CN116349918A - Recycling method of filter stick for waste cigarettes - Google Patents
Recycling method of filter stick for waste cigarettes Download PDFInfo
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- CN116349918A CN116349918A CN202310282832.6A CN202310282832A CN116349918A CN 116349918 A CN116349918 A CN 116349918A CN 202310282832 A CN202310282832 A CN 202310282832A CN 116349918 A CN116349918 A CN 116349918A
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- Prior art keywords
- filter
- waste
- filter stick
- cigarettes
- recycling
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 137
- 239000002699 waste material Substances 0.000 title claims abstract description 97
- 238000000034 method Methods 0.000 title claims abstract description 38
- 238000004064 recycling Methods 0.000 title claims abstract description 31
- 238000007493 shaping process Methods 0.000 claims abstract description 25
- 239000000463 material Substances 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims description 43
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical group CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims description 34
- 229910052782 aluminium Inorganic materials 0.000 claims description 28
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 28
- 239000004014 plasticizer Substances 0.000 claims description 22
- 239000001087 glyceryl triacetate Substances 0.000 claims description 17
- 235000013773 glyceryl triacetate Nutrition 0.000 claims description 17
- 229960002622 triacetin Drugs 0.000 claims description 17
- OVOUKWFJRHALDD-UHFFFAOYSA-N 2-[2-(2-acetyloxyethoxy)ethoxy]ethyl acetate Chemical compound CC(=O)OCCOCCOCCOC(C)=O OVOUKWFJRHALDD-UHFFFAOYSA-N 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 12
- 239000012535 impurity Substances 0.000 claims description 10
- 239000011248 coating agent Substances 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 241000405070 Percophidae Species 0.000 claims description 7
- 239000002131 composite material Substances 0.000 claims description 3
- 238000009998 heat setting Methods 0.000 claims description 3
- 239000011218 binary composite Substances 0.000 abstract description 2
- 239000011219 quaternary composite Substances 0.000 abstract description 2
- 239000011206 ternary composite Substances 0.000 abstract description 2
- 230000000391 smoking effect Effects 0.000 description 38
- 230000000694 effects Effects 0.000 description 14
- 229920006239 diacetate fiber Polymers 0.000 description 9
- 238000005516 engineering process Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- 239000000835 fiber Substances 0.000 description 7
- 230000001953 sensory effect Effects 0.000 description 7
- 241000208125 Nicotiana Species 0.000 description 6
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 239000004411 aluminium Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- 229920006221 acetate fiber Polymers 0.000 description 2
- 238000009960 carding Methods 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000000053 physical method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000001172 regenerating effect Effects 0.000 description 2
- 238000009987 spinning Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 229920001747 Cellulose diacetate Polymers 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000007602 hot air drying Methods 0.000 description 1
- 238000010902 jet-milling Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0229—Filter rod forming processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J11/00—Recovery or working-up of waste materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to recycling of filter sticks for waste cigarettes, which comprises the steps of pretreatment, filter stick softening, filter stick shaping and the like. The invention provides a method for recycling waste filter sticks for cigarettes, which has the advantages of simple process, low operation cost and high industrialization implementation, solves the recycling problem of the filter sticks for waste cigarettes, and can be used alone or combined with filter sticks made of other materials into binary, ternary or quaternary composite filter sticks.
Description
[ field of technology ]
The invention belongs to the technical field of cigarette material production. More particularly, the invention relates to a recycling method of filter sticks for waste cigarettes.
[ background Art ]
In order to reduce the harm of smoking to human body, the cigarette filter stick has become an indispensable cigarette material in the production of cigarette products, and in cigarette filter stick tow materials, diacetate fiber tow is an excellent cigarette filter stick material accepted in industry and has been widely used until now. The method has the advantages of recycling the waste diacetate fiber filter stick for cigarettes, meeting the basic national policy of national energy conservation, consumption reduction and pollution control, and having remarkable social value.
The waste cellulose diacetate filter sticks for cigarettes produced at home are concentrated in cigarette enterprises and filter stick production enterprises, and are relatively concentrated. Has higher feasibility and economic value for recycling the waste diacetate fiber filter stick for cigarettes.
At present, the waste diacetate fiber filter stick for the cigarettes is mainly prepared by adopting processes of cotton spinning, opening, carding, slivering, jet milling, cleaning with organic solvents and the like, and the recovery process has the problems of complex process, high energy consumption, low raw material utilization rate, use of the organic solvents and the like. CN1032283a, entitled "manufacturing cigarette filter rod by regenerating waste materials by physical method" discloses that the filter rod is manufactured by regenerating the waste materials of diacetate fiber process generated during the shaping and processing of filter rod in cigarette factories by physical methods such as opening and carding and forming in cotton spinning engineering. The process is complex, the utilization rate of raw materials is low, and the paper stripping time is limited to be within two hours after the waste filter rod is taken off the machine. CN1839718A, entitled "method for cleaning waste acetate fibers" discloses that waste acetate fibers are recovered by adopting an ethanol cleaning mode with concentration of more than 80%. The process is simple, but the actual application effect is not ideal, mainly because the formed paper can not be removed completely after the waste filter stick for cigarettes is crushed, the subsequent use is affected, and meanwhile, because the high-concentration ethanol is used, potential safety hazards exist in the production process. CN 103965507a, the title of the invention "recovery system and recovery process for waste diacetate fiber filter stick for tobacco" discloses that the waste diacetate fiber filter stick for tobacco is sent into a unpacking system for unpacking and impurity removal, then sent to a conveyer belt with a spraying system for wetting and conveying, then sent to a paper removal system for removing formed paper, then sent to a stirrer for stirring, sent to a drying box for hot air drying, sent to a fiber pulverizer for pulverization after the moisture of the waste diacetate fiber filter stick for tobacco is less than 8%, finally sent to a fiber dust separator for screening through wind power for fiber dust separation, and finally sent to packing through wind power to obtain recovered diacetate fiber. The process is simple, but has high running cost and complex procedure, and is not beneficial to industrialized implementation.
Thus, the present inventors have completed the present invention through a large number of experiments and analyses, aiming at a number of technical drawbacks of the prior art.
[ invention ]
[ problem to be solved ]
The invention aims to provide a recycling method of filter sticks for waste cigarettes.
Technical scheme
The invention is realized by the following technical scheme.
The invention relates to a recycling method of filter sticks for waste cigarettes.
The recycling method comprises the following steps:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
C, coating a plasticizer on the surface of the pretreated waste cigarette filter stick obtained in the step A, uniformly mixing, and standing for 2-4 hours at room temperature to obtain a softened waste cigarette filter stick;
C. filter stick shaping
And C, adding the softened filter sticks for the waste cigarettes obtained in the step B to cast aluminum heating plates with different shapes, heating and shaping, and solidifying to obtain the filter sticks with corresponding different shapes.
According to a preferred embodiment of the invention, in step B, the plasticizer is glyceryl triacetate, triethylene glycol diacetate or a mixture thereof.
According to another preferred embodiment of the invention, in step B, their mixture is composed of glyceryl triacetate and triethylene glycol diacetate in a weight ratio of 1:0.1 to 10.0 percent of the mixture.
According to another preferred embodiment of the invention, in step B, the plasticizer is added in an amount of 5 to 15% by weight of the pretreated waste tobacco filter rod.
According to another preferred embodiment of the invention, in step C, the heat setting temperature of the softened waste tobacco filter rod on a cast aluminium heating plate having a different shape is 80-120 ℃.
According to another preferred embodiment of the present invention, in the step C, the shape of the cast aluminum heating plate is a duckbill, five-star, cross or delta-star shape.
According to another preferred embodiment of the invention, in step C, the cast aluminium heating plate is shaped in the direction of the longitudinal axis of the cast aluminium heating plate, half of which is cylindrical and the other half of which is duckbill, pentagram, cross or delta-star.
According to another preferred embodiment of the present invention, in the step C, the heat-set waste tobacco filter rod is cured at room temperature for 22 to 26 hours.
The invention also relates to filter sticks with different shapes obtained by adopting the filter stick recycling method.
The invention also relates to the application of the filter rod with different shapes as an independent filter rod or the application of the filter rod with other material filter rods to manufacture a composite filter rod.
The present invention will be described in more detail below
The invention relates to a recycling method of filter sticks for waste cigarettes.
According to the present invention, the term waste cigarette filter rod is understood to mean a filter rod which is produced during the production of a cigarette and cannot be used for producing a cigarette, or a waste filter rod which is thrown away by a person after the smoking of a cigarette.
The recycling method comprises the following steps:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
the pretreated waste cigarette filter rod obtained in the step is detected for microorganisms, heavy metals and the like according to a detection method specified by GB/T5009-2003 and GB/T38483-2020 standards, and the pretreated waste cigarette filter rod meeting the specified standards can be subjected to subsequent treatment.
B. Filter stick softening
C, coating a plasticizer on the surface of the pretreated waste cigarette filter stick obtained in the step A, uniformly mixing, and standing for 2-4 hours at room temperature to obtain a softened waste cigarette filter stick;
in the invention, the plasticizer has the basic function in the softening treatment of the filter stick for the pretreated waste cigarettes, and can be combined with the filter stick fibers at normal temperature to dissolve and soften the surfaces of the fibers, and the fibers are mutually adhered to improve the hardness of the filter stick, so that the processing performance of the filter stick during molding is improved.
The plasticizer used in the present invention is triacetin, triethylene glycol diacetate or a mixture thereof. The mixture is prepared from glyceryl triacetate and triethylene glycol diacetate according to the weight ratio of 1:0.1 to 10.0 percent of the mixture. In the present invention, if the weight ratio of triacetin to triethylene glycol diacetate is greater than 1:0.1, the hardening speed is too high, which is unfavorable for the subsequent processing technology; if the weight ratio of glyceryl triacetate to triethylene glycol diacetate is less than 1:10.0, the hardening speed is too slow to meet the requirement of hardening the filter rod; thus, the weight ratio of glyceryl triacetate to triethylene glycol diacetate was 1:0.1 to 10.0 is suitable.
The glyceryl triacetate and the triethylene glycol diacetate used in the invention are plasticizers widely used in the cigarette filter stick industry, have the functions of being colorless, odorless, nontoxic, proper in dissolving power and solidifying speed and improving the quality of cigarette smoke, and are all products sold in the current market, such as the glyceryl triacetate sold under the trade name of the glyceryl triacetate by national pharmaceutical group chemical reagent company.
Of course, other plasticizers currently on the market can be used in the present invention, except that they should have the functions described in the specification of the present application and they do not have any adverse effect on the waste cigarette filter rods and their recycling methods, and these plasticizers are also within the scope of the present invention.
According to the invention, in step B, the addition amount of the plasticizer is 5-15% by weight of the pretreated waste cigarette filter rod. If the addition amount of the plasticizer is less than 5%, the hardness of the filter stick processed by the method is insufficient, and the process and the performance of the connection of the filter stick and cigarette are directly affected; if the addition amount of the plasticizer is higher than 15%, the plasticizer contained in the filter stick processed by the method is more transferred into smoke, so that the sensory quality of cigarette smoke is affected; therefore, the addition amount of the plasticizer is reasonable in the range of 5 to 15%, preferably 8 to 12%.
According to the invention, the filter stick for the pretreated waste cigarettes needs to be kept stand after the plasticizer is smeared on the surface of the filter stick, and the purpose of the invention is to enable the plasticizer to be fully contacted with the filter stick tows, so that the fiber surfaces of the filter stick tows are dissolved and softened to be mutually adhered, thereby being beneficial to the subsequent shaping of the filter stick. The time for this standing is 2 to 4 hours. If the standing time is shorter than 2 hours, the surface of the filter stick for the waste cigarettes is not completely softened or the softening degree is insufficient, and the subsequent processing effect of the filter stick for the waste cigarettes is affected; if the standing time is longer than 4 hours, the softening time is too long, and the softened filter stick for the waste cigarettes can be partially solidified, so that the subsequent processing is not facilitated. Therefore, the filtration standing time is suitably 2 to 4 hours, preferably 2.5 to 3.5 hours.
C. Filter stick shaping
And C, adding the softened filter sticks for the waste cigarettes obtained in the step B to cast aluminum heating plates with different shapes, heating and shaping, and solidifying to obtain the filter sticks with corresponding different shapes.
The main function of the step C of the method for recycling the filter sticks for the abandoned cigarettes is to heat and shape the filter sticks so that the filter sticks have a preliminary shape.
The cast aluminum heating plate is a cast aluminum heating plate which takes a tubular electric heating element as a heating body and takes a high-quality aluminum alloy material as a shell, the service temperature of the cast aluminum heating plate is generally 60-450 ℃, and the cast aluminum heating plate is widely applied to the technical fields of plastic machinery, die heads, cable machinery, chemical industry, rubber, petroleum and the like.
According to the invention, the heat setting temperature of the filter rod for softening waste cigarettes on the cast aluminum heating plates with different shapes is 80-120 ℃. The heating and shaping temperature exceeding the temperature range is not preferable because if the heating and shaping temperature is lower than 80 ℃, the shaping effect is poor, the loosening phenomenon is easy to occur in the later curing, and the shaping effect is not achieved; if the heating setting temperature is higher than 120 ℃, the heating temperature is too high, which is liable to cause the filter rod to be pasted and affect the appearance effect of the filter rod, so that the heating setting temperature is suitably 80-120 ℃, preferably 90-110 ℃.
The shape of the cast aluminum heating plate used in the invention is duckbill, five-pointed star, cross or triangle star.
The cast aluminium heating plate used according to the invention may also be shaped in the direction of the longitudinal axis of the cast aluminium heating plate, half of which is cylindrical and the other half of which is duckbill, pentagram, cross or delta-star. For example, when the length of the filter rod obtained by the method is 120mm and the target filter rod length is 30mm, the sections of the four-slit filter rod with the length of 0-15mm, 45-75mm and 95-120mm in the longitudinal axis direction of the cast aluminum heating plate are cylindrical, and the sections with the length of 15-45mm and 75-95mm are duckbill, five-pointed star, cross or triangular star. When the length of the target filter stick is 20mm, the sections of the six-slit filter stick, namely the 10 th to 10 th mm, the 30 th to 50 th mm, the 70 th to 90 th mm and the 110 th to 120 th mm, are cylindrical, the 10 th to 30 th mm, the 50 th to 70 th mm and the 90 th to 110 th mm sections are duckbill-shaped, five-pointed star-shaped, cross-shaped or triangular star-shaped, and the design has the advantages that the cylindrical section can be better rolled with cigarettes, and the special shape of the other end can play a role in beautifying cigarettes.
According to the invention, the heat-set filter stick for waste cigarettes is solidified for 22-26 hours at room temperature. If the solidification time is shorter than 22 hours, the filter stick is not thoroughly solidified, and the filter stick is easy to deform; if the curing time is longer than 26 hours, the curing time is too long, curing has no effect and the processing efficiency is affected. Therefore, a curing time of between 22 and 26 hours is preferable.
The invention also relates to filter sticks with different shapes obtained by adopting the filter stick recycling method.
The invention also relates to the application of the filter rod with different shapes as an independent filter rod or the application of the filter rod with other material filter rods to manufacture a composite filter rod.
[ advantageous effects ]
The beneficial effects of the invention are as follows:
the invention provides a method for recycling waste filter sticks for cigarettes, which has the advantages of simple process, low operation cost and high industrialization implementation, solves the recycling problem of the filter sticks for waste cigarettes, and can be used alone or combined with filter sticks made of other materials into binary, ternary or quaternary composite filter sticks.
[ detailed description ] of the invention
The invention will be better understood by the following examples.
Example 1: the invention relates to recycling of filter sticks for waste cigarettes
The specific implementation steps of this embodiment are as follows:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
C, coating a triacetin plasticizer on the surface of the pretreated waste cigarette filter stick obtained in the step A according to the weight of the pretreated waste cigarette filter stick, uniformly mixing, and standing for 2.4 hours at room temperature to obtain a softened waste cigarette filter stick;
C. filter stick shaping
And C, adding the softened filter stick for waste cigarettes obtained in the step B onto a duckbilled cast aluminum heating plate, heating and shaping, and solidifying for 25 hours at room temperature to obtain the filter stick with the corresponding shape.
According to the cigarette sensory technology requirement smoking standard of GB5606.4-2005, a smoking group consisting of 15 smoking experts is organized to carry out smoking on cigarettes using the filter stick of the invention and commercial traditional cigarettes as comparison samples, and the smoking result shows that the smoking experience effect of the cigarettes using the filter stick of the invention is basically the same as that of the comparison samples.
Example 2: the invention relates to recycling of filter sticks for waste cigarettes
The specific implementation steps of this embodiment are as follows:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
According to the weight of the pretreated waste cigarette filter stick, 5 percent of the weight of the pretreated waste cigarette filter stick is coated with triethylene glycol diacetate plasticizer, and the mixture is uniformly mixed and kept stand for 2.0 hours at room temperature to obtain a softened waste cigarette filter stick;
C. filter stick shaping
And C, adding the softened filter stick for waste cigarettes obtained in the step B onto a duckbilled cast aluminum heating plate, heating and shaping, and solidifying for 22 hours at room temperature to obtain the filter stick with the corresponding shape.
According to the cigarette sensory technology requirement smoking standard of GB5606.4-2005, a smoking group consisting of 15 smoking experts is organized to carry out smoking on cigarettes using the filter stick of the invention and commercial traditional cigarettes as comparison samples, and the smoking result shows that the smoking experience effect of the cigarettes using the filter stick of the invention is basically the same as that of the comparison samples.
Example 3: the invention relates to recycling of filter sticks for waste cigarettes
The specific implementation steps of this embodiment are as follows:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
And (C) coating the surface of the filter stick for the pretreated waste cigarette obtained in the step (A) with triacetin and triethylene glycol diacetate according to the weight ratio of 1:0.1, uniformly mixing, and standing for 4.0 hours at room temperature to obtain a softened filter stick for waste cigarettes;
C. filter stick shaping
And C, adding the softened filter stick for waste cigarettes obtained in the step B onto a cross-shaped cast aluminum heating plate, heating and shaping, and solidifying for 24 hours at room temperature to obtain the filter stick with the corresponding shape.
According to the cigarette sensory technology requirement smoking standard of GB5606.4-2005, a smoking group consisting of 15 smoking experts is organized to carry out smoking on cigarettes using the filter stick of the invention and commercial traditional cigarettes as comparison samples, and the smoking result shows that the smoking experience effect of the cigarettes using the filter stick of the invention is basically the same as that of the comparison samples.
Example 4: the invention relates to recycling of filter sticks for waste cigarettes
The specific implementation steps of this embodiment are as follows:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
And (C) coating the surface of the pretreated waste cigarette filter stick obtained in the step (A) with triacetin and triethylene glycol diacetate according to the weight ratio of 1:1.0, uniformly mixing, and standing for 3.2 hours at room temperature to obtain a softened filter stick for waste cigarettes;
C. filter stick shaping
And C, adding the softened filter stick for waste cigarettes obtained in the step B onto a triangular star-shaped cast aluminum heating plate, heating and shaping, and solidifying for 26 hours at room temperature to obtain the filter stick with the corresponding shape.
According to the cigarette sensory technology requirement smoking standard of GB5606.4-2005, a smoking group consisting of 15 smoking experts is organized to carry out smoking on cigarettes using the filter stick of the invention and commercial traditional cigarettes as comparison samples, and the smoking result shows that the smoking experience effect of the cigarettes using the filter stick of the invention is basically the same as that of the comparison samples.
Example 5: the invention relates to recycling of filter sticks for waste cigarettes
The specific implementation steps of this embodiment are as follows:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
And (C) coating the surface of the filter stick for the pretreated waste cigarette obtained in the step (A) with triacetin and triethylene glycol diacetate according to the weight ratio of 1:10.0, uniformly mixing, and standing for 2.8 hours at room temperature to obtain a softened filter stick for waste cigarettes;
C. filter stick shaping
And B, adding the softened waste cigarette filter rod obtained in the step B to a cast aluminum heating plate, wherein one half of the filter rod is cylindrical in the longitudinal axis direction of the cast aluminum heating plate, and the other half of the filter rod is five-pointed star-shaped, heating and shaping, and solidifying for 23 hours at room temperature to obtain the filter rod with the corresponding shape.
According to the cigarette sensory technology requirement smoking standard of GB5606.4-2005, a smoking group consisting of 15 smoking experts is organized to carry out smoking on cigarettes using the filter stick of the invention and commercial traditional cigarettes as comparison samples, and the smoking result shows that the smoking experience effect of the cigarettes using the filter stick of the invention is basically the same as that of the comparison samples.
Example 6: the invention relates to recycling of filter sticks for waste cigarettes
The specific implementation steps of this embodiment are as follows:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
And (C) coating the surface of the pretreated waste cigarette filter stick obtained in the step (A) with a mixture of triacetin and triethylene glycol diacetate according to the weight ratio of 1:5.0, uniformly mixing the mixture plasticizer, and standing for 3.6 hours at room temperature to obtain a softened filter stick for waste cigarettes;
C. filter stick shaping
And B, adding the softened waste cigarette filter rod obtained in the step B to a cast aluminum heating plate with half of the filter rod being cylindrical in the longitudinal axis direction of the cast aluminum heating plate and the other half of the filter rod being triangular star-shaped, heating and shaping, and solidifying for 24 hours at room temperature to obtain the filter rod with the corresponding shape.
According to the cigarette sensory technology requirement smoking standard of GB5606.4-2005, a smoking group consisting of 15 smoking experts is organized to carry out smoking on cigarettes using the filter stick of the invention and commercial traditional cigarettes as comparison samples, and the smoking result shows that the smoking experience effect of the cigarettes using the filter stick of the invention is basically the same as that of the comparison samples.
Claims (10)
1. The recycling method of the filter stick for the waste cigarettes is characterized by comprising the following steps of:
A. pretreatment of
Selecting a filter stick for waste cigarettes with complete appearance, removing impurities, and then removing forming paper wrapping the filter stick for cigarettes to obtain a pretreated filter stick for waste cigarettes;
B. filter stick softening
C, coating a plasticizer on the surface of the pretreated waste cigarette filter stick obtained in the step A, uniformly mixing, and standing for 2-4 hours at room temperature to obtain a softened waste cigarette filter stick;
C. filter stick shaping
And C, adding the softened filter sticks for the waste cigarettes obtained in the step B to cast aluminum heating plates with different shapes, heating and shaping, and solidifying to obtain the filter sticks with corresponding different shapes.
2. The method of claim 1, wherein in step B, the plasticizer is triacetin, triethylene glycol diacetate, or a mixture thereof.
3. The method for recycling filter rods according to claim 2, wherein in the step B, the mixture of the filter rods is prepared from triacetin and triethylene glycol diacetate according to a weight ratio of 1:0.1 to 10.0 percent of the mixture.
4. A filter rod recycling method according to any one of claims 1-3, characterized in that in step B, the plasticizer is added in an amount of 5-15% by weight of the pretreated waste cigarette filter rod.
5. The method of recycling filter rods according to claim 1, wherein in the step C, the heat setting temperature of the softened waste cigarette filter rods on the cast aluminum heating plates having different shapes is 80 to 120 ℃.
6. The method of claim 1, wherein in step C, the shape of the cast aluminum heating plate is duckbill, pentagram, cross or delta star.
7. The method of claim 1, wherein in step C, the cast aluminum heating plate is shaped such that one half thereof is cylindrical and the other half thereof is duckbill, five-star, cross or delta-star in the longitudinal direction of the cast aluminum heating plate.
8. The method for recycling filter rods according to claim 1, wherein in the step C, the heat-set waste cigarette filter rods are cured at room temperature for 22-26 hours.
9. Filter rods having different shapes obtained by the method for recycling filter rods according to any one of claims 1 to 8.
10. Use of a filter rod according to claim 9 having a different shape as a stand-alone filter rod or its use in a composite filter rod with other material filter rods.
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| CN202310282832.6A CN116349918A (en) | 2023-03-22 | 2023-03-22 | Recycling method of filter stick for waste cigarettes |
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| CN202310282832.6A CN116349918A (en) | 2023-03-22 | 2023-03-22 | Recycling method of filter stick for waste cigarettes |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3615997A (en) * | 1968-06-19 | 1971-10-26 | Reynolds Tobacco Co R | Method of making a reconstituted cigarette filter |
| CN103781374A (en) * | 2011-06-23 | 2014-05-07 | 英美烟草(投资)有限公司 | Filter material comprising polylactide fibres |
| CN103965507A (en) * | 2014-05-08 | 2014-08-06 | 云南瑞升烟草技术（集团）有限公司 | Recovery system and recovery process for waste cigarette diacetate fiber filter stick |
| CN106366339A (en) * | 2016-08-27 | 2017-02-01 | 湖北新阳特种纤维股份有限公司 | Method for recovering and utilizing cellulose diacetate waste filter rod in cigarette |
| CN109645564A (en) * | 2018-11-30 | 2019-04-19 | 湖北中烟工业有限责任公司 | A kind of filter stick for cigarettes composite elasticizer and its application |
| CN113815151A (en) * | 2021-09-14 | 2021-12-21 | 云南恒罡科技有限公司 | Method for recovering discarded filter rods of cigarettes |
-
2023
- 2023-03-22 CN CN202310282832.6A patent/CN116349918A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3615997A (en) * | 1968-06-19 | 1971-10-26 | Reynolds Tobacco Co R | Method of making a reconstituted cigarette filter |
| GB1260884A (en) * | 1968-06-19 | 1972-01-19 | Reynolds Tobacco Co R | Reconstituted cigarette filter and method of manufacture |
| CN103781374A (en) * | 2011-06-23 | 2014-05-07 | 英美烟草(投资)有限公司 | Filter material comprising polylactide fibres |
| CN103965507A (en) * | 2014-05-08 | 2014-08-06 | 云南瑞升烟草技术（集团）有限公司 | Recovery system and recovery process for waste cigarette diacetate fiber filter stick |
| CN106366339A (en) * | 2016-08-27 | 2017-02-01 | 湖北新阳特种纤维股份有限公司 | Method for recovering and utilizing cellulose diacetate waste filter rod in cigarette |
| CN109645564A (en) * | 2018-11-30 | 2019-04-19 | 湖北中烟工业有限责任公司 | A kind of filter stick for cigarettes composite elasticizer and its application |
| CN113815151A (en) * | 2021-09-14 | 2021-12-21 | 云南恒罡科技有限公司 | Method for recovering discarded filter rods of cigarettes |
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