CN103202795A - Walnut peel hair dye and preparation method thereof - Google Patents
Walnut peel hair dye and preparation method thereof Download PDFInfo
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- CN103202795A CN103202795A CN 201310122237 CN201310122237A CN103202795A CN 103202795 A CN103202795 A CN 103202795A CN 201310122237 CN201310122237 CN 201310122237 CN 201310122237 A CN201310122237 A CN 201310122237A CN 103202795 A CN103202795 A CN 103202795A
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Abstract
The invention relates to a walnut peel hair dye and a preparation method thereof. The walnut peel hair dye comprises a solvent A, a solvent B and a solvent C matched in use. The solvent A comprises the components in percentage by weight as follows: 3-8% of cysteine, 0-3% of hydroxyethyl cellulose and deionized water. The solvent B comprises the components in percentage by weight as follows: 2-20% of ferric salt, 2-20% of ferrite, 2-20% of azone, 0.5-3% of sodium sulfite and deionized water. The solvent C comprises the components in percentage by weight as follows: 10-20% of walnut peel, 3-10% of gallnut, 1-4% of mulberry, 2-6% of Semen sesami nigrum, 0.5-2% of Angelica sinensis and deionized water. The hair dye provided by the invention has the beneficial effects that natural plant extracts are used as main components of the hair dye which does not contain chemical substances such as aniline, strong oxidant and the like and is natural and free from toxicity, so that blue-black and purple black of hair after application of some hair dyes are avoided. In addition, nutritional components are added to promote hair to absorb nutrition, so that the hair is more gentle and agreeable.
Description
Technical field
The present invention relates to the chemicals field, relate in particular to a kind of juglans dyeing hair agent and preparation method thereof.
Background technology
At present, the dyeing hair agent has become the highest product of sales volume in the cosmetic field, and the retail sales in global hair dye every year is more than 7,000,000,000 dollars.At present, China silver hair consumer group is nearly 6,000 ten thousand, and along with the aging of Chinese people mouth structure, its quantity also will further enlarge, and therefore, domestic hair dye market is also increased rapidly in recent years.
At present, most of hair dyes are oxide hair dye, and its primary raw material is p-phenylenediamine (PPD) chemical compound and Benzodiazepines compounds, through the oxidation of hydrogen peroxide or perborate or percarbonate etc., thus colors such as demonstration black.But oxidative hair dyes has certain infringement to hair owing to contain toxic chemical substance, and irritated easily, causes discomforts such as red swelling of the skin, twinge, life-time service even can cause canceration.
Therefore, in recent years, nontoxic natural plant dyeing agent has become people's research and development focus.For example, US4801302 disclosed a kind of hair dye that contains Lignum Sappan and mantoquita on January 31st, 1989; It is the hair dye of dyestuff with the red sorghum pigment that CN120999ZA has introduced a kind of; CN101167689A has introduced a kind of with the formulated hair dye of Chinese herbal medicine such as Galla Chinensis, Melanteritum, Radix Polygoni Multiflori, Fructus Mori and Chinese liquor; CN101164528A has introduced a kind of natural hair dye that adopts the preparation of plant pigment catechu.Adopt these hair dye non-toxic and safe, but also exist the pigment dye-uptake low, not wash resistant, color and luster the nature etc. shortcoming.
Summary of the invention
The purpose of this invention is to provide a kind of juglans dyeing hair agent and preparation method thereof, to overcome at present existing hair dye above shortcomings.
The objective of the invention is to be achieved through the following technical solutions:
The agent of a kind of juglans dyeing hair is raw material with the natural plants, comprises matching used A solvent, B solvent and C solvent, and the A solvent is Reducing agent, and the B solvent is developer, and the C solvent is pigment agent; Described A solvent comprises following component by mass percent: cysteine 3～8%, hydroxyethyl-cellulose 0～3% and deionized water, and it is 8～12 that described A solvent is regulated pH by sodium hydroxide; Described B solvent comprises following component by mass percent: iron salt 2～20%, ferrous salt 2～20%, azone 2～20%, sodium sulfite 0.5～3% and deionized water; Described C solvent comprises following component by mass percent: juglans 10～20%, Galla Chinensis 3～10%, Fructus Mori 1～4%, Semen Sesami Nigrum 2～6%, Radix Angelicae Sinensis 0.5～2% and deionized water.
Further, the cysteine described in the A solvent can be replaced by TGA.
Further, the iron salt described in the B solvent is iron chloride, iron sulfate or ferric nitrate; Ferrous salt described in the B solvent is ferrous chloride, ferrous sulfate or ferrous nitrate.
Further, can add hydroxyethyl-cellulose in the B solvent is thickening agent.
The preparation method of above-mentioned juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: cysteine, sodium hydroxide, hydroxyethyl-cellulose are mixed, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron salt, ferrous salt, azone and sodium sulfite are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Beneficial effect of the present invention is: it is the hair dye main component that the present invention adopts natural plant extracts, does not contain chemical substances such as phenyl amines, strong oxidizer, Nantural non-toxic.The hair dye that the present invention makes can infiltrate hair preferably, and dyeing speed is very fast, and dye-uptake is greater than 30%; Washing fastness is good, can anti-ly soap about 10 times after dying; Dye the back color development and be nature black, present blue-black, purple phenomenon such as black after effectively having avoided some hair dye to dye; And owing to added nutritional labeling, promote hair to absorb nutrition, make hair quality submissiveer.
The specific embodiment
The agent of the described a kind of juglans dyeing hair of the embodiment of the invention is raw material with the natural plants, comprises matching used A solvent, B solvent and C solvent, and the A solvent is Reducing agent, and the B solvent is developer, and the C solvent is pigment agent; Described A solvent comprises following component by mass percent: cysteine 3～8%, hydroxyethyl-cellulose 0～3% and deionized water, and it is 8～12 that described A solvent is regulated pH by sodium hydroxide; Described B solvent comprises following component by mass percent: iron salt 2～20%, ferrous salt 2～20%, azone 2～20%, sodium sulfite 0.5～3% and deionized water; Described C solvent comprises following component by mass percent: juglans 10～20%, Galla Chinensis 3～10%, Fructus Mori 1～4%, Semen Sesami Nigrum 2～6%, Radix Angelicae Sinensis 0.5～2% and deionized water.Cysteine described in the A solvent can be replaced by TGA.Iron salt described in the B solvent is iron chloride, iron sulfate or ferric nitrate; Ferrous salt described in the B solvent is ferrous chloride, ferrous sulfate or ferrous nitrate.Can add hydroxyethyl-cellulose in the B solvent is thickening agent.
The preparation method of above-mentioned juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: cysteine, sodium hydroxide, hydroxyethyl-cellulose are mixed, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron salt, ferrous salt, azone and sodium sulfite are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Embodiment 1
Embodiment 1 described juglans dyeing hair agent, described A solvent comprises following component by mass percent: cysteine 3%, TGA 2%,, hydroxyethyl-cellulose 2%, an amount of sodium hydroxide and deionized water; Described B solvent comprises following component by mass percent: iron chloride 2%, ferrous chloride 2%, azone 2% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 5%, Fructus Mori 1%, Semen Sesami Nigrum 2%, Radix Angelicae Sinensis 0.5% and appropriate amount of deionized water.
The preparation method of embodiment 1 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: cysteine, TGA, sodium hydroxide, hydroxyethyl-cellulose are mixed, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron chloride, ferrous chloride, azone are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
Embodiment 2
Embodiment 2 described juglans dyeing hair agent, described A solvent comprises following component by mass percent: cysteine 5% and deionized water; Described B solvent comprises following component by mass percent: iron sulfate 5%, ferrous chloride 10%, azone 10%, hydroxyethyl-cellulose 0.5% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 10%, Fructus Mori 2%, Semen Sesami Nigrum 3%, Radix Angelicae Sinensis 0.5% and appropriate amount of deionized water.
The preparation method of embodiment 2 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: get cysteine, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron sulfate, ferrous chloride, hydroxyethyl-cellulose, azone are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
Embodiment 3
Embodiment 3 described juglans dyeing hair agent, described A solvent comprises following component by mass percent: cysteine 8% and deionized water; Described B solvent comprises following component by mass percent: iron sulfate 10%, ferrous nitrate 8%, azone 5%, hydroxyethyl-cellulose 1% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 8%, Fructus Mori 4%, Semen Sesami Nigrum 5%, Radix Angelicae Sinensis 1% and appropriate amount of deionized water.
The preparation method of embodiment 3 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: get cysteine, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron sulfate, ferrous nitrate, hydroxyethyl-cellulose, azone are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
Embodiment 4
Embodiment 4 described juglans dyeing hair agent, described A solvent comprises following component by mass percent: cysteine 7% and deionized water; Described B solvent comprises following component by mass percent: ferric nitrate 15%, ferrous sulfate 10%, azone 12% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 8%, Fructus Mori 2%, Semen Sesami Nigrum 5%, Radix Angelicae Sinensis 1% and appropriate amount of deionized water.
The preparation method of embodiment 4 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: get cysteine, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: ferric nitrate, ferrous sulfate, azone are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
Embodiment 5
Embodiment 5 described juglans dyeing hair agent, described A solvent comprises following component by mass percent: TGA 5% and deionized water; Described B solvent comprises following component by mass percent: ferric nitrate 5%, ferrous chloride 12%, azone 10%, hydroxyethyl-cellulose 2% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 7%, Fructus Mori 3%, Semen Sesami Nigrum 6%, Radix Angelicae Sinensis 1.5% and appropriate amount of deionized water.
The preparation method of embodiment 5 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: get TGA, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: ferric nitrate, ferrous chloride, azone, hydroxyethyl-cellulose are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
Embodiment 6
Embodiment 6 described juglans dyeing hair agent are raw material with the natural plants, and described A solvent comprises following component by mass percent: TGA 5% and deionized water; Described B solvent comprises following component by mass percent: ferric nitrate 2%, ferrous nitrate 8%, azone 5%, hydroxyethyl-cellulose 0.5% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 9%, Fructus Mori 1%, Semen Sesami Nigrum 3%, Radix Angelicae Sinensis 0.5% and appropriate amount of deionized water.
The preparation method of embodiment 6 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: get TGA, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: ferric nitrate, ferrous nitrate, azone, hydroxyethyl-cellulose are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
Embodiment 7
Embodiment 7 described juglans dyeing hair agent, described A solvent comprises following component by mass percent: sodium hydroxide 3% and deionized water; Described B solvent comprises following component by mass percent: iron chloride 20%, ferrous sulfate 2%, azone 2%, hydroxyethyl-cellulose 0.5% and appropriate amount of deionized water; Described C solvent comprises following component by mass percent: juglans 15%, Galla Chinensis 10%, Fructus Mori 2%, Semen Sesami Nigrum 5%, Radix Angelicae Sinensis 1% and appropriate amount of deionized water.
The preparation method of embodiment 7 described juglans dyeing hair agent may further comprise the steps:
(1) preparation of A solvent: get sodium hydroxide, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron chloride, ferrous sulfate, azone, hydroxyethyl-cellulose are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Earlier the A agent evenly is applied on the hair with small brushes, leaves standstill under the room temperature about 10 minutes; Again the B agent evenly is applied in hair, at room temperature left standstill 8-10 minute, can suitably heat hair or prolong time of repose if room temperature is low, with residual A agent and the B agent of clear water flush away; Then the C agent evenly is applied on the hair with small brushes etc. equally, leaves standstill under the room temperature about 10 minutes, hair is namely dyed black, and color and luster nature, hair quality are submissive, clean residual medicament with clear water and get final product.Use amount: general 10 centimetres are used each 25 milliliters of A, B, C agent with interior bob, and 30 centimetres of left and right sides long hairs respectively use 70 milliliters.
The present invention is not limited to above-mentioned preferred forms; anyone can draw other various forms of products under enlightenment of the present invention; no matter but do any variation in its shape or structure; every have identical with a application or akin technical scheme, all drops within protection scope of the present invention.
Claims (6)
1. juglans dyeing hair agent, comprise matching used A solvent, B solvent and C solvent, the A solvent is Reducing agent, the B solvent is developer, the C solvent is pigment agent, it is characterized in that: described A solvent comprises following component by mass percent: cysteine 3～8%, hydroxyethyl-cellulose 0～3% and deionized water, and it is 8～12 that described A solvent is regulated pH by sodium hydroxide; Described B solvent comprises following component by mass percent: iron salt 2～20%, ferrous salt 2～20%, azone 2～20%, sodium sulfite 0.5～3% and deionized water; Described C solvent comprises following component by mass percent: juglans 10～20%, Galla Chinensis 3～10%, Fructus Mori 1～4%, Semen Sesami Nigrum 2～6%, Radix Angelicae Sinensis 0.5～2% and deionized water.
2. juglans dyeing hair according to claim 1 agent is characterized in that: the cysteine described in the A solvent can be replaced by TGA.
3. juglans dyeing hair according to claim 1 agent is characterized in that: the iron salt described in the B solvent is iron chloride, iron sulfate or ferric nitrate.
4. juglans dyeing hair according to claim 3 agent is characterized in that: the ferrous salt described in the B solvent is ferrous chloride, ferrous sulfate or ferrous nitrate.
5. juglans dyeing hair according to claim 4 agent is characterized in that: adding hydroxyethyl-cellulose in the B solvent is thickening agent.
6. the preparation method of each described juglans dyeing hair agent of claim 1-5 is characterized in that, may further comprise the steps:
(1) preparation of A solvent: cysteine, sodium hydroxide, hydroxyethyl-cellulose are mixed, add deionized water to 100% again, be stirred to dissolving fully, treat to check, pack after the room temperature;
(2) preparation of B solvent: iron salt, ferrous salt, azone and sodium sulfite are mixed, add deionized water to 100% then, heat to 40 ℃, be stirred to and be dissolved into transparent homogeneous system fully, be cooled to room temperature then, check at last, pack;
(3) preparation of C solvent: natural plants juglans, Galla Chinensis, Fructus Mori, Semen Sesami Nigrum, Radix Angelicae Sinensis are evenly mixed, pulverize, add deionized water with its submergence, heat to 40～60 ℃, stirred 24 hours, filter and remove residue adds deionized water to 100% then while stirring in filtrate, be cooled to room temperature, check at last, pack.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
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| CN 201310122237 CN103202795A (en) | 2013-04-10 | 2013-04-10 | Walnut peel hair dye and preparation method thereof |
| CN201310354928.5A CN103494753A (en) | 2013-04-10 | 2013-08-15 | Black mulberry hair dye and preparation method thereof |
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| CN 201310122237 CN103202795A (en) | 2013-04-10 | 2013-04-10 | Walnut peel hair dye and preparation method thereof |
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| CN103202795A true CN103202795A (en) | 2013-07-17 |
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| CN201310354928.5A Pending CN103494753A (en) | 2013-04-10 | 2013-08-15 | Black mulberry hair dye and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103494753A (en) * | 2013-04-10 | 2014-01-08 | 济南益正生物科技有限公司 | Black mulberry hair dye and preparation method thereof |
| CN104800108A (en) * | 2014-11-20 | 2015-07-29 | 折改梅 | Preparation of constituents of cortex juglandis mandshuricae and manufacturing method of different-colored hair dyes |
| CN105411980A (en) * | 2015-12-21 | 2016-03-23 | 岳双辰 | Black mulberry hair dye and preparation method thereof |
| CN107412133A (en) * | 2017-08-13 | 2017-12-01 | 新疆农业科学院海南三亚农作物育种试验中心 | A kind of pure natural hair dye and its compound method, hair colouring methods |
| CN110025537A (en) * | 2019-05-21 | 2019-07-19 | 华中农业大学 | A kind of Shell of Water Chestnut hair dye and preparation method thereof |
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| CN105062724A (en) * | 2015-08-11 | 2015-11-18 | 理想科技集团有限公司 | Plant hair-dyeing tea soap and preparation method thereof |
| CN106176558A (en) * | 2016-09-28 | 2016-12-07 | 广西大学 | Pure natural black hair conditioner and preparation method thereof |
| CN108514525A (en) * | 2018-04-20 | 2018-09-11 | 安徽大学 | Disposable color hair care and hair dyeing gel and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101543550A (en) * | 2009-05-06 | 2009-09-30 | 陈传淑 | Traditional Chinese medicine liniment for treating white hair |
| CN101972222B (en) * | 2010-11-03 | 2011-09-21 | 宁夏欣发宝养发有限公司 | Hair-care liquid and preparation method thereof |
| CN103202795A (en) * | 2013-04-10 | 2013-07-17 | 济南益正生物科技有限公司 | Walnut peel hair dye and preparation method thereof |
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2013
- 2013-04-10 CN CN 201310122237 patent/CN103202795A/en active Pending
- 2013-08-15 CN CN201310354928.5A patent/CN103494753A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103494753A (en) * | 2013-04-10 | 2014-01-08 | 济南益正生物科技有限公司 | Black mulberry hair dye and preparation method thereof |
| CN104800108A (en) * | 2014-11-20 | 2015-07-29 | 折改梅 | Preparation of constituents of cortex juglandis mandshuricae and manufacturing method of different-colored hair dyes |
| CN104800108B (en) * | 2014-11-20 | 2018-04-10 | 折改梅 | The preparation of pericarpium juglandis pigment composition and its preparation method of multi-color system hair dye |
| CN105411980A (en) * | 2015-12-21 | 2016-03-23 | 岳双辰 | Black mulberry hair dye and preparation method thereof |
| CN107412133A (en) * | 2017-08-13 | 2017-12-01 | 新疆农业科学院海南三亚农作物育种试验中心 | A kind of pure natural hair dye and its compound method, hair colouring methods |
| CN110025537A (en) * | 2019-05-21 | 2019-07-19 | 华中农业大学 | A kind of Shell of Water Chestnut hair dye and preparation method thereof |
| CN110025537B (en) * | 2019-05-21 | 2022-04-01 | 华中农业大学 | Water chestnut shell hair dye and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103494753A (en) | 2014-01-08 |
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Application publication date: 20130717 |