CN103844749A - Preparation method of pillow interior filler - Google Patents
Preparation method of pillow interior filler Download PDFInfo
- Publication number
- CN103844749A CN103844749A CN201410062700.3A CN201410062700A CN103844749A CN 103844749 A CN103844749 A CN 103844749A CN 201410062700 A CN201410062700 A CN 201410062700A CN 103844749 A CN103844749 A CN 103844749A
- Authority
- CN
- China
- Prior art keywords
- pillow
- shitosan
- preparation
- concentrate
- seed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention relates to the field of a biotechnology, in particular to a preparation method of functional pillow interior filler. The method comprises the steps of taking the seeds of maiden cane as a base stock, forming a layer of protective film on the base stock absorbed with the effective ingredients of plants through chitosan by controlling the moisture content of the seeds of the maiden cane, mixing the mixed and extracted plant ingredients, and then drying after adding a chitosan solution to treat, and slowly releasing the effective ingredients of the plants through microwave treatment, thereby keeping the effects of the pillow interior filler warm and durable.
Description
Technical field
The invention belongs to biological technical field, relate to pillow fillings preparation method.
Background technology
Functional health pillow has referred to and can play the nerve of releiving by certain health-care effect, tranquilizing and allaying excitement, the health type pillow of the effects such as protection cervical vertebra.The physiotherapy principle of functional health pillow product can be summarized as two classes: " physical arrangement rehabilitation principle " and " natural plant material for treating principle ".
Physical arrangement rehabilitation principle refers to the shape (hollow pillow) by pillow, and the material (pillow as natural in neck supporting moulding, jade pillow, slow resilience pillow) of pillow plays protection cervical vertebra, improves the effects such as sleep comfort level.
Natural plant material for treating principle refers to by aromatotherapy or traditional Chinese medical theory comes compatibility Chinese medicine or fragrant plant, fills pillow with natural plants, utilizes the volatilization naturally of aromatic substance in pillow, plays due health-care effect after being absorbed by the body.Concrete can have tranquilizing and allaying excitement, promoting blood circulation and removing blood stasis, hypotensive, the effects such as Xie Yu of regulating the flow of vital energy.Famous in ancient physician Huatuo, Sun Simiao early have the theory of " Wen Xiang gets rid of illness ", control head, all diseases of neck with medicine-filled pillow.Ming Dynasty's Li Shizhen (1518-1593 A.D.) was also once repeatedly mentioned the principle that medicine-filled pillow is cured the disease in Compendium of Material Medica.The draft medicine-filled pillow of high-quality should condense more than all chis of pillow with its medicine perfume (or spice) especially, and its smell is light and quite well, for a long time and not a little less than, turbid clearly and not, quiet and loose, loose and do not walk.
At present, on market, occurred many seeds with natural plants, root, stem, leaf, flower and fruit etc. fill pillow make pillow, in this type of product utilization plant aromatic substance naturally volatilize, play tranquilizing and allaying excitement, hypotensive, the effects such as Xie Yu of regulating the flow of vital energy.This class functional health pillow is subject to liking of Chinese Consumer's deeply, occupies larger share in functional health pillow field.Although plant series functional health pillow has many advantages, but, adopt plant directly as the filler of pillow, there are two large shortcomings; The one,, the natural evaporation rate of the aromatic substance in natural plants is very fast, and using, initial stage volatile matter concentration is high, produces on the contrary spread effect; In use the concentration of phase and later stage volatile matter declines can affect again use effect.The 2nd,, seed, root, stem, leaf, flower and the fruit of natural plants repeatedly rubs and pushes in long-term use procedure, can cause historrhexis the powdered of plant itself, unhealthful on the contrary after being inhaled into.If can make the active ingredient of natural plants slowly discharge and avoid directly using the tissue filling of plant itself, will effectively overcome above drawback.
Maiden cane formal name used at school is millet, is grass family Panicum annual herb.A kind of precocity, drought-enduring grain and forage crop.The ancient Ji, Ji that claims of round-grained rice person, now claims millet, broom corn millet.The ancient broomcorn millet that claims of glutinous person, now claims broomcorn millet, sticky broom corn millet or yellow grain.The seed size homogeneous of its formation, quality are solid, have as pillow filler that gas permeability is good, good fluidity, the features such as fungus resistance is strong, are commonly used for main stuffing, then are aided with the plant components such as chrysanthemum, Cassia occidentalis, selfheal, honeysuckle and lophatherum gracile and make functional health pillow.
Shitosan (chitosan) is that the chitin (chitin) extensively being existed by nature obtains through deacetylation, and chemical name is Chitosan (1-4)-2-amino-B-D glucose.Shitosan has many good functional characters and potential using value, and wherein film forming is very noticeable, between its molecule, has been cross-linked to form spacial framework, easily film forming, and this film hot strength is large, good toughness, alkaline-resisting and organic solvent-resistant.Therefore shitosan, as a kind of good membranes material, can be widely used at industrial circles such as food, medicine, weaving, chemical industry, papermaking.Shitosan can be made various films, as food fresh keeping film, edible film and Preparation of Biodegradable Package Film, separate filter membrane, waterproof membrane, medical film etc., is more and more subject to people's attention.After shitosan film forming, there is good biocompatibility and permeability, aspect slow releasing pharmaceutical and targeting medicine, there is important R and D value, be commonly used for the carrier of medicament slow release.Medicine carrying membrane has good medicament slow release performance.In the multiple method of administration of clinical treatment, the normal and various medicine of shitosan is compound makes transdermal medicine film and the film of administration of swallowing, and reaches the object of protection and slowly-releasing.In addition, the growth that shitosan can also suppress various bacteria is with active.A large amount of experiments show, shitosan has obvious inhibitory action to the bacterium such as Escherichia coli and staphylococcus aureus.According to the study, shitosan is by infiltrating in cell body, and in adherent cell body, with the cytoplasm of anion, and there is flocculation and upset the normal physiological activity of cell, thus the growth of anti-bacteria.Therefore, shitosan is mainly used in the fresh-keeping and anticorrosion of food in field of food industry.
Summary of the invention
The object of the invention is to provide a kind of method and product of preparing spacetabs type functional health pillow filler with maiden cane seed and shitosan.
Use effect uniformity that seed, root, stem, leaf, flower and the fruit etc. of plant directly exist as the filler of pillow and persistence is poor and the shortcoming of resistance to use not for existing capability health pillow, the present invention adopts that quality is solid, gas permeability is good, good fluidity, the maiden cane seed that fungus resistance is strong is base-material, after dry, make it to there is good water imbibition and oil absorption; Extract the active ingredient in plant by modern Chinese herbal medicine extraction process of effective component such as water seaoning, the molten methods of alcohol, absorb with dried base-material again or absorption active ingredient, then add certain density chitosan solution processing, after dry, shitosan can be at the biomembrane that has adsorbed the densification of active ingredient base-material surface formation one deck, by having made pillow fillings after microwave sterilization.
The concrete technical scheme of the present invention is as follows:
A kind of preparation method of pillow fillings:
(1) selecting dry maiden cane seed is pillow base-material;
(2) by one or more mixture of chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, the concentrated concentrate that to obtain;
(3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture;
(4) by weight the ratio of 1:20, chitosan solution is added in pillow base-material and concentrate mixture, mixes;
(5) microwave 20kW heat treated 6-8 minute; Cooling.
The dry maiden cane seed moisture content of step (1) is lower than 10%.
The described chitosan solution of step (4) is processed as follows: get the shitosan that deacetylation is greater than 70%, be dissolved in 10% lactic acid, the content of shitosan is 2%, adjusts the pH value of solution to 3.0-6.5 with the NaHCO3 of 0.1Mol/L.
With ethanol or water effective component extracting, concentrate to obtain concentrate.Such as, can adopt conventional ethanol or water mild temperature to soak, the concentrated mode of filtrate decompression obtains concentrate as medicinal extract or dry powder, and this is routine techniques, no longer superfluous words.
Concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio.If concentrate is medicinal extract, dry processing again after mixing with pillow base-material.
Beneficial effect of the present invention:
(1) the present invention is by forming breathable diaphragm with shitosan at the maiden cane the surface of the seed that has adsorbed active ingredient of natural plant; aromatic substance in natural plants slowly and is equably discharged; fill the functional health pillow of pillow making with this filler and can accomplish that smell is light and quite well; for a long time and not, action temperature and lasting.
(2) the present invention is by extracting the active ingredient of plant, and can avoid is in use squeezed and is rubbed by the direct pillow of filling such as flower, leaf and fruit of plant, and the defect of fragmentation and powdered easily occurs.
(3) the inventive method, shitosan itself has again good antibacterial bacteriostatic effect, and the filler that can make continues the effect of performance antibacterial and mouldproof in use procedure from now on.
(4) the present invention adopts first shitosan processing, then the mode of microwave treatment, has collaborative bacteriostasis, can effectively kill the bacterium in material, has the effects such as good mildew-resistant.
Detailed description of the invention
Embodiment 1
A kind of preparation method of pillow fillings
1. selecting maiden cane seed is base-material, by modes such as oven dry, by maiden cane seed drying, makes it moisture lower than 10%;
2. chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, windproof, the bighead atractylodes rhizome, second alcohol and water are packed by a certain percentage into multipotency and extract concentration and recovery unit, effective component extracting, and concentrated;
3. the active ingredient after extracting and concentrating is joined in dried maiden cane seed in the ratio of 2%-5%, in anistree agitator, mix, then place 30-60 minute;
4. get the shitosan that deacetylation is greater than 70%, be dissolved in 10% lactic acid, the content of shitosan is 2%, with the NaHCO of 0.1Mol/L
3adjust the pH value of solution to 3.0-6.5;
5. by weight the ratio of 1:20, chitosan solution is added in the maiden cane seed that has adsorbed effective ingredients in plant, is uniformly mixed;
6. the maiden cane seed that has adsorbed effective ingredients in plant and shitosan is sent into tunnel type micro wave heater (power 20kW), processed 6 ~ 8 minutes;
7. the maiden cane of collection and treatment, cooling rear one-tenth pillow fillings.
Embodiment 2
1, a preparation method for pillow fillings, comprises the steps:
(1) selecting dry maiden cane seed is pillow base-material; Dry maiden cane seed moisture content is lower than 10%;
(2) by one or more mixture of chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, the concentrated concentrate that to obtain;
(3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture;
(4) by weight the ratio of 1:20, chitosan solution is added in pillow base-material and concentrate mixture, mixes; Described chitosan solution is processed as follows: get the shitosan that deacetylation is greater than 70%, be dissolved in 10% lactic acid, the content of shitosan is 0.5%-2%, adjusts the pH value of solution to 3.0-6.5 with the NaHCO3 of 0.1Mol/L;
(5) microwave 20kW heat treated 6-8 minute; Cooling, material-filling after treatment is made to pillow inner of pillow filler.
Embodiment 3
1, material preparation:
(1) selecting dry maiden cane seed is pillow base-material;
(2) by one or more mixture of chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, the concentrated concentrate that to obtain;
(3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture.
2, sterilization mode: shitosan microwave Combined Processing method for disinfection, conventional microwave sterilization method, use shitosan and the not comparison of sterilization processing to bacterium, mould and coliform germicidal efficiency and material maximum temperature in material (pillow base-material and concentrate mixture) separately.
3, chitosan solution preparation: get deacetylation and be greater than 500 grams of 70% shitosans, be dissolved in 10% lactic acid, the content of shitosan is 2%, with the NaHCO of 0.1Mol/L
3adjust the pH value to 3.0 of solution, 100 liters of cumulative volumes.
4, shitosan processing: the ratio by weight 1:20 is added on chitosan solution in pillow base-material and concentrate mixture, mixes;
Microwave treatment: microwave 20kW heat treated 6-8 minute.
5, after processing according to following table different condition, different samples are pressed national standard method (GB 4789.2-2010; GB4789.3-2010 and GB 4789.15-2010) measure total number of bacteria, coliform and fungi count, and measure the maximum temperature of material.
| Filler (maiden cane) | Total number of bacteria (cfu/g) | Coliform (MPN) | Fungi count (cfu/g) | Material maximum temperature |
| Not sterilization | 159000 | 1100 | 3560 | 20℃ |
| Shitosan (consumption 10%, 6 minutes time) separately | 125300 | 870 | 2943 | 20℃ |
| Microwave treatment (power 20kw, time 6 minutes) separately | 1860 | 59 | 311 | 96℃ |
| First microwave (power 20kw, time 6 minutes)+shitosan processing again (consumption 10%) | 1528 | 46 | 269 | 96℃ |
| First shitosan (consumption 10%)+microwave treatment (power 20kw, time 6 minutes) again | 102 | Do not detect | Do not detect | 85℃ |
Conclusion: first shitosan is processed in microwave treatment, has collaborative bacteriostasis, processes antibacterial action than shitosan after independent shitosan, microwave, first microwave better.
Claims (3)
1. a preparation method for pillow fillings, is characterized in that comprising the steps: that (1) selects dry maiden cane seed is pillow base-material; (2) by one or more mixture of chrysanthemum, cassia seed, selfheal, lophatherum gracile, honeysuckle, windproof, the bighead atractylodes rhizome, with ethanol or water effective component extracting, the concentrated concentrate that to obtain; (3) concentrate is joined in pillow base-material by weight 0.02-0.05:1 ratio, mix, then place 30-60 minute to obtain pillow base-material and concentrate mixture; (4) by weight the ratio of 1:20, chitosan solution is added in pillow base-material and concentrate mixture, mixes; (5) microwave 20kW heat treated 6-8 minute; Cooling.
2. preparation method according to claim 1, is characterized in that the dry maiden cane seed moisture content of step (1) is lower than 10%.
3. preparation method according to claim 1, it is characterized in that the described chitosan solution of step (4) processes as follows: get the shitosan that deacetylation is greater than 70%, be dissolved in 10% lactic acid, the content of shitosan is 0.5%-2%, adjusts the pH value of solution to 3.0-6.5 with the NaHCO3 of 0.1mol/L.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410062700.3A CN103844749B (en) | 2014-02-25 | 2014-02-25 | A kind of preparation method of pillow fillings |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410062700.3A CN103844749B (en) | 2014-02-25 | 2014-02-25 | A kind of preparation method of pillow fillings |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103844749A true CN103844749A (en) | 2014-06-11 |
| CN103844749B CN103844749B (en) | 2015-10-28 |
Family
ID=50853196
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410062700.3A Active CN103844749B (en) | 2014-02-25 | 2014-02-25 | A kind of preparation method of pillow fillings |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103844749B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104799642A (en) * | 2015-05-09 | 2015-07-29 | 福建农林大学 | Medicine healed cervical pillow and preparation method of medicine healed cervical pillow |
| CN105231740A (en) * | 2015-10-23 | 2016-01-13 | 李景超 | Pillow filled with plant seeds |
| CN108185750A (en) * | 2017-12-05 | 2018-06-22 | 重庆帕特企业管理咨询有限公司 | A kind of health taxad pillow and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2290264Y (en) * | 1996-05-22 | 1998-09-09 | 马君渭 | Health pillow for baby |
| CN101264254A (en) * | 2007-03-15 | 2008-09-17 | 朱建良 | Medicaments for silkworm excrement vein relaxing pillow and pillow made of the same and manufacturing method of the pillow |
| CN101361920A (en) * | 2008-08-25 | 2009-02-11 | 李富祥 | Traditional Chinese medicine combination of hypotension tranquilization pillow inner |
| CN101991319A (en) * | 2009-08-20 | 2011-03-30 | 安徽奥来新能源有限公司 | Novel Chinese medicament-plant health care pillow |
| CN102327011A (en) * | 2010-07-13 | 2012-01-25 | 江苏宝缦卧室用品有限公司 | Health-care traditional Chinese medicinal pillow |
-
2014
- 2014-02-25 CN CN201410062700.3A patent/CN103844749B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2290264Y (en) * | 1996-05-22 | 1998-09-09 | 马君渭 | Health pillow for baby |
| CN101264254A (en) * | 2007-03-15 | 2008-09-17 | 朱建良 | Medicaments for silkworm excrement vein relaxing pillow and pillow made of the same and manufacturing method of the pillow |
| CN101361920A (en) * | 2008-08-25 | 2009-02-11 | 李富祥 | Traditional Chinese medicine combination of hypotension tranquilization pillow inner |
| CN101991319A (en) * | 2009-08-20 | 2011-03-30 | 安徽奥来新能源有限公司 | Novel Chinese medicament-plant health care pillow |
| CN102327011A (en) * | 2010-07-13 | 2012-01-25 | 江苏宝缦卧室用品有限公司 | Health-care traditional Chinese medicinal pillow |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104799642A (en) * | 2015-05-09 | 2015-07-29 | 福建农林大学 | Medicine healed cervical pillow and preparation method of medicine healed cervical pillow |
| CN105231740A (en) * | 2015-10-23 | 2016-01-13 | 李景超 | Pillow filled with plant seeds |
| CN108185750A (en) * | 2017-12-05 | 2018-06-22 | 重庆帕特企业管理咨询有限公司 | A kind of health taxad pillow and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103844749B (en) | 2015-10-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104258319A (en) | Traditional Chinese medicinal spray for treating bovine foot rot | |
| CN103432287B (en) | Camellia oleosa seed lavipeditum powder and preparation method thereof | |
| CN108310339A (en) | A kind of toxin expelling clearing damp health foot patch | |
| CN104307015A (en) | Lemongrass incense and preparation method thereof | |
| CN105012183B (en) | A kind of eucommia bark toothpaste and preparation method thereof | |
| CN103844749B (en) | A kind of preparation method of pillow fillings | |
| CN106562921A (en) | Liquid oral composition containing TCM active substances and tea tree essential oil | |
| CN104096047A (en) | Externally-applied detoxification ointment for treatment of poisonous snake bite wound and preparation method thereof | |
| CN102327343A (en) | External essential oil formula for preventing and treating beriberi | |
| CN103463317B (en) | A kind of pharmaceutical composition for treating fish white head and mouth fish disease and preparation method thereof | |
| CN106266189A (en) | Compound recipe Radix Arnebiae (Radix Lithospermi) mosquito-expelling and antipruritic cream and preparation method thereof | |
| CN103330813B (en) | Traditional Chinese medicine composition for treating beriberi | |
| CN102949637A (en) | Foot bathing liquid for eliminating dampness and sterilizing | |
| CN108420960B (en) | A Chinese medicinal composition and its preparation method | |
| CN101879028B (en) | Method for making novel medicine fragrance health-care pillow | |
| CN104922449A (en) | Traditional Chinese medicine disinfection solution and preparation method thereof | |
| CN102805406B (en) | Multi-effect vinegar drink product | |
| CN103830633B (en) | A kind of algae health preserving powder for dipping feet | |
| CN106389280A (en) | Special moisturizing spray used for acne skins, and production method thereof | |
| CN105146537B (en) | The preparation method of healthy kitchen medicine materical crude slice | |
| CN105560373A (en) | New use of traditional Chinese medicine Clausena excavata Burm. in preparation of medicines | |
| CN104116806A (en) | Silkworm rearing instrument, silkworm rearing bed and silkworm body disinfectant and preparation method thereof | |
| CN109985178A (en) | A kind of medicinal tea of foot bath and its preparation method and application | |
| CN105192424A (en) | Meat rabbit immunoenhancer | |
| CN104840843A (en) | Female care solution and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |