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CN109827066A - A kind of external vacuum maintenance device and method - Google Patents

A kind of external vacuum maintenance device and method Download PDF

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Publication number
CN109827066A
CN109827066A CN201811544426.8A CN201811544426A CN109827066A CN 109827066 A CN109827066 A CN 109827066A CN 201811544426 A CN201811544426 A CN 201811544426A CN 109827066 A CN109827066 A CN 109827066A
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CN
China
Prior art keywords
temperature
low
evaporable getter
vacuum
piece
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811544426.8A
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Chinese (zh)
Inventor
成永军
冯天佑
孙雯君
陈联
赵澜
习振华
裴晓强
丁栋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lanzhou Institute of Physics of Chinese Academy of Space Technology
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Lanzhou Institute of Physics of Chinese Academy of Space Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lanzhou Institute of Physics of Chinese Academy of Space Technology filed Critical Lanzhou Institute of Physics of Chinese Academy of Space Technology
Priority to CN201811544426.8A priority Critical patent/CN109827066A/en
Publication of CN109827066A publication Critical patent/CN109827066A/en
Pending legal-status Critical Current

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Abstract

The present invention provides a kind of external vacuums to maintain device and method, can be realized vacuum acquirement and the maintenance of low-temperature (low temperature) vessel interlayer, and structure is simple, easy for installation, reliable operation.Apparatus of the present invention belong to external vacuum and maintain device, external can complete activation, avoid influence of the high temperature to interlayer, the vacuum keeping apparatus especially suitable for active gases;Apparatus of the present invention realize air-breathing using non-evaporable getter piece, and non-evaporable getter piece Balance Air forces down, gulp capacity is big, gettering rate is high, can effectively extract interlayer outlet and maintain higher vacuum;Non-evaporable getter piece pump of the invention is installed using flange, is easily changed inspiration piece, can effectively be extracted the gas of low-temperature (low temperature) vessel interlayer generation.

Description

A kind of external vacuum maintenance device and method
Technical field
The invention belongs to vacuum acquirement and maintain technical field, and in particular to a kind of external vacuum maintains device and side Method, the vacuum for low-temperature (low temperature) vessel interlayer maintain.
Background technique
The acquisition of laminated vacuum and maintenance are extremely important in low-temperature (low temperature) vessel, and the influence to insulation effect is very big.Vacuum interlayer Interior residual gas is mainly H2、CO、CH4And Ar, wherein H2Average content reach 80.93%, and with the change of standing time It is long, H2Partial pressure increasing always.It is important for effectively keeping the vacuum degree of interlayer space to have that suction sheet is set in interlayer Effect, the vacuum life of interlayer is heavily dependent on the characteristic and charge weight of suction sheet.Low-temperature (low temperature) vessel interlayer is often used Molecular sieve and active carbon can effectively maintain vacuum as suction sheet, but they are to H2Adsorption capacity it is poor;For H2Partial pressure The higher problem of power can effectively extract H at present using the method for placing PdO2, but PdO price is higher, considerably increases low The cost of warm container;Non-evaporable getter piece has stronger H2Abstraction ability, it is cheap, but its activationary temperature is higher, exceeds Interlayer tolerable temperature, for the vacuum of active gases maintains and is not suitable for.Therefore, it is badly in need of a kind of at low cost and no sharp The vacuum of temperature limiting living maintains product.
Summary of the invention
The present invention provides a kind of external vacuums to maintain device and method, and the vacuum that can be realized low-temperature (low temperature) vessel interlayer obtains With maintenance, structure is simple, easy for installation, reliable operation.
To achieve the above object, external vacuum of the invention maintains device, for carrying out vacuum to low-temperature (low temperature) vessel interlayer It maintains, including induction chamber, non-evaporable getter piece pump, temperature conditioning unit and pumping unit;
Wherein, non-evaporable getter piece pump is arranged inside induction chamber, including non-evaporable getter piece and heating rod;Its Middle non-evaporable getter piece is mounted on heating rod;
Induction chamber is respectively communicated with pumping unit and low-temperature (low temperature) vessel interlayer by the admission line equipped with shut-off valve;Wherein, lead to It crosses the pipeline equipped with interlayer connection valve to connect with low-temperature (low temperature) vessel interlayer, be connect by being equipped with the other pipeline for taking out valve with pumping unit; Induction chamber is equipped with power interface, and heating rod connects temperature conditioning unit by power interface;
Temperature conditioning unit is for regulating and controlling the temperature of non-evaporable getter piece.
Wherein, the non-evaporable getter piece uses the zirconium vanadium iron non evaporable getter material of porous structure.
Wherein, the induction chamber material is stainless steel material.
Wherein, the induction chamber structure is cylindrical structure.
Wherein, more than two non-evaporable getter pieces are mounted on heating rod along the arrangement of heating rod axial direction uniform intervals On, and pass through stainless steel washer space between adjacent two panels non-evaporable getter piece.
Wherein, it is connecting flange that induction chamber, which is equipped with an end wall surface of power interface,.
Wherein, the heating rod is made of nichrome;The temperature conditioning unit is realized using thermocouple to non-evaporable The measurement of inspiration piece temperature.
A kind of vacuum of the invention maintains method, maintains device using above-mentioned external vacuum, includes the following steps:
Step 1, other pumping valve and shut-off valve are opened, is vacuumized induction chamber by pumping unit, vacuum degree reaches setting value Afterwards, other pumping valve and shut-off valve are closed;
Step 2, starting heating rod heats non-evaporable getter piece, opens temperature conditioning unit to the temperature of non-evaporable getter piece It is adjusted, reaches activationary temperature;After the temperature of non-evaporable getter piece reaches activationary temperature setting time, temperature is closed Control unit;
Step 3, it maintains device to connect with low-temperature (low temperature) vessel interlayer the external vacuum, opens other pumping valve, utilize After pumping unit vacuumizes linkage section, other pumping valve is closed, interlayer connection valve and shut-off valve is opened, is tieed up using external vacuum The gas that device abstraction low-temperature (low temperature) vessel interlayer is released is held, low-temperature (low temperature) vessel laminated vacuum is maintained.
Wherein, if the vacuum degree of low-temperature (low temperature) vessel interlayer is less than setting value, disconnect the external vacuum maintain device with it is low Warm container interlayer repeats step 2- step 3.
Wherein, in the step 1, when the internal pressure of induction chamber is less than 1 × 10-2After Pa, temperature conditioning unit, temperature control list are opened Member control heating rod heats non-evaporable getter piece;In the step 2, make non-evaporable getter piece 400 DEG C~450 After keeping the temperature 30min or more under DEG C activationary temperature, temperature conditioning unit is closed, stops heating, naturally cools to non-evaporable getter piece Environment temperature.
The utility model has the advantages that
Apparatus of the present invention belong to external vacuum and maintain device, external can complete activation, avoid high temperature to interlayer It influences, the vacuum keeping apparatus especially suitable for active gases;Apparatus of the present invention realize air-breathing using non-evaporable getter piece, non- Evaporable inspiration piece Balance Air forces down, gulp capacity is big, gettering rate is high, can effectively extract interlayer outlet and maintain compared with Gao Zhen Reciprocal of duty cycle;Non-evaporable getter piece pump of the invention is installed using flange, is easily changed inspiration piece, can effectively extract low-temperature (low temperature) vessel folder The gas that layer generates.
Detailed description of the invention
Fig. 1 is schematic structural diagram of the device of the invention;
Wherein, 1- interlayer connection valve;Valve is taken out by 2-;3- shut-off valve;4- induction chamber;5- non-evaporable getter piece; 6- heating rod;7- mounting flange;8- power interface;9- temperature conditioning unit;10- is evacuated unit;11- low-temperature (low temperature) vessel interlayer.
Specific embodiment
With reference to the accompanying drawing, develop simultaneously embodiment, and the present invention will be described in further detail.
External vacuum of the present invention maintains device to be used to carry out vacuum maintenance, the present embodiment device to low-temperature (low temperature) vessel interlayer 11 Structure is as shown in Figure 1, include induction chamber 4, non-evaporable getter piece pump, temperature conditioning unit 9 and pumping unit 10.
Wherein, non-evaporable getter piece pump is arranged inside induction chamber 4, including non-evaporable getter piece 5 and heating rod 6;Wherein non-evaporable getter piece 5 is mounted on heating rod 6 and along the axial uniform intervals arrangement of heating rod 6 by stainless steel pad Space between adjacent two panels is enclosed, avoids adjacent two panels non-evaporable getter piece 5 from contacting, increases the suction of non-evaporable getter piece Gas area improves the uniformity that non-evaporable getter piece 5 activates;Wherein, non-evaporable getter piece 5 is the zirconium using porous structure Vanadium iron non evaporable getter material, can be used at normal temperature, have the characteristics that activationary temperature is low, gulp capacity is big;Heating rod 6 It is made of nichrome, heating efficiency is relatively high.
Induction chamber 4 is made by stainless steel material and is obtained, can reduced for placing non-evaporable getter piece pump, induction chamber 4 Deflation rate;4 structure of induction chamber is cylindrical structure, easy to process, and space utilization rate is high.4 one end wall surface of induction chamber is equipped with opening, leads to It crosses the admission line equipped with shut-off valve 3 and is respectively communicated with pumping unit 10 and low-temperature (low temperature) vessel interlayer 11;Wherein, connected by being equipped with interlayer The pipeline for connecing valve 1 is connect with low-temperature (low temperature) vessel interlayer 11, is connect by being equipped with the other pipeline for taking out valve 2 with pumping unit 10;Induction chamber 4 Another end wall surface is connecting flange 7, and the sealing of induction chamber 4 is realized by connecting flange 7, and connecting flange 7 is equipped with power interface 8, heating rod 6 connects temperature conditioning unit 9 by power interface 8;Heating rod 6 and power interface 8 are fixed on connecting flange 7.Due to Connecting flange 7 is detachable, so that the activation of non-evaporable getter piece 5 is readily achieved with replacement.Connecting flange 7 uses stainless steel material Production.
Temperature conditioning unit 9 is realized using thermocouple to non-evaporable getter piece for regulating and controlling the temperature of non-evaporable getter piece 5 The measurement of 5 temperature, and then the regulation by the control realization of heating rod 6 to 5 temperature of non-evaporable getter piece.
Pumping unit 10 be used between interlayer connection valve 1 and shut-off valve 3 connecting line and induction chamber 4 vacuumize.
Apparatus of the present invention can be with the other types suction sheet such as molecular sieve that is arranged in low-temperature (low temperature) vessel interlayer 11 etc. simultaneously It uses, removes other residual gas using molecular sieve, protect the non-evaporable getter piece in apparatus of the present invention, while utilizing this hair Bright device extracts H2, effectively obtain and maintain the vacuum degree of low-temperature (low temperature) vessel interlayer 11.
In use, first vacuumizing induction chamber 4 by being evacuated unit 10, temperature control list is then connected by power interface 8 Member 9, is adjusted by temperature of the temperature conditioning unit 9 to non-evaporable getter piece 5;The temperature of non-evaporable getter piece 5, which reaches, to be set Definite value for a period of time after, non-evaporable getter piece 5 is activated, close temperature conditioning unit 9;Apparatus of the present invention and low-temperature (low temperature) vessel are pressed from both sides Layer 11 connects, and vacuumizes linkage section using pumping unit 10, opens shut-off valve 3, device just can extract low-temperature (low temperature) vessel The gas that interlayer 11 is released maintains 11 vacuum of low-temperature (low temperature) vessel interlayer.After non-evaporable getter piece 5 activates, working life and dimension It is related to hold the gas flow generated in low-temperature (low temperature) vessel interlayer 11, when finding that pumping speed ability is decreased obviously, temperature conditioning unit 9 can be passed through Carrying out heat activation work again makes non-evaporable getter piece 5 have adsorption capacity.Specific workflow includes the following steps:
Step 1, shut-off valve 3 and other pumping valve 2 are opened, induction chamber 4 is vacuumized using pumping unit 10;
When the internal pressure of induction chamber 4 is less than 1 × 10-2After Pa, shut-off valve 3 and other pumping valve 2 are closed;
Step 2, temperature conditioning unit 9 is opened, temperature conditioning unit 9 controls heating rod 6 and heats to non-evaporable getter piece 5;It is non- After evaporable inspiration piece 5 keeps the temperature 30min or more under 400 DEG C~450 DEG C activationary temperatures, temperature conditioning unit 9 is closed, stops heating, Inspiration piece is set to naturally cool to environment temperature;
Step 3, induction chamber 4 is connect with low-temperature (low temperature) vessel interlayer 11, opens shut-off valve 3 and other pumping valve 2, and utilize air exhauster 10 pairs of linkage sections of group vacuumize, and close other pumping valve 2, open interlayer connection valve 1, extract low-temperature (low temperature) vessel interlayer 11 by induction chamber 4 The gas of releasing maintains 11 vacuum of low-temperature (low temperature) vessel interlayer;
In 11 course of work of low-temperature (low temperature) vessel interlayer, if (low-temperature (low temperature) vessel when 5 exhaust capacity of non-evaporable inspiration piece is decreased obviously The vacuum degree of interlayer is less than setting value), step 1~step 3 is repeated, non-evaporable getter piece is pumped and carries out heat activation again.
The present invention avoids non-evaporable getter piece 5 from swashing by the way that non-evaporable getter piece 5 to be isolated with low-temperature (low temperature) vessel interlayer 11 High temperature when living damages interlayer, maintains so as to be applied to the vacuum of low-temperature (low temperature) vessel interlayer 11, substitutes expensive oxygen Change palladium gettering material;The present invention can directly be utilized to existing low-temperature (low temperature) vessel or simple transformation, while can easily replace air-breathing Piece, it is easy to use.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.

Claims (10)

1. a kind of external vacuum maintains device, for carrying out vacuum maintenance to low-temperature (low temperature) vessel interlayer (11), which is characterized in that packet Include induction chamber (4), non-evaporable getter piece pump, temperature conditioning unit (9) and pumping unit (10);
Wherein, the setting of non-evaporable getter piece pump is internal in induction chamber (4), including non-evaporable getter piece (5) and heating rod (6);Wherein non-evaporable getter piece (5) is mounted on heating rod (6);
Induction chamber (4) is respectively communicated with pumping unit (10) and low-temperature (low temperature) vessel interlayer by the admission line equipped with shut-off valve (3) (11);Wherein, it is connect by being equipped with the pipeline of interlayer connection valve (1) with low-temperature (low temperature) vessel interlayer (11), by being equipped with other pumping valve (2) Pipeline with pumping unit (10) connect;Induction chamber (4) is equipped with power interface (8), and heating rod (6) passes through power interface (8) It connects temperature conditioning unit (9);
Temperature conditioning unit (9) is for regulating and controlling the temperature of non-evaporable getter piece (5).
2. external vacuum as described in claim 1 maintains device, which is characterized in that the non-evaporable getter piece (5) is adopted With the zirconium vanadium iron non evaporable getter material of porous structure.
3. external vacuum as described in claim 1 maintains device, which is characterized in that induction chamber (4) material is stainless Steel material.
4. external vacuum as described in claim 1 maintains device, which is characterized in that induction chamber (4) structure is cylinder Structure.
5. external vacuum as described in claim 1 maintains device, which is characterized in that more than two non-evaporables are inhaled Gas piece (5) is mounted on heating rod (6) along the axial uniform intervals arrangement of heating rod (6), and passes through stainless steel washer space between adjacent Two panels non-evaporable getter piece.
6. external vacuum as described in claim 1 maintains device, which is characterized in that induction chamber (4) is equipped with power interface (8) An end wall surface be connecting flange (7).
7. external vacuum as described in claim 1 maintains device, which is characterized in that the heating rod (6) is closed using nickel chromium triangle Gold production;The temperature conditioning unit (9) realizes the measurement to non-evaporable getter piece (5) temperature using thermocouple.
8. a kind of vacuum maintains method, device is maintained using external vacuum as described in claim 1, which is characterized in that packet Include following steps:
Step 1, other pumping valve (2) and shut-off valve (3) are opened, is vacuumized induction chamber (4) by pumping unit (10), vacuum degree reaches To after setting value, other pumping valve (2) and shut-off valve (3) are closed;
Step 2, starting heating rod (6) heating non-evaporable getter piece (5) opens temperature conditioning unit (9) to non-evaporable getter piece (5) temperature is adjusted, and reaches activationary temperature;When the temperature of non-evaporable getter piece (5) reaches activationary temperature setting Between after, close temperature conditioning unit (9);
Step 3, maintain device to connect with low-temperature (low temperature) vessel interlayer (11) external vacuum, open other pumping valve (2) with And shut-off valve (3), after being vacuumized linkage section using pumping unit (10), other pumping valve (2) is closed, is opened interlayer connection valve (1), The gas for maintaining device abstraction low-temperature (low temperature) vessel interlayer (11) to release using external vacuum maintains low-temperature (low temperature) vessel interlayer (11) true It is empty.
9. vacuum as claimed in claim 8 maintains method, which is characterized in that if the vacuum degree of low-temperature (low temperature) vessel interlayer (11) is less than Setting value disconnects the external vacuum and maintains device and low-temperature (low temperature) vessel interlayer (11), repeats step 2- step 3.
10. vacuum as claimed in claim 8 maintains method, in the step 1, when induction chamber (4) internal pressure less than 1 × 10-2It after Pa, opens temperature conditioning unit (9), non-evaporable getter piece (5) is heated in temperature conditioning unit (9) control heating rod (6); In the step 2, after so that non-evaporable getter piece (5) is kept the temperature 30min or more under 400 DEG C~450 DEG C activationary temperatures, temperature is closed It controls unit (9), stops heating, non-evaporable getter piece (5) is made to naturally cool to environment temperature.
CN201811544426.8A 2018-12-17 2018-12-17 A kind of external vacuum maintenance device and method Pending CN109827066A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114928934A (en) * 2022-06-20 2022-08-19 中国科学院近代物理研究所 Fixing device for accelerator vacuum chamber non-evaporable getter sheet and using method thereof

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CN102117723A (en) * 2010-01-05 2011-07-06 中国科学院物理研究所 Vacuum air pumping device
CN102814146A (en) * 2012-08-02 2012-12-12 上海交通大学 High-efficiency hydrogen removal device in high-vacuum multilayer heat-insulation cryogenic container
CN102938356A (en) * 2012-10-23 2013-02-20 北京市北分仪器技术有限责任公司 Vacuum maintaining system for vacuum device
CN103808383A (en) * 2013-12-24 2014-05-21 兰州空间技术物理研究所 Working volume measuring device and method for reducing device wall air outlet error
CN104235598A (en) * 2013-06-21 2014-12-24 青岛康威龙日用品有限公司 Interlayer adsorbent box of thermal insulating container
CN104728075A (en) * 2013-12-19 2015-06-24 北京有色金属研究总院 Internal-heating type getter element and high-pumping-speed getter pump
CN204805943U (en) * 2015-06-10 2015-11-25 汇达重工股份有限公司 Novel low temperature container manages to find time device
JP6016159B2 (en) * 2012-12-21 2016-10-26 大学共同利用機関法人 高エネルギー加速器研究機構 Non-evaporable getter pump
CN106224202A (en) * 2016-08-31 2016-12-14 兰州空间技术物理研究所 A kind of non-evaporable adsorption pump utilizing electrical heating to activate
CN108119329A (en) * 2017-12-20 2018-06-05 南京华东电子真空材料有限公司 A kind of compact-sized sundstrand pump of big pumping speed

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1995016166A1 (en) * 1993-12-10 1995-06-15 Saes Getters S.P.A. Vacuum stabilizer and method for the manufacture thereof
CN102117723A (en) * 2010-01-05 2011-07-06 中国科学院物理研究所 Vacuum air pumping device
CN102814146A (en) * 2012-08-02 2012-12-12 上海交通大学 High-efficiency hydrogen removal device in high-vacuum multilayer heat-insulation cryogenic container
CN102938356A (en) * 2012-10-23 2013-02-20 北京市北分仪器技术有限责任公司 Vacuum maintaining system for vacuum device
JP6016159B2 (en) * 2012-12-21 2016-10-26 大学共同利用機関法人 高エネルギー加速器研究機構 Non-evaporable getter pump
CN104235598A (en) * 2013-06-21 2014-12-24 青岛康威龙日用品有限公司 Interlayer adsorbent box of thermal insulating container
CN104728075A (en) * 2013-12-19 2015-06-24 北京有色金属研究总院 Internal-heating type getter element and high-pumping-speed getter pump
CN103808383A (en) * 2013-12-24 2014-05-21 兰州空间技术物理研究所 Working volume measuring device and method for reducing device wall air outlet error
CN204805943U (en) * 2015-06-10 2015-11-25 汇达重工股份有限公司 Novel low temperature container manages to find time device
CN106224202A (en) * 2016-08-31 2016-12-14 兰州空间技术物理研究所 A kind of non-evaporable adsorption pump utilizing electrical heating to activate
CN108119329A (en) * 2017-12-20 2018-06-05 南京华东电子真空材料有限公司 A kind of compact-sized sundstrand pump of big pumping speed

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114928934A (en) * 2022-06-20 2022-08-19 中国科学院近代物理研究所 Fixing device for accelerator vacuum chamber non-evaporable getter sheet and using method thereof

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Application publication date: 20190531