CN109881474A - A kind of reflective denim fabric and its production method - Google Patents
A kind of reflective denim fabric and its production method Download PDFInfo
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Abstract
The invention discloses a kind of reflective denim fabric and its production methods, belong to reflective denim fabric and its production technical field.Using chemical reduction method reflective yarn is prepared in PET fiber surface in Nano metal particles deposition by the present invention, again using reflective yarn and Duo Gen spun polyester thread doubling twisting as weft yarn, beam dyeing obtains jean yarn as warp thread, is weaved, and reflective denim fabric is prepared.The reflective yarn that the present invention is prepared substitutes traditional glass microballoon as reflectorized material using nano-Ag particles, it is harmless, wearing feeling is more comfortable, it overcomes prior art major part Reflection fabric major part Reflection fabric and is difficult to the problem for meeting the needs of moisture absorption is ventilative, soft using top finish, application range is wider；The reflective yarn that the present invention is prepared is post-processed by silicone oil, so that its nano-Ag particles is not easy to change, keeps good reflecting effect, and the fabric being prepared is reflective obvious, and fabric fashion, technology sense are strong.
Description
Technical field
The present invention relates to a kind of reflective denim fabric and its production methods, belong to reflective denim fabric and its production technology neck
Domain.
Background technique
With the raising of awareness of safety, Reflection fabric is widely used in traffic, the uniform of civil field, work clothes, prevents
The clothes such as shield clothes, and gradually apply in the dress ornaments such as housing, rain gear, knapsack, gloves field.Reflection fabric can reflect distant place direct projection
Light postback at light, for outdoor study, personnel provide safety guarantee.With the development of society and the change of consumption concept, mesh
Before, existing manufacturer applies reflective yarn or Reflection fabric in townwear fabric, makes fabric that fashion be presented, dazzle cruel, section
The styles such as skill sense have obtained the favor of young man.But most Reflection fabric is confined to using glass microballoon coating process
Or it is obtained using reflective yarn and cotton yarn and closing in conjunction with Study of Water-proof And Moisture Permecability, flexibility, comfort and the parent of Reflection fabric
Skin substantially reduces, and it is ventilative to the moisture absorption of townwear, soft that the mode of coating makes Reflection fabric be difficult to meet people
Demand.
Existing more than 150 years history of denim fabric, under the consumption concept for advocating comfortable, back to nature, denim fabric warp
It does not wane long, becomes the favorite of sports fashion trend fabric.But current denim fabric is woven fabric, lacks ductility, makes
It obtains when wearer moves outdoors and is fettered.
In addition, there are no the fabrics for mutually tying reflective yarn or Reflection fabric with denim fabric currently on the market, if it is possible to
The two is combined, pursuit of the part young man to fashion can be satisfied.
Summary of the invention
[technical problem]
In order to solve flexibility existing for the reflective yarn of the prior art or Reflection fabric, comfort and skin-friendly is poor asks
Topic.
[technical solution]
The present invention provides a kind of reflective denim fabric and its production method, this method simple processes, at low cost, Neng Gougai
The soft comfortable of kind Reflection fabric existing in the market.
Firstly, the described method comprises the following steps the present invention provides a kind of production method of reflective denim fabric:
(1) preparation of jean yarn: dyeing obtains jean yarn as warp thread, spare；
(2) preparation of reflective yarn: EtOH Sonicate cleans polyester filament 25-35min, dry, by the polyester filament after drying
It is immersed in 10~20min of dipping in the dimethyl sulphoxide solution containing alkali, is then washed with water 2~3 times, drying can obtain
To the polyester filament of surface hydroxylation, wherein alkali: DMSO: the ratio of water is 110~130mg:20~40mL:10~20mL；
Take the polyester filament of the above-mentioned surface hydroxylation being prepared to be immersed in mixed solution, the mixed solution be containing
There is the aqueous solution of glutaraldehyde, sodium citrate and polyvinylpyrrolidone PVP, wherein the mass ratio of glutaraldehyde, sodium citrate and water
For 1:(2~10): (10~12) add silver nitrate later, the mass ratio of silver nitrate and sodium citrate, PVP be 1:(0.5~
2): (0.02~2) is reacted 15~35min at 80~120 DEG C, is cooled to room temperature later, take out after impregnating 45min~90min
The long yarn of terylene, washing, drying, reflective yarn can be prepared by uniformly being coated using silicone oil；
Using the reflective yarn prepared and 2~4 spun polyester thread doubling twistings as weft yarn；
(3) it weaves；
(4) it singes；
(5) starching；
(6) final finishing, setting；
(7) preshrunk；
(8) fabric is washed: carrying out ENZYME WASH, reflective denim fabric can be obtained；
Wherein, the concentration of silver nitrate is 0.3~0.5mol/L.
In one embodiment of the invention, the alkali is sodium hydroxide or potassium hydroxide.
In one embodiment of the invention, in step (1), the dyeing is beam dyeing, the step of beam dyeing
Specifically: yarn setting, indigo dyeing and starching.
In one embodiment of the invention, dry described in step (2) is dry 1.5~2h at 60~80 DEG C,
The drying is dry preferably under hot wind.
In one embodiment of the invention, the bath raio in step (2) is 1:10~30.
In one embodiment of the invention, the preferred methyl-silicone oil of the silicone oil.
In one embodiment of the invention, the partial size of the nano-Ag particles is 300nm~5 μm.
In one embodiment of the invention, the ENZYME WASH is the cellulose for being 1.5%~2%o.w.f with concentration
Enzyme carries out 2~4h of cleaning, and bath raio is 1:20~30.
In one embodiment of the invention, the ENZYME WASH carries out under being 6.0~6.5 in pH value.
It is in one embodiment of the invention, described to be woven as carrying out woven weaving under relative humidity 65~75%,
The constant humidity for needing to be kept fixed causes weaving difficult and fault to avoid the generation of electrostatic.
In one embodiment of the invention, it is described singe for maintain 80~100 meters/min speed, quickly singe.
In one embodiment of the invention, the purpose of the starching is to maintain the stiffness of cowboy.
In one embodiment of the invention, the setting are as follows: shaped with boarding machine, oven temperature is 150~200
℃。
In one embodiment of the invention, the preshrunk are as follows:: preshrunk, control plane are carried out to fabric on squeezing machine
Expect that shrinkage is ± 5%.
In one embodiment of the invention, by controlling the time of ENZYME WASH, can make it is deep, in, the cowboy of light color
Fabric.
In one embodiment of the invention, the spun polyester thread is 75D/36F semi-gloss polyester DTY, 100D/48F half
Any one of light terylene, 120D/48F semi-gloss polyester DTY.
In one embodiment of the invention, the finished product Gram Mass of the reflective denim fabric is 220~350g/
m2。
In one embodiment of the invention, the operation involved in the present invention is routine operation, those skilled in the art
Member according to the present invention can describe that Reflection fabric of the invention is prepared.
Beneficial effects of the present invention:
(1) the reflective yarn that the present invention is prepared substitutes traditional glass microballoon as reflective material using nano-Ag particles
Material, harmless, wearing feeling is more comfortable, overcomes prior art major part Reflection fabric major part Reflection fabric and uses coating
The problem for being difficult to meet the needs of moisture absorption is ventilative, soft is arranged, application range is wider；The reflective yarn that the present invention is prepared
It is post-processed by silicone oil, so that its nano-Ag particles is not easy to change, keeps good reflecting effect, the fabric being prepared is reflective
Obviously, fabric fashion, technology sense are strong.
(2) the reflective yarn that uses of the present invention using nano silver as reflectorized material, can not only carry out it is reflective, also with good
Good antibacterial effect.
(3) washability for the reflective denim fabric that the present invention is prepared is strong, is still able to maintain after washing repeatedly good anti-
Optical property.
Specific embodiment
Cellulase: Novozymes Company, red granzyme 6400S.
Embodiment 1
(1) preparation of jean yarn: cowboy warp thread preparation include yarn setting, winder, warping, warp thread indigo dyeing and on
The processes such as slurry, specifically:
Yarn setting:
In denim production, pair warp and weft yarn, especially with the twist biggish warp and weft when, Yao Jinhang dewing and heating,
To stablize its twist；The purpose of dead twist be in order to warping, dye slurry process go on smoothly and reduce weave when sluff-offs, looped weft and
Phenomena such as looping, improves fabric quality；It is required that stablizing yarn twist, regain by increasing the methods of tension, dewing, heating
8%~9%；
Pulp
Equipment: sizing-dyeing machine；
Technique: warp beam → wettability treatment → dyeing → warm water washing → starching；
1. wettability treatment: bleeding agent (still or few bubble) FK-ST10C 1.5g/L, caustic soda 1g/L, 80 DEG C of temperature, time 20
±5s
2. dyeing: material uses vatting material method when using indigo dye and dyeing, and dyestuff includes bipseudoindoxyl dye 63g/L, insurance
Powder 85g/L, caustic soda 58g/L, bleeding agent FK-ST10C4.5g/L, dye liquor temperature are 20 DEG C, and padding number is that six leachings six are rolled, and are rolled remaining
Rate 80% pads time 20s
3. starching: slurries control under the conditions of meta-alkalescence, the use of temperature are 98 DEG C, second dipping and rolling starching, and pick-up rate is
80%, jean yarn is prepared as warp thread in the rate of sizing 12%, spare；
(2) preparation of reflective yarn: EtOH Sonicate cleans polyester filament 30min, dry, and the polyester filament after drying is impregnated
In the dimethyl sulphoxide solution containing potassium hydroxide (120mg KOH is dissolved in 30mL DMSO and 10mL deionized water), bath raio is
1:20 impregnates 10min, is then washed with water 2 times, then the polyester filament of surface hydroxylation can be obtained in dry 2h at 65 DEG C；
The polyester filament of the above-mentioned surface hydroxylation being prepared is taken to be immersed in containing glutaraldehyde, sodium citrate and polyethylene
In the mixed solution of pyrrolidones (PVP), wherein the mass ratio of glutaraldehyde, sodium citrate and water is 1:4:10, adds nitre
Sour silver, the concentration of silver nitrate are 0.4mol/L, and the mass ratio of silver nitrate and sodium citrate, PVP is 1:1:0.08, at 100 DEG C
React 20min, bath raio 1:20 is cooled to room temperature later, impregnate take out after 60min be coated with nano-Ag particles terylene it is long
Yarn, washing, drying, can be prepared reflective yarn；
Using the reflective yarn prepared and 3 100D/48F semi-gloss terylene doubling twistings as weft yarn；
(3) it weaves: carrying out woven weaving under being 65% in relative humidity；
(4) it singes: maintaining the speed of 80 meters/min, quickly singe；
(5) starching: the stiffness of cowboy is kept；
(6) final finishing: being shaped with boarding machine, and oven temperature is 160 DEG C, while controlling cloth requirement width and grammes per square metre；It is logical
The tension for overregulating each deflector roll prevents fabric from becoming after wash water tiltedly, cools down later；
(7) preshrunk: carrying out preshrunk to fabric on squeezing machine, controls finished product shrinkage ± 5%；
(8) fabric is washed: when pH value is 6.5, cleaning 3h is carried out with the cellulase that concentration is 1.5%, bath raio 1:
30, reflective denim fabric can be obtained.
Pass through scanning electron microscope analysis, it is known that the particle diameter of the nano silver on denim fabric is about 800nm~1.1 μm.
Embodiment 2
(1) preparation of jean yarn: cowboy warp thread preparation include yarn setting, winder, warping, warp thread indigo dyeing and on
The processes such as slurry, specifically:
Yarn setting:
In denim production, pair warp and weft yarn, especially with the twist biggish warp and weft when, Yao Jinhang dewing and heating,
To stablize its twist；The purpose of dead twist be in order to warping, dye slurry process go on smoothly and reduce weave when sluff-offs, looped weft and
Phenomena such as looping, improves fabric quality；It is required that stablizing yarn twist, regain by increasing the methods of tension, dewing, heating
8%~9%；
Pulp
Equipment: sizing-dyeing machine；
Technique: warp beam → wettability treatment → dyeing → warm water washing → starching；
1. wettability treatment: bleeding agent (still or few bubble) FK-ST10C 1.5g/L, caustic soda 1g/L, 80 DEG C of temperature, time 20
±5s
2. dyeing: material uses vatting material method when using indigo dye and dyeing, and dyestuff includes bipseudoindoxyl dye 63g/L, insurance
Powder 85g/L, caustic soda 58g/L, bleeding agent FK-ST10C4.5g/L, dye liquor temperature are 20 DEG C, and padding number is that six leachings six are rolled, and are rolled remaining
Rate 80% pads time 20s
3. starching: slurries control under the conditions of meta-alkalescence, the use of temperature are 98 DEG C, second dipping and rolling starching, and pick-up rate is
80%, jean yarn is prepared as warp thread in the rate of sizing 12%, spare；
(2) preparation of reflective yarn: EtOH Sonicate cleans polyester filament 30min, dry, and the polyester filament after drying is impregnated
In the dimethyl sulphoxide solution containing potassium hydroxide (120mg KOH is dissolved in 30mL DMSO and 10mL deionized water), bath raio is
1:20 impregnates 10min, is then washed with water 2 times, then the polyester filament of surface hydroxylation can be obtained in dry 2h at 65 DEG C；
The polyester filament of the above-mentioned surface hydroxylation being prepared is taken to be immersed in containing glutaraldehyde, sodium citrate and polyethylene
In the mixed solution of pyrrolidones (PVP), wherein the mass ratio of glutaraldehyde, sodium citrate and water is 1:4:10, adds nitre
Sour silver, the concentration of silver nitrate are 0.5mol/L, and the mass ratio of silver nitrate and sodium citrate, PVP is 1:1:0.08, at 100 DEG C
React 20min, bath raio 1:20 is cooled to room temperature later, impregnate take out after 60min be coated with nano-Ag particles terylene it is long
Yarn, washing, drying, can be prepared reflective yarn；
Using the reflective yarn prepared and 3 100D/48F semi-gloss terylene doubling twistings as weft yarn；
(3) it weaves: carrying out woven weaving under being 65% in relative humidity；
(4) it singes: maintaining the speed of 80 meters/min, quickly singe；
(5) starching: the stiffness of cowboy is kept；
(6) final finishing: being shaped with boarding machine, and oven temperature is 160 DEG C, while controlling cloth requirement width and grammes per square metre；It is logical
The tension for overregulating each deflector roll prevents fabric from becoming after wash water tiltedly, cools down later；
(7) preshrunk: carrying out preshrunk to fabric on squeezing machine, controls finished product shrinkage ± 5%；
(8) fabric is washed: when pH value is 6.5, cleaning 3h is carried out with the cellulase that concentration is 1.5%, bath raio 1:
30, reflective denim fabric can be obtained.
Pass through scanning electron microscope analysis, it is known that the particle diameter of the nano silver on denim fabric is about 2.4~3.5 μm.
Embodiment 3
(1) preparation of jean yarn: cowboy warp thread preparation include yarn setting, winder, warping, warp thread indigo dyeing and on
The processes such as slurry, specifically:
Yarn setting:
In denim production, pair warp and weft yarn, especially with the twist biggish warp and weft when, Yao Jinhang dewing and heating,
To stablize its twist；The purpose of dead twist be in order to warping, dye slurry process go on smoothly and reduce weave when sluff-offs, looped weft and
Phenomena such as looping, improves fabric quality；It is required that stablizing yarn twist, regain by increasing the methods of tension, dewing, heating
8%~9%；
Pulp
Equipment: sizing-dyeing machine；
Technique: warp beam → wettability treatment → dyeing → warm water washing → starching；
1. wettability treatment: bleeding agent (still or few bubble) FK-ST10C 1.5g/L, caustic soda 1g/L, 80 DEG C of temperature, time 20
±5s
2. dyeing: material uses vatting material method when using indigo dye and dyeing, and dyestuff includes bipseudoindoxyl dye 63g/L, insurance
Powder 85g/L, caustic soda 58g/L, bleeding agent FK-ST10C4.5g/L, dye liquor temperature are 20 DEG C, and padding number is that six leachings six are rolled, and are rolled remaining
Rate 80% pads time 20s
3. starching: slurries control under the conditions of meta-alkalescence, the use of temperature are 98 DEG C, second dipping and rolling starching, and pick-up rate is
80%, jean yarn is prepared as warp thread in the rate of sizing 12%, spare；
(2) preparation of reflective yarn: EtOH Sonicate cleans polyester filament 30min, dry, and the polyester filament after drying is impregnated
In the dimethyl sulphoxide solution containing potassium hydroxide (120mg KOH is dissolved in 30mL DMSO and 10mL deionized water), bath raio is
1:20 impregnates 10min, is then washed with water 3 times, the polyester filament of surface hydroxylation can be obtained in drying；
The polyester filament of the above-mentioned surface hydroxylation being prepared is taken to be immersed in containing glutaraldehyde, sodium citrate and polyethylene
In the mixed solution of pyrrolidones (PVP), wherein the mass ratio of glutaraldehyde, sodium citrate and water is 1:8:12, adds nitre
Sour silver, the concentration of silver nitrate are 0.3mol/L, and the mass ratio of silver nitrate and sodium citrate, PVP is 1:2:2, is reacted at 80 DEG C
35min, bath raio 1:15, is cooled to room temperature later, takes out the long yarn of terylene for being coated with nano-Ag particles after impregnating 45min, washes
It washs, dry, reflective yarn can be prepared；
Using the reflective yarn prepared and 3 100D/48F semi-gloss terylene doubling twistings as weft yarn；
(3) it weaves: carrying out woven weaving under being 65% in relative humidity；
(4) it singes: maintaining the speed of 90 meters/min, quickly singe；
(5) starching: keeping the stiffness of cowboy, while paying attention to the use of auxiliary agent, cannot destroy the brightness of reflective composite yarn；
(6) final finishing: 1. shape: shaped with boarding machine, oven temperature be 150 DEG C, while control cloth requirement width and
Grammes per square metre；By adjusting the tension of each deflector roll, prevents fabric from becoming after wash water tiltedly, 2. cool down；
(7) preshrunk: carrying out preshrunk to fabric on squeezing machine, controls finished product shrinkage ± 5%；
(8) fabric is washed: when pH value is 6.5, cleaning 3h is carried out with the cellulase that concentration is 1.5%, bath raio 1:
30, reflective denim fabric can be obtained.
Pass through scanning electron microscope analysis, it is known that the particle diameter of the nano silver on denim fabric is about 400~500nm.
Comparative example 1
(1) with (1) the step of embodiment 1；
(2) preparation of reflective yarn: EtOH Sonicate cleans polyester filament 30min, dry, and the polyester filament after drying is impregnated
In the dimethyl sulphoxide solution containing potassium hydroxide (120mg KOH is dissolved in 30mL DMSO and 10mL deionized water), bath raio is
1:20 impregnates 10min, is then washed with water 3 times, the polyester filament of surface hydroxylation can be obtained in drying；
The polyester filament of the above-mentioned surface hydroxylation being prepared is taken to be immersed in containing glutaraldehyde, sodium citrate and polyethylene
In the mixed solution of pyrrolidones (PVP), wherein the mass ratio of glutaraldehyde, sodium citrate and water is 1:8:12, adds nitre
Sour silver, the concentration of silver nitrate are 0.2mol/L, and the mass ratio of silver nitrate and sodium citrate, PVP is 1:2:2, is reacted at 80 DEG C
35min, bath raio 1:15, is cooled to room temperature later, takes out the long yarn of terylene for being coated with nano-Ag particles after impregnating 45min, washes
It washs, dry, reflective yarn can be prepared；
Using the reflective yarn prepared and 3 100D/48F semi-gloss terylene doubling twistings as weft yarn；
(3)~(8) are with (3) the step of embodiment 1~(8), the reflective denim fabric that is prepared.
Pass through scanning electron microscope analysis, it is known that, the particle diameter of the nano silver on denim fabric is about 80~100nm.
Comparative example 2
When after the preparation of reflective yarn without coating silicone oil, remaining step is consistent with embodiment 1, the reflective cowboy being prepared
Fabric.
Correlated performance test:
1, reflectance test: Example 1~3 and reflective denim fabric prepared by comparative example 1~2 and its corresponding ferment
Element wash after fabric sample 6cm*6cm piece sample, according to the measurement standard of GB/T 3979-2008 object color, using the U.S.
The UltraScan PRO superhigh precision profession spectrophotometric color measurement instrument of Hunterlab company production passes through product under D65 light conditions
Its reflectivity of d/8 ° of structured testing of bulb separation, reflectivity data be 380nm-780nm every the light wave of 5nm wavelength reflectivity plus
Weight average value, weight correspond to the ability distribution curve of D65 light source, and test data is recorded in table 1.
2, the fabric after ENZYME WASH will be prepared and wash 50 and 100 times in water, after the same method aspect of measure
The reflectivity of material, the results are shown in Table 1.
The reflectivity as it can be seen that reflectivity of denim fabric is prepared up to 60% or more in the present invention, and after washing 50 times
50% or more is still maintained, therefore, the denim fabric that reflectivity is high, reflecting properties are stable has been prepared in the present invention.
The reflectivity of reflective denim fabric and washed rear corresponding fabric that 1 Examples 1 to 3 of table is prepared with comparative example 1~2
Although the present invention has been described by way of example and in terms of the preferred embodiments, it is not intended to limit the invention, any to be familiar with this skill
The people of art can do various change and modification, therefore protection model of the invention without departing from the spirit and scope of the present invention
Enclosing subject to the definition of the claims.
Claims (10)
1. a kind of production method of reflective denim fabric, which is characterized in that the described method comprises the following steps:
(1) preparation of jean yarn: dyeing obtains jean yarn as warp thread, spare；
(2) preparation of reflective yarn: EtOH Sonicate cleans polyester filament 25-35min, dry, and the polyester filament after drying is impregnated
10~20min is impregnated in the dimethyl sulphoxide solution containing alkali, is then washed with water 2~3 times, table can be obtained in drying
The hydroxylated polyester filament in face, wherein alkali: DMSO: the ratio of water is 110~130mg:20~40mL:10~20mL；
The polyester filament of the above-mentioned surface hydroxylation being prepared is taken to be immersed in mixed solution, the mixed solution is to contain penta
The aqueous solution of dialdehyde, sodium citrate and polyvinylpyrrolidone PVP, wherein the mass ratio of glutaraldehyde, sodium citrate and water is 1:
(2~10): (10~12) add silver nitrate later, and the mass ratio of silver nitrate and sodium citrate, PVP is 1:(0.5~2):
(0.02~2) is reacted 15~35min at 80~120 DEG C, is cooled to room temperature later, takes out and washs after dipping 45min~90min
The long yarn of synthetic fibre, washing, drying, reflective yarn can be prepared by uniformly being coated using silicone oil；
Using the reflective yarn prepared and 2~4 spun polyester thread doubling twistings as weft yarn；
(3) it weaves；
(4) it singes；
(5) starching；
(6) final finishing, setting；
(7) preshrunk；
(8) fabric is washed: carrying out ENZYME WASH, reflective denim fabric can be obtained；
Wherein, the concentration of silver nitrate is 0.3~0.5mol/L.
2. a kind of production method of reflective denim fabric according to claim 1, which is characterized in that the alkali is hydroxide
Sodium or potassium hydroxide.
3. a kind of production method of reflective denim fabric according to claim 1 or 2, which is characterized in that in step (1),
The dyeing is beam dyeing, the step of beam dyeing specifically: yarn setting, indigo dyeing and starching.
4. the production method of any a kind of reflective denim fabric according to claim 1~3, which is characterized in that step (2)
Described in it is dry for 1.5~2h dry at 60~80 DEG C.
5. a kind of production method of reflective denim fabric according to any one of claims 1 to 4, which is characterized in that the silicon
Oil is methyl-silicone oil.
6. the production method of any a kind of reflective denim fabric according to claim 1~5, which is characterized in that described fixed
Shape are as follows: shaped with boarding machine, oven temperature is 150~200 DEG C.
7. the production method of any a kind of reflective denim fabric according to claim 1~6, which is characterized in that the ferment
Element wash for be 1.5%~2%o.w.f with concentration cellulase clean 2~4h, bath raio is 1:20~30.
8. the production method of any a kind of reflective denim fabric according to claim 1~7, which is characterized in that described to receive
The partial size of rice Argent grain is 300nm~5 μm.
9. the reflective denim fabric that a kind of production method of any reflective denim fabric of claim 1~8 is prepared.
10. the clothing being prepared using reflective denim fabric as claimed in claim 9.
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| CN204070687U (en) * | 2014-10-15 | 2015-01-07 | 黄美娟 | A kind of insulation insulation antibiosis denim |
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| CN107217366A (en) * | 2017-07-19 | 2017-09-29 | 佛山市立笙纺织有限公司 | A kind of weft yarn uses the elastic denim fabric and its technique of the core-spun elastic yarn of multiple cladding |
| CN108004802A (en) * | 2017-12-10 | 2018-05-08 | 江苏大同宝富纺织科技有限公司 | A kind of spring, the sub- dyed fabric colored appearance that spins increased deep method |
| CN108356282A (en) * | 2018-03-16 | 2018-08-03 | 南京林业大学 | The preparation method of flake silver powder in a kind of acid medium |
| CN108580920A (en) * | 2018-03-16 | 2018-09-28 | 南京林业大学 | A kind of preparation method of flake silver powder |
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