CN114721087B - 一种三包层铒镱共掺光纤及其制备方法与应用 - Google Patents
一种三包层铒镱共掺光纤及其制备方法与应用 Download PDFInfo
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- CN114721087B CN114721087B CN202210642201.6A CN202210642201A CN114721087B CN 114721087 B CN114721087 B CN 114721087B CN 202210642201 A CN202210642201 A CN 202210642201A CN 114721087 B CN114721087 B CN 114721087B
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- doped
- ytterbium
- layer
- cladding
- erbium
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- KWMNWMQPPKKDII-UHFFFAOYSA-N erbium ytterbium Chemical compound [Er].[Yb] KWMNWMQPPKKDII-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 239000013307 optical fiber Substances 0.000 title claims description 41
- 238000002360 preparation method Methods 0.000 title abstract description 8
- 238000005253 cladding Methods 0.000 claims abstract description 125
- 239000000835 fiber Substances 0.000 claims abstract description 101
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical group [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims abstract description 79
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 59
- 239000010453 quartz Substances 0.000 claims abstract description 49
- 239000011248 coating agent Substances 0.000 claims abstract description 35
- 238000000576 coating method Methods 0.000 claims abstract description 35
- 229910052691 Erbium Inorganic materials 0.000 claims abstract description 12
- UYAHIZSMUZPPFV-UHFFFAOYSA-N erbium Chemical compound [Er] UYAHIZSMUZPPFV-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract description 10
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 10
- 239000011574 phosphorus Substances 0.000 claims abstract description 10
- NAWDYIZEMPQZHO-UHFFFAOYSA-N ytterbium Chemical compound [Yb] NAWDYIZEMPQZHO-UHFFFAOYSA-N 0.000 claims abstract description 9
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000009826 distribution Methods 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims description 37
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 claims description 22
- 230000004888 barrier function Effects 0.000 claims description 20
- 238000000151 deposition Methods 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 11
- 239000000758 substrate Substances 0.000 claims description 10
- 230000008021 deposition Effects 0.000 claims description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 7
- 238000002791 soaking Methods 0.000 claims description 7
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 claims description 5
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 230000003247 decreasing effect Effects 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 238000005498 polishing Methods 0.000 claims description 5
- 239000005049 silicon tetrachloride Substances 0.000 claims description 5
- IEXRMSFAVATTJX-UHFFFAOYSA-N tetrachlorogermane Chemical compound Cl[Ge](Cl)(Cl)Cl IEXRMSFAVATTJX-UHFFFAOYSA-N 0.000 claims description 5
- 238000004017 vitrification Methods 0.000 claims description 5
- 238000005229 chemical vapour deposition Methods 0.000 claims description 4
- 238000005245 sintering Methods 0.000 claims description 4
- 229910001873 dinitrogen Inorganic materials 0.000 claims 1
- 235000012239 silicon dioxide Nutrition 0.000 description 42
- 229910018503 SF6 Inorganic materials 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- SFZCNBIFKDRMGX-UHFFFAOYSA-N sulfur hexafluoride Chemical compound FS(F)(F)(F)(F)F SFZCNBIFKDRMGX-UHFFFAOYSA-N 0.000 description 7
- 229960000909 sulfur hexafluoride Drugs 0.000 description 7
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 5
- -1 hydroxide ions Chemical class 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000005086 pumping Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 239000004925 Acrylic resin Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- YWEUIGNSBFLMFL-UHFFFAOYSA-N diphosphonate Chemical compound O=P(=O)OP(=O)=O YWEUIGNSBFLMFL-UHFFFAOYSA-N 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- DLYUQMMRRRQYAE-UHFFFAOYSA-N phosphorus pentoxide Inorganic materials O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229910003902 SiCl 4 Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- QPJSUIGXIBEQAC-UHFFFAOYSA-N n-(2,4-dichloro-5-propan-2-yloxyphenyl)acetamide Chemical compound CC(C)OC1=CC(NC(C)=O)=C(Cl)C=C1Cl QPJSUIGXIBEQAC-UHFFFAOYSA-N 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/02—Optical fibres with cladding with or without a coating
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/018—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by glass deposition on a glass substrate, e.g. by inside-, modified-, plasma-, or plasma modified- chemical vapour deposition [ICVD, MCVD, PCVD, PMCVD], i.e. by thin layer coating on the inside or outside of a glass tube or on a glass rod
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/018—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by glass deposition on a glass substrate, e.g. by inside-, modified-, plasma-, or plasma modified- chemical vapour deposition [ICVD, MCVD, PCVD, PMCVD], i.e. by thin layer coating on the inside or outside of a glass tube or on a glass rod
- C03B37/01853—Thermal after-treatment of preforms, e.g. dehydrating, consolidating, sintering
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/018—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by glass deposition on a glass substrate, e.g. by inside-, modified-, plasma-, or plasma modified- chemical vapour deposition [ICVD, MCVD, PCVD, PMCVD], i.e. by thin layer coating on the inside or outside of a glass tube or on a glass rod
- C03B37/01861—Means for changing or stabilising the diameter or form of tubes or rods
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/02—Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
- C03B37/025—Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor from reheated softened tubes, rods, fibres or filaments, e.g. drawing fibres from preforms
- C03B37/027—Fibres composed of different sorts of glass, e.g. glass optical fibres
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/104—Coating to obtain optical fibres
- C03C25/105—Organic claddings
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/104—Coating to obtain optical fibres
- C03C25/106—Single coatings
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/24—Coatings containing organic materials
- C03C25/26—Macromolecular compounds or prepolymers
- C03C25/28—Macromolecular compounds or prepolymers obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C03C25/285—Acrylic resins
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/02—Optical fibres with cladding with or without a coating
- G02B6/02395—Glass optical fibre with a protective coating, e.g. two layer polymer coating deposited directly on a silica cladding surface during fibre manufacture
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/02—Optical fibres with cladding with or without a coating
- G02B6/036—Optical fibres with cladding with or without a coating core or cladding comprising multiple layers
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2203/00—Fibre product details, e.g. structure, shape
- C03B2203/32—Eccentric core or cladding
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Physics & Mathematics (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Thermal Sciences (AREA)
- Lasers (AREA)
- Glass Compositions (AREA)
Abstract
Description
Claims (9)
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CN202210642201.6A CN114721087B (zh) | 2022-06-08 | 2022-06-08 | 一种三包层铒镱共掺光纤及其制备方法与应用 |
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CN202210642201.6A CN114721087B (zh) | 2022-06-08 | 2022-06-08 | 一种三包层铒镱共掺光纤及其制备方法与应用 |
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CN114721087B true CN114721087B (zh) | 2022-10-25 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115304266B (zh) * | 2022-10-11 | 2023-01-20 | 武汉长进激光技术有限公司 | 一种抗辐照保偏铒镱共掺光纤及其制备方法与应用 |
CN115818950B (zh) * | 2022-12-09 | 2024-05-03 | 长飞光纤光缆股份有限公司 | 多模铒镱共掺光纤、芯棒及其制备方法、应用 |
CN117849938B (zh) * | 2023-12-25 | 2025-02-11 | 武汉长进光子技术股份有限公司 | 一种扩展l波段放大带宽的增益光纤及其制备方法 |
CN118405842B (zh) * | 2024-06-04 | 2025-03-04 | 武汉长进光子技术股份有限公司 | 一种掺铋光纤及其制备方法 |
CN119371098A (zh) * | 2024-12-27 | 2025-01-28 | 聚芯光子科技(台州)有限责任公司 | Er-Yb共掺高P石英玻璃及其制备方法 |
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JP2002033536A (ja) * | 2000-07-14 | 2002-01-31 | Furukawa Electric Co Ltd:The | 光増幅用光ファイバ |
US7570856B1 (en) * | 2005-12-07 | 2009-08-04 | Lockheed Martin Corporation | Apparatus and method for an erbium-doped fiber for high peak-power applications |
CN102621628A (zh) * | 2012-03-22 | 2012-08-01 | 华中科技大学 | 一种环形掺杂层光纤、其制备方法及包含该光纤的激光器 |
CN104556674A (zh) * | 2015-02-03 | 2015-04-29 | 中国电子科技集团公司第四十六研究所 | 一种稀土离子共掺光纤预制棒的制备方法 |
CN109031516A (zh) * | 2018-07-11 | 2018-12-18 | 烽火通信科技股份有限公司 | 一种大模场双包层掺镱光纤 |
CN111574046A (zh) * | 2020-05-29 | 2020-08-25 | 中国电子科技集团公司第四十六研究所 | 一种制备掺稀土光纤的气相-液相复合掺杂方法 |
CN112596148A (zh) * | 2020-11-24 | 2021-04-02 | 法尔胜泓昇集团有限公司 | 一种用于高功率大模场掺镱有源光纤及其制备方法 |
CN113501669A (zh) * | 2021-08-11 | 2021-10-15 | 华南理工大学 | 铒镱共掺氟硫磷酸盐玻璃单模光纤及其制备方法和应用 |
CN113820783A (zh) * | 2021-08-12 | 2021-12-21 | 江苏法尔胜光电科技有限公司 | 一种高功率用光敏型铒镱共掺光纤及其制备方法 |
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US6816514B2 (en) * | 2002-01-24 | 2004-11-09 | Np Photonics, Inc. | Rare-earth doped phosphate-glass single-mode fiber lasers |
US7050686B2 (en) * | 2004-08-05 | 2006-05-23 | Nufern | Fiber optic article with inner region |
JPWO2008133242A1 (ja) * | 2007-04-25 | 2010-07-29 | 株式会社フジクラ | 希土類添加コア光ファイバ |
FR2962555B1 (fr) * | 2010-07-09 | 2013-05-17 | Ixfiber | Fibre optique dopee terre rare resistante aux radiations et procede de durcissement aux radiations d'une fibre optique dopee terre rare |
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JP2002033536A (ja) * | 2000-07-14 | 2002-01-31 | Furukawa Electric Co Ltd:The | 光増幅用光ファイバ |
US7570856B1 (en) * | 2005-12-07 | 2009-08-04 | Lockheed Martin Corporation | Apparatus and method for an erbium-doped fiber for high peak-power applications |
CN102621628A (zh) * | 2012-03-22 | 2012-08-01 | 华中科技大学 | 一种环形掺杂层光纤、其制备方法及包含该光纤的激光器 |
CN104556674A (zh) * | 2015-02-03 | 2015-04-29 | 中国电子科技集团公司第四十六研究所 | 一种稀土离子共掺光纤预制棒的制备方法 |
CN109031516A (zh) * | 2018-07-11 | 2018-12-18 | 烽火通信科技股份有限公司 | 一种大模场双包层掺镱光纤 |
CN111574046A (zh) * | 2020-05-29 | 2020-08-25 | 中国电子科技集团公司第四十六研究所 | 一种制备掺稀土光纤的气相-液相复合掺杂方法 |
CN112596148A (zh) * | 2020-11-24 | 2021-04-02 | 法尔胜泓昇集团有限公司 | 一种用于高功率大模场掺镱有源光纤及其制备方法 |
CN113501669A (zh) * | 2021-08-11 | 2021-10-15 | 华南理工大学 | 铒镱共掺氟硫磷酸盐玻璃单模光纤及其制备方法和应用 |
CN113820783A (zh) * | 2021-08-12 | 2021-12-21 | 江苏法尔胜光电科技有限公司 | 一种高功率用光敏型铒镱共掺光纤及其制备方法 |
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