CN103420577A - Plane double vacuum layer glass with sealing groove and mounting hole welded in glass - Google Patents
Plane double vacuum layer glass with sealing groove and mounting hole welded in glass Download PDFInfo
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- CN103420577A CN103420577A CN2013102985906A CN201310298590A CN103420577A CN 103420577 A CN103420577 A CN 103420577A CN 2013102985906 A CN2013102985906 A CN 2013102985906A CN 201310298590 A CN201310298590 A CN 201310298590A CN 103420577 A CN103420577 A CN 103420577A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
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Abstract
Plane double vacuum layer glass with sealing groove and mounting hole welded in glass comprises upper glass, lower glass and middle glass, and is characterized in that the mounting hole and an air extracting hole are combined into a whole, sealing strips are arranged on the lower surface of the upper glass and the middle glass and at the periphery of the middle glass; sealing grooves are formed in the upper surface of the middle glass and the lower glass and in the periphery of the air extracting hole; the peripheries of the upper glass, the lower glass and the middle are welded together under normal pressure in an edge bonding furnace through low-temperature glass solder; the air extracting hole is automatically sealed in a vacuum furnace through metal solder; two closed vacuum layers are formed among the upper glass, the lower glass and the middle glass. The plane double vacuum layer glass and the manufacturing technology thereof are simple; the vacuum glass and the toughened glass can facilitate the mounting and the use, and can guarantee the airtightness of the vacuum glass and improve the intensity, heat insulation performance and sound insulation performance of the glass.
Description
Technical field
The present invention relates to glass deep process technology field, relate in particular to a kind of glass and be welded with two vacuum layer glass in plane of sealing groove and open holes and preparation method thereof.
Background technology
Vacuum glass is a kind of novel energy-saving glass, and vacuum glass not only can solve " breathing " problem of the existing a large amount of double glazings that use, and has that the heat-and sound-insulating performance is good, wind pressure resistant strength is high, thickness is little and the advantage such as long service life.Vacuum glass generally consists of two to three sheet glass, between two adjacent sheet glass, forms cavity, at the periphery of glass, is provided with edge sealing structure, and cavity forms vacuum layer after being pumped into vacuum.Vacuum glass is according to the mode difference that forms vacuum layer, can be divided into two kinds, a kind of is vacuum glass without bleeding point, and the edge sealing of this vacuum glass carries out in vacuum oven, along with completing of edge sealing, the cavity self-assembling formation vacuum layer of sealing between two adjacent sheet glass; Another kind is the vacuum glass that bleeding point is arranged, the edge sealing of this vacuum glass carries out in High Temperature Furnaces Heating Apparatus under normal pressure, by prefabricated bleeding point, the cavity sealed between glass is vacuumized again after edge sealing completes, finally, at the end rear enclosed bleeding point of bleeding, complete the making of vacuum glass.
The present patent application people discloses a series of vacuum glass without bleeding point and preparation method thereof in the patent of the vacuum glass of in October, 2012 application, but when utilizing the low temperature glass solder edge sealing, because low temperature glass solder is to be made by many oxide, at high temperature, under vacuum, air and the moisture of scolder absorption, volatile substances in scolder, in the gas that scolder dissolves in process of production and scolder, decomposition of partial oxide etc. all can cause a large amount of bubble of generation in scolder, the properties that has greatly weakened scolder is resistance to air loss especially, cause the feasibility of this kind of mode to be greatly affected.The vacuum glass of existing mass production is all the vacuum glass that bleeding point is arranged, but exists that complex manufacturing technology, extraction temperature low (bleeding not thorough), monolithic vacuumize, cost is high, production capacity is low, can not make the shortcoming such as toughened vacuum glass.
Vacuum glass can substitute existing single-glass and be applied to require the ,You De installation site, place of heat insulation and sound insulation to install in punching on glass, and vacuum glass obviously can't punch when mounted thereon, otherwise can destroy its vacuum.
Summary of the invention
Technical problem to be solved by this invention is to be the defect existed for existing bleeding point vacuum glass, two vacuum layer glass in the plane that provides a kind of glass to be welded with sealing groove and open holes and preparation method thereof, the making method technique of this vacuum glass is simple, prepared vacuum glass and toughened vacuum glass not only are conducive to install and use, and can guarantee resistance to air loss and the transparency of vacuum glass, and can increase its intensity and heat insulation, sound-proofing properties.
In order to solve the problems of the technologies described above, the invention provides the two vacuum layer glass in plane that a kind of glass is welded with sealing groove and open holes, comprise upper glass, intermediate glass and lower-glass, it is characterized in that open holes and bleeding point unite two into one, described upper glass, intermediate glass and lower-glass are flat glasss, described upper glass, the lower surface periphery of intermediate glass and the periphery of described bleeding point have sealed strip, described intermediate glass, the upper surface periphery of lower-glass and the periphery of described bleeding point have sealing groove, the periphery of described upper glass and described lower-glass and described intermediate glass welds together in normal pressure lower sealing edge stove by low temperature glass solder, described bleeding point utilizes brazing metal self-closed in vacuum oven, form the vacuum layer of two sealings between described upper glass and described lower-glass and described intermediate glass, have in described vacuum layer and be the upholder that dot matrix is arranged.
In order to solve the problems of the technologies described above, the invention provides the preparation method of the two vacuum layer glass in plane or the two vacuum layer glass of plane tempering, it comprises:
The first step, according to the shape of the two vacuum layer glass in the plane of required making and three flat glasss of size cutting desired size, bleeding point and open holes are made in edge punching at three blocks of glass, offer sealing groove at the peripheral weld of lower-glass and intermediate glass and the periphery of bleeding point, and three blocks of glass are carried out to edging, chamfering, cleaning and drying treatment;
Second step, peripheral weld at upper glass and intermediate glass and bleeding point prepares sealed strip, sealed strip can insert in corresponding sealing groove, and, at least one making upholder on glass, three blocks of glass is sent in High Temperature Furnaces Heating Apparatus or annealing furnace carried out pyroprocessing or tempering processing subsequently;
The 3rd step, will evenly be coated with low temperature glass solder in the sealing groove of intermediate glass and lower-glass periphery, three blocks of glass are sent in the edge sealing stove after closing sheet;
The 4th step, carry out the heat temperature raising operation to described edge sealing stove, more than being warming up to the melt temperature of low temperature glass solder, reaches the edge sealing temperature, and sealed strip is under the action of gravity of glass in the embedding sealing groove; Stop heating, lower the temperature with stove, low temperature glass solder hermetic welds together three blocks of glass, and the fire door of opening the edge sealing stove obtains double glazing;
The 5th step, pack brazing metal in the bleeding point of double glazing into, and send in vacuum oven; To described vacuum sole vacuumize, limit heating, be evacuated to 0.1Pa following, be warming up to the temperature of fusion of brazing metal more than, brazing metal is fused into liquid, liquid retention is in the sealing groove of intermediate glass and lower-glass, the sealed strip of upper glass and intermediate glass also is submerged in liquid, and liquid is by the bleeding point self-sealing; Stop heating, with stove cooling, brazing metal solidifies realizes airtight sealing afterwards to bleeding point, opens vacuum oven, takes out the two vacuum layer glass in plane;
The 6th step is put into seal gum and protective casing, at the place suitable for reading of protective casing Paste Product trade mark in the bleeding point of the two vacuum layer glass in plane.
Wherein, the periphery of the lower surface periphery of described upper glass and intermediate glass or bleeding point at least respectively has a sealed strip.
Wherein, the periphery of the upper surface periphery of described intermediate glass and lower-glass or bleeding point at least respectively has a sealing groove.
Wherein, described sealed strip is corresponding with described sealing groove, and described sealed strip can insert in described sealing groove.
Wherein, described upper glass, described intermediate glass and described lower-glass are simple glass or toughened glass or semi-tempered glass.
Wherein, described upper glass, described intermediate glass and described lower-glass are simple glass or coated glass or Low-E glass.
Wherein, described sealed strip adopts printing, printing or mechanically spraying cryogenic glass powder or the modes such as glass ink or metal paste to prepare.
Wherein, described sealing groove is formed by mechanical workout or laser processing, and the preferred mechanical processing mode, as mechanical mill, mechanical cutting etc.
Wherein, the internal surface of the sealing groove of described bleeding point periphery can the paint metals slurry, and metal paste contributes to combining closely of brazing metal and glass.
Wherein, described brazing metal comprises low-temperature metal scolder and solder, and described material is existing commercial commodity.
Further, the fusing point of described brazing metal is lower than the fusing point of low temperature glass solder, and during the brazing metal fusing, the low temperature glass solder of edge sealing remains unchanged.
Further, described brazing metal is shaped as powdery, strip, sheet or bulk, ring-type, tubulose etc.
Wherein, between described brazing metal and described glass or described sealed strip, the metal paste coating is arranged, metal paste contributes to combining closely of brazing metal and glass.
Wherein, above support is made by metal, pottery, glass or high molecular polymer, matrix material, preferably adopts printing, sprayed glass printing ink or polymkeric substance preparation.
Wherein, above support has one deck or two-layer; Above support be printed on one on glass, or be printed on two on glass, conventional vacuum glass preferably be printed on one on glass, toughened vacuum glass preferably be printed on two on glass.
Wherein, above support is column, or is strip; When upholder is printed on one when on glass, be preferably cylindric; When upholder is printed on two when on glass simultaneously, be preferably strip, and vertical pile.
Wherein, described edge sealing stove can once heat one to the several piece plane two vacuum layer glass.
Wherein, described edge sealing stove can have basic heating system and local heating system, the basis heating system can adopt the mode of Hot-blast Heating or resistive heating as nichrome wire, electrothermal tube, hot plate etc. or suction ripple heating element, and the local heating system adopts the modes such as microwave heating or Infrared Heating;
Further, the heating of described basis, be that burner hearth or bulk glass are heated to a lower temperature, as 300 ~ 350 ℃, can not cause toughened glass obviously to be annealed;
Further, described local heating, be that scolder or glass periphery are heated to a higher temperature, as 400 ~ 450 ℃, prevents the whole obviously annealing of toughened glass;
Wherein, described vacuumizing and the bleeding point sealing can be carried out in batches in vacuum oven, also can implement by monolithic; Can wholely heat glass, also can the local heating bleeding point.
Wherein, described vacuum oven heating, can adopt conventional heating, Infrared Heating, also can adopt induction heating, LASER HEATING, can also adopt other suitable heating unit or heater meanses.
Further, described heating, can heat bulk glass, also can the local heating bleeding point.
Wherein, described seal gum preferably has secret sealing, more preferably hot melt adhesive, hot-setting adhesive or two component sealing gum.
Beneficial effect of the present invention:
Glass of the present invention is welded with two its upper glasses of vacuum layer glass in plane of sealing groove and open holes and the periphery of intermediate glass and the periphery of bleeding point sealed strip, the periphery of intermediate glass and lower-glass and the periphery of bleeding point have sealing groove, make edge sealing and the sealing of vacuum glass easier, more reliable, even the chimeric of sealed strip and sealing groove guaranteed vacuum glass in the situation that the sealing effectiveness of glass deformation, there is the bonding strength higher than low temperature welding glass between sealed strip and upper glass, chimeric sealing surface area and the airtight layer thickness increased between upper lower-glass of sealed strip and sealing groove, chimeric automatic-sealed and the mass sealing that has realized bleeding point of sealed strip and sealing groove, the open holes of vacuum glass of the present invention, simple in structure, safe and reliable, convenient for production, with low cost, open holes and the bleeding point of vacuum glass of the present invention unite two into one, and not only production technique is simple, and intensity is higher, the quantity of open holes is not limit, and can have one to several, not only facilitates and installs but also be conducive to vacuumize, its size of open holes of the present invention relatively can be very large, and inside can increase protective casing, thereby is conducive to improve the quality and performance of vacuum glass, extends its work-ing life, under normal pressure under low temperature glass solder edge sealing and vacuum brazing metal sealing solved the airtight integrity problem of scolder, increased the tightness of vacuum layer, improved the life-span of vacuum glass, greatly improved vacuum glass productivity and qualification rate, reduced the production cost of vacuum glass.
The accompanying drawing explanation
Fig. 1 is the two vacuum layer glass structural representations in plane of the present invention.
In figure: 1. upper glass, 2. lower-glass, 3. bleeding point and open holes, 4. low temperature glass solder, 5. sealed strip, 6. sealing groove, 7. brazing metal, 8. upholder, 9. intermediate glass, 10. seal gum, 11. protective casings, 12. product brands.
Embodiment
Below adopt embodiment and accompanying drawing to describe embodiments of the present invention in detail, to the present invention, how the utilisation technology means solve technical problem whereby, and the implementation procedure of reaching technique effect can fully understand and implement according to this.
Embodiment: referring to accompanying drawing, the two vacuum layer glass in plane are by upper glass 1, intermediate glass 9 and lower-glass 2 form, in three blocks of glass, at least go up, lower-glass is toughened glass or semi-tempered glass, wherein lower-glass 2 or and intermediate glass 9 or low emissivity glass, its making method is as follows: at first according to the shape of the two vacuum layer glass in the plane of required making and three flat glasss of size cutting desired size, form bleeding point and open holes 3 at three through holes that bore respectively on glass, offer sealing groove 6 at the upper surface periphery of intermediate glass 9 and lower-glass 2 and the periphery of bleeding point 3, and three blocks of glass are carried out to edging, chamfering, clean, drying treatment, secondly prepare sealed strip 5 at the lower surface periphery of upper glass 1 and intermediate glass 9 and the periphery printing of bleeding point 3, print and prepare upholder 8 on the upper surface of the lower surface of upper glass 1 and lower-glass 2, sealed strip 5 to middle glass 9 carries out high temperature sintering, and two blocks of upper and lower glass are carried out to the tempering processing, again by the method for mechanical workout, respectively upper and lower upholder on glass 8 is machined to the same level height, to in the sealing groove of intermediate glass 9 and lower-glass 2 peripheries, evenly fill low temperature glass solder, and three glass consistencies from top to bottom are stacked together, send in the edge sealing stove, the edge sealing stove and accessory has basic heating system and local heating system, first utilize basic heating system as Hot-blast Heating, make basal temperature rise to 300 ~ 350 ℃, the microwave heating of recycling local heating system is heated to 430 ~ 450 ℃ of melt temperatures by low temperature glass solder, and the low temperature glass solder 4 of melting by three glass cementations together, stop heating, lower the temperature with stove, low temperature glass solder 4 hermetic welds together three blocks of glass, the metallic zinc solder 7 of finally packing in bleeding point 3, send in vacuum oven, vacuumized and heating operation, be evacuated to below 0.1Pa, be warming up to the melt temperature of metallic zinc solder 7 more than 380 ℃, metallic zinc solder 7 is fused into liquid retention in sealing groove 6, sealed strip 5 also is submerged in liquid, and liquid is by the bleeding point self-sealing, stop heating, lower the temperature with stove, metallic zinc solder 7 condenses into solid, and bleeding point is realized to airtight sealing, opens vacuum oven, takes out the two vacuum layer glass in plane.Smear while hot seal gum 10 as butyl rubber in open holes, protective casing 11 packed in open holes 3, with seal gum 10, fill up the space between protective casing 11 and open holes 3, last on protective casing 11 covering product brand 12.
All above-mentioned these intellecture properties of primary enforcement, do not set restriction this product innovation of other forms of enforcement and/or novel method.The modification of those skilled in the art based on foregoing, can realize similar implementation status.But all modifications or transformation belong to the right of reservation based on product innovation of the present invention.
The above, be only preferred embodiment of the present invention, is not the present invention to be done to the restriction of other form, and any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the equivalent embodiment of equivalent variations.But every technical solution of the present invention content that do not break away from, any simple modification, equivalent variations and the remodeling above embodiment done according to technical spirit of the present invention, still belong to the protection domain of technical solution of the present invention.
Claims (10)
1. a glass is welded with the two vacuum layer glass in plane of sealing groove and open holes, comprise upper glass, intermediate glass and lower-glass, it is characterized in that: open holes and bleeding point unite two into one, described upper glass, intermediate glass and lower-glass are flat glasss, described upper glass, intermediate glass and lower-glass are simple glass or toughened glass or semi-tempered glass, described upper glass, the lower surface of intermediate glass and the periphery of described bleeding point have sealed strip, described intermediate glass, the upper surface periphery of lower-glass and the periphery of described bleeding point have sealing groove, the periphery of described upper glass and described lower-glass and described intermediate glass welds together in normal pressure lower sealing edge stove by low temperature glass solder, described bleeding point utilizes brazing metal self-closed in vacuum oven, described brazing metal comprises low-temperature metal scolder and solder, form the vacuum layer of two sealings between described upper glass and described lower-glass and described intermediate glass, have in described vacuum layer and be the upholder that dot matrix is arranged.
2. the two vacuum layer glass in plane according to claim 1, is characterized in that, between described brazing metal and described glass or described sealed strip, the metal paste coating is arranged, and metal paste contributes to combining closely of brazing metal and glass.
3. the two vacuum layer glass in plane according to claim 1 and 2, is characterized in that described upper glass, described intermediate glass and described lower-glass are simple glass or coated glass or Low-E glass.
4. according to the two vacuum layer glass in the described plane of claims 1 to 3 any one, it is characterized in that described sealed strip adopts the mode of printing, printing or mechanically spraying cryogenic glass powder or glass ink or metal paste to prepare.
5. according to the two vacuum layer glass in the described plane of claims 1 to 3 any one, it is characterized in that described sealing groove adopts mechanical workout or laser processing to form.
6. according to the two vacuum layer glass in the described plane of claim 1 to 5 any one, it is characterized in that above support has one deck or two-layer.
7. the preparation method of the two vacuum layer glass in the described plane of claim 1 to 6 any one, it is characterized in that: the two vacuum layer glass in described plane are the two vacuum layer glass in plane or the two vacuum layer glass of plane tempering, and the preparation method is as follows:
The first step, according to the shape of the two vacuum layer glass in the plane of required making and three flat glasss of size cutting desired size, bleeding point and open holes are made in edge punching at three blocks of glass, offer sealing groove at the peripheral weld of lower-glass and intermediate glass and the periphery of bleeding point, and three blocks of glass are carried out to edging, chamfering, cleaning and drying treatment;
Second step, peripheral weld at upper glass and intermediate glass and bleeding point prepares sealed strip, sealed strip can insert in corresponding sealing groove, and, at least one making upholder on glass, three blocks of glass is sent in High Temperature Furnaces Heating Apparatus or annealing furnace carried out high temperature or tempering processing subsequently;
The 3rd step, will evenly be coated with low temperature glass solder in the sealing groove of intermediate glass and lower-glass periphery, three blocks of glass are sent in the edge sealing stove after closing sheet;
The 4th step, carry out the heat temperature raising operation to described edge sealing stove, more than being warming up to the melt temperature of low temperature glass solder, reaches the edge sealing temperature, and sealed strip is under the action of gravity of glass in the embedding sealing groove; Stop heating, lower the temperature with stove, low temperature glass solder hermetic welds together three blocks of glass, and the fire door of opening the edge sealing stove obtains double glazing;
The 5th step, pack brazing metal in the bleeding point of double glazing into, and send in vacuum oven; To described vacuum sole vacuumize, limit heating, be evacuated to 0.1Pa following, be warming up to the temperature of fusion of brazing metal more than, brazing metal is fused into liquid, liquid retention is in the sealing groove of intermediate glass and lower-glass, the sealed strip of upper glass and intermediate glass also is submerged in liquid, and liquid is by the bleeding point self-sealing; Stop heating, with stove cooling, brazing metal solidifies realizes airtight sealing afterwards to bleeding point, opens vacuum oven, takes out the two vacuum layer glass in plane;
The 6th step is put into seal gum and protective casing, at the place suitable for reading of protective casing Paste Product trade mark in the bleeding point of the two vacuum layer glass in plane.
8. the preparation method of the two vacuum layer glass in plane according to claim 7, it is characterized in that described edge sealing stove can once heat one to the several piece plane two vacuum layer glass.
9. the preparation method of the two vacuum layer glass in plane according to claim 7, is characterized in that described edge sealing stove and accessory has basic heating system and local heating system.
10. the preparation method of the two vacuum layer glass in plane according to claim 9, it is characterized in that described basic heating system adopts one or several of Hot-blast Heating, resistive heating, Infrared Heating and far-infrared heating, described local heating system adopts the modes such as microwave heating or Infrared Heating.
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CN102951825A (en) * | 2012-10-06 | 2013-03-06 | 戴长虹 | Metal solder-welded and groove-edge-sealed planar vacuum glass and manufacturing method thereof |
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