CN102433594A - Production method of bamboo fiber - Google Patents
Production method of bamboo fiber Download PDFInfo
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- CN102433594A CN102433594A CN2011102917882A CN201110291788A CN102433594A CN 102433594 A CN102433594 A CN 102433594A CN 2011102917882 A CN2011102917882 A CN 2011102917882A CN 201110291788 A CN201110291788 A CN 201110291788A CN 102433594 A CN102433594 A CN 102433594A
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- bamboo
- bamboo fibre
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- fiber
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- 235000017166 Bambusa arundinacea Nutrition 0.000 title claims abstract description 92
- 235000017491 Bambusa tulda Nutrition 0.000 title claims abstract description 92
- 235000015334 Phyllostachys viridis Nutrition 0.000 title claims abstract description 92
- 241001330002 Bambuseae Species 0.000 title claims abstract description 90
- 239000011425 bamboo Substances 0.000 title claims abstract description 90
- 239000000835 fiber Substances 0.000 title claims abstract description 77
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 23
- 239000002023 wood Substances 0.000 claims abstract description 20
- 238000012545 processing Methods 0.000 claims abstract description 18
- 238000004061 bleaching Methods 0.000 claims abstract description 15
- 238000001035 drying Methods 0.000 claims abstract description 7
- 108090000790 Enzymes Proteins 0.000 claims abstract description 5
- 102000004190 Enzymes Human genes 0.000 claims abstract description 5
- 239000000243 solution Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
- 239000007844 bleaching agent Substances 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- 229940088598 enzyme Drugs 0.000 claims description 4
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 claims description 4
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 claims description 3
- 108010059892 Cellulase Proteins 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 239000003599 detergent Substances 0.000 claims description 3
- 238000010790 dilution Methods 0.000 claims description 3
- 239000012895 dilution Substances 0.000 claims description 3
- 229940059442 hemicellulase Drugs 0.000 claims description 3
- 108010002430 hemicellulase Proteins 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 230000035939 shock Effects 0.000 claims description 3
- 241000894006 Bacteria Species 0.000 abstract description 4
- 239000004566 building material Substances 0.000 abstract description 3
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- 230000035699 permeability Effects 0.000 abstract description 3
- 239000004753 textile Substances 0.000 abstract description 3
- 238000004332 deodorization Methods 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000005520 cutting process Methods 0.000 abstract 1
- 238000003795 desorption Methods 0.000 abstract 1
- 238000009991 scouring Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 241000209128 Bambusa Species 0.000 description 2
- 238000003754 machining Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000005213 imbibition Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention relates to a production method of bamboo fiber, which comprises the steps of cutting, softening, fiber opening, scouring, bleaching, cleaning, dehydrating, drying, enzyme treatment and the like. The splitting separator fully exerts the optimal splitting point of the softened bamboo wood, can adjust mechanical processing parameters according to the requirements to obtain different fiber slenderness ratios, enables the processed bamboo fiber to be thinner and more uniform than the original bamboo fiber, and has the advantages of reliable production process, high resource utilization rate, low processing cost, small environmental pollution and stable product quality. The refined bamboo fiber produced by the invention has the advantages of uniform length and fineness, high strength, good flexibility, strong moisture absorption and desorption property and air permeability of the fiber, and particularly outstanding bacterium deodorization performance, is a new generation of natural functional fiber with low price, high quality and superior cost performance, and can be widely applied to the fields of textiles, building materials, automobiles and the like.
Description
Technical field
The present invention relates to field of textiles, relate in particular to a kind of production method of bamboo fibre.
Background technology
Bamboo fibre is a kind of cellulose fibre that from the bamboo of self-sow, extracts, and is the fifth-largest natural fabric after cotton, fiber crops, hair, silk.Bamboo fibre has good gas property, moment water imbibition, stronger ABRASION RESISTANCE and the good characteristics such as dyeability selected, have again simultaneously natural Hangzhoupro bacterium, antibacterial, remove end, deodorization and anti-ultraviolet function.The expert points out that bamboo fibre is a kind of natural environmental-protective type green fiber truly.
But up to now; Operations such as the production of bamboo fibre is adopted intercept, burst basically, goes green grass or young crops, removed Huang, boiling, pressure rolling well-thought-out plan tow have broken away from not the technology that XianCheng's bamboo chip becomes bamboo fiber bundle again, and its process technology is more backward; Production efficiency is low; The process equipment function singleness, the rapidoprint waste is serious, can't process to realize high-efficiency large-scale production whole bamboo or bamboo leftover pieces.And the critical process among the present preparation method is underused the design feature of bamboo wood; Its processing choose opportunities is improper, implements to open fibre at the best mechanics performance point of bamboo wood, and the bamboo fibre technology that becomes more meticulous is unreasonable; The bamboo fibre of being produced is of poor quality; Fiber is thick, short, hard, the requirement that indexs such as the fiber uniformity, length, fineness, intensity not only do not reach textile fiber, even can't satisfy the requirement for preparing composite, nonwoven material.
Summary of the invention
In order to overcome above defective, the technical problem that the present invention will solve is: propose that a kind of production efficiency is high, processing cost is low, the production method of the stay-in-grade bamboo fibre of bamboo fibre.
The technical scheme that the present invention adopted is: a kind of production method of bamboo fibre comprises the steps:
One, cuts off:, again bamboo wood is cut into the little bamboo chip of designated length with mechanical shock and compressor squeezing;
Two, soften: the bamboo wood that cuts is sent in the bating liquor that softens the pond softened;
Three, open fibre, classification, screening: bamboo wood is delivered to out fine seperator realize that fine separation is separated, opened to comb, air-flow is classified, obtain the bamboo filamentary fibers, utilize vibrating screen that the powder of bamboo filamentary fibers is removed again;
Four, kiering: adopt autoclave that above-mentioned little bamboo chip is carried out the softening processing of autoclaving, pressure is 5-6 atmospheric pressure, and temperature is between 155-175 ℃, and the processing time is 1-3 hour;
Five, clean, dewater: the bamboo filamentary fibers after will bleaching drains, and cleans to pH value 6-7 with the dilution heat of sulfuric acid that contains 0.1-0.2% then, cleans the back dehydration with clear water again;
Six, dewatered drying: the bamboo fibre after will washing dewaters with mechanical drying mode or vacuum mode or plate pressure mode, sends in the drier oven dry or under sunshine, dries naturally, and oven dry back bamboo fibre moisture is 5-25%;
Seven, enzyme is handled: with shower nozzle pectase evenly is sprayed onto on the bamboo filamentary fibers.
According to another preferred embodiment; A kind of production method of bamboo fibre comprises that further softening the processing is that bamboo wood is put into softening pond in the step 2, adds the solution that contains alkali or liquefied ammonia and soaks, and solution concentration is 1-5%; Liquid level exceeds bamboo wood 1-3 millimeter, and soak time is 10-15 hour.
According to another preferred embodiment, a kind of production method of bamboo fibre comprises that further it is one or more the mixture in the 2-8g/l hemicellulase that bating liquor in the said softening processing can be selected the pectase of concentration 1-10g/l, lignoenzyme that concentration is 1-20g/l, cellulase, concentration that concentration is 1-30g/l for use.
According to another preferred embodiment; A kind of production method of bamboo fibre further comprises and also comprises the detergent bleach operation between said step 4 and the step 5: bamboo fibre is put into sink after the clear water washing; Send in the Bellmer and under agitation bleach, wash with clear water once more with bleaching liquid.
According to another preferred embodiment; A kind of production method of bamboo fibre comprises that further said bleaching liquid selects calcium hypochlorite solution or liquor natrii hypochloritis, postassium hypochlorite solution for use; The concentration of bleaching liquid is 0.02-0.1%, and solution temperature is at 2-15 ℃, and bleaching time is 5-10 minute.
According to another preferred embodiment, a kind of production method of bamboo fibre comprises that further bamboo fibre of the present invention is a diameter at 0.09-0.15 millimeter, the length bamboo fibre at the 80-250 millimeter.
The invention has the beneficial effects as follows: bamboo is driven fine seperator and is given full play to bamboo wood the best after softening and open fine point, can adjust the machining parameter as required, obtains different fiber slenderness ratios; The bamboo fibre that makes processing than originally more carefully, more even; Its production process is reliable, and resource utilization is high, low processing cost; Environmental pollution is little, constant product quality.The fine bamboo fiber that the present invention produces has that long fineness is even, intensity is high, pliability is good; Fiber absorb-discharge humid, gas permeability are strong; Hangzhoupro bacterium deodoriging properties is especially outstanding; Be a kind of good and cheap, the natural function fiber of new generation that the ratio of performance to price is superior can be widely used in fields such as weaving, building materials, automobile.
The specific embodiment
In conjunction with the preferred embodiments the present invention is done further detailed explanation now.
Specific embodiment of the present invention is following:
One, cuts off: select 3 years setation bamboos, cizu or green bamboos etc. for use,, again bamboo wood is cut into the little bamboo chip of designated length with mechanical shock and compressor squeezing;
Two, softening: the bamboo wood that cuts is sent in the softening pond, added the solution that contains alkali or liquefied ammonia and soak, solution concentration is 1-5%, and liquid level exceeds bamboo wood 1-3 millimeter, and soak time is 10-15 hour.Wherein, also can to select the pectase of concentration 1-10g/l, lignoenzyme that concentration is 1-20g/l, cellulase, concentration that concentration is 1-30g/l for use be one or more the mixture in the 2-8g/l hemicellulase to said bating liquor;
Three, clean: the bamboo wood after will softening is put into to specify in the service sink and soaked 20 minutes, delivers to zone to be processed after the flushing again and dries;
Four, open fibre, classification, screening: the bamboo wood that will dry is delivered to out in the fine seperator and is processed, and separates, opens fine separation, air-flow classification through comb, obtains the bamboo filamentary fibers, utilizes vibrating screen that the powder of bamboo filamentary fibers is removed again;
Five, kiering: adopt autoclave that above-mentioned little bamboo chip is carried out the softening processing of autoclaving, pressure is 5-6 atmospheric pressure, and temperature is between 155-175 ℃, and the processing time is 1-3 hour;
Six, detergent bleach: bamboo fibre is put into sink after the clear water washing, send in the Bellmer and under agitation bleach, wash with clear water once more with bleaching liquid; Said bleaching liquid is selected calcium hypochlorite solution for use, and concentration is 0.06%, and solution temperature is at 5 ℃; Bleaching time is 10 minutes
Seven, clean, dewater: the bamboo filamentary fibers after will bleaching drains, and cleans to pH value 6-7 (bath raio is 1:30, and the time is 10 minutes) with the dilution heat of sulfuric acid that contains 0.2% then, cleans the back dehydration with clear water again;
Eight, dewatered drying: the bamboo fibre after will washing dewaters with mechanical drying mode or vacuum mode or plate pressure mode, sends in the drier oven dry or under sunshine, dries naturally, and oven dry back bamboo fibre moisture is 5-25%;
Nine, enzyme is handled: with shower nozzle pectase evenly is sprayed onto on the bamboo filamentary fibers, wherein the pectase concentration of aqueous solution of preparation: 5g/l, time: 24h, pH:3.3,60 ℃ of temperature.After enzyme is handled, then can prepare diameter at 0.09-0.15 millimeter, length bamboo fibre at the 80-250 millimeter.
In the present invention, bamboo is driven fine seperator and is given full play to bamboo wood the best after softening and open fine point, can adjust the machining parameter as required; Obtain different fiber slenderness ratios, the bamboo fibre that makes processing than originally more carefully, more even, its production process is reliable; Resource utilization is high; Low processing cost, environmental pollution is little, constant product quality.The fine bamboo fiber that the present invention produces has that long fineness is even, intensity is high, pliability is good; Fiber absorb-discharge humid, gas permeability are strong; Hangzhoupro bacterium deodoriging properties is especially outstanding; Be a kind of good and cheap, the natural function fiber of new generation that the ratio of performance to price is superior can be widely used in fields such as weaving, building materials, automobile.
With above-mentioned foundation desirable embodiment of the present invention is enlightenment, and through above-mentioned description, the related work personnel can carry out various change and modification fully in the scope that does not depart from this invention technological thought.The technical scope of this invention is not limited to the content on the specification, must confirm its technical scope according to the claim scope.
Claims (6)
1. the production method of a bamboo fibre is characterized in that: comprise the steps:
One, cuts off:, again bamboo wood is cut into the little bamboo chip of designated length with mechanical shock and compressor squeezing;
Two, soften: the bamboo wood that cuts is sent in the bating liquor that softens the pond softened;
Three, open fibre, classification, screening: bamboo wood is delivered to out fine seperator realize that fine separation is separated, opened to comb, air-flow is classified, obtain the bamboo filamentary fibers, utilize vibrating screen that the powder of bamboo filamentary fibers is removed again;
Four, kiering: adopt autoclave that above-mentioned little bamboo chip is carried out the softening processing of autoclaving, pressure is 5-6 atmospheric pressure, and temperature is between 155-175 ℃, and the processing time is 1-3 hour;
Five, clean, dewater: the bamboo filamentary fibers after will bleaching drains, and cleans to pH value 6-7 with the dilution heat of sulfuric acid that contains 0.1-0.2% then, cleans the back dehydration with clear water again;
Six, dewatered drying: the bamboo fibre after will washing dewaters with mechanical drying mode or vacuum mode or plate pressure mode, sends in the drier oven dry or under sunshine, dries naturally, and oven dry back bamboo fibre moisture is 5-25%;
Seven, enzyme is handled: with shower nozzle pectase evenly is sprayed onto on the bamboo filamentary fibers.
2. the production method of a kind of bamboo fibre according to claim 1; It is characterized in that: the softening processing is that bamboo wood is put into softening pond in the step 2, adds the solution that contains alkali or liquefied ammonia and soaks, and solution concentration is 1-5%; Liquid level exceeds bamboo wood 1-3 millimeter, and soak time is 10-15 hour.
3. the production method of a kind of bamboo fibre according to claim 2 is characterized in that: can to select the pectase of concentration 1-10g/l, lignoenzyme that concentration is 1-20g/l, cellulase, concentration that concentration is 1-30g/l for use be one or more the mixture in the 2-8g/l hemicellulase to bating liquor in the said softening processing.
4. the production method of a kind of bamboo fibre according to claim 1; It is characterized in that: also comprise the detergent bleach operation between said step 4 and the step 5: bamboo fibre is put into sink after the clear water washing; Send in the Bellmer and under agitation bleach, wash with clear water once more with bleaching liquid.
5. the production method of a kind of bamboo fibre according to claim 4; It is characterized in that: said bleaching liquid is selected calcium hypochlorite solution or liquor natrii hypochloritis, postassium hypochlorite solution for use; The concentration of bleaching liquid is 0.02-0.1%, and solution temperature is at 2-15 ℃, and bleaching time is 5-10 minute.
6. the production method of a kind of bamboo fibre according to claim 1 is characterized in that: described bamboo fibre is a diameter at 0.09-0.15 millimeter, the length bamboo fibre at the 80-250 millimeter.
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CN2011102917882A CN102433594A (en) | 2011-09-30 | 2011-09-30 | Production method of bamboo fiber |
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CN2011102917882A CN102433594A (en) | 2011-09-30 | 2011-09-30 | Production method of bamboo fiber |
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Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102783711A (en) * | 2012-07-23 | 2012-11-21 | 湖北中烟工业有限责任公司 | Preparation method of tip rod for natural bamboo fiber cigarette |
CN103659627A (en) * | 2012-09-20 | 2014-03-26 | 周道林 | Bamboo linen polishing wheel and manufacturing method thereof |
CN103846990A (en) * | 2014-02-27 | 2014-06-11 | 浙江农林大学 | Production method for textile bamboo fibers |
CN104651954A (en) * | 2014-06-26 | 2015-05-27 | 广西融水县鑫源木业制品有限公司 | Method for producing bamboo fibers |
CN104947263A (en) * | 2015-05-29 | 2015-09-30 | 大竹县金桥麻业有限责任公司 | Production process of ramie blended yarn |
CN105019035A (en) * | 2015-07-29 | 2015-11-04 | 湖南莎丽袜业股份有限公司 | Preparation method of all bamboo fibers and sock |
CN106400190A (en) * | 2016-05-11 | 2017-02-15 | 苏州大学 | Preparation method for biomass cellulose/polymer composite fiber |
CN107916457A (en) * | 2017-12-26 | 2018-04-17 | 阜阳市卓创科技服务生产力促进中心 | A kind of production method of bamboo fibre |
CN108078043A (en) * | 2018-01-22 | 2018-05-29 | 孟婷婷 | Children's sweat absorbing towel prepared by a kind of blended yarn weaved fabric |
CN108248171A (en) * | 2018-01-22 | 2018-07-06 | 孟婷婷 | A kind of sweat absorbing towel containing ultra-fine bamboo fibre fabric |
CN108354250A (en) * | 2018-01-22 | 2018-08-03 | 孟婷婷 | A kind of child's sweat absorbing towel with automatic drying function |
CN109112641A (en) * | 2018-09-18 | 2019-01-01 | 浙江农林大学暨阳学院 | A kind of production method and equipment of bamboo fiber cloth |
CN111808203A (en) * | 2020-08-04 | 2020-10-23 | 江西吉润花炮新材料科技有限公司 | Direct nitration method of bamboo fibers |
CN111893788A (en) * | 2020-07-14 | 2020-11-06 | 江西吉润花炮新材料科技有限公司 | Pretreatment method of bamboo fiber for direct nitration |
CN114737260A (en) * | 2022-04-06 | 2022-07-12 | 叙永县竹原科技有限公司 | Production method of bamboo fiber |
-
2011
- 2011-09-30 CN CN2011102917882A patent/CN102433594A/en not_active Withdrawn
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102783711A (en) * | 2012-07-23 | 2012-11-21 | 湖北中烟工业有限责任公司 | Preparation method of tip rod for natural bamboo fiber cigarette |
CN103659627A (en) * | 2012-09-20 | 2014-03-26 | 周道林 | Bamboo linen polishing wheel and manufacturing method thereof |
CN103846990A (en) * | 2014-02-27 | 2014-06-11 | 浙江农林大学 | Production method for textile bamboo fibers |
CN103846990B (en) * | 2014-02-27 | 2016-02-17 | 浙江农林大学暨阳学院 | A kind of production method of bamboo fiber of weaving |
CN104651954A (en) * | 2014-06-26 | 2015-05-27 | 广西融水县鑫源木业制品有限公司 | Method for producing bamboo fibers |
CN104947263A (en) * | 2015-05-29 | 2015-09-30 | 大竹县金桥麻业有限责任公司 | Production process of ramie blended yarn |
CN105019035A (en) * | 2015-07-29 | 2015-11-04 | 湖南莎丽袜业股份有限公司 | Preparation method of all bamboo fibers and sock |
CN106400190A (en) * | 2016-05-11 | 2017-02-15 | 苏州大学 | Preparation method for biomass cellulose/polymer composite fiber |
CN107916457A (en) * | 2017-12-26 | 2018-04-17 | 阜阳市卓创科技服务生产力促进中心 | A kind of production method of bamboo fibre |
CN108078043A (en) * | 2018-01-22 | 2018-05-29 | 孟婷婷 | Children's sweat absorbing towel prepared by a kind of blended yarn weaved fabric |
CN108248171A (en) * | 2018-01-22 | 2018-07-06 | 孟婷婷 | A kind of sweat absorbing towel containing ultra-fine bamboo fibre fabric |
CN108354250A (en) * | 2018-01-22 | 2018-08-03 | 孟婷婷 | A kind of child's sweat absorbing towel with automatic drying function |
CN109112641A (en) * | 2018-09-18 | 2019-01-01 | 浙江农林大学暨阳学院 | A kind of production method and equipment of bamboo fiber cloth |
CN109112641B (en) * | 2018-09-18 | 2024-02-06 | 浙江农林大学暨阳学院 | Method and equipment for manufacturing bamboo fiber cloth |
CN111893788A (en) * | 2020-07-14 | 2020-11-06 | 江西吉润花炮新材料科技有限公司 | Pretreatment method of bamboo fiber for direct nitration |
CN111808203A (en) * | 2020-08-04 | 2020-10-23 | 江西吉润花炮新材料科技有限公司 | Direct nitration method of bamboo fibers |
CN114737260A (en) * | 2022-04-06 | 2022-07-12 | 叙永县竹原科技有限公司 | Production method of bamboo fiber |
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Open date: 20120606 |