again.
The dental Magnetic-resin filling material that Chinese patent literature CN1040920A introduced owing to be a kind of liquid, in use is difficult for being injected into desired area, operation inconvenience.And all contain white beeswax in the high magnetical solid filling material for periodontal duct that above-mentioned commercially available gutta percha point and Chinese patent literature CN1062835A introduce, pinch and in hands, do not have rigidity, feel like jelly, be difficult to insert in the root canal, the operation of therefore being a patient needs long time.Though the commercially available gutta percha point of its strength ratio of acupuncture needle and with the magnetic gutta percha point height that high magnetical solid filling material for periodontal duct is made is easy to insert in the root canal, it is low that the intensity of argent still shows, and inserts in tiny curved canals or extract still very hard.In addition, silver is poor with human compatibility, and acupuncture needle is run into the easy inflammation of tooth palate.
Purpose of the present invention just is to develop a kind of new filler that is used for root canal, and this filler has overcome above-mentioned commercially available gutta percha point, the shortcoming that exists in the prior arts such as root canal filling liquid, magnetic gutta percha point, acupuncture needle.
A kind of filler that is used for root canal of the present invention is the nickel of by 54.5~56.7% (percetages by weight, down with), and surplus is that the Nitinol of titanium constitutes, and it is shaped as wherein a kind of of circular cone spicule, cylinder.
In order to make this filler be easier to extract from root canal, it is good being little round with the big first end at the tooth root canal filling material of circular cone spicule.Equally, any end of cylinder tooth root canal filling material is little round for well.Circular cone spicule tooth root canal filling material, the diameter of major part be 0.10~1.0 millimeter for well, again with 0.15~1.0 millimeter for better.Length is the 10-40 millimeter.The diameter of cylinder tooth root canal filling material is 0.10~1.0 millimeter, again with 0.15~1.0 millimeter for better, length is 10~40 millimeters.The used Nitinol of the present invention also contains inevitably other impurity elements.
The vacuum melting method of all knowing with the those of ordinary skill under this area is made the nickel-titanium alloy material of required composition, draw wire, be raw material with the qualified thick titanium-nickel wire of composition again, draw with the drawing by high temperature method, general temperature at 400-700 ℃ stretches, and breaks the tooth root canal filling material that just forms the circular cone spicule.Do not move required diameter to and just form the cylindrical shape tooth root canal filling material if do not break.
The advantage of the tooth root canal filling material of being made by Nitinol of the present invention just is that it has excellent corrosion resistance.It in the physiology simulative corrosion test, its corrosion rate<6.8 * 10 -5In millimeter/year, belong to 1 grade of corrosion resistance.And it has the good compatibility again.Its another advantage is to have good super-elasticity, and its yield strength is significantly less than tensile strength sigma b=(2~4) σ 0.3, it loads the back martensitic phase transformation takes place, easily surrender.Restore to the original state again after the unloading, so it had both had super-elasticity, not brittle failure again so be easy to insert from root canal, is easy to again extract from root canal, and it is a kind of good root canal filling thing.
The stress strain curve figure of the Nitinol tooth root canal filling material that Fig. 1 Φ is 0.46 millimeter
Among the figure, abscissa is a deformation rate, %; Vertical coordinate is a volume unit: newton/square millimeter.
Fig. 2 circular cone spicule tooth root canal filling material sketch map.
Fig. 3 cylinder tooth root canal filling material sketch map.
Fig. 4 circular cone needle-like tooth root canal filling material stub end is ringlet shape sketch map.
Fig. 5 cylinder tooth root canal filling material is ringlet shape sketch map.
With following indefiniteness embodiment tooth root canal filling material of the present invention is further described, will helps the understanding to the present invention and advantage thereof, and not as a limitation of the invention, protection scope of the present invention is decided by claims.
Embodiment 1
Tooth root canal filling material in the present embodiment is by the nickel of 55.6% (percetage by weight), and surplus is that the Nitinol of titanium constitutes, and it is shaped as the circular cone spicule.0.46 millimeter of diameter at butt end Φ, long 30 millimeters, tensile strength sigma b1580MPa, yield strength σ m470MPa, percentage elongation 16%, its stress strain curve figure sees Fig. 1.Stretch in 650 ℃ with said method, break and make.See Fig. 2.
Embodiment 2
Present embodiment be used for the nickel of tooth root canal filling material by 55.0% (percetage by weight), surplus is that the Nitinol of titanium constitutes.It is shaped as cylinder, and its diameter of phi is 0.5 millimeter, tensile strength sigma bBe 1340MPa, see Fig. 3.
Embodiment 3
Present embodiment be used for the nickel of tooth root canal filling material by 55.2% (percetage by weight), surplus is that the Nitinol of titanium constitutes.It is shaped as the circular cone spicule, and diameter at butt end Φ is 0.5 millimeter, and tensile strength is σ b1360MPa, big first end is little round, sees Fig. 4.
Embodiment 4
Present embodiment be used for the nickel of tooth root canal filling material by 55.3% (percetage by weight), surplus is that the Nitinol of titanium constitutes.It is shaped as cylinder, and its diameter of phi is 0.5 millimeter, tensile strength sigma bBe 1400MPa, the one end long 30 millimeters, is seen Fig. 5 for being little round.
Embodiment 5
Present embodiment be used for the nickel of tooth root canal filling material by 55.4% (percetage by weight), surplus is that the Nitinol of titanium constitutes, it is shaped as the circular cone spicule, the diameter of phi of its major part is 0.5 millimeter, tensile strength sigma bBe 1440MPa, length is 30 millimeters.

Claims (5)

1. a filler that is used for root canal is characterized in that, the nickel of (percetages by weight, down with), the Nitinol that surplus is titanium constitute by 54.5~56.7%, and it is shaped as wherein a kind of of circular cone spicule, cylinder.
2. according to a kind of filler that is used for root canal of claim 1, it is characterized in that the big first end of the tooth root canal filling material of circular cone spicule is little round.
3. according to a kind of filler that is used for root canal of claim 1, it is characterized in that any end of cylinder tooth root canal filling material is little round.
4. according to a kind of filler that is used for root canal of claim 1 or 2, it is characterized in that circular cone spicule filler, the diameter of major part are 0.10~1.0 millimeter.
5. according to a kind of filler that is used for root canal of claim 1 or 3, it is characterized in that the diameter of cylinder tooth root canal filling material is 0.1~1.0 millimeter.
CN96106367A 1996-06-07 1996-06-07 Filling material for dental root-canals Expired - Fee Related CN1060034C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN96106367A CN1060034C (en) 1996-06-07 1996-06-07 Filling material for dental root-canals

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN96106367A CN1060034C (en) 1996-06-07 1996-06-07 Filling material for dental root-canals

Publications (2)

Publication Number Publication Date
CN1167609A true CN1167609A (en) 1997-12-17
CN1060034C CN1060034C (en) 2001-01-03

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN96106367A Expired - Fee Related CN1060034C (en) 1996-06-07 1996-06-07 Filling material for dental root-canals

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106377434A (en) * 2016-11-18 2017-02-08 莫总鸣 Manufacturing method of root canal filling tip

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07102217B2 (en) * 1991-05-23 1995-11-08 克成 西原 An artificial tooth root with the function of a natural tooth root
JPH05271032A (en) * 1992-03-30 1993-10-19 Daido Steel Co Ltd Artificial dental root

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106377434A (en) * 2016-11-18 2017-02-08 莫总鸣 Manufacturing method of root canal filling tip
CN106377434B (en) * 2016-11-18 2019-06-11 莫总鸣 The manufacturing method of canalis radicis dentis filling point

Also Published As

Publication number Publication date
CN1060034C (en) 2001-01-03

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Owner name: BE YANYIJIN NEW MATERIAL CO., LTD.

Free format text: FORMER OWNER: BEIJING NON-FERROUS METAL RESEARCH GENERAL ACADEMY

Effective date: 20020326

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Effective date of registration: 20020326

Address after: No. 2, Xinjie street, Xicheng District, Beijing

Patentee after: Youyan Yijin New Material Co., Ltd.

Address before: No. 2, Xinjie street, Beijing

Patentee before: General Research Institute for Nonferrous Metals

C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee