CN101760091A - Single-coating type matt transferring aluminum-plating paint and preparation method thereof - Google Patents
Single-coating type matt transferring aluminum-plating paint and preparation method thereof Download PDFInfo
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- CN101760091A CN101760091A CN200910201063A CN200910201063A CN101760091A CN 101760091 A CN101760091 A CN 101760091A CN 200910201063 A CN200910201063 A CN 200910201063A CN 200910201063 A CN200910201063 A CN 200910201063A CN 101760091 A CN101760091 A CN 101760091A
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Abstract
The invention relates to single-coating type matt transferring aluminum-plating paint and a preparation method thereof; the coating comprises the following ingredients by weight parts: 10-20 parts of main resin, 0-10 parts of auxiliary resin, 70-80 parts of dissolving solvent, 0.5-2 parts of matt powder, 0.2-0.5 part of white increasing powder, 0-0.5 part of dispersing accessory ingredient, 0-0.5 part of leveling agent, 0-0.5 part of defoaming agent, 0-0.5 part of anti-scuffing agent; after the materials are prepared, 90 percent of the dissolving solvent, the main resin, the auxiliary resin, the leveling agent, the anti-scuffing agent and the defoaming agent are arranged in an agitated reactor and are stirred for reaction, the matt powder, the white increasing powder and the remaining 10 percent of the dissolving solvent are added in another dispersing cylinder and are mixed and stirred to obtain the product. Compared with the prior art, the production cost is low, the paint is beneficial to environment protection, the production efficiency is improved, water and electrical energy consumption is reduced, the printing performance of the product is good, and the luster is stable.
Description
Technical field
The present invention relates to a kind of coating and preparation method thereof, especially relate to a kind of single-coating type matt transferring aluminum-plating paint and preparation method thereof.
Background technology
The matt transferring aluminum-plating paper that is used for the tobacco package printing at present all is to produce with two coating type matt transferring aluminum-plating paints, and the PET basement membrane is dried rolling after being coated with the first road coating earlier, unreels again after the rolling to be coated with the second road coating and to dry rolling more again.Two coating type matt transferring aluminum-plating paints exist following drawback: (1) is coated with and two are coated with matt transferring aluminum-plating paint and cause the plant factor height, but production capacity is low, the tediously long and merit of taking consuming time of operation; (2) the coating consumption is uneconomical greatly, the cost height, and rate of profit is low; (3) water, power consumption consumption are big, waste energy; (4) the big VOC discharging of coating consumption is many, not environmental protection; (5) two matt transferring aluminum-plating paints that are coated with are stung the end because of two interlayers sometimes and quality problems occurred.If problems such as unclean, form and aspect instability also can occur peeling off with common mute light single coating transfer aluminum plating coating.Above-mentioned all factors restricted the range of application of the two coating transfer aluminum plating coatings of mute light.
Summary of the invention
Purpose of the present invention is exactly that a kind of production efficiency height, cost is low, printing adaptability is good single-coating type matt transferring aluminum-plating paint and preparation method thereof are provided in order to overcome the defective that above-mentioned prior art exists.
Purpose of the present invention can be achieved through the following technical solutions:
A kind of single-coating type matt transferring aluminum-plating paint is characterized in that, this coating comprises following component and weight part content:
Main resin 10-20;
Assisted resin 0-10;
Dissolution solvent 70-80;
Mute light powder 0.5-2;
Whitening powder 0.2-0.5;
Dispersing auxiliary 0-0.5;
Leveling auxiliary agent 0-0.5;
Defoamer 0-0.5;
Anti scuffing agent 0-0.5.
Described main resin comprises one or both in acrylic resin, urethane resin, polyester, Synolac, resol, Vinylite, Resins, epoxy, pure dissolubility polymeric amide or the pure dissolubility nitro-cotton.
Described assisted resin comprises one or both in celluosic resin, vinyl-formal resin, polyvinyl butyral resin, isocyanate resin, urea-formaldehyde resin or the terpolycyantoamino-formaldehyde resin.
Described dissolution solvent comprises two or more in vinyl acetic monomer, n-propyl acetate, N-BUTYL ACETATE, acetone, butanone, propylene glycol monomethyl ether, ethanol or the propyl carbinol.
The silicon dioxide powder that described mute light powder is particle diameter 1-5um.
Described whitening powder comprises titanium dioxide or silicon dioxide powder.
Described dispersing auxiliary comprises one or more in vinylformic acid sodium salt, modified polyorganosiloxane or the non-ionic interfacial agent.
Described leveling auxiliary agent comprises organic silicon modified by polyether or polyester modification organosilicon.
Described defoamer comprises acrylate or modified siloxane.
Described anti scuffing agent comprises polyethylene wax powder or modified siloxane.
A kind of preparation method of single-coating type matt transferring aluminum-plating paint is characterized in that, this method may further comprise the steps:
(1) get the raw materials ready according to following component and content (weight part):
Main resin 10-20,
Assisted resin 0-10,
Dissolution solvent 70-80,
Mute light powder 0.5-2,
Whitening powder 0.2-0.5,
Dispersing auxiliary 0-0.5,
Leveling auxiliary agent 0-0.5,
Defoamer 0-0.5,
Anti scuffing agent 0-0.5;
(2) dissolution solvent with total amount 90% drops in the reactor, opens stirrer, and the control rotating speed is that 700-800rpm stirs;
(3) main resin is joined in the reactor, control stirrer rotating speed is 700-800rpm, stirs 60min and dissolves fully to reactant;
(4) control stirrer rotating speed is 1000-1200rpm, adds assisted resin, stirs 60min and dissolves fully to reactant;
(5) add leveling auxiliary agent, anti scuffing agent in reactor, the control rotating speed is that 700-800rpm stirs 10-20min;
(6) add defoamer in reactor, the control rotating speed is that 1000-1200rpm stirs 10-20min, obtains mute light base-material;
(7) disperse to add in the cylinder mute light powder and whitening powder at another, the solvent that remains 10% is joined disperse to soak two kinds of powders in the cylinder, controlling rotating speed again is that 700-800rpm disperses 10min;
(8) add mute light base-material in disperseing cylinder, the control rotating speed is 1000-1200rpm dispersed with stirring 30-60min;
(9) detect the viscosity that above-mentioned steps obtains sample, filter at last and obtain mute light single coating transfer aluminum plating coating.
Compared with prior art, the present invention has the following advantages:
(1) disposable coating of mute light single coating transfer aluminum plating coating of the present invention and production cost are low;
(2) discharging of minimizing VOC is beneficial to environmental protection;
(3) simplify production process, enhance productivity, reduce water, electric energy consumption;
(4) the product printing performance is excellent, and color and luster is stable.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A kind of preparation method of mute light single coating transfer aluminum plating coating, this method may further comprise the steps:
(1) get the raw materials ready according to (weight part) raw material of following component and content:
| Component | Weight part (kg) |
| Main resin: nitro-cotton | ??16 |
| Assisted resin: urethane resin | ??4 |
| Dissolution solvent: butanone, vinyl acetic monomer, n-propyl acetate, propylene glycol monomethyl ether | ??78.38 |
| Mute light powder: fine silica powder ML-386D | ??0.5 |
| Whitening powder: pre-processing titanium white powder | ??0.5 |
| Dispersing auxiliary: modified siloxane and mixture of carboxylic acids | ??0.01 |
| Leveling auxiliary agent: polyether-type modified organic silicon | ??0.1 |
| Defoamer: modified siloxane | ??0.01 |
| Anti scuffing agent: polyethylene micropowder wax | ??0.5 |
(2) dissolution solvent of total amount 90% is dropped in the reactor, open stirrer and stir to middling speed 700-800rpm;
(3) add under the rotating speed of middling speed 700-800rpm and become owner of the resin nitro-cotton, stir 60min to dissolving fully;
(4) assisted resin urethane is joined in the reactor, high speed 1000-1200rpm stirs 60min to dissolving fully;
(5) add leveling auxiliary agent, defoamer in reactor, it is stand-by that middling speed 700-800rpm stirs 10-20min;
(6) solvent and the dispersing auxiliary of adding residue 10% in another dispersion cylinder add make mute light powder, whitening powder, anti scuffing agent after dispersed with stirring is even, again middling speed 700-800rpm dispersion 10min again;
(7) add the materials for the treatment of that step (5) makes in disperseing cylinder, high speed 1200-1500rpm disperses more than the 30min again;
(8) viscosity of the above-mentioned sample of detection reaches 70～80mPa.S, obtains mute light single coating transfer aluminum plating coating at last after filtration, coating is packed get final product.
Embodiment 2
A kind of preparation method of mute light single coating transfer aluminum plating coating, this method may further comprise the steps:
(1) get the raw materials ready according to (weight part) raw material of following component and content:
| Component | Weight part (kg) |
| Main resin: nitro-cotton | ??16 |
| Component | Weight part (kg) |
| Assisted resin: polyvinyl butyral acetal | ??4 |
| Dissolution solvent: butanone, vinyl acetic monomer, n-propyl acetate, propylene glycol monomethyl ether | ??78.08 |
| Mute light powder: fine silica powder ML-386D | ??0.8 |
| Whitening powder: pre-processing titanium white powder | ??0.5 |
| Dispersing auxiliary: modified siloxane and mixture of carboxylic acids | ??0.01 |
| Leveling auxiliary agent: polyether-type modified organic silicon | ??0.1 |
| Defoamer: modified siloxane | ??0.01 |
| Anti scuffing agent: polyethylene micropowder wax | ??0.5 |
(2) dissolution solvent of total amount 90% is dropped in the reactor, open stirrer and stir to middling speed 700-800rpm;
(3) add under the rotating speed of middling speed 700-800rpm and become owner of the resin nitro-cotton, stir 60min to dissolving fully;
(4) the assisted resin polyvinyl butyral acetal is joined in the reactor, high speed 1000-1200rpm stirs 60min to dissolving fully;
(5) add leveling auxiliary agent, defoamer in reactor, it is stand-by that middling speed 700-800rpm stirs 10-20min;
(6) solvent and the dispersing auxiliary of adding residue 10% in another dispersion cylinder add make mute light powder, whitening powder, anti scuffing agent after dispersed with stirring is even, again middling speed 700-800rpm dispersion 10min again;
(7) add the materials for the treatment of that step (5) makes in disperseing cylinder, high speed 1200-1500rpm disperses more than the 30min again;
(8) viscosity of the above-mentioned sample of detection reaches 70～80mPa.S, obtains mute light single coating transfer aluminum plating coating at last after filtration, coating is packed get final product.
Embodiment 3
(1) get the raw materials ready according to (weight part) raw material of following component and content:
| Component | Weight part (kg) |
| Main resin: nitro-cotton | ??16 |
| Assisted resin: acrylic resin | ??4 |
| Component | Weight part (kg) |
| Dissolution solvent: butanone, vinyl acetic monomer, n-propyl acetate, | |
| Propylene glycol monomethyl ether | ??78.08 |
| Mute light powder: fine silica powder ML-386D | ??0.8 |
| Whitening powder: pre-processing titanium white powder | ??0.5 |
| Dispersing auxiliary: modified siloxane and mixture of carboxylic acids | ??0.01 |
| Leveling auxiliary agent: polyether-type modified organic silicon | ??0.1 |
| Defoamer: modified siloxane | ??0.01 |
| Anti scuffing agent: polyethylene micropowder wax | ??0.5 |
(2) dissolution solvent of total amount 90% is dropped in the reactor, open stirrer and stir to middling speed 700-800rpm;
(3) add under the rotating speed of middling speed 700-800rpm and become owner of the resin nitro-cotton, stir 60min to dissolving fully;
(4) the assisted resin acrylic resin is joined in the reactor, high speed 1000-1200rpm stirs 60min to dissolving fully;
(5) add leveling auxiliary agent, defoamer in reactor, it is stand-by that middling speed 700-800rpm stirs 10-20min;
(6) solvent and the dispersing auxiliary of adding residue 10% in another dispersion cylinder add make mute light powder, whitening powder, anti scuffing agent after dispersed with stirring is even, again middling speed 700-800rpm dispersion 10min again;
(7) add the materials for the treatment of that step (5) makes in disperseing cylinder, high speed 1200-1500rpm disperses more than the 30min again;
(8) viscosity of the above-mentioned sample of detection reaches 70～80mPa.S, obtains mute light single coating transfer aluminum plating coating at last after filtration, coating is packed get final product.
Embodiment 4
A kind of preparation method of single-coating type matt transferring aluminum-plating paint, this method may further comprise the steps:
(1) get the raw materials ready according to following component and content: 20kg Resins, epoxy is main resin, the mixture of 20kg n-propyl acetate, 30kg ethanol and 30kg propyl carbinol is a dissolution solvent, the 2kg particle diameter is that the silicon dioxide powder of 5um is mute light powder, 0.5kg titanium dioxide is as whitening powder, 0.5kg acrylate is a defoamer, 0.5kg polyethylene wax powder is as the anti scuffing agent;
(2) dissolution solvent with total amount 90% drops in the reactor, opens stirrer, and the control rotating speed is that 800rpm stirs;
(3) Resins, epoxy is joined in the reactor, control stirrer rotating speed is 800rpm, stirs 60min and dissolves fully to reactant;
(5) add anti scuffing agent polyethylene wax powder in reactor, the control rotating speed is that 800rpm stirs 10min;
(6) add defoamer in reactor, the control rotating speed is that 1200rpm stirs 10min, obtains mute light base-material;
(7) disperse to add in the cylinder mute light powder and whitening powder at another, the solvent that remains 10% is joined disperse to soak two kinds of powders in the cylinder, controlling rotating speed again is that 800rpm disperses 10min;
(8) add mute light base-material in disperseing cylinder, the control rotating speed is 1200rpm dispersed with stirring 30min;
(9) detect the viscosity that above-mentioned steps obtains sample and reach 80mPa.S, filter at last and obtain mute light single coating transfer aluminum plating coating.
Embodiment 5
A kind of preparation method of single-coating type matt transferring aluminum-plating paint, this method may further comprise the steps:
(1) get the raw materials ready according to following component and content: 10kg master's resin is a resol, 10kg assisted resin terpolycyantoamino-formaldehyde resin, 40kg acetone, 30kg butanone mixture are dissolution solvent, 0.5kg the silicon dioxide powder of particle diameter 1um is mute light powder, 0.2kg silicon dioxide powder is a whitening powder, 0.5kg sodium acrylate is a dispersing auxiliary, 0.5kg leveling auxiliary agent organic silicon modified by polyether;
(2) dissolution solvent with total amount 90% drops in the reactor, opens stirrer, and the control rotating speed is that 700rpm stirs;
(3) resol is joined in the reactor, control stirrer rotating speed is 700rpm, stirs 60min and dissolves fully to reactant;
(4) control stirrer rotating speed is 1000rpm, adds terpolycyantoamino-formaldehyde resin, stirs 60min and dissolves fully to reactant;
(5) add organic silicon modified by polyether in reactor, the control rotating speed is that 700rpm stirs 20min, obtains mute light base-material;
(6) another silicon dioxide powder that disperses to add in cylinder particle diameter 1um as mute light powder and silicon dioxide powder as whitening powder, the solvent of residue 10% joined disperses to soak two kinds of powders in the cylinder, controlling rotating speed again is that 800rpm disperses 10min;
(7) add mute light base-material in disperseing cylinder, the control rotating speed is 1000rpm dispersed with stirring 60min;
(8) detect the viscosity that above-mentioned steps obtains sample and reach 70mPa.S, filter at last and obtain mute light single coating transfer aluminum plating coating.
Embodiment 6
A kind of preparation method of single-coating type matt transferring aluminum-plating paint, this method may further comprise the steps:
(1) get the raw materials ready according to following component and content: 15kg alcohol dissolubility polymeric amide is as main resin, 5kg urea-formaldehyde resin, 2kg vinyl-formal resin mixture are as assisted resin, 30kg vinyl acetic monomer, 45kg n-propyl acetate mixture are as dissolution solvent, the silicon dioxide powder of 1kg particle diameter 3um is as mute light powder, 0.3kg titanium dioxide is as whitening powder, 0.3kg polyoxyethylate amide is as dispersing auxiliary, 0.2kg the polyester modification organosilicon is as leveling auxiliary agent, 0.2kg acrylate is as defoamer, the 0.1kg modified siloxane is as the anti scuffing agent;
(2) dissolution solvent with total amount 90% drops in the reactor, opens stirrer, and the control rotating speed is that 800rpm stirs;
(3) pure dissolubility polymeric amide is joined in the reactor, control stirrer rotating speed is 800rpm, stirs 60min and dissolves fully to reactant;
(4) control stirrer rotating speed is 1000rpm, adds vinyl-formal resin, stirs 60min and dissolves fully to reactant;
(5) add leveling auxiliary agent, anti scuffing agent in reactor, the control rotating speed is that 700rpm stirs 20min;
(6) add defoamer in reactor, the control rotating speed is that 1200rpm stirs 10min, obtains mute light base-material;
(7) disperse to add in the cylinder mute light powder and whitening powder at another, the solvent that remains 10% is joined disperse to soak two kinds of powders in the cylinder, controlling rotating speed again is that 800rpm disperses 10min;
(8) add mute light base-material in disperseing cylinder, the control rotating speed is 1200rpm dispersed with stirring 30min;
(9) detect the viscosity that above-mentioned steps obtains sample and reach 70mPa.S, filter at last and obtain mute light single coating transfer aluminum plating coating.
Embodiment 7
A kind of preparation method of single-coating type matt transferring aluminum-plating paint, this method may further comprise the steps:
(1) get the raw materials ready according to following component and content: 15kg alcohol dissolubility polymeric amide is as main resin, 4kg celluosic resin, 4kg isocyanate resin mixture are as assisted resin, 30kg vinyl acetic monomer, 20kg propyl carbinol, 35kg acetone mixture are as dissolution solvent, 1.5kg the silicon dioxide powder of particle diameter 2um is as mute light powder, 0.4kg silicon dioxide powder is as whitening powder, 0.2kg polyoxyethylate amide is as dispersing auxiliary, 0.2kg organic silicon modified by polyether is as leveling auxiliary agent, 0.1kg modified siloxane is as defoamer, 0.1kg polyethylene wax powder is as the anti scuffing agent;
(2) dissolution solvent with total amount 90% drops in the reactor, opens stirrer, and the control rotating speed is that 700rpm stirs;
(3) pure dissolubility polymeric amide is joined in the reactor, control stirrer rotating speed is 750rpm, stirs 60min and dissolves fully to reactant;
(4) control stirrer rotating speed is 1100rpm, adds assisted resin, stirs 60min and dissolves fully to reactant;
(5) add leveling auxiliary agent, anti scuffing agent in reactor, the control rotating speed is that 750rpm stirs 15min;
(6) add defoamer in reactor, the control rotating speed is that 1100rpm stirs 15min, obtains mute light base-material;
(7) disperse to add in the cylinder mute light powder and whitening powder at another, the solvent that remains 10% is joined disperse to soak two kinds of powders in the cylinder, controlling rotating speed again is that 800rpm disperses 10min;
(8) add mute light base-material in disperseing cylinder, the control rotating speed is 1100rpm dispersed with stirring 40min;
(9) detect the viscosity that above-mentioned steps obtains sample and reach 80mPa.S, filter at last and obtain mute light single coating transfer aluminum plating coating.
Claims (11)
1. a single-coating type matt transferring aluminum-plating paint is characterized in that, this coating comprises following component and weight part content:
Main resin 10-20;
Assisted resin 0-10;
Dissolution solvent 70-80;
Mute light powder 0.5-2;
Whitening powder 0.2-0.5;
Dispersing auxiliary 0-0.5;
Leveling auxiliary agent 0-0.5;
Defoamer 0-0.5;
Anti scuffing agent 0-0.5.
2. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1, it is characterized in that described main resin comprises one or both in acrylic resin, urethane resin, polyester, Synolac, resol, Vinylite, Resins, epoxy, pure dissolubility polymeric amide or the pure dissolubility nitro-cotton.
3. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1, it is characterized in that described assisted resin comprises one or both in celluosic resin, vinyl-formal resin, polyvinyl butyral resin, isocyanate resin, urea-formaldehyde resin or the terpolycyantoamino-formaldehyde resin.
4. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1, it is characterized in that described dissolution solvent comprises two or more in vinyl acetic monomer, n-propyl acetate, N-BUTYL ACETATE, acetone, butanone, propylene glycol monomethyl ether, ethanol or the propyl carbinol.
5. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1 is characterized in that, the silicon dioxide powder that described mute light powder is particle diameter 1-5um.
6. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1 is characterized in that described whitening powder comprises titanium dioxide or silicon dioxide powder.
7. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1 is characterized in that described dispersing auxiliary comprises one or more in vinylformic acid sodium salt, modified polyorganosiloxane or the non-ionic interfacial agent.
8. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1 is characterized in that, described leveling auxiliary agent comprises organic silicon modified by polyether or polyester modification organosilicon.
9. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1 is characterized in that described defoamer comprises acrylate or modified siloxane.
10. a kind of single-coating type matt transferring aluminum-plating paint according to claim 1 is characterized in that, described anti scuffing agent comprises polyethylene wax powder or modified siloxane.
11. the preparation method of a single-coating type matt transferring aluminum-plating paint is characterized in that, this method may further comprise the steps:
(1) get the raw materials ready according to following component and content (weight part):
Main resin 10-20,
Assisted resin 0-10,
Dissolution solvent 70-80,
Mute light powder 0.5-2,
Whitening powder 0.2-0.5,
Dispersing auxiliary 0-0.5,
Leveling auxiliary agent 0-0.5,
Defoamer 0-0.5,
Anti scuffing agent 0-0.5;
(2) dissolution solvent with total amount 90% drops in the reactor, opens stirrer, and the control rotating speed is that 700-800rpm stirs;
(3) main resin is joined in the reactor, control stirrer rotating speed is 700-800rpm, stirs 60min and dissolves fully to reactant;
(4) control stirrer rotating speed is 1000-1200rpm, adds assisted resin, stirs 60min and dissolves fully to reactant;
(5) add leveling auxiliary agent, anti scuffing agent in reactor, the control rotating speed is that 700-800rpm stirs 10-20min;
(6) add defoamer in reactor, the control rotating speed is that 1000-1200rpm stirs 10-20min, obtains mute light base-material;
(7) disperse to add in the cylinder mute light powder and whitening powder at another, the solvent that remains 10% is joined disperse to soak two kinds of powders in the cylinder, controlling rotating speed again is that 700-800rpm disperses 10min;
(8) add mute light base-material in disperseing cylinder, the control rotating speed is 1000-1200rpm dispersed with stirring 30-60min;
(9) detect the viscosity that above-mentioned steps obtains sample, filter at last and obtain mute light single coating transfer aluminum plating coating.
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| CN200910201063A CN101760091A (en) | 2009-12-14 | 2009-12-14 | Single-coating type matt transferring aluminum-plating paint and preparation method thereof |
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2009
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Application publication date: 20100630 |