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CN103351773A - Ultraviolet resistant heat dissipation coating and preparation method thereof - Google Patents

Ultraviolet resistant heat dissipation coating and preparation method thereof Download PDF

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Publication number
CN103351773A
CN103351773A CN2013102095088A CN201310209508A CN103351773A CN 103351773 A CN103351773 A CN 103351773A CN 2013102095088 A CN2013102095088 A CN 2013102095088A CN 201310209508 A CN201310209508 A CN 201310209508A CN 103351773 A CN103351773 A CN 103351773A
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CN
China
Prior art keywords
parts
diatomite
ultraviolet
powder
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN2013102095088A
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Chinese (zh)
Other versions
CN103351773B (en
Inventor
朱兴堂
朱亮亮
陈军彦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong dope paint Chemical Co., Ltd.
Original Assignee
BENGBU TIMES ELECTRONICS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BENGBU TIMES ELECTRONICS Co Ltd filed Critical BENGBU TIMES ELECTRONICS Co Ltd
Priority to CN201310209508.8A priority Critical patent/CN103351773B/en
Publication of CN103351773A publication Critical patent/CN103351773A/en
Application granted granted Critical
Publication of CN103351773B publication Critical patent/CN103351773B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The invention discloses an ultraviolet resistant heat dissipation coating and a preparation method thereof. The coating comprises 65-70 parts of a ketone-aldehyde resin, 2.0-2.5 parts of triethanolamine, 80-90 parts of methyl ethyl ketone, 5.0-5.5 parts of nanocarbon, 3.5-4.0 parts of tributyl citrate, 4.5-5.0 parts of ultramicro wax powder, 7.0-8.5 parts of methyl silicate, 0.5-0.7 parts of an ultraviolet ray absorber, 2.0-2.5 parts of calcium stearate, 0.9-1.1 parts of diatomite powder, 1.5-2.0 parts of bis-myristyl alcohol ester, 28-32 parts of aluminum nitride and 1-2 parts of butylmercaptooxo stannane. The preparation method adopts a reaction of the ultraviolet ray absorber with diatomite, bis-myristyl alcohol ester and butylmercaptooxo stannane, so the ultraviolet ray absorber is well attached to diatomite and can well absorb ultraviolet rays, thereby the ultraviolet resistance of the heat dissipation coating is improved; and the film of the coating has the advantages of good durability, good water resistance, good moisture resistance, good corrosion resistance and extremely good adhesiveness.

Description

A kind of anti-ultraviolet heat radiation coating and preparation method thereof
Technical field
The present invention relates to technical field of coatings, be specifically related to a kind of anti-ultraviolet heat radiation coating and preparation method thereof.
Background technology
Along with the rapid expansion of light fixture use range, prolong light fixture and also become urgent problem work-ing life; Adopt at present heat-conducting glue to solve the light fixture heat dissipation problem, but there is heatproof and ageing-resistant poor in its employed material, the technical problem little to the base material cohesive force, that radiating effect is not good and construction is inconvenient is difficult to satisfy people to the requirement of light fixture heat radiation.
Summary of the invention
The object of the present invention is to provide a kind of anti-ultraviolet heat radiation coating and preparation method thereof.
The present invention adopts following technical scheme:
A kind of anti-ultraviolet heat radiation coating is characterized in that the weight part of its constitutive material is: ketone resin 65-70, trolamine 2.0-2.5, methylethylketone 80-90, nano-sized carbon 5.0-5.5, tributyl citrate 3.5-4.0, ultra micro wax powder 4.5-5.0, methyl silicate 7.0-8.5, UV light absorber 0.5-0.7, calcium stearate 2.0-2.5, diatomite in powder 0.9-1.1, two ten four carbon alcohols ester 1.5-2.0 and aluminium nitride 28-32, butanethiol tin 1-2.
Described anti-ultraviolet heat radiation coating is characterized in that the weight part of its constitutive material is: ketone resin 68, trolamine 2.2, methylethylketone 85, nano-sized carbon 5.2, tributyl citrate 3.8, ultra micro wax powder 4.8, methyl silicate 7.8, UV light absorber 0.6, calcium stearate 2.2, diatomite in powder 1.0, two ten four carbon alcohols esters 1.8 and aluminium nitride 30, butanethiol tin 1.
The preparation method of described anti-ultraviolet heat radiation coating is characterized in that may further comprise the steps:
(1) tributyl citrate, diatomite in powder, UV light absorber, two ten four carbon alcohols esters, butanethiol tin are mixed, be heated to 70-80 ℃, stirring reaction 1-2 hour;
(2) weight part by constitutive material takes by weighing other residue constitutive material and step (1) mixing of materials such as ketone resin, stirs, when being ground to 40-50 μ m; Stop to grind packing.
Beneficial effect of the present invention:
The present invention adopts the reaction of UV light absorber and diatomite, two ten four carbon alcohols esters, butanethiol tin, so that UV light absorber is attached on the diatomite better, has better the absorbing ultraviolet function, improved the anti-ultraviolet property of heat radiation coating, the persistence of filming, water-fast, moisture-proof, good corrosion resistance, adhesion property is good.
During construction, the heat radiation coating spraying application 60 ℃ of lower oven dry 1 hour, gets final product film forming, makes 40-50 μ m heat radiation coating.
Embodiment
Embodiment 1: anti-ultraviolet heat radiation coating, the weight part of its constitutive material (kg) is: ketone resin 68, trolamine 2.2, methylethylketone 85, nano-sized carbon 5.2, tributyl citrate 3.8, ultra micro wax powder 4.8, methyl silicate 7.8, UV light absorber 0.6, calcium stearate 2.2, diatomite in powder 1.0, two ten four carbon alcohols esters 1.8 and aluminium nitride 30, butanethiol tin 1.
The preparation method is characterized in that may further comprise the steps:
(1) tributyl citrate, diatomite in powder, UV light absorber, two ten four carbon alcohols esters, butanethiol tin are mixed, be heated to 70-80 ℃, stirring reaction 1-2 hour;
(2) weight part by constitutive material takes by weighing other residue constitutive material and step (1) mixing of materials such as ketone resin, stirs, when being ground to 40-50 μ m; Stop to grind packing.
The heat radiation coating direct spraying that above-described embodiment 1 makes is in through on the glass lamp that cleans up, the heatproof test: behind the 210 ℃/3h of baking oven baking, the baking oven baking after 145 ℃/15 days glass lamp coat color and luster without considerable change; Uviolizing 3.8h, not shedding of coating is non-yellowing, artificial accelerated aging test under 135 ℃ and 270W ultraviolet light irradiation condition, 5280 hours ageing-resistant time, 245 ℃ of heatproof high temperature, bonding shearing force 20.7MPa, thermal conductivity 305W/(mK).

Claims (3)

1. an anti-ultraviolet heat radiation coating is characterized in that the weight part of its constitutive material is: ketone resin 65-70, trolamine 2.0-2.5, methylethylketone 80-90, nano-sized carbon 5.0-5.5, tributyl citrate 3.5-4.0, ultra micro wax powder 4.5-5.0, methyl silicate 7.0-8.5, UV light absorber 0.5-0.7, calcium stearate 2.0-2.5, diatomite in powder 0.9-1.1, two ten four carbon alcohols ester 1.5-2.0 and aluminium nitride 28-32, butanethiol tin 1-2.
2. anti-ultraviolet heat radiation coating according to claim 1 is characterized in that the weight part of its constitutive material is: ketone resin 68, trolamine 2.2, methylethylketone 85, nano-sized carbon 5.2, tributyl citrate 3.8, ultra micro wax powder 4.8, methyl silicate 7.8, UV light absorber 0.6, calcium stearate 2.2, diatomite in powder 1.0, two ten four carbon alcohols esters 1.8 and aluminium nitride 30, butanethiol tin 1.
3. the preparation method of an anti-ultraviolet heat radiation coating as claimed in claim 1 is characterized in that may further comprise the steps:
(1) tributyl citrate, diatomite in powder, UV light absorber, two ten four carbon alcohols esters, butanethiol tin are mixed, be heated to 70-80 ℃, stirring reaction 1-2 hour;
(2) weight part by constitutive material takes by weighing other residue constitutive material and step (1) mixing of materials such as ketone resin, stirs, when being ground to 40-50 μ m; Stop to grind packing.
CN201310209508.8A 2013-05-30 2013-05-30 A kind of anti-ultraviolet heat radiation coating and preparation method thereof Expired - Fee Related CN103351773B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310209508.8A CN103351773B (en) 2013-05-30 2013-05-30 A kind of anti-ultraviolet heat radiation coating and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310209508.8A CN103351773B (en) 2013-05-30 2013-05-30 A kind of anti-ultraviolet heat radiation coating and preparation method thereof

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CN103351773A true CN103351773A (en) 2013-10-16
CN103351773B CN103351773B (en) 2016-06-29

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103965732A (en) * 2014-05-09 2014-08-06 安徽猛牛彩印包装有限公司 Heat-dissipation coating containing nanometer diatomite
CN104293072A (en) * 2014-09-28 2015-01-21 芜湖县双宝建材有限公司 Flame-retardant and corrosion-resistant modified coating
CN107163836A (en) * 2017-07-11 2017-09-15 合肥东恒锐电子科技有限公司 The manufacture method of a kind of electronic equipment heat radiation coating
CN108250890A (en) * 2018-02-06 2018-07-06 合肥东恒锐电子科技有限公司 It is a kind of for heat radiation coating of electronic equipment and preparation method thereof
CN108530964A (en) * 2018-05-09 2018-09-14 合肥展游软件开发有限公司 A kind of heat radiation coating and preparation method thereof for electronic equipment casing
CN108641442A (en) * 2018-05-16 2018-10-12 合肥酷睿网络科技有限公司 A kind of heat radiation coating and preparation method thereof for server cabinet

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006094847A1 (en) * 2005-03-10 2006-09-14 Degussa Gmbh Aqueous printing ink compositions
CN1856556A (en) * 2004-02-03 2006-11-01 德古萨公司 Utilization of radiohardenable resins based on ketone and/or urea aldehyde resins
CN1942544A (en) * 2005-03-10 2007-04-04 德古萨公司 Aqueous coating substance compositions having an improved resistance to stoning
CN102516852A (en) * 2011-12-16 2012-06-27 新高电子材料(中山)有限公司 Weather-resistant and high thermal conductive coating, radiating solar rear panel and efficient solar cell panel
CN102993831A (en) * 2012-05-30 2013-03-27 北京世纪永峰防水材料有限公司 Metal roof heat-insulation waterproof paint

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1856556A (en) * 2004-02-03 2006-11-01 德古萨公司 Utilization of radiohardenable resins based on ketone and/or urea aldehyde resins
WO2006094847A1 (en) * 2005-03-10 2006-09-14 Degussa Gmbh Aqueous printing ink compositions
CN1942544A (en) * 2005-03-10 2007-04-04 德古萨公司 Aqueous coating substance compositions having an improved resistance to stoning
CN102516852A (en) * 2011-12-16 2012-06-27 新高电子材料(中山)有限公司 Weather-resistant and high thermal conductive coating, radiating solar rear panel and efficient solar cell panel
CN102993831A (en) * 2012-05-30 2013-03-27 北京世纪永峰防水材料有限公司 Metal roof heat-insulation waterproof paint

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103965732A (en) * 2014-05-09 2014-08-06 安徽猛牛彩印包装有限公司 Heat-dissipation coating containing nanometer diatomite
CN104293072A (en) * 2014-09-28 2015-01-21 芜湖县双宝建材有限公司 Flame-retardant and corrosion-resistant modified coating
CN104293072B (en) * 2014-09-28 2016-07-27 芜湖县双宝建材有限公司 A kind of fire-retardant corrosion-resistant modified coating
CN107163836A (en) * 2017-07-11 2017-09-15 合肥东恒锐电子科技有限公司 The manufacture method of a kind of electronic equipment heat radiation coating
CN108250890A (en) * 2018-02-06 2018-07-06 合肥东恒锐电子科技有限公司 It is a kind of for heat radiation coating of electronic equipment and preparation method thereof
CN108530964A (en) * 2018-05-09 2018-09-14 合肥展游软件开发有限公司 A kind of heat radiation coating and preparation method thereof for electronic equipment casing
CN108641442A (en) * 2018-05-16 2018-10-12 合肥酷睿网络科技有限公司 A kind of heat radiation coating and preparation method thereof for server cabinet

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C06 Publication
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C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Jiang Lingjun

Inventor before: Zhu Xingtang

Inventor before: Zhu Liangliang

Inventor before: Chen Junyan

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20180117

Address after: Xinhui District of Guangdong Province in 529000 in Luokeng town of Jiangmen City Jinfeng Industrial Development Zone (office building)

Patentee after: Guangdong dope paint Chemical Co., Ltd.

Address before: 233010 Bengbu high tech Development Zone, Anhui Province Road No. 555

Patentee before: Bengbu Times Electronics Co., Ltd.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160629

Termination date: 20200530