CN114814094A - Experimental device and experimental method for visually simulating gas drilling and sealing - Google Patents
Experimental device and experimental method for visually simulating gas drilling and sealing Download PDFInfo
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Abstract
一种可视化模拟瓦斯钻孔封孔的实验装置及试验方法,其中装置包括:钻孔模拟系统,系统包括至少一侧面为透明材质的实验箱体,实验箱体内填充有形成模拟煤体的填料;注浆系统,包括注浆泵、注浆管、压力表和流量计,注浆泵通过注浆管连接至钻孔以将添加有荧光粉的封孔材料的浆液注入钻孔内,压力表和流量计设置在注浆管上以用于监测注浆时注浆管内的压力及流量;可视化观测系统,用于在封孔材料的浆液注入到钻孔内时通过图像记录该浆液在钻孔的孔周裂隙中的渗透扩散情况。本发明确定的封孔材料的最佳工艺参数及最佳配比的封孔材料应用于实际瓦斯抽采钻孔的注浆封孔中,使得封孔材料凝固之后与煤体形成一个整体,粘结性好,强度高。
An experimental device and a test method for visually simulating gas drilling and sealing, wherein the device comprises: a drilling simulation system, the system comprises an experimental box whose at least one side is made of transparent material, and the experimental box is filled with a filler for forming a simulated coal body; The grouting system includes a grouting pump, a grouting pipe, a pressure gauge and a flow meter. The grouting pump is connected to the borehole through the grouting pipe to inject the slurry of the sealing material added with phosphor powder into the borehole. The pressure gauge and the The flow meter is set on the grouting pipe to monitor the pressure and flow in the grouting pipe during grouting; the visual observation system is used to record the slurry in the borehole through images when the slurry of the sealing material is injected into the borehole. Osmosis diffusion in peripore fractures. The optimal process parameters of the sealing material and the sealing material with the optimal ratio determined by the invention are applied to the grouting and sealing of the actual gas drainage drilling hole, so that the sealing material forms a whole with the coal body after solidification, and sticks to the grouting hole. Good knot and high strength.
Description
技术领域technical field
本发明涉及封孔材料实验装置领域,具体涉及一种可视化模拟瓦斯钻孔封孔的实验装置及实验方法。The invention relates to the field of experimental devices for sealing materials, in particular to an experimental device and an experimental method for visually simulating gas drilling and sealing.
背景技术Background technique
我国高瓦斯、低透气性矿井居多,瓦斯治理问题较为严重。瓦斯是威胁煤矿安全生产的重要因素,而降低瓦斯含量最关键的措施是瓦斯抽采。目前我国大多数矿井瓦斯抽采效率不高,影响瓦斯抽采效率的一个关键因素是封孔方法。封孔方法是瓦斯抽采的一个重要环节,若封孔方法不合理将直接导致瓦斯抽采效率低。There are many mines with high gas and low permeability in my country, and the problem of gas control is more serious. Gas is an important factor that threatens the safe production of coal mines, and the most critical measure to reduce gas content is gas extraction. At present, the gas extraction efficiency of most mines in my country is not high, and a key factor affecting the gas extraction efficiency is the sealing method. The sealing method is an important part of gas drainage. If the sealing method is unreasonable, it will directly lead to low gas drainage efficiency.
目前我国封孔方法主要有注浆封孔,注浆封孔时无法肉眼观察到注浆的浆液在煤层中的流动及渗透情况,从而难以确定合适的注浆压力或流量,当注浆压力或流量不足时,注浆难以渗透进孔周裂隙(孔周裂隙是指孔的周围裂隙)而无法封堵钻孔周边裂隙,即对裂隙发育区域未起到封堵密闭的作用,从而导致空气通过漏气通道进入钻孔,造成瓦斯抽采效率低。At present, the main sealing methods in my country are grouting and sealing. When grouting and sealing, the flow and penetration of the grouting slurry in the coal seam cannot be observed with the naked eye, so it is difficult to determine the appropriate grouting pressure or flow. When the grouting pressure or When the flow rate is insufficient, it is difficult for grouting to penetrate into the cracks around the hole (the cracks around the hole refer to the cracks around the hole) and cannot seal the cracks around the borehole, that is, it does not play a role in sealing and sealing the area where the cracks develop, resulting in the passage of air. The leakage channel enters the borehole, resulting in low gas drainage efficiency.
由于不同材质的封孔材料的流动性、粘稠度、缓凝时间等均不相同,不同压力及流量下注入到钻孔中对孔周裂隙的渗透扩展也均不相同,现有技术判断钻孔注浆工艺参数(注浆的压力、流量及时间)一般依靠经验,即待钻孔注浆压力不变时则认为注浆浆液已满,不需要注浆,这种主观判断依据不严谨。对于如何确定其注入的最佳工艺参数,以及如何确定最佳的封孔材料,均缺乏实验性指导。因此,亟需一种能模拟井下钻孔环境的实验装置,通过实验方法确定最佳注浆工艺,以便根据实验数据来指导现场实际注浆施工。Since the fluidity, viscosity and retardation time of different materials of the sealing material are different, the penetration and expansion of the fissures around the hole are also different when injected into the borehole under different pressures and flow rates. Hole grouting process parameters (grouting pressure, flow rate and time) generally rely on experience, that is, when the grouting pressure of the hole remains unchanged, it is considered that the grouting slurry is full and grouting is not required. This subjective judgment is not rigorous. There is a lack of experimental guidance on how to determine the optimal process parameters for its implantation and how to determine the best sealing material. Therefore, there is an urgent need for an experimental device that can simulate the environment of downhole drilling, and the optimal grouting process can be determined through the experimental method, so as to guide the actual grouting construction on site according to the experimental data.
发明内容SUMMARY OF THE INVENTION
为了解决现有技术存在的上述技术问题,本发明提供了一种可视化模拟瓦斯钻孔封孔的实验装置及实验方法。In order to solve the above technical problems existing in the prior art, the present invention provides an experimental device and an experimental method for visually simulating gas drilling and sealing.
为实现上述目的,本发明提供了一种可视化模拟瓦斯钻孔封孔的实验装置,其包括:In order to achieve the above purpose, the present invention provides an experimental device for visual simulation of gas drilling and sealing, which includes:
钻孔模拟系统,用于模拟井下钻孔环境,所述钻孔模拟系统包括至少一侧面为透明材质的实验箱体,所述实验箱体内填充有形成模拟煤体的填料,所述模拟煤体的顶部压接有加载机构,所述填料中设有钻孔;A drilling simulation system for simulating a downhole drilling environment, the drilling simulation system includes an experimental box with at least one side made of transparent material, the experimental box is filled with a filler for forming a simulated coal body, and the simulated coal body is A loading mechanism is crimped on the top of the packing, and a drill hole is arranged in the packing;
注浆系统,用于模拟井下注浆过程,所述注浆系统包括注浆泵、注浆管、压力表和流量计,所述注浆泵通过所述注浆管连接至所述钻孔以用于将添加有荧光粉的封孔材料的浆液注入钻孔内,所述压力表和流量计设置在所述注浆管上以用于监测注浆时注浆管内的压力及流量;以及A grouting system for simulating a downhole grouting process, the grouting system includes a grouting pump, a grouting pipe, a pressure gauge and a flow meter, and the grouting pump is connected to the borehole through the grouting pipe to for injecting the slurry of the plugging material added with phosphor powder into the borehole, the pressure gauge and the flow meter are arranged on the grouting pipe to monitor the pressure and flow in the grouting pipe during grouting; and
可视化观测系统,用于在封孔材料的浆液注入到钻孔内时通过图像记录该浆液在钻孔的孔周裂隙中的渗透扩散情况,所述可视化观测系统包括相机,所述相机的焦点正对所述实验箱体上具有透明材质的一侧面。A visual observation system is used for recording the penetration and diffusion of the slurry in the peri-hole fissures of the drilled hole through images when the slurry of the plugging material is injected into the drilled hole, the visual observation system includes a camera, and the focus of the camera is A side surface with transparent material is provided on the experimental box body.
作为本发明的进一步优选技术方案,所述实验箱体内的模拟煤体包括自上至下依次设置的储气空间、岩层和煤层,所述加载机构通过钢板密封衔接于所述储气空间的顶部;所述钻孔模拟系统还包括温度控制装置,所述温度控制装置的加热器件连接到实验箱体,以用于将实验箱体内新铺设的模拟煤体烘干。As a further preferred technical solution of the present invention, the simulated coal body in the experimental box includes a gas storage space, a rock layer and a coal seam sequentially arranged from top to bottom, and the loading mechanism is sealed and connected to the top of the gas storage space through a steel plate ; The drilling simulation system further includes a temperature control device, and the heating device of the temperature control device is connected to the experimental box for drying the newly laid simulated coal in the experimental box.
作为本发明的进一步优选技术方案,所述实验箱体的长宽高分别为100cm、20cm、100cm,所述储气空间高度为20cm,所述岩层厚度为20cm,所述煤层厚度为60cm。As a further preferred technical solution of the present invention, the length, width and height of the experimental box are respectively 100cm, 20cm and 100cm, the height of the gas storage space is 20cm, the thickness of the rock layer is 20cm, and the thickness of the coal seam is 60cm.
作为本发明的进一步优选技术方案,所述岩层以河沙为骨料,以及水泥和水为胶结剂混合而成,河沙、水泥和水的重量比为10:2:1。As a further preferred technical solution of the present invention, the rock formation is formed by mixing river sand as aggregate and cement and water as binder, and the weight ratio of river sand, cement and water is 10:2:1.
作为本发明的进一步优选技术方案,所述煤层由煤粉、原煤和玉米粉混合而成,其中煤粉与原煤重量比为2:8,原煤的粒径为5mm。As a further preferred technical solution of the present invention, the coal seam is formed by mixing pulverized coal, raw coal and corn meal, wherein the weight ratio of pulverized coal to raw coal is 2:8, and the particle size of the raw coal is 5 mm.
作为本发明的进一步优选技术方案,所述钻孔的中心位置在煤层中心处,钻孔的孔径φ为113mm。As a further preferred technical solution of the present invention, the center of the borehole is at the center of the coal seam, and the hole diameter φ of the borehole is 113 mm.
作为本发明的进一步优选技术方案,所述实验箱体为内腔密闭的箱体,实验箱体的四周设有对其内腔进行密封的密封件,且注浆管与钻孔的开孔为密封衔接。As a further preferred technical solution of the present invention, the experimental box is a box with a closed inner cavity, the surrounding of the experimental box is provided with seals for sealing the inner cavity, and the openings of the grouting pipe and the drilling are as follows: Sealed connection.
作为本发明的进一步优选技术方案,所述相机为多个,多个相机以不同视角同时聚集于实验箱体上具有透明材质的一侧面,以采集不同角度的图像信息。As a further preferred technical solution of the present invention, there are multiple cameras, and the multiple cameras are simultaneously gathered on one side of the experimental box with transparent material from different viewing angles to collect image information from different angles.
作为本发明的进一步优选技术方案,所述可视化观测系统还包括辅助光源和计算机,所述辅助光源用于提供光源辅助相机进行图像采集,所述计算机与所述相机连接以获取采集的图像信息并进行分析处理。As a further preferred technical solution of the present invention, the visual observation system further includes an auxiliary light source and a computer, the auxiliary light source is used to provide a light source to assist the camera to perform image acquisition, and the computer is connected to the camera to acquire the acquired image information and Perform analytical processing.
根据本发明的另一方面,本发明还提供了一种采用上述任一项所述的可视化模拟瓦斯钻孔封孔的实验装置的实验方法,包括以下步骤:According to another aspect of the present invention, the present invention also provides an experimental method using the experimental device for visually simulating gas drilling and sealing according to any of the above, comprising the following steps:
1)在实验箱体内模拟井下钻孔环境填充填料以形成模拟煤体,并在模拟煤体的顶面设置加载机构,待模拟煤体干燥后,采用钻机在模拟煤体上钻取钻孔;1) Filling the simulated underground drilling environment in the experimental box to form the simulated coal body, and set a loading mechanism on the top surface of the simulated coal body. After the simulated coal body is dried, a drilling rig is used to drill holes on the simulated coal body;
2)将注浆泵通过注浆管密封连接至钻孔,注浆泵的输入端通过进浆管与提供封孔材料的浆液桶连接,注浆管上安装压力表和流量计;2) The grouting pump is sealed and connected to the borehole through the grouting pipe, the input end of the grouting pump is connected to the slurry barrel which provides the sealing material through the grouting pipe, and the pressure gauge and the flow meter are installed on the grouting pipe;
3)将相机聚焦于所述实验箱体上具有透明材质的一侧面;3) Focus the camera on the side of the experimental box with transparent material;
4)按照预设压力和预设流量启动注浆泵进行带压注浆,由相机采集注浆过程中浆液在模拟煤体中渗透的图像信息,当浆液流动到模拟煤体的内部裂隙尖端且无法流动时,确定为注浆完成,否则注浆继续;当注浆完成后,关闭注浆泵,并记录注浆所用时间;4) Start the grouting pump according to the preset pressure and preset flow to carry out grouting under pressure. The camera collects the image information of the infiltration of the slurry in the simulated coal body during the grouting process. When the slurry flows to the inner crack tip of the simulated coal body and When it cannot flow, it is determined that the grouting is completed, otherwise the grouting continues; when the grouting is completed, the grouting pump is turned off, and the time used for grouting is recorded;
5)以相同的封孔材料并通过改变注浆压力、流量和时间,或者以不同的封孔材料并通过相同的注浆压力、流量和时间分别重复重复步骤1)-4)进行实验,以采集注浆时浆液在模拟煤体中渗透的图像信息;5) Repeat steps 1)-4) with the same sealing material and by changing the grouting pressure, flow rate and time, or with different sealing materials and with the same grouting pressure, flow rate and time, respectively. Collect image information of the infiltration of slurry in the simulated coal body during grouting;
6)对采集的图像信息进行综合比对分析,以得到封孔材料在注浆时的最佳压力、流量和时间,或者得到最佳的封孔材料的配料及配比。6) Comprehensively compare and analyze the collected image information to obtain the optimal pressure, flow rate and time of the sealing material during grouting, or obtain the best ingredients and proportions of the sealing material.
本发明的可视化模拟瓦斯钻孔封孔的实验装置及实验方法,通过采用上述技术方案,可以达到如下有益效果:The experimental device and the experimental method for visually simulating gas drilling and sealing of the present invention can achieve the following beneficial effects by adopting the above technical scheme:
1)本发明的实验装置在搭建的钻孔模拟系统中对模拟煤体的钻孔进行带压注浆,通过可视化观测系统可以准确判断浆液流动到钻孔孔周裂隙尖端所用的时间,从而确定最佳注浆工艺参数,如注浆时间、压力及流量;1) The experimental device of the present invention performs pressure grouting on the borehole of the simulated coal body in the built borehole simulation system, and the visual observation system can accurately judge the time it takes for the slurry to flow to the tip of the fissure around the borehole, so as to determine Optimal grouting process parameters, such as grouting time, pressure and flow;
2)本发明的实验方法可应用于对封孔材料的封孔质量进行评估,以获取最佳的原料配比,例如封孔材料中的催化剂占比影响其材料的凝固时间,通过可视化观察注浆时注浆的渗透变化,并通过改变封孔材料的原料配比反复进行实验,即可确定催化剂的最佳占比。2) The experimental method of the present invention can be applied to evaluate the sealing quality of the sealing material to obtain the best ratio of raw materials. For example, the proportion of catalyst in the sealing material affects the solidification time of the material. The best proportion of catalyst can be determined by changing the penetration change of grouting during grouting, and by changing the raw material ratio of the sealing material to conduct repeated experiments.
3)通过本发明的实验装置及实验方法所得到的封孔材料的最佳工艺参数及最佳配比的封孔材料应用于实际瓦斯抽采钻孔的注浆封孔中,使得封孔材料凝固之后与煤体形成一个整体,粘结性好,强度高,而且封孔材料在流动到裂隙尖端之后可封堵裂隙,凝固之后不会发生收缩,可以实现裂隙修复,从而提高了瓦斯抽采钻孔的封孔质量,进而提高了瓦斯抽采效率。3) The optimal process parameters of the sealing material obtained by the experimental device and the experimental method of the present invention and the sealing material of the optimal proportion are applied to the grouting sealing of the actual gas drainage drilling hole, so that the sealing material After solidification, it forms a whole with the coal body, with good cohesion and high strength, and the sealing material can seal the crack after flowing to the tip of the crack. After solidification, it will not shrink, and the crack can be repaired, thereby improving gas drainage. The sealing quality of the boreholes improves the gas drainage efficiency.
附图说明Description of drawings
下面结合附图和具体实施方式对本发明作进一步详细的说明。The present invention will be described in further detail below with reference to the accompanying drawings and specific embodiments.
图1为本发明可视化模拟瓦斯钻孔封孔的实验装置提供的一实例的结构示意图;1 is a schematic structural diagram of an example provided by an experimental device for visually simulating gas drilling and sealing according to the present invention;
图2为本发明实验箱体提供的一实例的结构示意图;2 is a schematic structural diagram of an example provided by the experimental box of the present invention;
图3为本发明可视化观测系统的装配示意图;Fig. 3 is the assembly schematic diagram of the visual observation system of the present invention;
图4为调整封孔材料中催化剂异辛酸钾的配比后封孔材料凝固时间图。4 is a diagram showing the solidification time of the sealing material after adjusting the proportion of the catalyst potassium isooctanoate in the sealing material.
图中:1、计算机,2、相机,3、压力表,4、流量计,5、注浆泵,6、注浆管,7、实验箱体,8、温度控制装置,9、钻孔,10、辅助光源。In the picture: 1. Computer, 2. Camera, 3. Pressure gauge, 4. Flowmeter, 5. Grouting pump, 6. Grouting pipe, 7. Experimental box, 8. Temperature control device, 9. Drilling hole, 10. Auxiliary light source.
本发明目的实现、功能特点及优点将结合实施例,参照附图做进一步说明。The object realization, functional features and advantages of the present invention will be further described with reference to the accompanying drawings in conjunction with the embodiments.
具体实施方式Detailed ways
下面将结合附图以及具体实施方式,对本发明做进一步描述。较佳实施例中所引用的如“上”、“下”、“左”、“右”、“中间”及“一”等用语,仅为便于叙述的明了,而非用以限定本发明可实施的范围,其相对关系的改变或调整,在无实质变更技术内容下,当亦视为本发明可实施的范畴。The present invention will be further described below with reference to the accompanying drawings and specific embodiments. Terms such as "up", "down", "left", "right", "middle" and "one" quoted in the preferred embodiment are only for the convenience of description and clarity, and are not intended to limit the scope of the present invention. The scope of implementation, the change or adjustment of the relative relationship, and the technical content without substantial change, shall also be regarded as the scope of implementation of the present invention.
如图1-3所示,本发明提供了一种可视化模拟瓦斯钻孔封孔的实验装置,包括:As shown in Figures 1-3, the present invention provides an experimental device for visually simulating gas drilling and sealing, including:
钻孔模拟系统,用于模拟井下钻孔9环境,所述钻孔模拟系统包括至少一侧面为透明材质的实验箱体7,所述实验箱体7内填充有形成模拟煤体的填料,所述模拟煤体的顶部压接有加载机构以模拟煤体在煤矿井下应力状态,所述填料中设有模拟瓦斯抽采钻孔9的钻孔9,侧面为透明材质的实验箱体7便于注浆时观察到浆液在模拟煤体中孔隙中的渗透情况,所述实验箱体7内的模拟煤体包括自上至下依次设置的储气空间、岩层和煤层,所述加载机构通过钢板密封衔接于所述储气空间的顶部;所述钻孔模拟系统还包括温度控制装置8,所述温度控制装置8的加热器件连接到实验箱体7,以用于将实验箱体7内新铺设的模拟煤体烘干;The drilling simulation system is used to simulate the environment of the
注浆系统,用于模拟井下注浆过程,所述注浆系统包括注浆泵5、注浆管6、压力表3和流量计4,所述注浆泵5通过所述注浆管6连接至所述钻孔9以用于将添加有荧光粉的封孔材料的浆液注入钻孔9内,所述压力表3和流量计4设置在所述注浆管6上以用于监测注浆时注浆管6内的压力及流量,通过添加荧光粉,便于观察封孔材料在煤体中的流动情况,荧光粉为黄绿色,且为油性,不与高分子材料(封孔材料)互相反应;A grouting system for simulating a downhole grouting process, the grouting system includes a
可视化观测系统,用于在封孔材料的浆液注入到钻孔9内时通过图像记录该浆液在钻孔9的孔周裂隙中的渗透扩散情况,所述可视化观测系统包括相机2,所述相机2的焦点正对所述实验箱体7上具有透明材质的一侧面,所述可视化观测系统还包括辅助光源10和计算机1,所述辅助光源10用于提供光源辅助相机2进行图像采集,辅助光源10从两侧照入,使得采集的图像信息尽量避免阴影和反光,所述计算机1与所述相机2连接以获取采集的图像信息并进行分析处理。A visual observation system for recording the penetration and diffusion of the slurry in the peri-hole fissures of the drilled
在一具体实施例中,所述实验箱体7的长宽高分别为100cm、20cm、100cm,所述储气空间高度为20cm,所述岩层厚度为20cm,所述煤层厚度为60cm,所述钻孔9的中心位置在煤层中心处,钻孔9的孔径φ为113mm。所述岩层以河沙为骨料,以及水泥和水为胶结剂混合而成,河沙、水泥和水的重量比为10:2:1;所述煤层由煤粉、原煤和玉米粉混合而成,其中煤粉与原煤重量比为2:8,原煤的粒径为5mm,其中玉米粉的添加可保证煤层具有良好的透气性。In a specific embodiment, the length, width and height of the
优选地,所述实验箱体7为内腔密闭的箱体,实验箱体7的四周设有对其内腔进行密封的密封件,且注浆管6与钻孔9的开孔为密封衔接。Preferably, the
进一步优选地,所述相机2为多个,多个相机2以不同视角同时聚集于实验箱体7上具有透明材质的一侧面,以采集不同角度的图像信息,获得更清晰,更直观的动态图像,便于后续分析。Further preferably, there are multiple cameras 2, and multiple cameras 2 are simultaneously gathered on one side of the
本发明还提供了一种采用可视化模拟瓦斯钻孔封孔的实验装置进行的实验方法,包括以下步骤:The present invention also provides an experimental method using an experimental device for visually simulating gas drilling and sealing, comprising the following steps:
1)搭建钻孔模拟系统:在实验箱体7内模拟井下钻孔9环境填充填料以形成模拟煤体,并在模拟煤体的顶面设置加载机构,待模拟煤体干燥后,采用钻机在模拟煤体上钻取钻孔9;1) Build a drilling simulation system: Fill the simulated
2)注浆系统连接:将注浆泵5通过注浆管6密封连接至钻孔9,注浆泵5的输入端通过进浆管与提供封孔材料的浆液桶连接,注浆管6上安装压力表3和流量计4;2) Connection of the grouting system: the
3)可视化观测系统组装:将相机2聚焦于所述实验箱体7上具有透明材质的一侧面;3) Visual observation system assembly: focus the camera 2 on the side of the
4)按照预设压力和预设流量启动注浆泵5进行带压注浆,由相机2采集注浆过程中浆液在模拟煤体中渗透的图像信息,当浆液流动到模拟煤体的内部裂隙尖端且无法流动时,确定为注浆完成,否则注浆继续;当注浆完成后,关闭注浆泵5,并记录注浆所用时间;4) Start the
5)以相同的封孔材料并通过改变注浆压力、流量和时间,或者以不同的封孔材料并通过相同的注浆压力、流量和时间分别重复重复步骤1)-4)进行实验,以采集注浆时浆液在模拟煤体中渗透的图像信息,此处的不同的封孔材料是指根据配料的不同或配比的不同而不同;5) Repeat steps 1)-4) with the same sealing material and by changing the grouting pressure, flow rate and time, or with different sealing materials and with the same grouting pressure, flow rate and time, respectively. Collect the image information of the infiltration of the slurry in the simulated coal body during grouting. The different sealing materials here refer to different ingredients or different proportions;
6)对采集的图像信息进行综合比对分析,以得到封孔材料在注浆时的最佳压力、流量和时间,或者得到最佳的封孔材料的配料及配比。6) Comprehensively compare and analyze the collected image information to obtain the optimal pressure, flow rate and time of the sealing material during grouting, or obtain the best ingredients and proportions of the sealing material.
本实施例中,所采用的封孔材料由以下配料及配比(如表1)混合配制而成:聚醚305,聚醚204,阻燃剂TCPP,稳定剂硅油,催化剂异辛酸钾,二苯甲烷二异氰酸酯(MDI)。配制步骤为:首先将聚醚305、聚醚204、阻燃剂TCPP、稳定剂硅油、催化剂异辛酸钾按比例进行高精度计量混合以得到混合料;然后在混合料中加入二苯甲烷二异氰酸酯,得到封孔材料的浆液。In this embodiment, the sealing material used is prepared by mixing the following ingredients and proportions (as shown in Table 1): polyether 305, polyether 204, flame retardant TCPP, stabilizer silicone oil, catalyst potassium isooctanoate, two Benzylmethane diisocyanate (MDI). The preparation steps are as follows: first, polyether 305, polyether 204, flame retardant TCPP, stabilizer silicone oil, and catalyst potassium isooctanoate are mixed with high precision in proportion to obtain a mixture; then diphenylmethane diisocyanate is added to the mixture , to obtain the slurry of the sealing material.
表1.封孔材料的原料配比Table 1. Raw material ratio of sealing material
以不同的封孔材料(催化剂异辛酸钾含量不同)并通过相同的注浆压力、流量和时间分别重复重复步骤1)-4)进行实验,可通过调节催化剂在材料中的占比来调节材料的凝固时间,通过调整材料的凝固时间进行钻孔9封孔,从而对封孔材料在煤岩体中的扩散时间进行调控。调整配比后封孔材料的凝固时间如图4所示。封孔材料的凝固时间可根据钻孔9孔周裂隙长度及范围相应进行材料的凝固时间的调节,通过多组对比实验,以确定最佳的催化剂的含量,当催化剂异辛酸钾含量为0.15%时为最优。Repeat steps 1)-4) with different sealing materials (with different content of potassium isooctanoate as catalyst) and through the same grouting pressure, flow rate and time, respectively. The material can be adjusted by adjusting the proportion of catalyst in the material. By adjusting the solidification time of the material, the
在另一具体实施中,考虑到不同注浆压力和注浆时间,本实施例中分别进行以下三组测试(每重复上述步骤1)-4)为一组),各组的注浆泵5设置的注浆压力为0.5、1、1.5MPa,注浆时间为30、60、90s,而且做完一组实验后及时清洗管道,以免残留液体凝结堵塞管道。最后,将采集的图像信息进行对比,以确定最佳压力、流量和时间参数。In another specific implementation, considering different grouting pressures and grouting times, in this embodiment, the following three sets of tests are carried out respectively (each repeating the above steps 1)-4) is a set), the grouting pumps of each group are 5 The set grouting pressure is 0.5, 1, 1.5MPa, and the grouting time is 30, 60, 90s, and the pipeline is cleaned in time after a set of experiments is completed to prevent the residual liquid from condensing and blocking the pipeline. Finally, the acquired image information is compared to determine optimal pressure, flow and time parameters.
虽然以上描述了本发明的具体实施方式,但是本领域熟练技术人员应当理解,这些仅是举例说明,可以对本实施方式做出多种变更或修改,而不背离本发明的原理和实质,本发明的保护范围仅由所附权利要求书限定。Although the specific embodiments of the present invention are described above, those skilled in the art should understand that these are only examples, and various changes or modifications can be made to the embodiments without departing from the principle and essence of the present invention. The scope of protection is limited only by the appended claims.
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