CN101130663A - Fire resistant anticorrosive paint of organosilicon - Google Patents
Fire resistant anticorrosive paint of organosilicon Download PDFInfo
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- CN101130663A CN101130663A CNA2007101444264A CN200710144426A CN101130663A CN 101130663 A CN101130663 A CN 101130663A CN A2007101444264 A CNA2007101444264 A CN A2007101444264A CN 200710144426 A CN200710144426 A CN 200710144426A CN 101130663 A CN101130663 A CN 101130663A
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Abstract
The invention discloses an organic silicon fire resistant antiseptic eroding paint, which is characterized by the following: comprising with 15-40% organic silicon resin and hardener, 15-60% thermostable filler, 0. 01-0. 5% dryer, 0. 05-0. 5% additive, 0. 1-5% coupling agent and 1-64% dissolvent; getting the product. This invention possesses simple craft good coating property and strong adhesive force.
Description
Technical field
The present invention relates to a kind of coating.
Background technology
High-temperature resistant coating is meant in temperature more than 200 ℃, the paint film nondiscoloration, do not come off, still can keep the coated material of suitable physical and mechanical properties.High-temperature resistant coating is widely used in aspects such as chimney, high temperature steam pipeline, heat exchanger, High Temperature Furnaces Heating Apparatus, petroleum cracking equipment, engine position and vapor pipe.Along with developing rapidly of industry such as Aeronautics and Astronautics, weapons, demand to the particular component resistance to elevated temperatures is more and more higher, high temperature-resistant coating material is good with its large-scale construction technology performance, and advantage such as can not come off significantly causes countries in the world scholar's concern gradually.Heat resisting coating of a great variety, but the most common with organosilicon heat-resistant coating and inorganic heat-resisting coating.Wherein pure silicone varnish can anti-200-250 ℃ (thermal weight loss be less than 10%), is base-material with the silicone resin, and add coatings formulated such as metal powder, heat-resisting color stuffing, frit can anti-300-700 ℃.Report for organosilicon heat-resistant coating is a lot, as the heat resisting coating that is mixed with pure silicone resin, modified organic silicone resin, tinting pigment, pigment extender, glass powder, zinc powder, anti-settling agent, solidifying agent and solvent etc. in the patent CN86104951 silicon resin, heat-resistant paint (bulletin on February 10th, 1988), can anti-200-600 ℃ high temperature.Black with silicone resin, ferrochrome in patent CN1295102 high temperature organosilicon paint (bulletin on May 16 calendar year 2001) and the CN1560156 high temperature organosilicon paint (bulletin on January 5th, 2005), talcum powder, glass powder, Graphite Powder 99 are that preparation of raw material becomes heat resisting coating with dimethylbenzene, and its upper limit temperature of heat tolerance can reach 800 ℃.
Though the resistance to elevated temperatures of existing high-temperature resistant coating is better, all exists the common shortcoming, promptly needs hot setting (being generally 150-200 ℃), paint film adhesion difference and the relatively poor shortcoming of solidity to corrosion.
Summary of the invention
The objective of the invention is needs for solving existing coating that hot setting, paint film adhesion are poor, the problem of solidity to corrosion difference, and a kind of fire resistant anticorrosive paint of organosilicon now is provided.Fire resistant anticorrosive paint of organosilicon is by weight percentage mainly by 15～40% silicone resin and solidifying agent, 15～60% high temperature resistant filler, 0.01～0.5% siccative, 0.05～0.5% additive, 0.1～5% coupling agent and 1～64% solvent composition.Fire resistant anticorrosive paint of organosilicon of the present invention also increases the high-temperature resisting pigment that above-mentioned all material gross weight 5～25% is arranged, and described high-temperature resisting pigment is that Stainless Steel Powder or ferrochrome are black, and the granularity that Stainless Steel Powder or ferrochrome are black is 1 μ m.
Compare with existing high-temperature resistant coating, the present invention has following beneficial effect: one, coating process is simple.Coating of the present invention can directly be brushed or be sprayed on the workpiece surface, and drying at room temperature curing gets final product, and need not at high temperature to solidify.Two, coating performance is good.The formed paint adhesion of the present invention is strong, and solidity to corrosion, acid resistance are good.
Embodiment
Embodiment one: the fire resistant anticorrosive paint of organosilicon of present embodiment is by weight percentage by 15～40% silicone resin and solidifying agent, 15～60% high temperature resistant filler, 0.01～0.5% siccative, 0.05～0.5% additive, 0.1～5% coupling agent and 1～64% solvent composition.Wherein silicone resin and solidifying agent mass ratio are 10～14: 1 mix, and described silicone resin is an epoxy modified silicone resin, and described solidifying agent is a polymeric amide, and polymeric amide is polyamide 6 50, polyamide 6 51 or kymene 00#, plays solidification.Described high temperature resistant filler is a kind of or wherein several mixing in glass powder, mica powder or the talcum powder, when high temperature resistant filler is mixture, and can be between various high temperature resistant fillers by any than mixing; Glass powder, mica powder and talcous granularity are all less than 1 μ m.Described siccative is octylate, zinc, cobalt, magnesium, iron or naphthenate, and described octylate is a kind of or wherein several mixing in zinc octoate, cobalt octoate, sad magnesium or the iron octoate, and ratio was any when several materials mixed.Described naphthenate is cobalt naphthenate, nickel naphthenate, manganese naphthenate, zinc naphthenate, calcium naphthenate, cyclic potassium naphthenate, zirconium naphthenate or naphthenic acid vanadium.Described additive is chromic anhydride, potassium wolframate, potassium molybdate, potassium vanadate, potassium permanganate or potassium bichromate; The effect of additive is that the raising corrosion resistance coating reaches the resistance to institute's Service Environment medium.Described coupling agent is a silane coupling agent, and silane coupling agent is γ-An Jibingjisanyiyangjiguiwan, γ-sulfydryl propyl-triethoxysilicane or γ-glycidyl ether Trimethoxy silane.Described solvent is a kind of or wherein several mixing in dimethylbenzene, vinyl acetic monomer, propyl carbinol or the pimelinketone; When solvent is mixture, can be between all kinds of SOLVENTS by any than mixing.
Embodiment two: the fire resistant anticorrosive paint of organosilicon of present embodiment also increases the high-temperature resisting pigment that embodiment one all material gross weight 5～25% is arranged, described high-temperature resisting pigment is that Stainless Steel Powder or ferrochrome are black, and the granularity that Stainless Steel Powder or ferrochrome are black is 1 μ m.
Embodiment three: the fire resistant anticorrosive paint of organosilicon of present embodiment is by weight percentage by mixture 30%, Stainless Steel Powder 20%, glass powder 38%, chromic anhydride 0.2%, zinc octoate 0.2%, γ-sulfydryl propyl-triethoxysilicane 2.5%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, pimelinketone 1.1% is formed, and wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment four: by mixture 30%, glass powder 58%, chromic anhydride 0.2%, zinc octoate 0.2%, γ-sulfydryl propyl-triethoxysilicane 2.5%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.1% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment five: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.1%, zinc octoate 0.05%, γ-sulfydryl propyl-triethoxysilicane 0.5%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 3.35% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment six: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.15%, sad magnesium 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.75% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment seven: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.15%, iron naphthenate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.75% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment eight: the fire resistant anticorrosive paint of organosilicon of present embodiment is black 20% by the mixture 30% of epoxy modified silicone resin and polymeric amide, ferrochrome by weight percentage, talcum powder 18%, glass powder 20%, chromic anhydride 0.15%, zinc octoate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, dimethylbenzene 8%, and pimelinketone 1.75% is formed; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment nine: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.15%, zinc octoate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.75% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment ten: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, zinc octoate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.9% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment 11: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.15%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.85% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment 12: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.15%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 3.85% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment 13: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, chromic anhydride 0.2%, zinc octoate 0.2%, γ-sulfydryl propyl-triethoxysilicane 2.5%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.1% for the fire resistant anticorrosive paint of organosilicon of present embodiment.
Embodiment 14: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, potassium bichromate 0.15%, zinc octoate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.75% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment 15: the fire resistant anticorrosive paint of organosilicon of present embodiment is made up of mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, potassium wolframate 0.15%, zinc octoate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, dimethylbenzene 8%, the pimelinketone 1.75% of epoxy modified silicone resin and polymeric amide by weight percentage; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Embodiment 16: by mixture 30%, Stainless Steel Powder 20%, talcum powder 18%, glass powder 20%, potassium molybdate 0.15%, zinc octoate 0.1%, γ-sulfydryl propyl-triethoxysilicane 2%, the dimethylbenzene 8% of epoxy modified silicone resin and polymeric amide, form by weight percentage by pimelinketone 1.75% for the fire resistant anticorrosive paint of organosilicon of present embodiment; Wherein the mass ratio of epoxy modified silicone resin and polymeric amide is 12: 1.
Above-mentioned embodiment three to the test result of embodiment 16 sees Table 1.
As can be seen from Table 1:
(1) in modified organic silicone resin, add additives such as chromic anhydride, potassium wolframate after, gained corrosion resistance coating, acid resistance all significantly improve.Acid resistance is from bringing up to greater than 300 hours less than 50 hours, and salt fog resistance is from bringing up to greater than 1000 hours less than 96 hours.
(2) in modified organic silicone resin, add siccative (zinc octoate) after, the dry solidification temperature has dropped to room temperature from 50～80 ℃.
(3) in modified organic silicone resin, add silicone couplet after, paint film adhesion also significantly improves, sticking power is brought up to 1 grade of level from 3 grades.
Table 1 organosilicon heat-resistant coating technical indicator
| Embodiment 10 | Drying at room temperature is solidified | Do not chap, do not come off | 1 | Less than 96 hours | Less than 300 hours |
| Embodiment 11 | 50～80 ℃ of dry republicanisms are solidified | Do not chap, do not come off | 1 | Greater than 300 hours | Greater than 1000 hours |
| Embodiment 12 | Drying at room temperature is solidified | Do not chap, do not come off | 3 | Greater than 300 hours | Greater than 1000 hours |
| Embodiment 13 | Drying at room temperature is solidified | Do not chap, do not come off | 1 | Greater than 300 hours | Greater than 1000 hours |
| Embodiment 14 | Drying at room temperature is solidified | Do not chap, do not come off | 1 | Greater than 300 hours | Greater than 1000 hours |
| Embodiment 15 | Drying at room temperature is solidified | Do not chap, do not come off | 1 | Greater than 300 hours | Greater than 1000 hours |
| Embodiment 16 | Drying at room temperature is solidified | Do not chap, do not come off | 1 | Greater than 300 hours | Greater than 1000 hours |
Annotate: 1. adopt standard GB 1735-89 2. to adopt standard GB 1720-89
3. adopt standard GB 1763-89; Sulfuric acid: 30% (weight ratio), temperature: 30 ℃.
4. adopt standard GB/T 1771-91
Embodiment 17: the compound method of the fire resistant anticorrosive paint of organosilicon of present embodiment: earlier with high-temperature resisting pigment, filler and additive (as, chromic anhydride etc.) mix, and constantly stir, add siccative again, or else disconnected the stirring, add modified organic silicone resin, coupling agent and solidifying agent at last, promptly be made into described fire resistant anticorrosive paint of organosilicon.When fire resistant anticorrosive paint of organosilicon is lower than 300 ℃ in temperature, with silicone resin is main high temperature resistant material, behind the elevated temperature, the fracture of side chain organic radical only takes place when utilizing organopolysiloxane to be subjected to thermooxidizing and the ruined hardly characteristics of silicon-oxygen backbone, add high temperature resistant color stuffing, as glass powder etc., when organic silicone resin decomposes and charing when losing enough adhesive properties, glass ceramic material just begins to melt, thereby take over silicone resin, continue to play the filming function that sticks pigment and matrix metal.The effect of additive is that the raising corrosion resistance coating reaches the resistance to institute's Service Environment medium.
Embodiment 18: the using method of the fire resistant anticorrosive paint of organosilicon of present embodiment: before the use, earlier the greasy dirt and the rusty scale of workpiece surface are removed and cleaned up, or adopt sandblasting to eliminate rust, then workpiece surface is directly brushed or be sprayed on to fire resistant anticorrosive paint of organosilicon, seasoning got final product in 48 hours at ambient temperature.
Claims (10)
1. fire resistant anticorrosive paint of organosilicon, it is characterized in that fire resistant anticorrosive paint of organosilicon by weight percentage mainly by 15～40% silicone resin and solidifying agent, 15～60% high temperature resistant filler, 0.01～0.5% siccative, 0.05～0.5% additive, 0.1～5% coupling agent and 1～64% solvent composition, wherein silicone resin and solidifying agent mass ratio are 10～14: 1 mix.
2. fire resistant anticorrosive paint of organosilicon according to claim 1 is characterized in that described fire resistant anticorrosive paint of organosilicon also comprises the high-temperature resisting pigment of claim 1 raw material gross weight 5～25% by weight percentage.
3. fire resistant anticorrosive paint of organosilicon according to claim 2 is characterized in that described high-temperature resisting pigment is that Stainless Steel Powder or ferrochrome are black, and the granularity that Stainless Steel Powder or ferrochrome are black is 1 μ m.
4. fire resistant anticorrosive paint of organosilicon according to claim 1 is characterized in that described silicone resin is an epoxy modified silicone resin, and described solidifying agent is a polymeric amide, and polymeric amide is polyamide 6 50, polyamide 6 51 or kymene 00#.
5. fire resistant anticorrosive paint of organosilicon according to claim 1 is characterized in that described high temperature resistant filler is a kind of or wherein several mixing in glass powder, mica powder or the talcum powder, and glass powder, mica powder or talcous granularity are less than 1 μ m.
6. fire resistant anticorrosive paint of organosilicon according to claim 1 is characterized in that described siccative is octylate, zinc, cobalt, magnesium, iron or naphthenate.
7. fire resistant anticorrosive paint of organosilicon according to claim 6 is characterized in that octylate is a kind of or wherein several mixing in zinc octoate, cobalt octoate, sad magnesium or the iron octoate; Naphthenate is a kind of or wherein several mixing of cobalt naphthenate, nickel naphthenate, manganese naphthenate, zinc naphthenate, calcium naphthenate, cyclic potassium naphthenate, zirconium naphthenate or naphthenic acid vanadium.
8. fire resistant anticorrosive paint of organosilicon according to claim 1 is characterized in that described additive is chromic anhydride, potassium wolframate, potassium molybdate, potassium vanadate, potassium permanganate or potassium bichromate.
9. fire resistant anticorrosive paint of organosilicon according to claim 1, it is characterized in that described coupling agent is a silane coupling agent, silane coupling agent is γ-An Jibingjisanyiyangjiguiwan, γ-sulfydryl propyl-triethoxysilicane or γ-glycidyl ether Trimethoxy silane.
10. fire resistant anticorrosive paint of organosilicon according to claim 1 is characterized in that described solvent is a kind of or wherein several mixing in dimethylbenzene, vinyl acetic monomer, propyl carbinol or the pimelinketone.
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