CN114521668A - 一种含有乳化剂的尼古丁口含烟制品及其制备方法 - Google Patents
一种含有乳化剂的尼古丁口含烟制品及其制备方法 Download PDFInfo
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
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- Agronomy & Crop Science (AREA)
- Botany (AREA)
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- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
本发明涉及一种含有乳化剂的尼古丁口含烟制品及制备方法，属于无烟气烟草领域。由以下组分及重量比组成：40‑80份填充剂、0‑10份水、10‑40份香味物质、10‑20份保润剂、1‑10份尼古丁物质及0.5‑3份乳化剂。通过乳化剂的加入，提高香味物质的稳定性，降低香味物质在储存过程中的衰减，满足香味物质的口感要求。
Description
技术领域
本发明属于无烟气烟草领域，具体涉及一种含乳化剂的尼古丁口含烟制品及其制备方法。
背景技术
在不含烟草的尼古丁口含制品中，由于填充剂不含烟草成分，所采用的成分均不具有特征香味，因此并不能提供烟草或者其他天然提取物、精油、香精等带来的味觉感受，仅作为载体以负载香味物质、保润剂及尼古丁来赋予尼古丁口含制品，而香味物质通过外加的形式，并不能长时间被填充剂所保留，即使密封在口含烟专用的盒子中，保存在冷藏的条件下，香味的损失依然比较明显，尤其是一些高挥发性的香味物质，如薄荷醇，柠檬烯等。通过在含有高挥发性香味物质的尼古丁口含制品中，添加水包油型乳化剂，如单/双甘油脂肪酸酯，植物三甘油脂肪酸酯，聚甘油酯等，一定程度上能够减缓香味物质在储存过程中的损失，增加尼古丁口含制品的香味物质的稳定性，提高产品的感官品质。
发明内容
本发明为克服现有技术不足，提供一种含有乳化剂的尼古丁口含制品及制备方法，解决目前技术现有不足：
为实现上述目的及其他相关目的，本发明提供一种含有乳化剂的尼古丁口含烟制品，包括填充剂、水、香味物质、保润剂、尼古丁物质、乳化剂。
优选的，所述的填充剂包括玉米淀粉、木薯淀粉、马铃薯淀粉、红薯淀粉、预糊化淀粉、豌豆淀粉、麦芽糊精、微晶纤维素、羧甲基纤维素、玉米纤维、大豆纤维、豌豆纤维、小麦纤维、燕麦纤维、荞麦纤维、木糖醇、赤藓糖醇、异麦芽酮糖醇、甘露醇、麦芽糖醇、山梨糖醇、碳酸钠、碳酸钾、碳酸氢钠、碳酸氢钾、氢氧化钠、氢氧化钾、氯化钠。再优选，玉米淀粉、微晶纤维素、羧甲基纤维素、玉米纤维、燕麦纤维、木糖醇、碳酸钠、氯化钠中的一种或两种以上的组合。
进一步地，所述的填充剂为白色颗粒；且所述的白色颗粒粒径在0.35-1.00mm之间。
优选的，所述的香味物质包括植物提取物、天然精油、合成香精、香味物质单体中的一种或两种以上的组合。
优选的，所述的保润剂包括丙二醇、丙三醇中的一种或两种的组合。
优选的，尼古丁物质包括尼古丁单体、尼古丁尼古丁苯甲酸盐、尼古丁苹果酸盐、尼古丁酒石酸盐、尼古丁水杨酸盐、尼古丁离子交换树脂。再优选尼古丁苹果酸盐、尼古丁酒石酸盐中的一种或两种以上的组合。
优选的，所述的乳化剂包括单/双甘油酯、聚甘油酯、可可油、蓖麻油、棕榈油、葵花籽油、油菜花籽油、玉米胚芽油、小麦胚芽油。再优选，单/双甘油酯，聚甘油酯，棕榈油中的一种或两种以上的组合。
此外，本发明一种含乳化剂的尼古丁口含烟制品的制备方法，其成分重量比及制备方法如下：1)将0-10份水加入到填充剂中，混合10-30min，静置吸收1-5h；2)将10-40份香味物质、10-20份保润剂、1-10份尼古丁物质搅拌混合5-30min，再加入0.5-3份乳化剂，于磁力搅拌仪上搅拌1-5h；3)将2)所得的液体加入1)中，在搅拌机中搅拌20-60min，静置12-24h，得到含乳化剂的尼古丁口含制品。
本发明涉及一种含有乳化剂的尼古丁口含制品及制备方法，属于无烟气烟草领域。由以下组分及重量比组成：40-80份填充剂、0-10份水、10-40份香味物质、10-20份保润剂、1-10份尼古丁物质及0.5-3份乳化剂。通过乳化剂的加入，提高香味物质的稳定性，降低香味物质在储存过程中的衰减，满足香味物质的口感要求。
附图说明
图1A样品1-4通过溶液萃取方式，GC-MS测定薄荷醇的含量；
图1B样品5-8通过溶液萃取方式，GC-MS测定薄荷醇的含量；
图2A样品1-4通过溶液萃取方式，GC-MS测定茴香脑的含量；
图2B样品5-8通过溶液萃取方式，GC-MS测定茴香脑的含量。
具体实施方式
实施例1
本实例含乳化剂的尼古丁口含制品制备方法包括以下步骤，各组分重量比见表1：
1)将丙二醇、薄荷香精、薄荷精油、尼古丁苯甲酸盐搅拌混合5min；
2)将乳化剂加入1)，于磁力搅拌器上搅拌20min，形成均匀的乳浊液
3)再将2)加入颗粒填充剂中，于混合机中混合40min，密封静置12h，制得含乳化剂的尼古丁口含制品颗粒。
表1
实施例2
本实例含乳化剂的尼古丁口含制品制备方法包括以下步骤，各组分重量比见表2：
1)将水加入颗粒填充剂中，搅拌均匀，静止吸收1h
2)将丙二醇、薄荷香精、薄荷精油、尼古丁苯甲酸盐搅拌混合5min；
3)将乳化剂加入2)，于磁力搅拌器上搅拌20min，形成均匀的乳浊液
4)再将3)加入1)中的颗粒填充剂，于混合机中混合40min，密封静置12h，制得含乳化剂的尼古丁口含制品颗粒。
表2
实施例3
本实例的挥发性香味物质的稳定性实验包括以下步骤：
1)称量0.5g样品于口含烟无纺布袋子中，再放入包装盒密封，于室温条件下保存。
2)测定储存第0周、2周、4周、6周时4个样品中的成分含量。薄荷醇，茴香脑作为香味物质稳定性的测定指标。
3)样品通过溶液萃取方式，GC-MS测定薄荷醇和茴香脑的含量，结果见图1A，1B，2A，2B。
由结果可见：不论无水分添加和添加水分的情况，乳化剂单/双甘油酯和聚甘油酯对挥发性香味成分薄荷醇和茴香脑在尼古丁口含制品的的稳定性，具有一定的作用。对于薄荷醇的保留效果，聚甘油酯较单双甘油酯好一些，而单/双甘油酯对茴香脑的保留效果优于聚甘油酯。除聚甘油酯在无水添加的尼古丁口含制品中，1.0％的添加量较0.5％的添加量表现较好外，两种乳化剂的添加量，0.5％和1.0％对于薄荷醇和茴香脑的稳定性影响差异并不太大。
以上所述仅为本发明的较佳实施例而已，是结合具体的优选实施方式对本发明所作的进一步详细说明，不能认定本发明的具体实施只局限于这些说明。凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等，均应包含在本发明的保护范围之内。
Claims (10)
1.一种含有乳化剂的尼古丁口含烟制品，包括填充剂、水、香味物质、保润剂、尼古丁物质、乳化剂。
2.根据权利要求1所述尼古丁口含烟制品，其特征在于，包括40-80份填充剂、0-10份水、10-40份香味物质、10-20份保润剂、1-10份尼古丁物质及0.5-3份乳化剂。
3.权利要求1或2所述尼古丁口含烟制品，其特征在于，所述的填充剂为白色颗粒。
4.权利要求3所述尼古丁口含烟制品，其特征在于，所述的白色颗粒粒径在0.35-1.00mm之间。
5.权利要求1或2所述尼古丁口含烟制品，其特征在于，所述的填充剂包括玉米淀粉、木薯淀粉、马铃薯淀粉、红薯淀粉、预糊化淀粉、豌豆淀粉、麦芽糊精、微晶纤维素、羧甲基纤维素、玉米纤维、大豆纤维、豌豆纤维、小麦纤维、燕麦纤维、荞麦纤维、木糖醇、赤藓糖醇、异麦芽酮糖醇、甘露醇、麦芽糖醇、山梨糖醇、碳酸钠、碳酸钾、碳酸氢钠、碳酸氢钾、氢氧化钠、氢氧化钾、氯化钠中的一种或两种以上组合。
6.权利要求1或2所述尼古丁口含烟制品，其特征在于，所述的香味物质包括植物提取物、天然精油、合成香精、香味物质单体中的一种或两种以上的组合。
7.权利要求1或2所述尼古丁口含烟制品，其特征在于，所述的保润剂包括丙二醇或丙三醇中的一种或两种组合。
8.权利要求1或2所述尼古丁口含烟制品，其特征在于，所述的尼古丁物质包括尼古丁单体、尼古丁苯甲酸盐、尼古丁苹果酸盐、尼古丁酒石酸盐、尼古丁水杨酸盐、尼古丁离子交换树脂中的一种或两种以上的组合。
9.权利要求1或2所述尼古丁口含烟制品，其特征在于，所述的乳化剂包括单/双甘油酯、聚甘油酯、可可油、蓖麻油、棕榈油、葵花籽油、油菜花籽油、玉米胚芽油、小麦胚芽油中的一种或两种以上的组合。
10.一种含乳化剂的尼古丁口含烟制品的制备方法，其成分重量比及制备方法如下：1)将0-10份水加入到填充剂中，混合10-30min，静置吸收1-5h；2)将10-40份香味物质、10-20份保润剂、1-10份尼古丁物质搅拌混合5-30min，再加入0.5-3份乳化剂，于磁力搅拌仪上搅拌1-5h；3)将2)所得的液体加入1)中，在搅拌机中搅拌20-60min，静置12-24h，得到含乳化剂的尼古丁口含制品。
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| CN115381129A (zh) * | 2022-08-23 | 2022-11-25 | 深圳市吉迩科技有限公司 | 一种含有槟榔提取物的口含烟制品及其制备方法 |
| CN115813007A (zh) * | 2022-12-22 | 2023-03-21 | 东莞市吉纯生物技术有限公司 | 尼古丁口含制品及制备方法和碱性电解水的制备方法 |
| WO2024201280A1 (en) * | 2023-03-31 | 2024-10-03 | Nicoventures Trading Limited | Emulsions for nicotine encapsulation |
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| US20200297026A1 (en) * | 2017-12-15 | 2020-09-24 | Swedish Match North Europe Ab | Flavoured moist oral pouched nicotine product comprising monoglyceride |
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| CN115381129A (zh) * | 2022-08-23 | 2022-11-25 | 深圳市吉迩科技有限公司 | 一种含有槟榔提取物的口含烟制品及其制备方法 |
| CN115813007A (zh) * | 2022-12-22 | 2023-03-21 | 东莞市吉纯生物技术有限公司 | 尼古丁口含制品及制备方法和碱性电解水的制备方法 |
| WO2024201280A1 (en) * | 2023-03-31 | 2024-10-03 | Nicoventures Trading Limited | Emulsions for nicotine encapsulation |
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