CN103084133A - Acidification reaction device - Google Patents
Acidification reaction device Download PDFInfo
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- CN103084133A CN103084133A CN2013100547343A CN201310054734A CN103084133A CN 103084133 A CN103084133 A CN 103084133A CN 2013100547343 A CN2013100547343 A CN 2013100547343A CN 201310054734 A CN201310054734 A CN 201310054734A CN 103084133 A CN103084133 A CN 103084133A
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- heat collector
- acidification
- pipe
- acidifying still
- valve
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
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Abstract
The invention discloses an acidification reaction device, comprising an acidification kettle, and a heat collector, wherein a feeding tube and a discharge tube are arranged on the acidification kettle; the feeding tube extends into the kettle from the top part of the acidification kettle; the discharge tube is connected and fixed to the lateral wall of the acidification kettle; the acidification kettle for continuous reaction is provided with a feeding branch pipe extending inside from the top part of the acidification kettle; a valve is arranged on the feeding branch pipe outside the acidification kettle; a speed controller is arranged on the discharge tube; one end of the heat collector is connected to a saponin supply device; the other end is connected to the acidification kettle via the feeding tube; the heat collector is provided with a steam pipe penetrating through the heat collector; and a waste water recovery device is connected to a downstream of the steam pipe. The acidification reaction device has the beneficial effects that lasting acidification reaction can be achieved; the reaction material is preheated in advance; and the production efficiency is improved.
Description
Technical field
The present invention relates to a kind of reaction unit, especially the acidification reaction device.
Background technology
Traditional acidification oil production is all that soap stock is first squeezed into the acidifying still, then begins heating, and squeezes into sulfuric acid, after temperature reaches reaction temperature, stirs certain hour, until react completely.Then reactant liquor is squeezed into the layering groove, standing minute desulfuration acid waste water, then dehydration.There are the shortcomings such as reaction efficiency is low, production is discontinuous, pollution is large in such device, does not meet the requirement of present energy-conserving and environment-protective.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of acidification reaction device, can realize continuing acidification reaction, and reaction material is shifted to an earlier date preheating, enhances productivity.
The present invention is achieved through the following technical solutions.
a kind of acidification reaction device, comprise the acidifying still, heat collector, above-mentioned acidifying still is provided with feed pipe and discharge nozzle, above-mentioned feed pipe is stretched in still by acidifying still top, above-mentioned discharge nozzle is fastened on above-mentioned acidifying still sidewall, the acidifying still of above-mentioned successive reaction is provided with the feed-inputing branched pipe that is stretched into by acidifying still top, and above-mentioned feed-inputing branched pipe is positioned at above-mentioned acidifying still and is outside equipped with valve, above-mentioned discharge nozzle is provided with speed control, above-mentioned heat collector one end connecting pipe is to the Chinese honey locust feeding mechanism, the other end connects above-mentioned feed pipe to the acidifying still, above-mentioned heat collector is provided with the steam pipe that runs through above-mentioned heat collector, the downstream of above-mentioned steam pipe connects waste water reclaiming device.
Further, above-mentioned discharge nozzle is provided with branched pipe, and above-mentioned branched pipe is provided with valve.
Further, the above-mentioned heat collector install pipeline that is connected to above-mentioned acidifying still has valve.
Further, two sections outside above-mentioned steam pipe heat collector in place are provided with valve.
Beneficial effect of the present invention:
After feed pipe is sent reaction mass into the acidifying still and be in when stopping feed status, by feed-inputing branched pipe is set, the speed control unit that coordinates again discharge nozzle to arrange, can realize continuing feeding, production is carried out always continuously, obviously like this shorten the reaction time, improved utilization rate of equipment and installations, improved exactly production efficiency; Simultaneously, be provided with the branch of valve at discharge nozzle, can open valve, at any time the discharging thing is detected, to guarantee the quality of production;
By heat collector and the steam pipe that runs through heat collector are set outside the acidifying still, the heat of steam in steam pipe can be conducted conversion to the Chinese honey locust in heat collector by heat, played and in advance Chinese honey locust has been carried out the effect of preheating, improved the efficient in the acidifying still; Simultaneously, also can use the steam that other operations produce, realize the recycling of energy, provide cost savings.
Description of drawings
Fig. 1 is the structural representation of acidification reaction device of the present invention.
The specific embodiment
The below is described in further detail the present invention according to drawings and embodiments.
Fig. 1 is the structural representation of acidification reaction device of the present invention, with reference to Fig. 1, the present invention, the acidification reaction device comprises acidifying still 1, heat collector 2, acidifying still 1 is provided with feed pipe 11, discharge nozzle 12, feed-inputing branched pipe 13, feed pipe 11 is stretched in still by acidifying still 1 top, and discharge nozzle 12 is fastened on acidifying still 1 sidewall, and feed-inputing branched pipe 13 is stretched at acidifying still 1 top, and feed-inputing branched pipe 13 is positioned at acidifying still 1 and is outside equipped with valve 130, and discharge nozzle 12 is provided with speed control 14.
When the acidifying still is in running order, the valve 130 of feed-inputing branched pipe 13 first is in closed condition, when feed pipe 11 is completed the conveying task, and be in when stopping carrying the reaction mass state, open valve 130, continue reaction mass is inputted acidifying still 1, in addition, by governing speed controller 14, control the discharging speed of discharge nozzle 12, Comprehensive Control is adjusted, and realizes the sustained response of acidifying still.
In the implementation case, discharge nozzle 12 is provided with branched pipe 121, and branched pipe 121 is provided with valve 122.
Comprise heat collector 2, heat collector 2 one end connecting pipes 21 are to Chinese honey locust feeding mechanism (not shown), and the other end connects feed pipe 11 to acidifying still 1, and heat collector 2 arranges steam pipe 3, steam pipe 3 runs through heat collector 2, and the downstream of steam pipe 3 connects the waste water reclaiming device (not shown).
In the implementation case, the feed pipe 11 that heat collector 2 is connected to acidifying still 1 is provided with valve 110.If in the time of can not reaching the temperature requirement of Chinese honey locust in the acidifying still to the preheating of Chinese honey locust in heat collector 2, can first valve 110 be closed, make the Chinese honey locust in heat collector 2 continue preheating, to meet the requirement of 1 pair of Chinese honey locust temperature of acidifying still, open valve 110, the Chinese honey locust that temperature is qualified is sent into acidifying still 1 by feed pipe 11 again.
In the implementation case, two sections outside steam pipe 3 heat collector 2 in place are provided with valve, are respectively valve 31 and valve 32.By the switch of valve 31 and valve 32, also can make certain adjustment to the Chinese honey locust preheating in heat collector 2.
The present invention, the acidification reaction device, after feed pipe is sent reaction mass into the acidifying still and be in when stopping feed status, by feed-inputing branched pipe is set, then the speed control unit that coordinates discharge nozzle to arrange, can realize continuing feeding, production is carried out always continuously, obviously like this shorten the reaction time, improved utilization rate of equipment and installations, improved exactly production efficiency; Simultaneously, be provided with the branch of valve at discharge nozzle, can open valve, at any time the discharging thing is detected, to guarantee the quality of production;
By heat collector and the steam pipe that runs through heat collector are set outside the acidifying still, the heat of steam in steam pipe can be conducted conversion to the Chinese honey locust in heat collector by heat, played and in advance Chinese honey locust has been carried out the effect of preheating, improved the efficient in the acidifying still; Simultaneously, also can use the steam that other operations produce, realize the recycling of energy, provide cost savings.
Above-described embodiment only is explanation technical conceive of the present invention and characteristics, and its purpose is to allow the personage who is familiar with this art can understand content of the present invention and be implemented, and can not limit protection scope of the present invention with this.All equivalences that Spirit Essence is done according to the present invention change or modify, and all should be encompassed in protection scope of the present invention.
Claims (4)
1. acidification reaction device, comprise the acidifying still, heat collector, described acidifying still is provided with feed pipe and discharge nozzle, described feed pipe is stretched in still by acidifying still top, described discharge nozzle is fastened on described acidifying still sidewall, it is characterized in that, the acidifying still of described successive reaction is provided with the feed-inputing branched pipe that is stretched into by acidifying still top, and described feed-inputing branched pipe is positioned at described acidifying still and is outside equipped with valve, described discharge nozzle is provided with speed control, described heat collector one end connecting pipe is to the Chinese honey locust feeding mechanism, the other end connects described feed pipe to the acidifying still, described heat collector is provided with the steam pipe that runs through described heat collector, the downstream of described steam pipe connects waste water reclaiming device.
2. acidification reaction device according to claim 1, is characterized in that, described discharge nozzle is provided with branched pipe, and described branched pipe is provided with valve.
3. acidification reaction device according to claim 1, is characterized in that, the install pipeline that described heat collector is connected to described acidifying still has valve.
4. acidification reaction device according to claim 1, is characterized in that, two sections outside described steam pipe heat collector in place are provided with valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013100547343A CN103084133A (en) | 2013-02-20 | 2013-02-20 | Acidification reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013100547343A CN103084133A (en) | 2013-02-20 | 2013-02-20 | Acidification reaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103084133A true CN103084133A (en) | 2013-05-08 |
Family
ID=48197565
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013100547343A Pending CN103084133A (en) | 2013-02-20 | 2013-02-20 | Acidification reaction device |
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| Country | Link |
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| CN (1) | CN103084133A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108285426A (en) * | 2017-10-30 | 2018-07-17 | 赵君 | A kind of continuously acidizing device and its technique |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB777413A (en) * | 1954-09-02 | 1957-06-19 | Sharples Corp | Improvements relating to processes for the production of fatty acids |
| GB787715A (en) * | 1955-02-25 | 1957-12-11 | Separator Ab | Method for the recovery of free fatty and/or resinous acids from an aqueous solution of soap |
| US3428660A (en) * | 1964-01-20 | 1969-02-18 | Baker Perkins Inc | Process for recovering fatty acids and triglyceride oil from soapstock |
| DE2639596A1 (en) * | 1975-09-04 | 1977-03-17 | Unilever Nv | METHOD AND DEVICE FOR NEUTRALIZING A SOAP SOLUTION |
| US4118407A (en) * | 1977-01-06 | 1978-10-03 | Scm Corporation | Fatty acid recovery from soapstock |
| CN2239433Y (en) * | 1996-01-26 | 1996-11-06 | 张兆海 | Novel device for recovering residual oil from soapstock of vegetable oil plant |
| WO2001072934A1 (en) * | 2000-03-24 | 2001-10-04 | Kru Feed Energy Company | Method for soapstock acidulation |
| CN202519227U (en) * | 2012-04-10 | 2012-11-07 | 浙江卓尚环保能源有限公司 | Oil residue treating and oil-extracting device |
| CN203184008U (en) * | 2013-02-20 | 2013-09-11 | 安徽天意环保科技有限公司 | Acidification reaction device |
-
2013
- 2013-02-20 CN CN2013100547343A patent/CN103084133A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB777413A (en) * | 1954-09-02 | 1957-06-19 | Sharples Corp | Improvements relating to processes for the production of fatty acids |
| GB787715A (en) * | 1955-02-25 | 1957-12-11 | Separator Ab | Method for the recovery of free fatty and/or resinous acids from an aqueous solution of soap |
| US3428660A (en) * | 1964-01-20 | 1969-02-18 | Baker Perkins Inc | Process for recovering fatty acids and triglyceride oil from soapstock |
| DE2639596A1 (en) * | 1975-09-04 | 1977-03-17 | Unilever Nv | METHOD AND DEVICE FOR NEUTRALIZING A SOAP SOLUTION |
| US4118407A (en) * | 1977-01-06 | 1978-10-03 | Scm Corporation | Fatty acid recovery from soapstock |
| CN2239433Y (en) * | 1996-01-26 | 1996-11-06 | 张兆海 | Novel device for recovering residual oil from soapstock of vegetable oil plant |
| WO2001072934A1 (en) * | 2000-03-24 | 2001-10-04 | Kru Feed Energy Company | Method for soapstock acidulation |
| CN202519227U (en) * | 2012-04-10 | 2012-11-07 | 浙江卓尚环保能源有限公司 | Oil residue treating and oil-extracting device |
| CN203184008U (en) * | 2013-02-20 | 2013-09-11 | 安徽天意环保科技有限公司 | Acidification reaction device |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108285426A (en) * | 2017-10-30 | 2018-07-17 | 赵君 | A kind of continuously acidizing device and its technique |
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Application publication date: 20130508 |