CN109757768A - A kind of cigarette filter tip rod and its preparation process - Google Patents
A kind of cigarette filter tip rod and its preparation process Download PDFInfo
- Publication number
- CN109757768A CN109757768A CN201910117828.8A CN201910117828A CN109757768A CN 109757768 A CN109757768 A CN 109757768A CN 201910117828 A CN201910117828 A CN 201910117828A CN 109757768 A CN109757768 A CN 109757768A
- Authority
- CN
- China
- Prior art keywords
- extract
- polypropylene fibre
- added
- modified
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention discloses a kind of cigarette filter tip rod and its preparation process, which is made of modified fibre, compound additive and modified forming paper conversion；Preparation process of the present invention is modified polypropylene fibre by dilute alkaline soln and polymer emulsion, wherein dilute alkaline soln, which corrodes polypropylene fibre surface irregularities, forms the pit-hole of out-of-flatness on polypropylene fibre surface, adhered to again by polymer emulsion particles on the surface of polypropylene fibre, the degree of roughness on polypropylene fibre surface is improved, to improve polypropylene fibre to the adsorption capacity of tar；Compound additive is added in the present invention in a binder; compound additive is using attapulgite as skeleton; and tobacco material extract and carragheen are loaded on attapulgite; carragheen plays good protecting effect to tobacco material extract; in smoking cigarette; the smell of tar is covered by the fragrance of tobacco, and filter rod is promoted to the adsorption capacity of tar by attapulgite.
Description
Technical field
The invention belongs to technical field of cigarette production.Specifically, being related to a kind of cigarette filter tip rod and its preparation process.
Background technique
Cigarette is the tobacco product that pipe tobacco is made to strip with cigarette paper, and relatively common at home at present is fire-cured tobacco type and mixed
Mould assembly, cigarette structure mainly include filter rod and cigarette, and filter rod and cigarette are by connecting paper joint forming, and wherein filter rod is
Filtering material is processed into the filter tip shape of strip by forming paper, filter rod can be by tar, the nicotine, one in cigarette
The noxious substances such as carbonoxide a part, to reduce smoking cigarette to the harm of human body and the pollution of environment.
In the prior art, cigarette filter tip rod mainly uses cellulose acetate fibre and both materials of polypropylene fibre,
Wherein polypropylene fibre is non-polar material, and one side adsorption capacity is poor, can not effectively retain the harmful substances such as tar, another
Aspect adhesive force is poor, and the forming technology of cigarette filter tip rod is caused to complicate, and cellulose acetate fibre adsorption effect is compared to poly-
Tacryl has higher promotion, but its adsorption effect still has very high room for promotion, and cellulose acetate is fine
The higher cost of dimension, degradation time is longer, present cigarette in aspiration procedure, with the tar content adsorbed on filter rod by
It is gradually promoted, bitterness sense of the cigarette in suction can also greatly promote, and influence the suction taste of cigarette, therefore how to be promoted in filter rod and inhaled
Enclosure material reduces in smoking cigarette the adsorption capacities of the harmful substances such as tar, and influence of the tar to taste is inhaled, is current
One of cigarette manufacture industry problem to be solved, in order to solve this problem, the present invention provides following technical schemes.
Summary of the invention
The purpose of the present invention is to provide a kind of cigarette filter tip rod and its preparation processes.
The technical problem to be solved in the invention are as follows:
In the prior art, cigarette filter tip rod is to the limited sorption capacity of smoke tar, can not be to generating in cigarette aspiration procedure
Smoke tar realize a large amount of absorption, meanwhile, with the suction of cigarette, the tar content contained in filter rod also can be promoted gradually,
And there is bitterness sense in the second half section that the tar that attachment is largely adsorbed on filter rod will lead to cigarette suction；
In the prior art, filtering material used in the filter rod of cigarette mainly uses cellulose acetate, and low grade is rolled up
The filtering material of cigarette then selects polyethylene fibre to prepare, but mouthfeel when polyethylene fibre is to cigarette smoking is affected.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of cigarette filter tip rod is made of modified fibre, compound additive and modified forming paper conversion；
The modified fibre is modified polypropylene fiber, by being modified to polypropylene fibre, improves polypropylene fibre
The ability of oil is protected in the oil suction of dimension；
The compound additive is prepared by tobacco material extract, attapulgite, carragheen, stearoylketene calcium lactate,
It is able to ascend fragrance, covers the bitter taste of tar；
As further scheme of the invention, the modified forming paper is added by the forming paper that air permeability is 8000-12000cu
Work is prepared, and the forming paper of high-air-permeability is able to ascend the flow measurement air capacity of filter rod, to reduce the cigarette by filter rod
Tolerance can play the effect of tar reduction；
The preparation process of the cigarette filter tip rod includes the following steps:
Step 1: polypropylene fibre is added in 5% sodium hydroxide solution and impregnates 4-8h by the preparation of modified fibre, will
Polypropylene fibre, which is rinsed after pulling out with deionized water, dries, and the polypropylene fibre after drying is added in polymer emulsion and is impregnated
20-40 minutes, as further scheme of the invention, during immersion of the polypropylene fibre in polymer emulsion, simultaneously
Polypropylene fibre is ultrasonically treated, the dispersion degree of promotion polymer beads in the fibre, by polypropylene fibre after separation of solid and liquid
Dimension is dried for standby, and during this, forms rough etch pit on the surface of polypropylene fibre by dilute alkaline soln first
Hole, then adhered to by polymer emulsion particles on the surface of polypropylene fibre, further improve the thick of polypropylene fibre surface
Rough degree, so that the adsorption capacity of polypropylene fibre is promoted, as further scheme of the invention, the list of the polymer emulsion
Body is preferably oleophylic monomer, and oleophylic monomer surface has a large amount of non-polar groups, is able to ascend the oil-retaining of polypropylene fibre；
Step 2: shredding, it will be spare after modified fibre shredding；
Step 3: the preparation of compound additive, specific preparation process include the following steps:
S1, offal, offal are cleaned in the dehydrated alcohol for be added after drying 35-60 DEG C and impregnates 2-7h, solid-to-liquid ratio 1:4-
7, offal and the fragrance matter in offal are extracted, dehydrated alcohol extract can lower significantly protein in extracting solution,
Dehydrated alcohol is concentrated after separation of solid and liquid, it is stand-by to obtain tobacco material extract paste by the substances such as starch；
S2, the carragheen that 4-5 parts by weight are added into 100 parts by weight of deionized water, reduce after ebuillition of heated 8-12min and go
The stearoylketene calcium lactate of 1-2 parts by weight is added to 65-80 DEG C in ion coolant-temperature gage thereto, continues stirring to stearoylketene calcium lactate
It is completely dissolved and stearoylketene calcium lactate is uniformly mixed with carragheen, obtain mixing liquid, keeping the temperature of mixing liquid is 65-80
℃；
S3, tobacco material extract obtained in step S1 is added in mixing liquid obtained in step S2, wherein cream
The weight ratio of shape object and mixing liquid is 1-1.5:100, is made by stirring or ultrasonication non-in tobacco material extract
Water-soluble substances can be evenly dispersed in the liquid phase, and the temperature of holding liquid-phase system is in the dispersion process of tobacco material extract
65-80 DEG C, and whole process at least carries out 10-20min, and the ethyl alcohol in paste is made sufficiently to volatilize, treatment fluid is obtained, at holding
The temperature for managing liquid is 65-80 DEG C；
In S4, the treatment fluid for obtaining attapulgite addition previous step, it is ultrasonically treated during stirring, ultrasound
Time is 11-14min, is separated by solid-liquid separation after ultrasound and obtains attapulgite, which can extend the micropore knot of attapulgite
Structure promotes the specific surface area of attapulgite, promotes the adsorption capacity and load capacity of attapulgite；
After 15-25 DEG C S5, the attapulgite for obtaining previous step of cold wind drying, attapulgite is fully dispersed
To compound additive, dispersion is dispersed by one of pulverizer crushing, grinding, ball milling, prevents carragheen cooling solidification
A large amount of attapulgites are made to be bonded together.
Step 4: compound additive and binder are uniformly applied on tow by sizing after evenly mixing；
Step 5: the preparation of modified forming paper, on the two sides that air permeability is the forming paper that air permeability is 8000-12000cu
Extract coating is coated, the extract coating is made by integrating extract, oxidized starch active carbon particle and expanded graphite processing
At comprehensive extract is the extract of various plants, and the preparation process of modified forming paper specifically comprises the following steps:
SS1, it weighs to crush after 5-10 portions of lemongrass, 20-25 portions of jasmines, 15-20 portions of cloves according to parts by weight and is slurried, be added
In 80-120 parts of deionized water, 80-95 DEG C at a temperature of heating extraction 1-2h after filter, after separation of solid and liquid, be concentrated to get
Extract paste；
It is mixed in SS2, the paste extract for taking active carbon particle to obtain with the mixture of expanded graphite addition previous step
Ball milling in ball mill is added after uniformly and obtains additive package, wherein the matter of active carbon particle, expanded graphite and paste extract
Amount is than being 1:2-3:0.5-2；
SS3, take oxidized starch be added deionized water in obtain mass percent be 8%-12% starch emulsion, heating starch
Additive package obtained in emulsion temperature to addition previous step after 45-50 DEG C, the quality of additive package and starch emulsion
Than obtaining extract coating for 1:8-10, continuation insulated and stirred 25-40min；
SS4, extract coating roll is coated on the two sides of forming paper, drying forms extract coating.
By the way that plant extracts is added in step 5, improve smell specific to forming paper itself fiber, while can cover
Lid improves the smell of tar, and added with active carbon particle and expanded graphite also in extract coating in the step, active carbon is to different
Taste has good adsorption effect, and has certain adsorption effect to tar, and expanded graphite is then to tar with good
Adsorption effect, and there is outstanding flame retardant effect.
Step 6: wrapping up in paper cutting, the tow after sizing is wrapped up forming by modified forming paper, and seal cutting and filtered
Mouth stick.
As further scheme of the invention, the binder is polyvinyl acetate emulsion, polyacrylate dispersion, gathers
One of acrylate copolymer emulsion, modified starch adhesive or at least two mixing.
Beneficial effects of the present invention:
1, the present invention is modified polypropylene fibre by dilute alkaline soln and polymer emulsion, and wherein dilute alkaline soln is to poly-
Tacryl surface irregularities, which corrode, forms the pit-hole of out-of-flatness on polypropylene fibre surface, then by polymer emulsion particles poly-
The surface of tacryl is adhered to, and the degree of roughness on polypropylene fibre surface is further improved, to improve polypropylene fibre
To the adsorption capacity of tar；
2, compound additive is added in the present invention in a binder, and compound additive is using attapulgite as skeleton, and recessed
Tobacco material extract is loaded on convex stick soil and carragheen, carragheen play good protecting effect to tobacco material extract,
It preventing in processing, transport with storing process, the tobacco flavor of tobacco material extract largely volatilizees, in smoking cigarette, volume
Cigarette is finished closer to suction, and flue-gas temperature is higher, and high-temperature flue gas can promote to volatilize, and the gas of tar is covered by the fragrance of tobacco
Taste, and filter rod is promoted to the adsorption capacity of tar by attapulgite.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's all other embodiment obtained without creative efforts belongs to the model that the present invention protects
It encloses.
Embodiment 1:
A kind of preparation process of cigarette filter tip rod includes the following steps:
Step 1: polypropylene fibre is added in 5% sodium hydroxide solution and impregnates 6h, will gather by the preparation of modified fibre
Tacryl, which is rinsed after pulling out with deionized water, dries, and the polypropylene fibre after drying is added in polymer emulsion and impregnates 30 points
Clock during immersion of the polypropylene fibre in polymer emulsion, while being ultrasonically treated polypropylene fibre, solid-liquid point
Polypropylene fibre is dried for standby from after, the monomer of the polymer emulsion is preferably oleophylic monomer；
Step 2: shredding, it will be spare after modified fibre shredding；
Step 3: the preparation of compound additive, specific preparation process include the following steps:
S1, offal, offal are cleaned in the dehydrated alcohol for be added after drying 40 DEG C and impregnates 5h, solid-to-liquid ratio 1:5, by offal
It extracts with the fragrance matter in offal, dehydrated alcohol is concentrated after separation of solid and liquid, obtain tobacco material paste and extract
Object is stand-by；
S2, the carragheen that 4 parts by weight are added into 100 parts by weight of deionized water reduce deionization after ebuillition of heated 10min
The stearoylketene calcium lactate of 1.5 parts by weight is added to 70 DEG C in coolant-temperature gage thereto, continues stirring to stearoylketene calcium lactate and is completely dissolved
And stearoylketene calcium lactate is uniformly mixed with carragheen, obtains mixing liquid, keeping the temperature of mixing liquid is 70 DEG C；
S3, tobacco material extract obtained in step S1 is added in mixing liquid obtained in step S2, wherein cream
The weight ratio of shape object and mixing liquid is 1.5:100, by being ultrasonically treated the non-water soluble substance made in tobacco material extract
Can be evenly dispersed in the liquid phase, it is 70 DEG C that the temperature of liquid-phase system is kept in the dispersion process of tobacco material extract, and whole
A process at least carries out 15min, so that the ethyl alcohol in paste is sufficiently volatilized, obtains treatment fluid, and keeping the temperature for the treatment of fluid is 70
℃；
In S4, the treatment fluid for obtaining attapulgite addition previous step, it is ultrasonically treated during stirring, ultrasound
Time is 12min, is separated by solid-liquid separation after ultrasound and obtains attapulgite；
After S5, the attapulgite for obtaining previous step 20 DEG C of cold wind drying, obtain attapulgite is fully dispersed
Compound additive, dispersion are crushed by pulverizer.
Step 4: compound additive and binder are uniformly applied on tow by sizing after evenly mixing；
Step 5: the preparation of modified forming paper, the preparation process of the modified forming paper include the following steps:
SS1, weigh to crush after 5 portions of lemongrass, 20 portions of jasmines, 20 portions of cloves according to parts by weight and be slurried, be added 100 parts go from
In sub- water, 95 DEG C at a temperature of heating extraction 1.5h after filter, after separation of solid and liquid, be concentrated to get extract paste；
It is mixed in SS2, the paste extract for taking active carbon particle to obtain with the mixture of expanded graphite addition previous step
Ball milling in ball mill is added after uniformly and obtains additive package, wherein the matter of active carbon particle, expanded graphite and paste extract
Amount is than being 1:2:0.5；
SS3, take oxidized starch be added deionized water in obtain mass percent be 8% starch emulsion, heating starch lotion
The mass ratio of additive package obtained in temperature to addition previous step after 45 DEG C, additive package and starch emulsion is 1:8,
Continue insulated and stirred 40min and obtains extract coating；
SS4, extract coating roll is coated on the two sides of forming paper, drying forms extract coating；
Step 6: wrapping up in paper cutting, the tow after sizing is wrapped up forming by modified forming paper, and seal cutting and filtered
Mouth stick.
The binder is polyvinyl acetate emulsion.
Embodiment 2:
A kind of preparation process of cigarette filter tip rod includes the following steps:
Step 1: polypropylene fibre is added in 5% sodium hydroxide solution and impregnates 8h, will gather by the preparation of modified fibre
Tacryl, which is rinsed after pulling out with deionized water, dries, and the polypropylene fibre after drying is added in polymer emulsion and impregnates 25 points
Clock during immersion of the polypropylene fibre in polymer emulsion, while being ultrasonically treated polypropylene fibre, solid-liquid point
Polypropylene fibre is dried for standby from after, the monomer of the polymer emulsion is preferably oleophylic monomer；
Step 2: shredding, it will be spare after modified fibre shredding；
Step 3: the preparation of compound additive, specific preparation process include the following steps:
S1, offal, offal are cleaned in the dehydrated alcohol for be added after drying 45 DEG C and impregnates 3.5h, solid-to-liquid ratio 1:5, by cigarette
Stalk is extracted with the fragrance matter in offal, and dehydrated alcohol is concentrated after separation of solid and liquid, obtains tobacco material paste and mentions
Take object stand-by；
S2, the carragheen that 4 parts by weight are added into 100 parts by weight of deionized water reduce deionization after ebuillition of heated 12min
The stearoylketene calcium lactate of 1 parts by weight is added to 65 DEG C in coolant-temperature gage thereto, continue stirring be completely dissolved to stearoylketene calcium lactate and
Stearoylketene calcium lactate is uniformly mixed with carragheen, obtains mixing liquid, and keeping the temperature of mixing liquid is 65 DEG C；
S3, tobacco material extract obtained in step S1 is added in mixing liquid obtained in step S2, wherein cream
The weight ratio of shape object and mixing liquid is 1.2:100, is made by stirring or ultrasonication non-aqueous in tobacco material extract
Soluble substance can be evenly dispersed in the liquid phase, and it is 65 that the temperature of liquid-phase system is kept in the dispersion process of tobacco material extract
DEG C, and whole process at least carries out 20min, so that the ethyl alcohol in paste is sufficiently volatilized, obtains treatment fluid, keeps the temperature for the treatment of fluid
Degree is 65 DEG C；
In S4, the treatment fluid for obtaining attapulgite addition previous step, it is ultrasonically treated during stirring, ultrasound
Time is 14min, is separated by solid-liquid separation after ultrasound and obtains attapulgite；
After S5, the attapulgite for obtaining previous step 15 DEG C of cold wind drying, obtain attapulgite is fully dispersed
Compound additive, dispersion are carried out by grinding.
Step 4: compound additive and binder are uniformly applied on tow by sizing after evenly mixing；
The preparation process of the modified forming paper includes the following steps:
SS1, it weighs to crush after 10 portions of lemongrass, 25 portions of jasmines, 15 portions of cloves according to parts by weight and is slurried, be added 100 parts and go
In ionized water, 95 DEG C at a temperature of heating extraction 2h after filter, after separation of solid and liquid, be concentrated to get extract paste；
It is mixed in SS2, the paste extract for taking active carbon particle to obtain with the mixture of expanded graphite addition previous step
Ball milling in ball mill is added after uniformly and obtains additive package, wherein the matter of active carbon particle, expanded graphite and paste extract
Amount is than being 1:3:1；
SS3, take oxidized starch be added deionized water in obtain mass percent be 12% starch emulsion, heating starch lotion
The mass ratio of additive package obtained in temperature to addition previous step after 50 DEG C, additive package and starch emulsion is 1:8,
Continue insulated and stirred 30min and obtains extract coating；
SS4, extract coating roll is coated on the two sides of forming paper, drying forms extract coating；
Step 6: wrapping up in paper cutting, the tow after sizing is wrapped up forming by forming paper, and seal cutting and obtain filter tip
Stick.
As further scheme of the invention, the binder is modified starch adhesive.
Comparative example 1:
Comparative example 1, is not modified polypropylene fibre.
Comparative example 2:
Comparative example 1, is not added compound additive in a binder.
Comparative example 3:
Comparative example 1, was not both modified polypropylene fibre, and compound addition is not also added in adhesive
Agent.
Comparative example 4:
Comparative example 1 is not modified modified fibre paper.
Cigarette filter tip rod performance test:
The volume that will be prepared according to the technique of embodiment 1, embodiment 2, comparative example 1, comparative example 2, comparative example 3 and comparative example 4
Cigarette is divided into 6 groups, and every group of test cigarette quantity is 20, detects to the tar content of each group cigarette, resistance to suction with suction taste.
Cigarette filter tip rod the performance test results are shown in Table 1:
Table 1
| Detection project | Tar content (mg) | Resistance to suction (pa) | Inhale taste |
| Embodiment 1 | 9.11 | 2763 | There is no the bitter taste of tar, has compared with warmth odor |
| Comparative example 1 | 10.22 | 2684 | There is no the bitter taste of tar, has compared with warmth odor |
| Comparative example 2 | 9.76 | 2755 | There is light tar bitter taste |
| Comparative example 3 | 11.03 | 2631 | Tar bitter taste is more apparent |
| Comparative example 4 | 9.46 | 2799 | There is light tar bitter taste |
| Embodiment 2 | 9.23 | 2758 | There is no the bitter taste of tar, has compared with warmth odor |
In conclusion more tar can be retained by being modified to polyethylene, while compound additive can be into one
Step tar adsorption simultaneously covers tar bitter taste, promotes the suction taste of cigarette.
Above content is only to structure of the invention example and explanation, affiliated those skilled in the art couple
Described specific embodiment does various modifications or additions or is substituted in a similar manner, without departing from invention
Structure or beyond the scope defined by this claim, is within the scope of protection of the invention.
Claims (6)
1. a kind of preparation process of cigarette filter tip rod, which comprises the steps of:
Step 1: the preparation of modified fibre is modified polypropylene fibre by diluted sodium hydroxide solution and polymer emulsion,
Obtain modified fibre；
Step 2: shredding, it will be spare after modified fibre shredding；
Step 3: the preparation of compound additive, specific preparation process include the following steps:
S1, offal, offal are cleaned in the dehydrated alcohol for be added after drying 35-60 DEG C and impregnates 2-7h, solid-to-liquid ratio 1:4-7, it will
Offal is extracted with the fragrance matter in offal, and dehydrated alcohol is concentrated after separation of solid and liquid, obtains tobacco material paste
Extract is stand-by；
S2, the carragheen that 4-5 parts by weight are added into 100 parts by weight of deionized water, reduce deionization after ebuillition of heated 8-12min
The stearoylketene calcium lactate of 1-2 parts by weight is added to 65-80 DEG C in coolant-temperature gage thereto, and it is complete to stearoylketene calcium lactate to continue stirring
It dissolves and stearoylketene calcium lactate is uniformly mixed with carragheen, obtain mixing liquid, keeping the temperature of mixing liquid is 65-80 DEG C；
S3, tobacco material extract obtained in step S1 is added in mixing liquid obtained in step S2, wherein paste
Weight ratio with mixing liquid is 1-1.5:100, is made by stirring or ultrasonication non-aqueous in tobacco material extract
Property substance can be evenly dispersed in the liquid phase, in the dispersion process of tobacco material extract keep liquid-phase system temperature be 65-
80 DEG C, and whole process at least carries out 10-20min, obtains treatment fluid, keeping the temperature for the treatment of fluid is 65-80 DEG C；
In S4, the treatment fluid for obtaining attapulgite addition previous step, it is ultrasonically treated during stirring, ultrasonic time
For 11-14min, it is separated by solid-liquid separation after ultrasonic and obtains attapulgite；
After S5, the attapulgite for obtaining previous step 15-25 DEG C of cold wind drying, answered attapulgite is fully dispersed
Additive is closed, dispersion is carried out by one of pulverizer crushing, grinding, ball milling；
Step 4: compound additive and binder are uniformly applied on tow by sizing after evenly mixing；
Step 5: the preparation of modified forming paper coats on the two sides that air permeability is the forming paper that air permeability is 8000-12000cu
Extract coating, the extract coating is processed by integrating extract, oxidized starch active carbon particle and expanded graphite, comprehensive
Close the extract that extract is various plants；
Step 6: wrapping up in paper cutting, the tow after sizing is wrapped up forming by modified forming paper, and seal cutting and obtain filter tip
Stick.
2. a kind of preparation process of cigarette filter tip rod according to claim 1, which is characterized in that poly- third in the step 1
The modification of alkene fiber specifically comprises the following steps:
Polypropylene fibre is added in 5% sodium hydroxide solution and impregnates 4-8h, uses deionized water after polypropylene fibre is pulled out
It is dried after flushing；
Polypropylene fibre after drying is added in polymer emulsion and is impregnated 20-40 minutes, polypropylene fibre is in polymer emulsion
In immersion during, while polypropylene fibre is ultrasonically treated, is dried for standby polypropylene fibre after separation of solid and liquid,
The monomer of the polymer emulsion is preferably oleophylic monomer.
3. a kind of preparation process of cigarette filter tip rod according to claim 1, which is characterized in that the modified forming paper
Preparation process includes the following steps:
SS1, it weighs to crush after 5-10 portions of lemongrass, 20-25 portions of jasmines, 15-20 portions of cloves according to parts by weight and is slurried, 80-120 is added
Part deionized water in, 80-95 DEG C at a temperature of heating extraction 1-2h after filter, after separation of solid and liquid, be concentrated to get paste
Extract；
It is uniformly mixed in SS2, the paste extract for taking active carbon particle to obtain with the mixture of expanded graphite addition previous step
Ball milling in ball mill is added afterwards and obtains additive package, wherein the mass ratio of active carbon particle, expanded graphite and paste extract
For 1:2-3:0.5-2；
SS3, take oxidized starch be added deionized water in obtain mass percent be 8%-12% starch emulsion, heating starch lotion
To being added additive package obtained in previous step after 45-50 DEG C, the mass ratio of additive package and starch emulsion is temperature
1:8-10 continues insulated and stirred 25-40min and obtains extract coating；
SS4, extract coating roll is coated on the two sides of forming paper, drying forms extract coating.
4. a kind of preparation process of cigarette filter tip rod according to claim 1, which is characterized in that the forming paper is selected saturating
Manner is the forming paper of 8000-12000cu.
5. a kind of preparation process of cigarette filter tip rod according to claim 1, which is characterized in that the binder is poly-vinegar
One of vinyl acetate lotion, polyacrylate dispersion, Polyacrylate Emulsion, modified starch adhesive or at least two
The mixing of kind.
6. a kind of cigarette filter tip rod, which is characterized in that cigarette filter tip rod preparation work according to claim 1-4
Skill is prepared.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910117828.8A CN109757768B (en) | 2019-02-15 | 2019-02-15 | Cigarette filter tip and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910117828.8A CN109757768B (en) | 2019-02-15 | 2019-02-15 | Cigarette filter tip and preparation process thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109757768A true CN109757768A (en) | 2019-05-17 |
| CN109757768B CN109757768B (en) | 2021-05-04 |
Family
ID=66456756
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910117828.8A Active CN109757768B (en) | 2019-02-15 | 2019-02-15 | Cigarette filter tip and preparation process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109757768B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111227303A (en) * | 2020-03-20 | 2020-06-05 | 中国科学院宁波材料技术与工程研究所 | Cigarette filter tip additive material and preparation method and application thereof |
| CN112841717A (en) * | 2020-12-31 | 2021-05-28 | 江苏都梁矿业集团有限公司 | Aromatized attapulgite based cigarette filter tip additive material as well as preparation method and application thereof |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0281967A1 (en) * | 1987-03-06 | 1988-09-14 | Kimberly-Clark Corporation | Smoking article with double wrapper |
| US20020062833A1 (en) * | 2000-04-20 | 2002-05-30 | Xue Lixin Luke | Cigarette filters of shaped micro cavity fibers impregnated with flavorant materials |
| CN1528214A (en) * | 2003-10-14 | 2004-09-15 | 盱眙欧佰特粘土材料有限公司 | Attapulgus stone as cut tobacco additive and/or filter tip in to bacco industry |
| CN102599651A (en) * | 2010-12-13 | 2012-07-25 | 河北中烟工业公司 | Preparation method for composite cigarette filter stick capable of reducing harmful components of cigarette |
| CN102783710A (en) * | 2011-05-19 | 2012-11-21 | 湖北中烟工业有限责任公司 | Preparation method for plant swelling fiber composite cigarette filter tip |
| CN102783711A (en) * | 2012-07-23 | 2012-11-21 | 湖北中烟工业有限责任公司 | Preparation method of tip rod for natural bamboo fiber cigarette |
| CN106263023A (en) * | 2016-11-18 | 2017-01-04 | 江西中烟工业有限责任公司 | A kind of cigarette filter compositions that can effectively reduce tar and content of nitrosamines |
| CN108968134A (en) * | 2018-06-08 | 2018-12-11 | 李华 | A kind of composition for substituting conventional cigarette and helping to give up smoking |
-
2019
- 2019-02-15 CN CN201910117828.8A patent/CN109757768B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0281967A1 (en) * | 1987-03-06 | 1988-09-14 | Kimberly-Clark Corporation | Smoking article with double wrapper |
| US20020062833A1 (en) * | 2000-04-20 | 2002-05-30 | Xue Lixin Luke | Cigarette filters of shaped micro cavity fibers impregnated with flavorant materials |
| CN1528214A (en) * | 2003-10-14 | 2004-09-15 | 盱眙欧佰特粘土材料有限公司 | Attapulgus stone as cut tobacco additive and/or filter tip in to bacco industry |
| CN102599651A (en) * | 2010-12-13 | 2012-07-25 | 河北中烟工业公司 | Preparation method for composite cigarette filter stick capable of reducing harmful components of cigarette |
| CN102783710A (en) * | 2011-05-19 | 2012-11-21 | 湖北中烟工业有限责任公司 | Preparation method for plant swelling fiber composite cigarette filter tip |
| CN102783711A (en) * | 2012-07-23 | 2012-11-21 | 湖北中烟工业有限责任公司 | Preparation method of tip rod for natural bamboo fiber cigarette |
| CN106263023A (en) * | 2016-11-18 | 2017-01-04 | 江西中烟工业有限责任公司 | A kind of cigarette filter compositions that can effectively reduce tar and content of nitrosamines |
| CN108968134A (en) * | 2018-06-08 | 2018-12-11 | 李华 | A kind of composition for substituting conventional cigarette and helping to give up smoking |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111227303A (en) * | 2020-03-20 | 2020-06-05 | 中国科学院宁波材料技术与工程研究所 | Cigarette filter tip additive material and preparation method and application thereof |
| CN112841717A (en) * | 2020-12-31 | 2021-05-28 | 江苏都梁矿业集团有限公司 | Aromatized attapulgite based cigarette filter tip additive material as well as preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109757768B (en) | 2021-05-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5327917A (en) | Method for providing a reconstituted tobacco material | |
| EP0196775B1 (en) | Printing inks and printed substrates | |
| CN104479871B (en) | A kind of carbon dioxide solid Flavouring ball pinched brokenly and its application in cigarette filter rod | |
| CN109757768A (en) | A kind of cigarette filter tip rod and its preparation process | |
| CN108308695B (en) | Smoking agent, preparation method thereof and cigarette containing smoking agent | |
| CN108851216A (en) | A kind of wax packet emulsion type cigarette capsule and preparation method thereof | |
| MXPA03002190A (en) | Tobacco smoke filter. | |
| JP2020533003A (en) | Aerosolizable products | |
| CN106666823A (en) | Compound extract for cigarette, microcapsule containing extract and preparation methods thereof | |
| JPH06343448A (en) | Tobacco smoke emission filter and method of sucking tar, nicotine and toxic gas into said filter | |
| CN103478903B (en) | A kind of tobacco stalk fibre composite filter and preparation method thereof | |
| CN206354420U (en) | A kind of dry process reproduction tobacco leaf filter stick | |
| CN108936804A (en) | A kind of cigarette filter rod for improving flue gas and protecting fragrant effect | |
| JPH11500926A (en) | Cigarette filter containing microcapsules | |
| CN113331469A (en) | Multi-particle smoking-based smoking segment, cigarette comprising same and preparation method | |
| CN107319632A (en) | A kind of preparation method of paper filter stick | |
| CN107981404A (en) | A kind of coating fluid for improving papermaking-method reconstituted tobaccos combustibility and preparation method thereof | |
| CN106965280A (en) | A kind of wood preservation insect-proof agent | |
| CN103110186B (en) | Dibasic compound hollow tobacco fiber paper filtering stick and preparation method thereof | |
| CN115644491A (en) | Tea flavor particle for cigarette filter stick and preparation method thereof | |
| CN101914869A (en) | Porous-starch-containing water-based paint for cigarette wrapping paper | |
| CN110302745A (en) | A kind of smoke abatement detergent and preparation method thereof | |
| CN102599651B (en) | Preparation method for composite cigarette filter stick capable of reducing harmful components of cigarette | |
| KR20240000552A (en) | Tobacco sheet for non-combustion heating type flavor inhaler, non-combustion heating type flavor inhaler, and non-combustion heating type flavor inhalation system | |
| CN108851208A (en) | A kind of cigarette filter rod and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 239000 No. 1436 Qingliu East Road, Chuzhou economic and Technological Development Zone, Anhui Province Patentee after: Chuzhou Cigarette Material Factory Address before: 239000 No. 1436 Qingliu East Road, Chuzhou economic and Technological Development Zone, Anhui Province Patentee before: CHUZHOU CIGARETTE MATERIALS FACTORY |