CN103750535B - Preparation method of heating non-combustion type cigarette block - Google Patents
Preparation method of heating non-combustion type cigarette block Download PDFInfo
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- CN103750535B CN103750535B CN201410030011.4A CN201410030011A CN103750535B CN 103750535 B CN103750535 B CN 103750535B CN 201410030011 A CN201410030011 A CN 201410030011A CN 103750535 B CN103750535 B CN 103750535B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 159
- 238000002360 preparation method Methods 0.000 title claims abstract description 64
- 238000010438 heat treatment Methods 0.000 title claims abstract description 51
- 238000002485 combustion reaction Methods 0.000 title claims abstract description 23
- 241000208125 Nicotiana Species 0.000 claims abstract description 151
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 142
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 29
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000008367 deionised water Substances 0.000 claims abstract description 15
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 15
- 235000010443 alginic acid Nutrition 0.000 claims abstract description 8
- 229920000615 alginic acid Polymers 0.000 claims abstract description 8
- 239000000284 extract Substances 0.000 claims description 63
- 239000003921 oil Substances 0.000 claims description 28
- 235000019198 oils Nutrition 0.000 claims description 28
- 239000002893 slag Substances 0.000 claims description 21
- 239000002002 slurry Substances 0.000 claims description 21
- 229940098465 tincture Drugs 0.000 claims description 21
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 claims description 14
- IGIDLTISMCAULB-UHFFFAOYSA-N 3-methylvaleric acid Chemical compound CCC(C)CC(O)=O IGIDLTISMCAULB-UHFFFAOYSA-N 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 claims description 14
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 14
- 238000010298 pulverizing process Methods 0.000 claims description 14
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 claims description 14
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 7
- MOMFXATYAINJML-UHFFFAOYSA-N 2-Acetylthiazole Chemical group CC(=O)C1=NC=CS1 MOMFXATYAINJML-UHFFFAOYSA-N 0.000 claims description 7
- 244000061520 Angelica archangelica Species 0.000 claims description 7
- 241000167854 Bourreria succulenta Species 0.000 claims description 7
- 240000008886 Ceratonia siliqua Species 0.000 claims description 7
- 235000013912 Ceratonia siliqua Nutrition 0.000 claims description 7
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 7
- 241000219764 Dolichos Species 0.000 claims description 7
- 235000001287 Guettarda speciosa Nutrition 0.000 claims description 7
- 241001632576 Hyacinthus Species 0.000 claims description 7
- 235000019501 Lemon oil Nutrition 0.000 claims description 7
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 claims description 7
- 235000017587 Medicago sativa ssp. sativa Nutrition 0.000 claims description 7
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 7
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 7
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 claims description 7
- 240000004760 Pimpinella anisum Species 0.000 claims description 7
- 235000012550 Pimpinella anisum Nutrition 0.000 claims description 7
- 244000018633 Prunus armeniaca Species 0.000 claims description 7
- 235000009827 Prunus armeniaca Nutrition 0.000 claims description 7
- 244000182022 Salvia sclarea Species 0.000 claims description 7
- 235000002911 Salvia sclarea Nutrition 0.000 claims description 7
- 244000299461 Theobroma cacao Species 0.000 claims description 7
- 235000009470 Theobroma cacao Nutrition 0.000 claims description 7
- 235000009499 Vanilla fragrans Nutrition 0.000 claims description 7
- 244000263375 Vanilla tahitensis Species 0.000 claims description 7
- 235000012036 Vanilla tahitensis Nutrition 0.000 claims description 7
- 229940069765 bean extract Drugs 0.000 claims description 7
- 235000019693 cherries Nutrition 0.000 claims description 7
- 239000001072 coriandrum sativum l. fruit oil Substances 0.000 claims description 7
- 239000001902 eugenia caryophyllata l. bud oil Substances 0.000 claims description 7
- 235000019717 geranium oil Nutrition 0.000 claims description 7
- 239000010648 geranium oil Substances 0.000 claims description 7
- 235000011187 glycerol Nutrition 0.000 claims description 7
- 229940087603 grape seed extract Drugs 0.000 claims description 7
- 235000002532 grape seed extract Nutrition 0.000 claims description 7
- 239000000171 lavandula angustifolia l. flower oil Substances 0.000 claims description 7
- 239000010501 lemon oil Substances 0.000 claims description 7
- 229940043353 maltol Drugs 0.000 claims description 7
- 229940041616 menthol Drugs 0.000 claims description 7
- 239000003595 mist Substances 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 238000000465 moulding Methods 0.000 claims description 7
- 235000019719 rose oil Nutrition 0.000 claims description 7
- 239000010666 rose oil Substances 0.000 claims description 7
- 235000002020 sage Nutrition 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims description 7
- 239000001717 vitis vinifera seed extract Substances 0.000 claims description 7
- 240000004658 Medicago sativa Species 0.000 claims 1
- 239000000843 powder Substances 0.000 abstract 2
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 abstract 1
- 229940072056 alginate Drugs 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 abstract 1
- 235000019634 flavors Nutrition 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 7
- 239000003546 flue gas Substances 0.000 description 7
- 241000219823 Medicago Species 0.000 description 6
- 230000000391 smoking effect Effects 0.000 description 5
- 239000000126 substance Substances 0.000 description 4
- 239000000945 filler Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
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- 150000001875 compounds Chemical class 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
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- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 238000001303 quality assessment method Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a preparation method of a heating non-combustion type cigarette block. The tobacco block is composed of 50-70% of tobacco leaf powder, 5-20% of tobacco stem powder, 3-7% of tobacco flavor, 10-20% of deionized water, 7-11% of alginate and 1-2% of glycerol, all the components are uniformly mixed to prepare tobacco pulp, the tobacco pulp is molded by a mold to form a cylindrical tobacco block with holes, the formed tobacco block is dried in a drying oven at 40 ℃, tobacco essence with the weight of 1-3% of that of the tobacco block is uniformly sprayed on the tobacco block, and the prepared tobacco block is balanced in a constant temperature and humidity box. The tobacco block of the invention is used for heating non-burning cigarettes. The tobacco block fills the blank in the preparation of the non-combustion cigarette tobacco block, and meanwhile, the heating efficiency of the tobacco block can be improved, and the number of suction openings of cigarettes can be obviously increased.
Description
Technical field
The invention belongs to tobacco processing preparing technical field, be specifically related to the preparation method of the higher heating non-combustion type cigarette block of a kind of efficiency of heating surface.
Background technology
The multiple harmful components that traditional cigarette produces due to result of combustion of tobacco and thermal cracking, and heat non-combustion-type cigarette produce flue gas and traditional cigarette comparatively close, and flow measurement flue gas and part harmful components obviously reduce, domestic and international many tobacco enterprises, institute continue to increase R&D intensity for this reason, are devoted to research and the exploitation of heating non-combustion-type cigarette.
At present, heat non-combustion-type cigarette and mainly contain electrical heating cigarette, carbonaceous heating cigarette and chemical heat cigarette three types: (1) electrical heating cigarette." Accord ", " Heatbar ", " EHP " three sections of electrical heating cigarette products that Philip Mirris Products Inc successively releases, all adopt electric heater to produce flue gas to the mode that cigarette products heats, cigarette products has the structure similar with traditional cigarette and profile; The patent of invention " smoking article containing tobacco " of R.J. Rainolds Tobacco CO. describes a kind of electrical heating cigarette, and adopt stratie heat tobacco and produce flue gas, wherein tobacco is generally chopping filler; The utility model patent " electrical heating type cigarette " of Hubei Zhong Yan Industrial Co., Ltd discloses a kind of electrical heating cigarette, this cigarette carries out heating by porous heating plate and additional hot wall to smoked sheet and sends flue gas, but formula of smoked sheet and preparation method thereof yet there are no open.(2) carbonaceous heating cigarette.The cigarette of the type is successively sold by R.J. Rainolds Tobacco CO. with trade mark Premier and Eclipse, wherein Eclipse cigarette adopts the heat heating expanding tobacco filler of carbon heat source burning release and produces flue gas for people's suction, and expanding tobacco filler is reconstituted tobacco; The patent of invention " non-combustible smoking article carbonaceous heat source composition and non-combustible smoking article " of Japan tobacco Inc discloses a kind of carbonaceous heating cigarette, and this cigarette is also the heat heating smoked sheet or the pipe tobacco that adopt carbon heat source burning release.(3) chemical heat cigarette.Olig AG's invention disclosed patent " smokeless cigarette " belongs to chemical heat cigarette, and this cigarette adopts the principle of crystallizable substances crystallization release heat to heat nicotine reservoir and discharges volatile ingredient for consumer's suction; Stagemode OY discloses a patent of invention " smoking product ", and this smoking product provides heat heat tobacco to produce flue gas by the reaction of some compound, and wherein this tobacco can be the tobacco of processing in many different ways.
Known from the above mentioned, a large amount of research and development are carried out to the thermal source of all kinds of heating non-combustion-type cigarette both at home and abroad, but technical know-how factor may be in, seldom mentioned the cigarette preparation method for material of heating non-combustion-type cigarette.The preparation method of the cigarette block therefore providing a kind of efficiency of heating surface higher, has great importance for heating non-combustion-type cigarette field.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of preparation method heating non-combustion type cigarette block is provided, not only filled up the blank of heating non-combustion type cigarette block preparation field, and the efficiency of heating surface of cigarette block effectively improves, puff count also obviously increases.
Object of the present invention is achieved by the following technical programs.
* except as otherwise noted, percentage of the present invention is mass percent.
Heat a preparation method for non-combustion type cigarette block, it is characterized in that: comprise the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use,
(5) cigarette slurry preparation: measure the tobacco slag of 50 ~ 70%, 5 ~ 20% offal end, the tobacco aromatics of 3 ~ 7%, the deionized water of 10 ~ 20%, the alginates of 7 ~ 11% and the glycerine of 1 ~ 2%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 1 ~ 3% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and within 48 hours, namely obtains heating non-flammability cigarette block.
Wherein, described tobacco leaf is at least one in cured tobacco leaf, Turkish tobaccos tobacco leaf, airing cigarette tobacco leaf, burley tobaccos tobacco leaf.
Wherein, described offal is at least one in flue-cured tobacco offal, Turkish tobaccos offal, airing cigarette offal, burley tobaccos offal.
Wherein, the hole of described cylindric cigarette block is for circular, square, rhombus or triangle and quantity is 1 ~ 19.
Wherein, the diameter of described cylindric cigarette block is 5.0 ~ 12.0mm, and length is 1 ~ 20mm.
Compared with prior art, the present invention has following beneficial effect:
1, the present invention has filled up the blank of heating non-combustion type cigarette block preparation field, extends tobacco type.
2, the heating non-combustion type cigarette block that the present invention obtains adopts porose design, makes heating element heater can stretch into the inside of cigarette block, to the homogeneous heating that cigarette block carries out from inside to outside, significantly improves its efficiency of heating surface.
3, the present invention adopts the design of solid block, and the inventory of heating increases, and after adding a cigarette block, the cigarette that the puff count of cigarette comparatively heats pipe tobacco obviously increases.
4, cigarette block of the present invention is prepared easy, and can accomplish scale production.
Accompanying drawing explanation
Fig. 1 is the cross sectional representation that the present invention heats non-combustion type cigarette block.
In figure: the cigarette block of 1-circular opening; The cigarette block of 2-square aperture; The cigarette block of 3-rhombus hole; The cigarette block of 4-triangle hole.
Detailed description of the invention
Be illustrated the present invention below in conjunction with drawings and the specific embodiments, it should be noted that specific embodiment is limited the present invention never in any form, according to the teachings of the present invention done any change or replacement, all belong to protection scope of the present invention.
Embodiment 1
The preparation method of the heating non-combustion type cigarette block described in the present embodiment, comprises the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the cured tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the flue-cured tobacco offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use,
(5) cigarette slurry preparation: measure the tobacco slag of 70%, 6% offal end, the tobacco aromatics of 3%, the deionized water of 10%, the alginates of 10% and the glycerine of 1%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 1% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and within 48 hours, namely obtains heating non-flammability cigarette block; Wherein, the hole of described cylindric cigarette block is for circular, square, rhombus or triangle and quantity is 9; The diameter of described cylindric cigarette block is 9.0mm, and length is 10.0mm.
Embodiment 2
The preparation method of the heating non-combustion type cigarette block described in embodiment, comprises the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the cured tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the flue-cured tobacco offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use,
(5) cigarette slurry preparation: measure the tobacco slag of 50%, 18% offal end, the tobacco aromatics of 5%, the deionized water of 11.5%, the alginates of 10% and the glycerine of 1.5%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 2% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and within 48 hours, namely obtains heating non-flammability cigarette block; Wherein, the hole of described cylindric cigarette block is for circular, square, rhombus or triangle and quantity is 9; The diameter of described cylindric cigarette block is 9.0mm, and length is 10.0mm.
Embodiment 3
The preparation method of the heating non-combustion type cigarette block described in embodiment, comprises the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the cured tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the flue-cured tobacco offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use,
(5) cigarette slurry preparation: measure the tobacco slag of 50%, 18% offal end, the tobacco aromatics of 7%, the deionized water of 13%, the alginates of 10% and the glycerine of 2%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 3% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and within 48 hours, namely obtains heating non-flammability cigarette block; Wherein, the hole of described cylindric cigarette block is for circular, square, rhombus or triangle and quantity is 9; The diameter of described cylindric cigarette block is 9.0mm, and length is 10.0mm.
Embodiment 4
The preparation method of the heating non-combustion type cigarette block described in embodiment, comprises the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the cured tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the flue-cured tobacco offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use,
(5) cigarette slurry preparation: measure the tobacco slag of 60%, 5% offal end, the tobacco aromatics of 5%, the deionized water of 10%, the alginates of 7% and the glycerine of 1%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 1% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and within 48 hours, namely obtains heating non-flammability cigarette block; Wherein, the hole of described cylindric cigarette block is for circular, square, rhombus or triangle and quantity is 1; The diameter of described cylindric cigarette block is 5.0mm, and length is 1.0mm.
Embodiment 5
The preparation method of the heating non-combustion type cigarette block described in embodiment, comprises the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the cured tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the flue-cured tobacco offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use,
(5) cigarette slurry preparation: measure the tobacco slag of 65%, 20% offal end, the tobacco aromatics of 7%, the deionized water of 20%, the alginates of 11% and the glycerine of 1.5%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 1% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and within 48 hours, namely obtains heating non-flammability cigarette block; Wherein, the hole of described cylindric cigarette block is for circular, square, rhombus or triangle and quantity is 19; The diameter of described cylindric cigarette block is 12.0mm, and length is 20.0mm.
Embodiment 6
Repeat embodiment 1, have following difference: tobacco leaf used is Turkish tobaccos tobacco leaf, offal used is Turkish tobaccos offal.
Embodiment 7
Repeat embodiment 2, have following difference: tobacco leaf used is airing cigarette tobacco leaf, offal used is airing cigarette offal.
Embodiment 8
Repeat embodiment 3, have following difference: tobacco leaf used is burley tobaccos tobacco leaf, offal used is burley tobaccos offal.
Embodiment 9
Repeat embodiment 4, have following difference: tobacco leaf used is cured tobacco leaf and Turkish tobaccos tobacco leaf, offal used is flue-cured tobacco offal and Turkish tobaccos offal.
Embodiment 10
Repeat embodiment 4, have following difference: tobacco leaf used is cured tobacco leaf, Turkish tobaccos tobacco leaf, airing cigarette tobacco leaf and burley tobaccos tobacco leaf, offal used is flue-cured tobacco offal, Turkish tobaccos offal, airing cigarette offal and burley tobaccos offal.
Application Example 1
Preparation-obtained for embodiment 1 ~ 3 cigarette block is arranged on identical electrical heating cigarette respectively, and carries out puff number, the homogeneity of every mouthful of amount of smoke and sensory quality assessment, the results are shown in following table:
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. heat a preparation method for non-combustion type cigarette block, it is characterized in that: comprise the following steps:
(1) preparation of tobacco slag: water intaking sub-control, built in the tobacco leaf of 6 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain tobacco slag with pulverizer, for subsequent use;
(2) preparation at offal end: water intaking sub-control, built in the offal of 5 ~ 13%, is crossed 40 mesh sieves after pulverizing obtain offal end with pulverizer, for subsequent use;
(3) preparation of tobacco aromatics: get Fructus Monordicae extract 3%, cocoa shell extract 4%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 6%, red date extract 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 8%, apple extract 6%, deionized water 15% and propane diols 25%, after said components is mixed, stir under 50 ~ 60 DEG C of conditions and namely obtain tobacco aromatics in 40 minutes, for subsequent use; Percentage is mass percent;
(4) preparation of flavouring essence for tobacco: get vanillic aldehyde 0.2%, menthol 0.2%, sage clary oil 0.1%, aniseed oil 10%EA0.4%, Tolu concrete 0.1%, maltol 0.1%, cloud and mist absolute oil 0.6%, coriander seed oil 1%EA2.5%, clove bud oil 0.1%, geranium oil 1%EA3.0%, bay leaves oil 1%EA0.1%, rose oil 1%EA1.2%, 2-acetyl group pyrazine 1.2%, 2, 3, 5-trimethylpyrazine 0.6%, lavender oil 1%EA1.0%, angelica grosseserrata root tincture 3.2%, vanilla bean tincture 5.0%, red date tincture 8.0%, 3 methylvaleric acid 0.04%, ethanol 51.36% and propane diols 21.0%, after said components is mixed, within 1 hour, namely flavouring essence for tobacco is obtained in stirred at ambient temperature, for subsequent use, percentage is mass percent,
(5) cigarette slurry preparation: measure the tobacco slag of 50 ~ 70%, 5 ~ 20% offal end, the tobacco aromatics of 3 ~ 7%, the deionized water of 10 ~ 20%, the alginates of 7 ~ 11% and the glycerine of 1 ~ 2%, in stirred at ambient temperature 30 minutes after mixing, form cigarette slurry; Percentage is mass percent;
(6) preparation of cigarette block: the cigarette slurry mould molding obtained by step (5), form the pertusate cylindric cigarette block of tool, be placed in baking oven to toast under 40 DEG C of conditions after 10 hours, measure the flavouring essence for tobacco that weight equals cigarette block weight 1 ~ 3% and be evenly sprayed on cigarette block surface, after flavouring essence for tobacco is absorbed by cigarette block, cigarette block is placed in the climatic chamber balance that temperature is 22 DEG C, humidity is 60% and namely obtains heating non-combustion type cigarette block in 48 hours.
2. the preparation method of heating non-combustion type cigarette block as claimed in claim 1, is characterized in that: the tobacco leaf described in step (1) is at least one in cured tobacco leaf, Turkish tobaccos tobacco leaf, airing cigarette tobacco leaf or burley tobaccos tobacco leaf.
3. the preparation method of heating non-combustion type cigarette block as claimed in claim 1, is characterized in that: offal described in step (2) is at least one in flue-cured tobacco offal, Turkish tobaccos offal, airing cigarette offal or burley tobaccos offal.
4. the preparation method of heating non-combustion type cigarette block as claimed in claim 1, is characterized in that: the hole of cylindric cigarette block described in step (6) is circle, square, rhombus or triangle and quantity is 1 ~ 19.
5. the preparation method of heating non-combustion type cigarette block as claimed in claim 1, it is characterized in that: described in step (6), the diameter of cylindric cigarette block is 5.0 ~ 12.0mm, length is 1 ~ 20mm.
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