CN101747835A - Elastic anti-corrosion coating - Google Patents
Elastic anti-corrosion coating Download PDFInfo
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- CN101747835A CN101747835A CN200810227903A CN200810227903A CN101747835A CN 101747835 A CN101747835 A CN 101747835A CN 200810227903 A CN200810227903 A CN 200810227903A CN 200810227903 A CN200810227903 A CN 200810227903A CN 101747835 A CN101747835 A CN 101747835A
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Abstract
The invention relates to an elastic anti-corrosion coating, which is a room-temperature silicon sulfide-based functional compound with high property. The formula of the coating comprises(in part by weight): 30 to 70 parts of polyorganosiloxane, 1 to 80 parts of pigments and fillers, 30 to 10 parts of crosslinking agent, 1 to 10 parts of auxiliary agent and 10 to 80 parts of thinning agent. The elastic anti-corrosion coating has high weathering resistance, water resistance, acid resistance, solvent resistance and oil resistance and alkali resistance; the paint film can be desirably adhered onto glass, ceramics, steel structural members, concrete, various resin primers and the like, and the paint film is good in elasticity and hydrophobicity and high in tensile strength and breaking elongation, can be widely used for the corrosion prevention of bridges, tanks and various steel structural members and the corrosion and leakage protection of ground, drainage channels and the like.
Description
Technical field
The invention belongs to the chemical engineering of materials field, specifically relate to a kind of elastic anti-corrosion coating, particularly a kind of anticorrosion room temperature silicon sulfide rubber composition.
Background technology
Material surfaces such as metal, concrete, timber are subjected to the physics of surrounding environment medium, chemical action through regular meeting corrosion damage to take place.The whole world all suffer of all kinds because of the massive losses that brought of corrosion.About 8,000 hundred million yuan of the annual because financial loss that corrosion causes of China accounts for about 3% of GDP, and at oil, chemical industry, building materials field, the various potential safety hazards of being brought because of corrosion, the accident of initiation are startling especially.
In order to tackle corrosion, people have taked various measures, and are wherein most economical, actual effect or the most general with the coating protective system.The ultimate principle of protective system is by Isolated Shield, passivation inhibition and three kinds of mechanism of electro-chemical protection material surface to be protected.Present protective system divides acid-proof, alkali prevention, anti-salt etc. substantially, and the easy alkali prevention difficulty of acid-proof.Protective system commonly used comprises: epoxy-based coatings, the advantage of this coating are that sticking power is good, solidity to corrosion is strong, but weathering resistance is poor, is commonly used to do priming paint; The alkyd varnish weathering resistance is better, but water-fast, anti-saponifiability is relatively poor; Coal tar coating, its water tolerance is better, but poor solvent resistance; Polyurethane coating, chlorosulfonated polythylene coatings, fluorocarbon coating, water tolerance, the weathering resistance of this class coating are better, and has certain chemical resistance, but it does not have resistance to corrosion preferably to alkali and 40% above concentrated acid, and paint film is harder, to cement etc. sticking power is bad, can't directly be used as terrace paint.
It is anticorrosion, the waterproof paint of major ingredient with Resins, epoxy and deposed polystyrene that CN1056397 discloses a kind of, but its solvent resistance is relatively poor; CN1422914 disclose a kind of by add styrene-butadiene rubber(SBR), Resins, epoxy p-poly-phenyl ethenoid resin carries out the polystyrene styrene-butadiene rubber anticorrosive coating that modification obtains, because it contains Resins, epoxy, though increased the sticking power to base material, photostabilization will be subjected to negative impact.
Summary of the invention
Purpose of the present invention is exactly the limitation that overcomes present traditional coating, and a kind of elastic anti-corrosion coating with good weathering resistance, water tolerance, solvent resistance, oil-proofness and while acid-fast alkali-proof is provided.
The objective of the invention is to realize by the following technical solutions:
Elastic anti-corrosion coating provided by the invention is the high-performance with the room temperature vulcanized silicone rubber basis, functional composition, and its prescription comprises following component (weight part):
Organopolysiloxane 30～70 weight parts
Color stuffing 1～80 weight part
Linking agent 3～10 weight parts
Auxiliary agent 1～10 weight part
Thinner 10～80 weight parts
Above-mentioned each composition is evenly mixed in proportion, can obtain elastic anti-corrosion coating of the present invention.
Elastic anti-corrosion coating provided by the invention has good weathering resistance, water tolerance, acid resistance, solvent resistance, oil-proofness and alkaline resistance properties preferably.Paint film all has outstanding sticking power to glass, pottery, steel construction piece, concrete and various types of resins priming paint etc., paint film elasticity, hydrophobic nature are good, tensile strength, elongation at break are higher, can be widely used in anticorrosion, the leakproof of anticorrosion and ground, the drainage tray etc. of bridge, storage tank, various steel construction pieces.
Embodiment
Elastic anti-corrosion coating with good weathering resistance, water tolerance, solvent resistance, oil-proofness and while acid-fast alkali-proof provided by the invention is the composition with the room temperature vulcanized silicone rubber basis, and its prescription comprises following component (weight part):
Organopolysiloxane 30～70 weight parts
Color stuffing 1～80 weight part
Linking agent 3～10 weight parts
Auxiliary agent 1～10 weight part
Thinner 10～80 weight parts
Described organopolysiloxane is to be selected from polydimethylsiloxane that at least one end is hydroxyl, alkoxyl group or ethenyl blocking, PSI, poly-diphenyl siloxane, the poly-methyl trifluoro propyl siloxanes one or more.
Described color stuffing comprises white carbon black, nano-calcium carbonate, titanium dioxide, talcum powder, silicon powder, barium sulfate, organic fluorine micro mist, zinc oxide, aluminum oxide, ferric oxide, cerium oxide, titanium white, iron oxide red, iron oxide black, carbon black, chromoxide green, the blue or green orchid of phthalein etc.
Described linking agent is for being selected from methyl triacetoxysilane, methyl tri acetylacetonate oximino silane, methyl tributanoximo silane, the vinyl tributanoximo silane, methyltrimethoxy silane, Union carbide A-162, poly-methyltrimethoxy silane, vinyltrimethoxy silane, vinyltriethoxysilane, methyl three (N-methylacetamide base) silane, dimethyl two (N-methylacetamide base) silane, methyl ethylene two (N-methylacetamide base) silane, in the methyl tricyclohexyltin amine base silane etc. one or more.
Described auxiliary agent comprises catalyzer, for example organotin, titanic acid ester and organic titanium inner complex, organic aluminium compound etc.;
Described auxiliary agent comprises promotor, for example γ-An Jibingjisanyiyangjiguiwan, dichloromethyl triethoxyl silane, anilinomethyl trimethoxy silane, anilinomethyl three ethoxy silane, diethylin methyl three ethoxy silane, γ-urea groups propyl trimethoxy silicane, γ-isocyanate group propyl-triethoxysilicane, N-β-aminoethyl-γ-An Bingjisanyiyangjiguiwan;
Described auxiliary agent comprises dispersion agent, BYK-110, BYK-P104, the Disperbyk-130 of for example German BYK Chemie company; Efka-766, the Efka Polymer452 etc. of Holland EFKA company;
Described auxiliary agent comprises flow agent, BYK-354, the BYK-300 of for example German BYK Chemie company; Efka-30, the Efka-772 etc. of Holland EFKA company;
Described auxiliary agent comprises defoamer, BYK-065, the BYK-052 of for example German BYK Chemie company; The Efka-20 of Holland EFKA company; The Airex970 of Germany Tego company etc.;
Described auxiliary agent comprises thickening material, for example comprises polyethers, cyanoethyl Trimethoxy silane, contains silica-based polyoxyethylene glycol, polyether silane class etc., as German Henkel company
Deng.
Described thinner is selected from one or more in non-reacted dimethyl silicone oil, dimethylbenzene, toluene, acetone, ether, sherwood oil, industrial naptha, glycerine, aromatic alcohol, the vinyl acetic monomer.
In embodiments of the present invention, more preferred prescription comprises following component (weight part):
Organopolysiloxane 30～70 weight parts
Silicon-dioxide 3～20 weight parts
Linking agent 5～8 weight parts
Catalyzer 0.01～0.5 weight part
Promotor 0.3～1 weight part
Wherein, described organopolysiloxane is that at least one end is one or more in the polydimethylsiloxane, PSI of hydroxyl, alkoxyl group or ethenyl blocking, poly-diphenyl siloxane, the poly-methyl trifluoro propyl siloxanes.
Described linking agent is one or more in methyl tributanoximo silane, vinyl tributanoximo silane, methyltrimethoxy silane, Union carbide A-162, poly-Union carbide A-162, vinyltrimethoxy silane, the vinyltriethoxysilane.
Described catalyzer is stannous octoate or dibutyl tin laurate.
Described promotor is one or more of γ-An Jibingjisanyiyangjiguiwan, dichloromethyl triethoxyl silane, anilinomethyl trimethoxy silane, anilinomethyl three ethoxy silane, diethylin methyl three ethoxy silane, γ-urea groups propyl trimethoxy silicane, γ-isocyanate group propyl-triethoxysilicane, N-β-aminoethyl-γ-An Bingjisanyiyangjiguiwan.
Above-mentioned each composition is evenly mixed in proportion, can obtain elastic anti-corrosion coating of the present invention.
In the preferred embodiment of the present invention, at first with organopolysiloxane, filler, pigment premix, forward batch mixing to vacuum kneader after grinding thin-pass, be warmed up to 50～200 ℃ of vacuum kneading 3～120min, after adding linking agent, auxiliary agent and thinner, mediate 5～60min again and can obtain required anticorrosion elastic coating.Embodiment 1, transparent type elastic anti-corrosion coating
The prescription of transparent type elastic anti-corrosion coating provided by the invention and performance are listed in table 1, table 2 respectively.
Table 1, transparent type elastic anti-corrosion coating prescription 1
Table 2, performance test
Embodiment 2, be used for bridge weather resistant elastic anti-corrosion coating
The prescription of second kind of transparent type elastic anti-corrosion coating provided by the invention and performance are listed in table 3, table 4 respectively.
Table 3, be used for bridge weather resistant elastic anti-corrosion coating prescription
Table 4, performance test
Embodiment 3, be used for the steel construction elastic anti-corrosion coating
The prescription of the third transparent type elastic anti-corrosion coating provided by the invention and performance are listed in table 5, table 6 respectively.
Table 5, be used for steel construction elastic anti-corrosion coating prescription
Table 6, performance test
Embodiment 4, be used for terrace, tank elastic anti-corrosion coating
The prescription and the performance of the 4th kind of transparent type elastic anti-corrosion coating provided by the invention are listed in table 7, table 8 respectively.
Table 7, be used for terrace, tank elastic anti-corrosion coating prescription
Table 8, performance test
Embodiment 5, high solid elastic anti-corrosion coating
The prescription and the performance of the 5th kind of transparent type elastic anti-corrosion coating provided by the invention are listed in table 9, table 10 respectively.
Table 9, high solid elastic anti-corrosion coating prescription
Table 10, performance test
Embodiment 6, high solid elastic anti-corrosion coating
The prescription and the performance of the 6th kind of transparent type elastic anti-corrosion coating provided by the invention are listed in table 11, table 12 respectively.
Table 11, high solid elastic anti-corrosion coating prescription
Table 12, performance test
Therefore elastic anti-corrosion coating provided by the invention has good weathering resistance, water tolerance, acid resistance, solvent resistance, oil-proofness and alkaline resistance properties preferably.Paint film all has outstanding sticking power to glass, pottery, steel construction piece, concrete and various types of resins priming paint etc., paint film elasticity, hydrophobic nature are good, tensile strength, elongation at break are higher, thereby can be widely used in anticorrosion, the leakproof of anticorrosion and ground, the drainage tray etc. of bridge, storage tank, various steel construction pieces.
Claims (10)
1. an elastic anti-corrosion coating is the composition with the room temperature vulcanized silicone rubber basis, and its prescription comprises:
Organopolysiloxane 30～70 weight parts
Color stuffing 1～80 weight part
Linking agent 3～10 weight parts
Auxiliary agent 1～10 weight part
Thinner 10～80 weight parts
Above-mentioned each composition is evenly mixed in proportion, obtain required elastic anti-corrosion coating.
2. elastic anti-corrosion coating according to claim 1 is characterized in that: described organopolysiloxane is to be selected from polydimethylsiloxane that at least one end is hydroxyl, alkoxyl group or ethenyl blocking, PSI, poly-diphenyl siloxane, the poly-methyl trifluoro propyl siloxanes one or more.
3. elastic anti-corrosion coating according to claim 1 is characterized in that: described color stuffing is that white carbon black, nano-calcium carbonate, titanium dioxide, talcum powder, silicon powder, barium sulfate, organic fluorine micro mist, zinc oxide, aluminum oxide, ferric oxide, cerium oxide, titanium white, iron oxide red, iron oxide black, carbon black, chromoxide green or phthalein are blue or green blue.
4. elastic anti-corrosion coating according to claim 1 is characterized in that: described linking agent is for being selected from methyl triacetoxysilane, methyl tri acetylacetonate oximino silane, methyl tributanoximo silane, the vinyl tributanoximo silane, methyltrimethoxy silane, Union carbide A-162, poly-methyltrimethoxy silane, vinyltrimethoxy silane, vinyltriethoxysilane, methyl three (N-methylacetamide base) silane, dimethyl two (N-methylacetamide base) silane, methyl ethylene two (N-methylacetamide base) silane, in the methyl tricyclohexyltin amine base silane one or more.
5. elastic anti-corrosion coating according to claim 1 is characterized in that: described auxiliary agent comprises one or more in catalyzer, promotor, dispersion agent, flow agent, defoamer and the thickening material;
Described catalyzer is organotin, titanic acid ester and organic titanium inner complex or organic aluminium compound;
Described promotor is γ-An Jibingjisanyiyangjiguiwan, dichloromethyl triethoxyl silane, anilinomethyl trimethoxy silane, anilinomethyl three ethoxy silane, diethylin methyl three ethoxy silane, γ-urea groups propyl trimethoxy silicane, γ-isocyanate group propyl-triethoxysilicane or N-β-aminoethyl-γ-An Bingjisanyiyangjiguiwan;
Described dispersion agent is BYK-110, BYK-P104, the Disperbyk-130 of German BYK Chemie company; Or Efka-766, the Efka Polymer452 of Dutch EFKA company;
Described flow agent is BYK-354, the BYK-300 of German BYK Chemie company; Or Efka-30, the Efka-772 of Dutch EFKA company;
Described defoamer is BYK-065, the BYK-052 of German BYK Chemie company; The Efka-20 of Holland EFKA company; Or the Airex970 of German Tego company;
Described thickening material is polyethers, cyanoethyl Trimethoxy silane, contain silica-based polyoxyethylene glycol, polyether silane class or German Henkel company
6. elastic anti-corrosion coating according to claim 1 is characterized in that: described thinner is selected from one or more in non-reacted dimethyl silicone oil, dimethylbenzene, toluene, acetone, ether, sherwood oil, industrial naptha, glycerine, aromatic alcohol, the vinyl acetic monomer.
7. elastic anti-corrosion coating, its prescription comprises:
Organopolysiloxane 30～70 weight parts
Silicon-dioxide 3～20 weight parts
Linking agent 5～8 weight parts
Catalyzer 0.01～0.5 weight part
Promotor 0.3～1 weight part
Wherein, described organopolysiloxane is that at least one end is one or more in the polydimethylsiloxane, PSI of hydroxyl, alkoxyl group or ethenyl blocking, poly-diphenyl siloxane, the poly-methyl trifluoro propyl siloxanes.
8. elastic anti-corrosion coating according to claim 7 is characterized in that: described linking agent is one or more in methyl tributanoximo silane, vinyl tributanoximo silane, methyltrimethoxy silane, Union carbide A-162, poly-Union carbide A-162, vinyltrimethoxy silane, the vinyltriethoxysilane.
9. elastic anti-corrosion coating according to claim 7 is characterized in that: described catalyzer is stannous octoate or dibutyl tin laurate.
10. elastic anti-corrosion coating according to claim 7 is characterized in that: described promotor is one or more of γ-An Jibingjisanyiyangjiguiwan, dichloromethyl triethoxyl silane, anilinomethyl trimethoxy silane, anilinomethyl three ethoxy silane, diethylin methyl three ethoxy silane, γ-urea groups propyl trimethoxy silicane, γ-isocyanate group propyl-triethoxysilicane, N-β-aminoethyl-γ-An Bingjisanyiyangjiguiwan.
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