CN102020461B - High-temperature bright red ceramic and preparation method thereof - Google Patents
High-temperature bright red ceramic and preparation method thereof Download PDFInfo
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- CN102020461B CN102020461B CN2010105138912A CN201010513891A CN102020461B CN 102020461 B CN102020461 B CN 102020461B CN 2010105138912 A CN2010105138912 A CN 2010105138912A CN 201010513891 A CN201010513891 A CN 201010513891A CN 102020461 B CN102020461 B CN 102020461B
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- red
- glaze
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- biscuit
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Abstract
The invention discloses a high-temperature bright red ceramic and a preparation method thereof. The preparation method is as follows: preparing a ceramic blank body according to the conventional technique, calcining the ceramic blank body into a bisque, applying bright red glaze on the bisque, preparing a red blank by calcining, then applying transparent glaze on the red blank, and calcining to form the bright red ceramic. The ceramic blank body consists of the following components: SiO2, Al2O3, CaO, MgO, K2O, Na2O, Fe2O3, TiO, P2O5 and BaO; the bright red glaze consists of the following components: SiO2, Al2O3, CaO, MgO, K2O, Na2O, ZnO, BaO, Ba2O3, Fe2O3 and TiO2; and the transparent glaze comprises the following components: SiO2, Al2O3, CaO, MgO, K2O, Na2O, ZnO, Ba2O3, Fe2O3 and TiO2. The high-temperature bright red ceramic provided by the invention has unique components; secondary glaze firing is adopted, and the color-emitting red glaze is positioned at the bottom layer of a transparent glaze; and the high-temperature bright red ceramic has the advantages of stable color emitting, high glossiness, wear resistance, bright color formation, high glossiness, and no dissolving out of lead and cadmium, and can be used for manufacturing art ceramics and ceramics for daily use.
Description
Technical field the invention belongs to the ceramic production technology field, relates to a kind of high temperature scarlet pottery and preparation method thereof.
Background technology red glaze porcelain is exactly famous and precious artwork since ancient times, the Lang Hong of prior art, hold a memorial ceremony for red, chicken is blood red etc. all is famous and precious red glaze, but these red glaze color developments are dark partially, are not pure large reds.The red glaze product has been arranged on the market in recent years, but glaze smoothness degree is not high, color development is unstable and not bright-coloured, and lead release is high.Pure high temperature scarlet glaze pottery is one of difficult problem of Production of Ceramics always.
Summary of the invention the objective of the invention is to solve prior art and has that glaze smoothness degree is not high, color development is unstable and technical problem not bright-coloured, that lead release is high; Stable and bright-coloured high temperature scarlet pottery of a kind of color development and preparation method thereof is provided, to overcome the deficiency of prior art.
To achieve these goals, high temperature scarlet of the present invention pottery prepares ceramic body by common process, processes biscuit through calcining again, on biscuit, imposes bright red glaze, processes red base through calcining again, on red base, executes marzacotto then and calcines and form; Its main points are:
Said ceramic body is made up of by the quality proportioning following material composition:
SiO
2?39.65 Al
2O
3?12.80 CaO?23.90 MgO?0.56 K
2O?1.77
Na
2O?0.54 Fe
2O
3?0.23 TiO
2?0.08 P
2O
5?20.21 BaO?0.02
Said bright red glaze is made up of by the quality proportioning following material composition:
SiO
2?69.35 Al
2O
3?11.61 CaO?9.62 MgO?0.81 K
2O?4.26 Na
2O?0.92
ZnO?1.12 BaO?0.80 B
2O
3?0.86 Fe
2O
3?0.16 TiO
2?0.13
Said marzacotto is made up of by the quality proportioning following material composition:
SiO
2?57.83 Al
2O
3?12.52 CaO?10.69 MgO?1.03 K
2O?2.32
Na
2O?5.42?ZnO?5.21 B
2O
3?4.12 Fe
2O
3?0.31 TiO
2?0.12
The preparation method of high temperature scarlet pottery of the present invention, its main points are undertaken by following process step:
1), prepares bright red glaze slip: above-mentioned each component of bright red glaze is mixed; Prepare glaze slip with the ball milling wet method; Become basic powdered frit in 24 hours 200 ℃ of oven dry, more basic powdered frit, red stain and the water mass ratio by 1: 0.3: 0.9 is mixed, process red glaze slip;
2), prepare transparent glaze slip: above-mentioned marzacotto and the water mass ratio by 1: 1 is mixed, become transparent glaze slip with the ball milling wet grinding;
3), burning till of biscuit: ceramic body 1280～1310 ℃ of calcinings, is incubated 0.5 hour, and firing atmosphere is an oxydizing flame;
4), biscuit glazing: the biscuit surface after burning till sprays bright red glaze slip, and the glaze layer thickness is 0.15～0.20mm;
5), burning till of red base: the glazing biscuit 1260～1280 ℃ of calcinings, is incubated 0.5 hour, and firing atmosphere is an oxydizing flame;
6), red base glazing: the red base surface after burning till sprays transparent glaze slip, glaze layer thickness 0.12～0.15mm;
7), burning till of high temperature scarlet pottery: the red base of glazing is burnt till at 1150 ℃, be incubated 15 minutes, firing atmosphere is an oxydizing flame;
Said red stain is made up of by the quality proportioning following material composition:
ZrO
2?38.19 SO
2?6.62 CdO?20.28 SeO
2?7.8 SiO
2?27.11。
The invention provides stable and bright-coloured high temperature scarlet pottery of a kind of color development and preparation method thereof.This method not only can be produced art pottery product, but also productive life is used porcelain, like tableware, tea set and coffee service, coffee set etc., has solved prior art and has had that glaze smoothness degree is not high, color development is unstable and technical problem not bright-coloured, that lead release is high.
Embodiment high temperature scarlet of the present invention pottery at first prepares ceramic body, processes biscuit through calcining, on biscuit, imposes bright red glaze, processes red base through calcining again, on red base, executes marzacotto then and calcines and form;
It is formulated that ceramic body is pressed mass ratio by following compositions:
SiO
2?39.65 Al
2O
3?12.80 CaO?23.90 MgO?0.56 K
2O?1.77
Na
2O?0.54 Fe
2O
3?0.23 TiO
2?0.08 P
2O
5?20.21 BaO?0.02
It is formulated that bright red glaze is pressed mass ratio by following compositions:
SiO
2?69.35 Al
2O
3?11.61 CaO?9.62 MgO?0.81 K
2O?4.26 Na
2O?0.92
ZnO?1.12 BaO?0.80 B
2O
3?0.86 Fe
2O
3?0.16 TiO
2?0.13
It is formulated that marzacotto is pressed mass ratio by following compositions:
SiO
2?57.83 Al
2O
3?12.52 CaO?10.69 MgO?1.03 K
2O?2.32
Na
2O?5.42 ZnO?5.21 B
2O
3?4.12 Fe
2O
3?0.31 TiO
2?0.12
The preparation method of high temperature scarlet pottery of the present invention, undertaken by following process step:
1), prepares bright red glaze slip: above-mentioned each component of bright red glaze is mixed; Prepare glaze slip with the ball milling wet method; Became basic powdered frit in 24 hours 200 ℃ of oven dry; Again basic powdered frit is added red stain and water and mix by 1: 0.3: 0.9 mass ratio, process red glaze slip, it is formulated that red stain is pressed mass ratio by following compositions: ZrO
238.19 SO
26.62 CdO 20.28 SeO
27.8 SiO
227.11;
2), prepare transparent glaze slip: above-mentioned marzacotto and the water mass ratio by 1: 1 is mixed, become transparent glaze slip with the ball milling wet grinding;
3), burning till of biscuit: ceramic body 1300 ℃ of calcinings, is incubated 0.5 hour, and firing atmosphere is an oxydizing flame;
4), biscuit glazing: the biscuit surface after burning till sprays bright red glaze slip, and the glaze layer thickness is 0.18mm;
5), burning till of red base: the glazing biscuit 1270 ℃ of calcinings, is incubated 0.5 hour, and firing atmosphere is an oxydizing flame;
6), red base glazing: the red base surface after burning till sprays transparent glaze slip, glaze layer thickness 0.14mm;
7), burning till of high temperature scarlet pottery: the red base of glazing is burnt till at 1150 ℃, be incubated 15 minutes, firing atmosphere is an oxydizing flame.
Make the high temperature scarlet pottery through above process step.
Main innovation characteristics of the present invention:
1, component is unique.Newly body recipe, red glaze prescription and the transparent prescription of development have been used;
2, adopt the method for secondary glaze firing, the red glaze of color development is in the bottom of transparent, thereby color development is stable, glossiness is high, wear-resistant;
3, the product glaze is smoothly bright, quality is bright-coloured, glossiness is high, the lead and cadmium free stripping, not only is used to make the art pottery, can also make life and using porcelain, has significantly promoted value-added content of product.
Claims (3)
1. high temperature scarlet pottery, by common process prepare ceramic body, biscuit is processed in calcining, on biscuit, imposes bright red glaze, processes red base through calcining again, on red base, execute marzacotto then and calcine again and form; It is characterized in that:
Said ceramic body is made up of by the quality proportioning following material composition:
SiO
2?39.65 Al
2O
3?12.80 CaO?23.90 MgO?0.56 K
2O?1.77
Na
2O?0.54 Fe
2O
3?0.23 TiO
2?0.08 P
2O
5?20.21 BaO?0.02
Said bright red glaze is made up of by the quality proportioning following material composition:
SiO
2?69.35 Al
2O
3?11.61 CaO?9.62 MgO?0.81 K
2O?4.26 Na
2O?0.92
ZnO?1.12 BaO?0.80 B
2O
3?0.86 Fe
2O
3?0.16 TiO
2?0.13
Said marzacotto is made up of by the quality proportioning following material composition:
SiO
2?57.83 Al
2O
3?12.52 CaO?10.69 MgO?1.03 K
2O?2.32
Na
2O?5.42 ZnO?5.21 B
2O
3?4.12 Fe
2O
3?0.31 TiO
2?0.12。
2. the preparation method of high temperature scarlet according to claim 1 pottery is characterized in that being undertaken by following process step:
1), prepares bright red glaze slip: above-mentioned each component of bright red glaze is mixed; Prepare glaze slip with the ball milling wet method; Become basic powdered frit in 24 hours 200 ℃ of oven dry, more basic powdered frit, red stain and the water mass ratio by 1: 0.3: 0.9 is mixed, process red glaze slip;
2), prepare transparent glaze slip: above-mentioned marzacotto and the water mass ratio by 1: 1 is mixed, become transparent glaze slip with the ball milling wet grinding;
3), burning till of biscuit: ceramic body 1280～1310 ℃ of calcinings, is incubated 0.5 hour, and firing atmosphere is an oxydizing flame;
4), biscuit glazing: the biscuit surface after burning till sprays bright red glaze slip, and the glaze layer thickness is 0.15～0.20mm;
5), burning till of red base: the glazing biscuit 1260～1280 ℃ of calcinings, is incubated 0.5 hour, and firing atmosphere is an oxydizing flame;
6), red base glazing: the red base surface after burning till sprays transparent glaze slip, glaze layer thickness 0.12～0.15mm;
7), burning till of high temperature scarlet pottery: the red base of glazing is burnt till at 1150 ℃, be incubated 15 minutes, firing atmosphere is an oxydizing flame.
3. the preparation method of high temperature scarlet according to claim 2 pottery is characterized in that said red stain is made up of by the quality proportioning following material composition:
ZrO
2?38.19 SO
2?6.62 CdO?20.28 SeO
2?7.8 SiO
2?27.11。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105138912A CN102020461B (en) | 2010-10-16 | 2010-10-16 | High-temperature bright red ceramic and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105138912A CN102020461B (en) | 2010-10-16 | 2010-10-16 | High-temperature bright red ceramic and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN102020461A CN102020461A (en) | 2011-04-20 |
| CN102020461B true CN102020461B (en) | 2012-11-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010105138912A Expired - Fee Related CN102020461B (en) | 2010-10-16 | 2010-10-16 | High-temperature bright red ceramic and preparation method thereof |
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Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102515862B (en) * | 2011-12-14 | 2014-01-08 | 广东松发陶瓷股份有限公司 | Bright red glaze for decoration |
| CN104058726B (en) * | 2014-06-18 | 2015-07-22 | 福建省德化县恒星陶瓷有限公司 | Degradable sand red pottery |
| CN104860720B (en) * | 2015-05-07 | 2017-01-04 | 广东宏陶陶瓷有限公司 | Ceramic decoration high temperature scarlet color ink-jet ink and preparation method and applications |
| CN105542553A (en) * | 2016-01-12 | 2016-05-04 | 陕西科技大学 | Iron oxide red ceramic glaze ink and preparation method thereof |
| CN106316131A (en) * | 2016-08-23 | 2017-01-11 | 福建省德化世盛陶瓷有限公司 | Bright monochrome-glazed porcelain and preparing method thereof |
| CN106830687A (en) * | 2017-02-16 | 2017-06-13 | 内江师范学院 | A kind of ceramic sintering process that red glaze is fabricated to Chinese painting color ink effect |
| CN114671610B (en) * | 2019-08-26 | 2023-05-23 | 福建省德化县天俊陶瓷有限公司 | Low-temperature transparent glaze ceramic product and preparation method thereof |
| CN111116043B (en) * | 2019-12-30 | 2022-07-12 | 江西新明珠建材有限公司 | 4-level wear-resistant glaze marble tile and manufacturing method thereof |
| CN113860923A (en) * | 2021-09-26 | 2021-12-31 | 蒙娜丽莎集团股份有限公司 | Bright red rock glaze and preparation method thereof |
| CN117383966A (en) * | 2023-10-18 | 2024-01-12 | 景德镇陶瓷大学 | Red glaze ceramic and its prepn process |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1803712A (en) * | 2005-12-31 | 2006-07-19 | 河北理工大学 | High temperature scarlet ceramic pigment and production method thereof |
| CN1887809A (en) * | 2006-07-24 | 2007-01-03 | 胡天霏 | Bright red underglaze color, overglaze and their prepn process |
| CN101224990A (en) * | 2008-01-29 | 2008-07-23 | 中国人民解放军国防科学技术大学 | High temperature resistant ceramic matrix composite material and preparation method thereof |
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2010
- 2010-10-16 CN CN2010105138912A patent/CN102020461B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1803712A (en) * | 2005-12-31 | 2006-07-19 | 河北理工大学 | High temperature scarlet ceramic pigment and production method thereof |
| CN1887809A (en) * | 2006-07-24 | 2007-01-03 | 胡天霏 | Bright red underglaze color, overglaze and their prepn process |
| CN101224990A (en) * | 2008-01-29 | 2008-07-23 | 中国人民解放军国防科学技术大学 | High temperature resistant ceramic matrix composite material and preparation method thereof |
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| CN102020461A (en) | 2011-04-20 |
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