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CN109654375A - A kind of safe feeding device and its air supply method of high pressure combustibility experimental gas - Google Patents

A kind of safe feeding device and its air supply method of high pressure combustibility experimental gas Download PDF

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Publication number
CN109654375A
CN109654375A CN201910089921.2A CN201910089921A CN109654375A CN 109654375 A CN109654375 A CN 109654375A CN 201910089921 A CN201910089921 A CN 201910089921A CN 109654375 A CN109654375 A CN 109654375A
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China
Prior art keywords
valve
gas
pipeline
pressure
gas cylinder
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CN201910089921.2A
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Inventor
段强领
曾倩
李萍
孙金华
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University of Science and Technology of China USTC
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University of Science and Technology of China USTC
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Priority to CN201910089921.2A priority Critical patent/CN109654375A/en
Publication of CN109654375A publication Critical patent/CN109654375A/en
Pending legal-status Critical Current

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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17DPIPE-LINE SYSTEMS; PIPE-LINES
    • F17D1/00Pipe-line systems
    • F17D1/02Pipe-line systems for gases or vapours
    • F17D1/04Pipe-line systems for gases or vapours for distribution of gas
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17DPIPE-LINE SYSTEMS; PIPE-LINES
    • F17D3/00Arrangements for supervising or controlling working operations
    • F17D3/01Arrangements for supervising or controlling working operations for controlling, signalling, or supervising the conveyance of a product

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

The invention discloses a kind of safe feeding device of high pressure combustibility experimental gas and its air supply methods.The device includes flammable experimental gas gas cylinder, inert gas gas cylinder, filter, pipeline pressure reducing valve, hand stop valve, pneumatic stopping valve, pressure transmitter, vacuum pump, pressure gauge, vacuum meter, solenoid valve, combustible gas probe, alarm controller for combustible gas base, metallic conduit etc..The device can be used for: 1) transporting imflammable gas safely to experimental facilities;2) gamut adjustment is carried out to gas pressure in use;3) laboratory equipment is persistently supplied or intermittent gas supply;4) to equipment test before airtight test and, experiment rear molding gas cleanup supplied;5) high pressure gas cylinder is safely and conveniently replaced;6) the flammable gas concentration of real-time detection safeguards laboratory safety.The present invention have good air-tightness, high cleanliness, high durability and security reliability, be able to satisfy laboratory equipment is persistently supplied, intermittent gas supply.

Description

A kind of safe feeding device and its air supply method of high pressure combustibility experimental gas
Technical field
The present invention relates to flammable experimental gas transport system more particularly to a kind of safety of high pressure combustibility experimental gas Feeding device and its air supply method.
Background technique
Flammable experimental gas includes hydrogen, acetylene, methane etc., is often supplied to reality by Pipeline transport by gas bomb Experiment device, instrument etc. use.However, may cause combustible gas leakage in gas transport and improper use, once encounter igniting Source, easily initiation fire explosion, to cause casualties and property loss.For example, certain Scientific Research in University Laboratory hair in 2015 Raw explosion causes 1 people dead, and preliminary confirmation is since hydrogen improper use causes gas burst.How battle support laboratory is flammable It is a problem that laboratory safety need to be paid close attention to that the safety of property gas, especially high pressure gas, which is transported and operated,.High pressure can Combustion property experimental gas to the air-tightness of pipeline, durability, security reliability and it is functional there is high requirement, therefore to using Reasonable gas supply is carried out when high pressure imflammable gas is as experimental gas and transports the design of pipe-line system.
Current laboratory air supply system is divided into dispersion gas supply and central gas supply by its method of supplying.Dispersion gas supply is by gas Bottle is individually placed to each Instrumental Analysis Lab, close to instrument gas point;Central gas supply is that all kinds of gas bombs are put together at reality It tests in outdoor independent gas cylinder, then is transported to the different experiment instrument in each laboratory according to different requirements in the form of pipeline On device.It is poor to disperse convenient air supplying operation, saving gas but safety;Central gas supply high reliablity, functional but steam line It is inconvenient for use between gas cylinder to open or close gas source for long waste gas.For the high pressure imflammable gas of independent laboratory It transports, generallys use distributing air supply method.If the advantages of central gas supply method, can be fused in distributing air supply system, The delivery safety and functionality of flammable experimental gas will obtain larger raising.Based on this, the present invention combines two kinds of gas supply The advantages of mode, devises a kind of safe transport system of flammable experimental gas suitable for high pressure gas.
Summary of the invention
The purpose of the present invention is to provide one kind to have good air-tightness, high cleanliness, high durability and security reliability, Be able to satisfy laboratory equipment is persistently supplied, intermittent gas supply, and can be in use according to operating condition to gas pressure Carry out the safe feeding device of flammable experimental gas and its air supply method of gamut adjustment.
The technical solution adopted by the present invention are as follows: a kind of safe feeding device of high pressure combustibility experimental gas, the device packet Include gas cylinders group, supply air line unit, vacuum unit and combustible gas alarm unit;The effect of gas cylinders group and supply air line unit is Steadily persistently gas supply or intermittent gas supply into laboratory equipment, while can also be to promote after the inspection of air-tightness, experiment before testing Discharge into device inner exhaust gas provides gas source, and supply air line unit can be according to requirement of experiment in the entire experiment process to gas Pressure carries out gamut adjustment;Vacuum unit extracts the gas in experimental provision before being used to test;Combustible gas alarm unit is used In when gas leaks sending sound when concentration reaches warning concentration, light alarm and reminding takes safety measures and linkage exhaust, cutting electricity Source guarantees the safety of experiment.
Further, the specific structure of the device is as follows: gas cylinders group is mainly by flammable experimental gas gas cylinder, inert gas Gas cylinder composition.Supply air line unit is mainly by the first, second filter, the first, second, third pipeline pressure reducing valve, and first, Two, third, the four, the 5th hand stop valves, the first, second, third pneumatic stopping valve, pressure transmitter, control cabinet, metal tube Road composition;Flammable experimental gas bottle by pipeline and first filter, the first pipeline pressure reducing valve, the first pneumatic stopping valve and with Its first manual shut-off valve in parallel, pressure transmitter are connected, and inert gas gas cylinder passes through pipeline and the second filter, the second pipe Road pressure reducing valve, the second pneumatic stopping valve and the second hand stop valve connected in parallel are connected, two pipeline parallel connections;Evacuated tube passes through 4th hand stop valve is controlled, and is connect and is pooled on main pressure piping with combustible gas and inertia feed channel, for discharging dress Set interior gas;First, second, third pipeline pressure reducing valve is installing 2 pressure gauges with gas cylinder connecting side, main pipeline connecting side, point The gas pressure in the bottle and manifold pressure variation are not shown;Multiple electromagnetic valve switch are provided in control cabinet, to first, second, Three pneumatic stopping valves are opened and closed control, cabinet by third hand stop valve, third pipeline pressure reducing valve and metallic conduit with it is lazy Property gas cylinders connection, pass through inert gas gas cylinder and third pipeline pressure reducing valve and required pressure in control cabinet be provided;Pressure becomes Sending device for judging equipment when imflammable gas supplies experimental facilities, whether pressure maintaining is successful.Pumped vacuum systems includes pneumatic cuts Only valve, the vacuum pump with vacuum meter, the vacuum pump with vacuum meter are connected by pipeline with third pneumatic stopping valve, then by Pipeline is connected on main pressure piping;The opening and closing of third pneumatic stopping valve and vacuum pump is opened by solenoid valve corresponding in control cabinet Close: third pneumatic stopping valve releases the button, third pneumatic stopping valve close button and vacuum pump are released the button, vacuum pump close by Button control.Combustible gas alarm unit includes gas detector and gas alarm controller;When gas leakage, alarm movement hair Audible and visible alarm out exports electric signal;Urgent stop button is installed, laboratory technician, which can press the button, when system alarm makes in control cabinet Electromagnetism valve events in control cabinet close the pneumatic control valve on supply air line, cut off gas circuit;Gas alarm controller receives simultaneously Electric signal, linkage exhaust, cutting off the power closes solenoid valve and then cuts off gas circuit.
Further, the course of work of the device is as follows:
1, gas cylinder main valve, the first, second, the 4th hand stop valve, the first, second, third pneumatic cut-off are confirmed before experiment Valve, the first, second pipeline pressure reducing valve are closed;2, third, the 5th hand stop valve are normally opened, and experiment front opening inert gas gas cylinder is total Valve confirms that third pipeline pressure reducing valve leads to solenoid valve lateral pressure and reaches its operating pressure by pressure gauge.3, according to requirement of experiment And purpose, the specific work process of the system are as follows:
(1) it checks sealing device air-tightness and vacuumizes
If experimental provision is in closed state, check device airtightness is realized using this system and is vacuumized.Airtightness Test operating procedure: confirmation inert gas gas cylinder main valve is opened, and the solenoid valve that the second pneumatic stopping valve is controlled on control cabinet is opened Switch, manually adjusting the second pipeline pressure reducing valve makes experimental provision pressure maintaining to certain pressure value, closes on control cabinet and controls the second gas The electromagnetic valve switch of dynamic shut-off valve, test experience device airtightness after airtightness passes through, open the 4th hand stop valve pressure release, It is then turned off the shut-off valve, closes the second pipeline pressure reducing valve.Vacuum pumping process: confirmation inert gas gas cylinder main valve is opened, The electromagnetic valve switch of control third pneumatic stopping valve and vacuum pump on control cabinet is opened to start switch, after vacuumizing, according to The electromagnetic valve switch and vacuum pump shutdown switch of third pneumatic stopping valve on secondary closing control cabinet.
(2) intermittent gas supply is carried out to experimental facilities
Flammable experimental gas gas cylinder main valve is opened, opens the control switch of the first pneumatic stopping valve on control cabinet, manually Adjusting the first pipeline pressure reducing valve makes main pipeline lateral pressure table data reach experimental pressure;If experimental provision is in closed state, close The control switch of the first pneumatic stopping valve is closed, whether observation is obviously reduced in pressure transmitter data 3 minutes, if unchanged It supplies successfully;The control switch of the first pneumatic stopping valve is closed after experiment, closes the first pipeline pressure reducing valve;Then turn on control The electromagnetic valve switch that the second pneumatic stopping valve is controlled on case processed manually adjusts the second pipeline pressure reducing valve, with inert gas purge pipe The electromagnetic valve switch that the second pneumatic stopping valve on control cabinet is closed behind road, closes the second pipeline pressure reducing valve, closes flammable experiment Gas cylinders main valve and inert gas gas cylinder main valve.
(3) stable lasting gas supply is carried out to experimental facilities
Confirm that inert gas gas cylinder main valve is opened, open the electromagnetic valve switch for controlling the second pneumatic stopping valve on control cabinet, The second pipeline pressure reducing valve is manually adjusted, with the electromagnetic valve switch for closing the second pneumatic stopping valve after inert gas purge pipeline, is closed It closes after the second pipeline pressure reducing valve, opens flammable experimental gas gas cylinder main valve, open the pneumatically cut-off of control first on control cabinet The electromagnetic valve switch of valve, manually adjusting the first pipeline pressure reducing valve makes main pipeline lateral pressure table data reach supply gas pressure;Observation pressure Whether power transmitter data have obvious fluctuation, and the stabilization to experimental facilities, lasting gas supply are realized if unchanged.
(4) gas cylinder safely changes in gas cylinders group
Flammable experimental gas gas cylinder replacement: it checks that flammable experimental gas gas cylinder is in close state, opens the first He 4th hand stop valve adjusts the first pipeline pressure reducing valve for experimental gas flammable in pipeline and drains (the first pipeline pressure reducing valve two When lateral pressure table is illustrated as 0), the first pipeline pressure reducing valve remains stationary, and more renews gas cylinder;Ensure that experimental facilities is in sealed shape State need to install the 5th normally opened hand stop valve at main pipeline, close the cut-off at this time if experimental facilities is open type device Valve is to form loop;Close the 4th hand stop valve;Inert gas gas cylinder main valve is opened, it is pneumatic to open third on control cabinet The control switch and vacuum pump of shut-off valve, which start switch, to be vacuumized, wait vacuumize after close first manual shut-off valve and First pipeline pressure reducing valve, then successively close the control switch and vacuum pump shutdown switch of third pneumatic stopping valve on control cabinet;It beats Open the 5th hand stop valve;Flammable experimental gas gas cylinder main valve is opened, by the first pipeline pressure reducing valve in gas cylinder lateral pressure table Determine gross pressure in combustibility experimental gas gas cylinder.
The replacement of inert gas gas cylinder: it checks that inert gas gas cylinder is in close state, closes third hand stop valve, open Second hand stop valve adjusts the second pipeline pressure reducing valve for inert gas in pipeline and drains (the second pipeline pressure reducing valve pressure at both sides When table is illustrated as 0), the second pipeline pressure reducing valve remains stationary, and more renews gas cylinder;Close the second hand stop valve and the second pipeline Pressure reducing valve is opened inert gas gas cylinder main valve, is determined in inert gas gas cylinder by the second pipeline pressure reducing valve gas cylinder lateral pressure table Gross pressure;Third hand stop valve is opened, adjustment third pipeline pressure reducing valve makes to reach its operating pressure towards solenoid valve lateral pressure.
Using the present invention of technical solution as above, safety is had the following beneficial effects:, it is reliably, easy to operate, it saves and uses Gas, functional.The safety that the flammable safe transport system of experimental gas is used to carry out combustible gas to experimental facilities transports, and can To carry out gamut adjustment to gas pressure in use, to guarantee that gas meets requirement of experiment in experimental provision;It can also Satisfaction is persistently supplied to laboratory equipment and intermittent gas supply, provides more selections for experimental design.
Detailed description of the invention
Fig. 1 is a kind of safe feeding device general structure schematic diagram of high pressure combustibility experimental gas of the present invention;
Fig. 2 is control cabinet structural schematic diagram in feeding device;
Fig. 3 is the spontaneous combustion of embodiment mesohigh combustible gas leakage and SHOCK WAVE INDUCED fire trial schematic device.
Transport system the names of the parts table corresponding with number in attached drawing
Specific embodiment
Below in conjunction with Detailed description of the invention embodiments of the present invention.
A kind of safe feeding device of high pressure combustibility experimental gas of the present invention, mainly by flammable experimental gas gas cylinder 1, Inert gas gas cylinder 2, the first, second filter 3,4, the first, second, third pipeline pressure reducing valve 5,6,19, first, second, Three, the four, the 5th hand stop valve 7,8,18,15,14, the first, second, third pneumatic stopping valve 9,10,12, pressure transmitter 11, control cabinet 20, metallic conduit composition;Flammable experimental gas bottle 1 is depressurized by pipeline and first filter 3, the first pipeline Valve 5, the first pneumatic stopping valve 9 and first manual shut-off valve 7 connected in parallel, pressure transmitter 11 are connected, inert gas gas cylinder 2 It is cut manually by pipeline and the second filter 4, the second pipeline pressure reducing valve 6, the second pneumatic stopping valve 10 and connected in parallel second Only valve 8 is connected, two pipeline parallel connections;Evacuated tube is controlled by the 4th hand stop valve 15, with combustible gas and safe tracheae Road connection is pooled on main pressure piping 16, for gas in tapping equipment;First, second, third pipeline pressure reducing valve 5,6,19 2 pressure gauges are being installed with gas cylinder connecting side, main pipeline connecting side, are showing the gas pressure in the bottle and manifold pressure variation respectively; Control cabinet 20 is provided with multiple electromagnetic valve switch, and control, case is opened and closed to the first, second, third pneumatic stopping valve 9,10,12 Body is connect by third hand stop valve 18, third pipeline pressure reducing valve 19 and metallic conduit with inert gas gas cylinder 2, and inertia is passed through Gas cylinders 2 and third pipeline pressure reducing valve 19 provide required pressure in control cabinet;Pressure transmitter 11 is used for when flammable gas When body persistently supplies experimental facilities, judging equipment, whether pressure maintaining is successful.Pumped vacuum systems includes third pneumatic stopping valve 12, band The vacuum pump 13 of vacuum meter, the vacuum pump 13 with vacuum meter are connected by pipeline with third pneumatic stopping valve 12, then by pipe Road is connected on main pressure piping 16;The opening and closing of third pneumatic stopping valve 12 and vacuum pump 13 is by corresponding electromagnetism in control cabinet 20 Threshold switch: third pneumatic stopping valve 12 releases the button 30, third pneumatic stopping valve, 12 close button 31 and vacuum pump is released the button 24, vacuum pump close button 25 controls.Combustible gas alarm system includes gas detector 21 and gas alarm controller 22;It is flammable When gas leakage, alarm movement issues audible and visible alarm, exports electric signal;Urgent stop button 32, system report are installed in control cabinet Laboratory technician, which can press the button, when alert makes electromagnetism valve events in control cabinet, closes the pneumatic control valve on supply air line, cuts off gas Road;Gas alarm controller 22 receives electric signal simultaneously, and linkage exhaust, cutting off the power closes solenoid valve and then cut off gas circuit.
Further, the course of work of the invention is as follows:
1, flammable experimental gas gas cylinder 1,2 main valve of inert gas gas cylinder are confirmed before experiment, the first, second, the 4th manually Shut-off valve 7,8,15, the first, second, third pneumatic stopping valve 9,10,12, the first, second pipeline pressure reducing valve 5,6 are closed;2, Three, the 5th hand stop valve 18,14 is normally opened, tests 2 main valve of front opening inert gas gas cylinder, confirms third pipeline by pressure gauge Pressure reducing valve 19 leads to 20 lateral pressure of solenoid valve and reaches its operating pressure;
(1) it checks sealing device air-tightness and vacuumizes
If experimental provision is in closed state, check device airtightness is realized using the present apparatus and is vacuumized.Airtightness Test operating procedure: confirmation 2 main valve of inert gas gas cylinder is opened, press the unlatching of the second pneumatic stopping valve 10 on control cabinet 20 by Button 28, manually adjusting the second pipeline pressure reducing valve 6 makes experimental provision pressure maintaining to certain pressure value, and it is pneumatic to press on control cabinet 20 second The close button 29 of shut-off valve 10, test experience device airtightness after airtightness passes through, are opened the 4th hand stop valve 15 and are let out Pressure is then turned off the shut-off valve, closes the second pipeline pressure reducing valve 6.Vacuum pumping process: confirmation 2 main valve of inert gas gas cylinder Open, press third pneumatic stopping valve 12 on control cabinet 20 release the button 30 and vacuum pump release the button 24, wait vacuumize knot Shu Hou successively presses the close button 31 and vacuum pump close button 25 of third pneumatic stopping valve 12 on control cabinet.
(2) intermittent gas supply is carried out to experimental facilities
Flammable 1 main valve of experimental gas gas cylinder is opened, releasing the button for the first pneumatic stopping valve 9 on control cabinet 20 is pressed 26, manually adjusting the first pipeline pressure reducing valve 5 makes main pipeline lateral pressure table data reach experimental pressure;If experimental provision is in closing State presses the close button 27 of the first pneumatic stopping valve 9, and whether observation has in 11 data of pressure transmitter 3 minutes obviously subtracts It is small, success is supplied if unchanged;The close button 27 of the first pneumatic stopping valve 9 is pressed after experiment, closes the first pipeline Pressure reducing valve 5;That then presses the second pneumatic stopping valve 10 on control cabinet 20 releases the button 28, manually adjusts the second pipeline pressure reducing valve 6, with the close button 29 for pressing the second pneumatic stopping valve 10 on control cabinet 20 after inert gas purge pipeline, close the second pipeline Pressure reducing valve 6 closes flammable 1 main valve of experimental gas gas cylinder and 2 main valve of inert gas gas cylinder.
(3) stable lasting gas supply is carried out to experimental facilities
Confirm that 2 main valve of inert gas gas cylinder is opened, that presses the second pneumatic stopping valve 10 on control cabinet 20 releases the button 28, The second pipeline pressure reducing valve 6 is manually adjusted, with the close button 29 for pressing the second pneumatic stopping valve 10 after inert gas purge pipeline, It closes after the second pipeline pressure reducing valve 6, opens flammable 1 main valve of experimental gas gas cylinder, press on control cabinet 20 first pneumatic section Only valve 9 releases the button 26, and manually adjusting the first pipeline pressure reducing valve 5 makes main pipeline lateral pressure table data reach supply gas pressure;It sees It examines whether 11 data of pressure transmitter have obvious fluctuation, the stabilization to experimental facilities, lasting gas supply is realized if unchanged.
(4) gas cylinder safely changes in transport system
Flammable experimental gas gas cylinder replacement: it checks that flammable experimental gas gas cylinder 1 is in close state, opens the first He 4th hand stop valve 7,15 adjusts the first pipeline pressure reducing valve 5 for experimental gas flammable in pipeline and drains (the first pipeline decompression When valve pressure at both sides table is illustrated as 0), the first pipeline pressure reducing valve 5 remains stationary, and more renews gas cylinder;Ensure that experimental facilities is in Air-tight state need to install the 5th normally opened hand stop valve 14 at main pipeline, close at this time if experimental facilities is open type device The shut-off valve is closed to form loop;Close the 4th hand stop valve 15;2 main valve of inert gas gas cylinder is opened, control is pressed On case 20 third pneumatic stopping valve 12 release the button 30 and vacuum pump 13 release the button and 24 vacuumized, to the end of vacuumizing First manual shut-off valve 7 and the first pipeline pressure reducing valve 5 are closed afterwards, then successively press third pneumatic stopping valve 12 on control cabinet 20 13 close button 25 of close button 31 and vacuum pump;Open the 5th hand stop valve 14;It is total to open flammable experimental gas gas cylinder 1 Valve determines gross pressure in flammable experimental gas gas cylinder 1 in gas cylinder lateral pressure table by the first pipeline pressure reducing valve 5.
The replacement of inert gas gas cylinder: checking that inert gas gas cylinder 2 is in close state, close third hand stop valve 18, The second hand stop valve 8 is opened, the second pipeline pressure reducing valve 6 is adjusted by inert gas in pipeline and drains (i.e. the second pipeline pressure reducing valve When pressure at both sides table is illustrated as 0), the second pipeline pressure reducing valve 6 remains stationary, and more renews gas cylinder;Close the second hand stop valve 8 With the second pipeline pressure reducing valve 6,2 main valve of inert gas gas cylinder is opened, is determined by 6 gas cylinder lateral pressure table of the second pipeline pressure reducing valve lazy Gross pressure in property gas cylinders 2;Third hand stop valve 18 is opened, adjustment third pipeline pressure reducing valve 19 makes to lead to solenoid valve side pressure Power reaches its operating pressure.
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description.
As shown in figure 3, experimental facilities is the spontaneous combustion of high pressure combustible gas leakage and SHOCK WAVE INDUCED fire trial device.This is sent out Bright to be connect by main pipeline 16 with the device, flammable experimental gas is hydrogen, and inert gas is nitrogen.Experimental provision it is brief The course of work are as follows: hydrogen is delivered to high pressure storage tank 33 using the present invention, hydrogen is filled to certain pressure, simulates the storage of hydrogen high pressure It deposits;Rupture disk clamper 36 is connected with high pressure storage tank 33, quick-fried when pressure of storage tank is higher than the receiving of rupture disk 35 pressure in clamper Fragmentation rupture, hydrogen are released in protective housing 42 by downstream line 39.Pressure and auto-ignition are passed by pressure in downstream line Sensor 37 and photodiode 38 measure, and protective housing flame structure is measured by High Speed System 41, transfers data to data and adopt Collect in instrument 40.The device is closed-type device, without installing the 5th hand stop valve 14.It is of the invention in conjunction with the experimental facilities The course of work is as follows:
Before step 1, experiment and after confirm flammable experimental gas gas cylinder 1,2 main valve of inert gas gas cylinder, first, the Two, the 4th hand stop valve 7,8,15, the first, second, third pneumatic stopping valve 9,10,12, the first, second pipeline pressure reducing valve 5, 6 close;
Step 2, third hand stop valve 18 are normally opened, test 2 main valve of front opening inert gas gas cylinder, are confirmed by pressure gauge Third pipeline pressure reducing valve 19 leads to solenoid valve lateral pressure and reaches its operating pressure 5bar;
Step 3, airtightness test: rupture disk 35 after the installation is completed, opens 2 main valve of inert gas gas cylinder, presses control cabinet 20 Upper second pneumatic stopping valve 10 releases the button 28, and adjusting the second pipeline pressure reducing valve 6 makes 33 pressure maintaining of high pressure chest to certain pressure value, The close button 29 of the second pneumatic stopping valve 10 on control cabinet 20 is pressed, test experience device airtightness after airtightness passes through, is beaten 15 pressure release of the 4th hand stop valve is opened, the shut-off valve is then turned off, closes the second pipeline pressure reducing valve 6;
Step 4 vacuumizes: confirmation 2 main valve of inert gas gas cylinder is opened, and third pneumatic stopping valve 12 on control cabinet 20 is pressed Release the button 30 and vacuum pump release the button 24, after vacuumizing, successively press third pneumatic stopping valve on control cabinet 12 close button 31 and vacuum pump close button 25;
Step 5 supplies for experimental provision intermittence: opening flammable 1 main valve of experimental gas bottle, presses on control cabinet 20 the One pneumatic stopping valve 9 releases the button 26, adjusts after the first pipeline pressure reducing valve 5 ruptures rupture disk 35, presses the first gas immediately The close button 27 of dynamic shut-off valve 9.That then presses the second pneumatic stopping valve 10 on control cabinet 20 releases the button 28, adjusts second Pipeline pressure reducing valve 6 closes the with the close button 29 for pressing the second pneumatic stopping valve 10 on control cabinet 20 behind nitrogen sparge tube road One, the second pipeline pressure reducing valve 5,6 changes rupture disk 35 and carries out next group of experiment.
Step 6 replaces flammable experimental gas bottle: checking that flammable 1 main valve of experimental gas bottle is in close state, opens The first, the 4th hand stop valve 7,15 adjusts the first pipeline pressure reducing valve 5 for hydrogen in pipeline and drains (i.e. 5 two sides of pipeline pressure reducing valve When pressure gauge is illustrated as 0), the first pipeline pressure reducing valve 5 remains stationary, and more renews gas cylinder.Rupture disk 35 is loaded onto, the 4th hand is closed Dynamic shut-off valve 15, opens 2 main valve of inert gas gas cylinder, presses 30 Hes of releasing the button of third pneumatic stopping valve 12 on control cabinet 20 Vacuum pump 13 releases the button 24, wait vacuumize after close first manual shut-off valve 7 and pipeline pressure reducing valve 5, then successively press 13 close button 25 of the close button 31 of third pneumatic stopping valve 12 and vacuum pump on control cabinet 20.Open flammable experimental gas 1 main valve of bottle determines gross pressure in flammable experimental gas bottle by the flammable experimental gas bottle lateral pressure table of pipeline pressure reducing valve 5.
Step 7, replacement inert gas gas cylinder: it checks that 2 main valve of inert gas gas cylinder is in close state, it is manual to close third Shut-off valve 18 opens the second hand stop valve 8, adjusts the second pipeline pressure reducing valve 6 and nitrogen in pipeline drains to (i.e. the second pipeline subtracts When 6 pressure at both sides table of pressure valve is illustrated as 0), more renew gas cylinder.The second hand stop valve 8 and the second pipeline pressure reducing valve 6 are closed, 2 main valve of inert gas gas cylinder is opened, stagnation pressure in inert gas gas cylinder 2 is determined by 6 gas cylinder lateral pressure table of the second pipeline pressure reducing valve Power.Third hand stop valve 18 is opened, adjustment third pipeline pressure reducing valve 19 makes to lead to solenoid valve lateral pressure to be about 5bar.
The foregoing description of the disclosed embodiments makes professional and technical personnel in the field can be realized or use the application. Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the application.Therefore, the application It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one The widest scope of cause.

Claims (3)

1.一种高压可燃性实验气体的安全输运装置,其特征在于:该装置包括气瓶组,供气管路单元,抽真空单元和可燃气报警单元;气瓶组和供气管路单元的作用是向实验室设备内稳定地持续供气或间歇供气,同时还可为实验前气密性的检验、实验后促进装置内尾气的排放提供气源,供气管路单元能够根据实验要求在整个实验过程中对气体压力进行全量程调整;抽真空单元用于实验前抽取实验装置内的气体;可燃气报警单元用于当气体泄漏浓度达到报警浓度时发出声、光警报提醒采取安全措施及联动排风、切断电源,保证实验的安全性。1. a safety transport device for high pressure flammable experimental gas, is characterized in that: this device comprises gas cylinder group, gas supply pipeline unit, vacuuming unit and combustible gas alarm unit; the effect of gas cylinder group and gas supply pipeline unit It is a stable continuous or intermittent supply of air to laboratory equipment, and it can also provide an air source for air tightness inspection before the experiment and after the experiment to promote the discharge of exhaust gas in the device. During the experiment, the gas pressure is adjusted in the full range; the vacuum unit is used to extract the gas in the experimental device before the experiment; the combustible gas alarm unit is used to issue sound and light alarms when the gas leakage concentration reaches the alarm concentration to remind you to take safety measures and linkage Exhaust air and cut off the power supply to ensure the safety of the experiment. 2.根据权利要求1所述的高压可燃性实验气体的安全输运装置,其特征在于,该装置的具体结构如下:气瓶组主要由可燃性实验气体气瓶(1),惰性气体气瓶(2)组成;供气管单元主要由第一、第二过滤器(3、4),第一、第二、第三管路减压阀(5、6、19),第一、第二、第三、第四、第五手动截止阀(7、8、18、15、14),第一、第二、第三气动截止阀(9、10、12),压力变送器(11),控制箱(20),金属管道组成;可燃性实验气体瓶(1)通过管道与第一过滤器(3)、第一管路减压阀(5)、第一气动截止阀(9)及与其并联的第一手动截止阀(7)、压力变送器(11)相连,惰性气体气瓶(2)通过管道与第二过滤器(4)、第二管路减压阀(6)、第二气动截止阀(10)及与其并联的第二手动截止阀(8)相连,两条管路并联;排空管通过第四手动截止阀(15)进行控制,与可燃气和惰性气管道连接汇集到主高压管道(16)上,用于排放装置内气体;第一、第二、第三管路减压阀(5、6、19)在与气瓶连接侧、主管道连接侧安装2个压力表,分别显示气瓶内压力和管道内压力变化;控制箱(20)设置有多个电磁阀开关,对第一、第二、第三气动截止阀(9、10、12)进行开闭控制,箱体通过第三手动截止阀(18)、第三管路减压阀(19)及金属管道与惰性气体气瓶(2)连接,通过惰性气体气瓶(2)以及第三管路减压阀(19)提供控制箱内所需压力;压力变送器(11)用于当可燃性气体对实验设备持续供气时,判断设备是否保压成功;抽真空系统包括第三气动截止阀(12)、带有真空表的真空泵(13),带有真空表的真空泵(13)通过管道与第三气动截止阀(12)相连接,再由管道连接到主高压管道(16)上;第三气动截止阀(12)及真空泵(13)的开闭由控制箱(20)中对应的电磁阀开关:第三气动截止阀(12)开启按钮(30)、第三气动截止阀(12)关闭按钮(31)及真空泵开启按钮(24)、真空泵关闭按钮(25)控制;可燃气报警单元包括气体探测器(21)和气体报警控制器(22);可燃气泄漏时,报警器动作发出声光警报,输出电信号;控制箱中安装紧急制停按钮(32),系统报警时实验员可按下该按钮使控制箱中电磁阀动作,关闭供气管路上的气动控制阀,切断气路;同时气体报警控制器(22)接受电信号,联动排风、切断电源使电磁阀关闭进而切断气路。2. the safe transportation device of high-pressure flammable experimental gas according to claim 1, is characterized in that, the concrete structure of this device is as follows: gas cylinder group is mainly composed of flammable experimental gas cylinder (1), inert gas cylinder (2) Composition; the air supply pipe unit is mainly composed of the first and second filters (3, 4), the first, second and third pipeline pressure reducing valves (5, 6, 19), the first, second, The third, fourth and fifth manual stop valves (7, 8, 18, 15, 14), the first, second and third pneumatic stop valves (9, 10, 12), pressure transmitters (11), The control box (20) is composed of metal pipes; the combustible experimental gas cylinder (1) is connected with the first filter (3), the first pipeline pressure reducing valve (5), the first pneumatic shut-off valve (9) and its The parallel first manual shut-off valve (7) and pressure transmitter (11) are connected, and the inert gas cylinder (2) is connected to the second filter (4), the second pipeline pressure reducing valve (6), the second filter (4), the second pipeline pressure reducing valve (6), the first Two pneumatic shut-off valves (10) and the second manual shut-off valve (8) connected in parallel with it, and the two pipelines are connected in parallel; The connection is collected to the main high pressure pipeline (16) for discharging the gas in the device; the first, second and third pipeline pressure reducing valves (5, 6, 19) are installed on the connection side with the gas cylinder and the main pipeline connection side 2 pressure gauges, respectively showing the pressure change in the gas cylinder and the pressure in the pipeline; the control box (20) is provided with a plurality of solenoid valve switches, and the first, second and third pneumatic shut-off valves (9, 10, 12) are Opening and closing control, the box is connected to the inert gas cylinder (2) through the third manual stop valve (18), the third pipeline pressure reducing valve (19) and the metal pipeline, and the inert gas cylinder (2) and the third The pipeline pressure reducing valve (19) provides the required pressure in the control box; the pressure transmitter (11) is used for judging whether the pressure maintaining of the equipment is successful when the combustible gas is continuously supplied to the experimental equipment; the vacuum pumping system includes a third A pneumatic shut-off valve (12), a vacuum pump (13) with a vacuum gauge, and the vacuum pump (13) with a vacuum gauge are connected to the third pneumatic shut-off valve (12) through a pipeline, which is then connected to the main high-pressure pipeline (16) ); the opening and closing of the third pneumatic cut-off valve (12) and the vacuum pump (13) are switched by the corresponding solenoid valves in the control box (20): the third pneumatic cut-off valve (12) opens the button (30), the third pneumatic cut-off The valve (12) close button (31) and the vacuum pump open button (24), the vacuum pump close button (25) are controlled; the combustible gas alarm unit includes a gas detector (21) and a gas alarm controller (22); when the combustible gas leaks, The action of the alarm will give out an audible and visual alarm, and output an electrical signal; an emergency stop button (32) is installed in the control box. When the system alarms, the experimenter can press the button to activate the solenoid valve in the control box and close the pneumatic control valve on the gas supply pipeline. , cut off the gas circuit; at the same time, the gas alarm controller (22) receives the electrical signal, links the exhaust air and cuts off the power supply to close the solenoid valve and then cuts off the gas circuit. 3.一种高压可燃性实验气体的安全输运装置的供气方法,利用权利要求1或2所述的高压可燃性实验气体的安全输运装置,其特征在于,该供气方法包括如下步骤:3. the gas supply method of the safety transportation device of a high-pressure flammable experimental gas, utilizes the safety transportation device of the high-pressure flammable experimental gas described in claim 1 or 2, it is characterized in that, this air supply method comprises the steps : 3.1、实验前确认气瓶总阀,第一、第二、第四手动截止阀,第一、第二、第三气动截止阀,第一、第二管路减压阀关闭;3.2、第三、第五手动截止阀常开,实验前打开惰性气体气瓶总阀,通过压力表确认第三管路减压阀通往电磁阀侧压力达到其工作压力;3.3、根据实验要求和目的,该装置的具体工作过程如下:3.1. Before the experiment, confirm that the main valve of the gas cylinder, the first, second and fourth manual stop valves, the first, second and third pneumatic stop valves, and the first and second pipeline pressure reducing valves are closed; 3.2, the third . The fifth manual stop valve is normally open. Open the main valve of the inert gas cylinder before the experiment, and confirm through the pressure gauge that the pressure on the side of the third pipeline pressure reducing valve leading to the solenoid valve reaches its working pressure; 3.3. According to the experimental requirements and purposes, the The specific working process of the device is as follows: (一)检查密封装置气密性以及抽真空(1) Check the air tightness of the sealing device and vacuum 若实验装置处于封闭状态,可利用本系统实现检查装置密闭性及抽真空;密闭性测试操作过程:确认惰性气体气瓶总阀开启,打开控制箱上控制第二气动截止阀的电磁阀开关,手动调节第二管路减压阀使实验装置保压至一定压力值,关闭控制箱上控制第二气动截止阀的电磁阀开关,检测实验装置密闭性,密闭性通过后,打开第四手动截止阀泄压,随后关闭该截止阀,关闭第二管路减压阀;抽真空操作过程:确认惰性气体气瓶总阀开启,打开控制箱上控制第三气动截止阀的电磁阀开关和真空泵启动开关,待抽真空结束后,依次关闭控制箱上第三气动截止阀的电磁阀开关和真空泵停止开关;If the experimental device is in a closed state, the system can be used to check the airtightness of the device and evacuate; the airtightness test operation process: confirm that the main valve of the inert gas cylinder is open, and open the solenoid valve switch on the control box that controls the second pneumatic shut-off valve. Manually adjust the second pipeline pressure reducing valve to keep the pressure of the experimental device to a certain pressure value, close the solenoid valve switch on the control box that controls the second pneumatic shut-off valve, and check the airtightness of the experimental device. After the airtightness passes, open the fourth manual shut-off valve. Pressure relief valve, then close the stop valve, and close the second pipeline pressure reducing valve; vacuum operation process: confirm that the main valve of the inert gas cylinder is open, open the solenoid valve switch on the control box that controls the third pneumatic stop valve, and start the vacuum pump After the vacuuming is completed, turn off the solenoid valve switch of the third pneumatic stop valve on the control box and the vacuum pump stop switch in turn; (二)对实验设备进行间歇供气(2) Intermittent gas supply to the experimental equipment 打开可燃性实验气体气瓶总阀,打开控制箱上第一气动截止阀的控制开关,手动调节第一管路减压阀使主管道侧压力表数据达到实验压力;若实验装置处于封闭状态,关闭第一气动截止阀的控制开关,观察压力变送器数据3分钟内是否有明显减小,若无变化则供气成功;实验结束后关闭第一气动截止阀的控制开关,关闭第一管路减压阀;随后打开控制箱上控制第二气动截止阀的电磁阀开关,手动调节第二管路减压阀,用惰性气体吹扫管路后关闭控制箱上第二气动截止阀的电磁阀开关,关闭第二管路减压阀,关闭可燃性实验气体气瓶总阀和惰性气体气瓶总阀;Open the main valve of the flammable experimental gas cylinder, open the control switch of the first pneumatic stop valve on the control box, and manually adjust the first pipeline pressure reducing valve to make the pressure gauge data on the main pipeline side reach the experimental pressure; if the experimental device is in a closed state, Close the control switch of the first pneumatic stop valve, and observe whether the pressure transmitter data is significantly reduced within 3 minutes. If there is no change, the gas supply is successful; after the experiment, close the control switch of the first pneumatic stop valve, and close the first pipe Then open the solenoid valve switch on the control box that controls the second pneumatic stop valve, manually adjust the second pipeline pressure reducing valve, purge the pipeline with inert gas, and then close the solenoid valve of the second pneumatic stop valve on the control box. Valve switch, close the pressure reducing valve of the second pipeline, close the main valve of the flammable experimental gas cylinder and the main valve of the inert gas cylinder; (三)对实验设备进行稳定的持续供气(3) Stable and continuous gas supply to the experimental equipment 确认惰性气体气瓶总阀开启,打开控制箱上控制第二气动截止阀的电磁阀开关,手动调节第二管路减压阀,用惰性气体吹扫管路后关闭第二气动截止阀的电磁阀开关,关闭第二管路减压阀之后,打开可燃性实验气体气瓶总阀,打开控制箱上控制第一气动截止阀的电磁阀开关,手动调节第一管路减压阀使主管道侧压力表数据达到供气压力;观察压力变送器数据是否有明显波动,若无变化则实现对实验设备的稳定、持续供气;Confirm that the main valve of the inert gas cylinder is open, turn on the solenoid valve switch on the control box that controls the second pneumatic stop valve, manually adjust the pressure reducing valve of the second pipeline, purge the pipeline with inert gas, and then close the solenoid valve of the second pneumatic stop valve. Valve switch, after closing the second pipeline pressure reducing valve, open the main valve of the flammable experimental gas cylinder, open the solenoid valve switch on the control box that controls the first pneumatic shut-off valve, and manually adjust the first pipeline pressure reducing valve to make the main pipeline The data of the side pressure gauge reaches the air supply pressure; observe whether the data of the pressure transmitter has obvious fluctuations, and if there is no change, realize the stable and continuous air supply to the experimental equipment; (四)输运系统中气瓶的安全更换(4) Safe replacement of gas cylinders in the transportation system 可燃性实验气体气瓶更换:检查可燃性实验气体气瓶处于关闭状态,打开第一和第四手动截止阀,调节第一管路减压阀将管道中可燃性实验气体排尽(即第一管路减压阀两侧压力表均显示为0时),第一管路减压阀保持不动,更换新气瓶;确保实验设备处于密闭状态,若实验设备为敞开型装置,需在主管道处安装常开的第五手动截止阀,此时关闭该截止阀以形成封闭回路;关闭第四手动截止阀;打开惰性气体气瓶总阀,打开控制箱上第三气动截止阀的控制开关和真空泵启动开关进行抽真空,待抽真空结束后关闭第一手动截止阀和第一管路减压阀,再依次关闭控制箱上第三气动截止阀的控制开关和真空泵停止开关;打开第五手动截止阀;打开可燃性实验气体气瓶总阀,通过第一管路减压阀于气瓶侧压力表确定可燃性实验气体气瓶内总压力;Flammable test gas cylinder replacement: Check that the flammable test gas cylinder is closed, open the first and fourth manual stop valves, and adjust the first pipeline pressure reducing valve to exhaust the flammable test gas in the pipeline (that is, the first When the pressure gauges on both sides of the pipeline pressure reducing valve show 0), keep the first pipeline pressure reducing valve still, and replace with a new gas cylinder; ensure that the experimental equipment is in a closed state. If the experimental equipment is an open device, it must be A normally open fifth manual stop valve is installed at the pipeline. At this time, the stop valve is closed to form a closed circuit; the fourth manual stop valve is closed; the main valve of the inert gas cylinder is opened, and the control switch of the third pneumatic stop valve on the control box is opened. Vacuum pumping with the vacuum pump start switch, close the first manual stop valve and the first pipeline pressure reducing valve after vacuuming, and then turn off the control switch of the third pneumatic stop valve on the control box and the vacuum pump stop switch in turn; open the fifth Manual shut-off valve; open the main valve of the flammable experimental gas cylinder, and determine the total pressure in the flammable experimental gas cylinder through the pressure gauge on the side of the cylinder through the first pipeline pressure reducing valve; 惰性气体气瓶更换:检查惰性气体气瓶处于关闭状态,关闭第三手动截止阀,打开第二手动截止阀,调节第二管路减压阀将管道中惰性气体排尽(即第二管路减压阀两侧压力表均显示为0时),第二管路减压阀保持不动,更换新气瓶;关闭第二手动截止阀和第二管路减压阀,打开惰性气体气瓶总阀,通过第二管路减压阀气瓶侧压力表确定惰性气体气瓶内总压力;打开第三手动截止阀,调整第三管路减压阀使通往电磁阀侧压力达到其工作压力。Inert gas cylinder replacement: check that the inert gas cylinder is closed, close the third manual stop valve, open the second manual stop valve, and adjust the second pipeline pressure reducing valve to exhaust the inert gas in the pipeline (that is, the second pipe When the pressure gauges on both sides of the pressure reducing valve of the second pipeline show 0), the pressure reducing valve of the second pipeline remains unchanged, and a new gas cylinder is replaced; close the second manual stop valve and the pressure reducing valve of the second pipeline, and open the inert gas The main valve of the gas cylinder, determine the total pressure in the inert gas cylinder through the pressure gauge on the gas cylinder side of the second pipeline pressure reducing valve; open the third manual stop valve, and adjust the third pipeline pressure reducing valve so that the pressure on the side leading to the solenoid valve reaches its work pressure.
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