CN109646377A - A kind of naturally black composition for hair dying and preparation method thereof - Google Patents
A kind of naturally black composition for hair dying and preparation method thereof Download PDFInfo
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- CN109646377A CN109646377A CN201910074293.0A CN201910074293A CN109646377A CN 109646377 A CN109646377 A CN 109646377A CN 201910074293 A CN201910074293 A CN 201910074293A CN 109646377 A CN109646377 A CN 109646377A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/411—Aromatic amines, i.e. where the amino group is directly linked to the aromatic nucleus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The present invention discloses a kind of naturally black composition for hair dying, including A composition and composition B, the A composition includes the raw material of following weight percent: hydroxyethyl cellulose 0.1%-10%, compound amino acid 0.1%-10%, EDTA-2 sodium 0.01%-2%, p-phenylenediamine 0.01%-2%, resorcinol 0.01%-1.25%, vitamin C 0.1%-15%, sodium sulfite 0.1%-10%, triethanolamine 0.1%-15%, ethanol amine 0.1%-10%, stripe aloe vera extract 0.1%-10%, ginseng extract 0.01%-10%, cockscomb flower extract 0.1%-10%, great Ye Pu'er tea 0.1%-10%, -7 0.1%-10% of polyquaternium, anticorrosive composite 0.01%-2%, phosphoric acid 0.1%-10%, potassium hydroxide 0.1%-15%, essence 0.01%-2%, balance deionized water；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose 0.1%-10%, going back virgin rubber 0.1%-5%, hydrogen peroxide 6%-20%, hydrogen peroxide stabilizers composition 0.01%-1%, potassium hydroxide 0.1%-10%, phosphoric acid 0.1%-10%, balance deionized water.Composition for hair dying of the present invention can quickly have hair dyed, and allergy, which is effectively reduced, allergic phenomena will not even occurs, and hair follicle is protected to damage from chemical contamination, reduce hair mechanical damage and thermal damage, prevent hair loss.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of naturally black composition for hair dying and preparation method thereof.
Background technique
With the continuous development of society, modern more pursues self-expression and individual character is interspersed.People need to pass through hair dyeing
Composition come white hair caused by modifying because of factor of waiting for a long time in heredity, nutrition, disease, year, while many people hair primary colors is changed or
The popular colours such as gold, yellow are adjusted to show individual character, are followed the fashion.As it can be seen that hair dyeing has become a kind of social trend.
Current composition for hair dying can be mainly divided into 3 major class: natural plants composition for hair dying, mineral composition for hair dying and
Oxidized form composition for hair dying.Plant composition for hair dying is using polyatomic phenol vegetable dyes active constituent, such as: hematoxylin, richness
Plant etc. containing tannic acid (tannic acid) is adsorbed by pigment or forms coloured complexing using active botanical ingredient and metallic salt
Object is covered on hair surface or penetrates into hair epidermis, cortical layer and enter hair medullary substance layer and realizes hair dyeing.Plant hair dyeing
Composition is safe and non-toxic, there is preferable Environmental compatibility, but since phytochrome extraction step is cumbersome, recovery rate is low, stablizes
Property the reasons such as difference, lead to high production cost, and coloration time it is long, not persistently, washable and wearable it is poor, it is more difficult at this stage to capture rapidly
The big share in composition for hair dying market.It is penetrative composition that mineral composition for hair dying, which is using strong acid, strong base substance, makes lead, copper
Equal metals, which penetrate into hair epidermis, cortical layer and enter hair medullary substance layer, realizes hair dyeing.It is contained in mineral composition for hair dying
Some heavy metals have certain toxicity, form compound in conjunction with enzyme-specifics certain in human body, direct interference and destructive enzyme
Normal physiological activity leads to the generation of various Poisoning illness, just gradually by market.Oxidized form composition for hair dying dye is main
Ingredient is aromatic amine compounds, oxidising composition and polyatomic phenol coupling composition, and hair dyeing principle is dyestuff intermediate and idol
After polymeric composition penetrates into hair epidermis, cortical layer and enters hair medullary substance layer, oxidation reaction, coupling reaction or contracting occurs
Reaction is closed, biggish dye molecule is formed and rests on hair epidermis, cortical layer and hair medullary substance layer and realize and have hair dyed.Chemistry hair dyeing
Composition coloring effect is good, and hue change range is wide, the duration is long, is the mainstream in current composition for hair dying market, however mesh
Before account for the biggish p-phenylenediamine class oxidation hair-dye composition of the market share there is toxicity and irritation, pole to human skin and eyes
Serious adverse reaction is easily caused by skin and hair absorption, therefore causes the case Shi Youfa of allergy using such composition for hair dying
It is raw, or even it has been reported that it has a possibility that carcinogenic.Three classes composition for hair dying advantage and disadvantage are obvious, and principle of having hair dyed
It is obvious variant.
With the scientific and technical innovation of composition for hair dying product and scientific and technological progress, no ammonia composition for hair dying, without allergy composition for hair dying,
Natural plants composition for hair dying, the colored composition for hair dying for pursuing individual character and multi-functional composition for hair dying become composition for hair dying
Industrial development trend.
Summary of the invention
In view of the deficiencies of the prior art, a kind of naturally black composition for hair dying and preparation method thereof, hair dyeing group of the present invention are proposed
Close object have many advantages, such as mildly without ammonia, efficiently quickly, without damaged after allergy, hair dyeing repair immediately, clear water is had hair dyed, and preparation process
And preparation method is simple for raw material extraction, is suitable for industrialized production.
In order to solve the above-mentioned technical problem, the technical solution of the present invention is as follows:
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 0.1%-10%, compound amino acid 0.1%-10%, EDTA-2 sodium 0.01%-2%, to benzene
Diamines 0.01%-2%, resorcinol 0.01%-1.25%, vitamin C 0.1%-15%, sodium sulfite 0.1%-10%, three
Ethanol amine 0.1%-15%, ethanol amine 0.1%-10%, stripe aloe vera extract 0.1%-10%, ginseng extract 0.01%-
10%, cockscomb flower extract 0.1%-10%, great Ye Pu'er tea 0.1%-10%, -7 0.1%-10% of polyquaternium,
Anticorrosive composite 0.01%-2%, phosphoric acid 0.1%-10%, potassium hydroxide 0.1%-15%, essence 0.01%-2%, surplus are gone
Ionized water；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose 0.1%-10%, going back virgin rubber
0.1%-5%, hydrogen peroxide 6%-20%, hydrogen peroxide stabilizers composition 0.01%-1%, potassium hydroxide 0.1%-10%, phosphorus
Sour 0.1%-10%, balance deionized water.
Preferably, the A composition includes the raw material of following weight percent: hydroxyethyl cellulose 1.5%, compounded amino
Sour 0.85%, EDTA-2 sodium 0.2%, p-phenylenediamine 1.4%, resorcinol 0.2%, vitamin C 4.5%, sodium sulfite
0.3%, triethanolamine 4.5%, ethanol amine 0.4%, stripe aloe vera extract 0.5%, ginseng extract 0.1%, cockscomb mention
Take object 0.5%, great Ye Pu'er tea 0.5%, polyquaternium -7 1%, DMDM hydantoin 0.4%, phosphoric acid 0.5%, hydrogen
Potassium oxide 2.5%, stripe aloe vera essential oil 0.5%, balance deionized water.
Preferably, the composition B includes the raw material of following weight percent: hydroxypropyl cellulose 1.5% goes back virgin rubber
0.3%, hydrogen peroxide 12%, sodium benzoate/sodium salicylate/resorcinol 0.15%, potassium hydroxide 0.8%, phosphoric acid 0.6%,
Balance deionized water.
Preferably, the anticorrosive composite is DMDM hydantoin, bis- (methylol) imidazoles gastral cavity base ureas/iodine propyl alcohol butyl
Mephenesin Carbamate, sorbic acid/potassium sorbate, benzoic acid/sodium benzoate, methylisothiazolinone, methylisothiazolinone/methyl chloride
The a combination of one or more object of isothiazolinone.
Preferably, the essence be menthol, vanillic aldehyde, stripe aloe vera essential oil, Lavender it is one or two kinds of with
On composition.
Preferably, the hydrogen peroxide stabilizers composition is benzoic acid/sodium benzoate, the western fourth of non-sodium, phosphoric acid, phosphoric acid hydrogen two
Sodium, Sodium Acid Pyrophosphate, sodium benzoate/sodium salicylate/resorcinol a combination of one or more object.
It is a further object of the present invention to provide a kind of preparation methods of naturally black composition for hair dying, include the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 250-
300r/min, time 20-30min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value control exists
Within the scope of 7.0-11.0, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 1.6-5.0 with phosphoric acid, control mixing speed in 250-300r/min, temperature is maintained at room temperature；Continue
After being stirred to react 2h, pH value is measured, pH value controls within the scope of 1.6-5.0, as finished product.
Dai medicine hair dyeing, hair care, the pharmacology of antiallergy component are as follows in the present invention:
Stripe aloe vera (Dai medicine name: refined youth): containing a large amount of amino acid, vitamin, polysaccharide compound, various enzymes and
Minerals have bactericidal antiphlogistic, improve cell viability, enhance immune, stimulating cellular growth, anti-allergic effects and can allow
The salubriouser effect of the skin on head, and a kind of natural preservative and wetting agent.
Ginseng: ginseng possesses the good reputation of " King of Herbs " since ancient times, and ginseng contains a variety of saponins and polysaccharide component, can expand
Scalp capillary, makes the telangiectasis on head, can increase the nutrition of hair, improves the toughness of hair, reduce alopecia,
Disconnected hair has protective effect to the hair of damage, and correct leatherware has anti-allergic effects.
Cockscomb (Dai medicine name: sieve carrys out Huang Gai): contain Kaempferitrin, amaranth glucoside, pine camphor and a large amount of potassium nitrate；Yellow inflorescence
In contain micro three-coloured amaranth red pigment, a large amount of three-coloured amaranth red pigments are contained in thin dyeing defect sequence, seed contains a variety of fatty acid.Modern medicine proves cockscomb
(Dai medicine name: sieve carrys out Huang Gai) has health care and Anti-hair loss to act on scalp, can be used for blood-heat type alopecia, there is refrigerant effect,
Blood circulation can also be stimulated to a certain extent.
Great Ye Pu'er tea (Dai medicine name: cured dragon): containing 10% Pu'er Tea Saponin, the washing effect of Pu'er Tea Saponin is very
It is good.Has the function of anti-dandruff, antipruritic by the shampoo of raw material of Pu'er Tea Saponin, to no skin irritation, hair is pure and fresh
It is elegant, while can take care of hair, alopecia can be prevented and treated, dandruff is removed.
Lavender oil: promoting cytothesis, and Bergamot Mint Extract is beneficial to improve skin, inhibits bacterial growth, helps
Natural on-off cycles of hair growth.Also because its energy balance skin fat secretion can more provide improvement for oily skin and oily hair instead,
The protection of dandruff and hair quality that the scalp of hair oil excessively causes, all while also has antiallergy, antipruritic function.
Compared with prior art the beneficial effects of the present invention are:
(1) present invention using traditional phenylenediamine oxidation hair-dye technology with by screened in Dai medicine classical prescription, proved recipe, it is whole
Manage out can have hair dyed, take care of hair, antiallergy active components of plants scientific compatibility, both effectively solved plant hair dyeing coloration time
It is long, not persistently, the problem of washable and wearable difference, and the problem of the traditional phenylenediamine oxidation hair-dye of effective solution easy allergy,
The advantages of having given full play to chemical hair dyeing and plant hair dyeing, can quickly have hair dyed, and allergy can be effectively reduced to go out
Existing allergic phenomena, protects hair follicle to damage from chemical contamination, reduces hair mechanical damage and thermal damage, prevents hair loss.
(2) colouring compositions of the present invention efficiently solve consumer to there is ammonia colouring compositions using no ammonium hydroxide hair color technology
The trouble and worry of produce product, no ammonia is mild, can any blending, and have hair dyed after can repair damage in time, can be effectively to dye
The protective film that the grease of the hair scale piece and naturally secret that are damaged after hair is constituted is repaired immediately, and hair is made to escape injury；Present invention dye
It sends out composition to have hair dyed using clear water, dark hair in hair dye, non-sticky scalp, non-sticky clothing is particularly suitable for residential use.
(3) hair can quickly be dyed 2.0 natural black by composition for hair dying of the present invention, and after hair dyeing, hair color is soft
Beautiful, 40 washings are colour-fast, and inherent quality meets QB/T1978-20016 standard requirements, and raw material selection meets 2015 editions and " changes
Cosmetic technical specification of security " it requires.
(4) preparation is simple for composition for hair dying of the present invention, and low energy consumption, compared with the production of traditional composition for hair dying
Production cost can be effectively reduced, industrialized production is suitable for.
Specific embodiment
Specific embodiments of the present invention will be further explained below.It should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but and does not constitute a limitation of the invention.In addition, invention described below
Technical characteristic involved in each embodiment can be combined with each other as long as they do not conflict with each other.
Embodiment 1
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 0.1%, compound amino acid 10%, EDTA-2 sodium 2%, p-phenylenediamine 0.01%, resorcinol
0.1%, vitamin C 0.1%, sodium sulfite 2%, triethanolamine 1%, ethanol amine 10%, stripe aloe vera extract 0.1%, people
Conopsea extraction 0.01%, cockscomb flower extract 0.1%, great Ye Pu'er tea 0.1%, polyquaternium -7 0.1%, bis- (hydroxyls
Methyl) imidazoles gastral cavity base urea/iodine propyl alcohol butyl mephenesin Carbamate 0.01%, phosphoric acid 0.1%, potassium hydroxide 0.1%, menthol
0.01%, deionized water 98.74%；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose 10%,
Also virgin rubber 0.1%, hydrogen peroxide 10%, benzoic acid/sodium benzoate 0.01%, potassium hydroxide 0.1%, phosphoric acid 0.1%, deionization
Water 74.06%.
A kind of preparation method of naturally black composition for hair dying, includes the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 250r/
Min, time 30min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value is controlled in 7.0 ranges
It is interior, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 1.6 with phosphoric acid, control mixing speed in 250r/min, temperature is maintained at room temperature；Continue to be stirred to react
After 2h, pH value is measured, pH value controls in 1.6, as finished product.
Embodiment 2
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 10%, compound amino acid 0.1%, EDTA-2 sodium 0.01%, p-phenylenediamine 2%, resorcinol
1.25%, vitamin C 11%, sodium sulfite 4%, triethanolamine 5%, ethanol amine 0.1%, stripe aloe vera extract 10%, people
Conopsea extraction 0.01%, cockscomb flower extract 0.1%, great Ye Pu'er tea 0.1%, polyquaternium -7 1%, sorbic acid/
Potassium sorbate 0.01%, phosphoric acid 0.1%, potassium hydroxide 1%, vanillic aldehyde 0.1%, deionized water 87.4%；The composition B packet
Include the raw material of following weight percent: hydroxypropyl cellulose 7% goes back virgin rubber 1%, hydrogen peroxide 6%, disodium hydrogen phosphate
0.05%, Sodium Acid Pyrophosphate 0.05%, potassium hydroxide 10%, phosphatase 11 %, deionized water 64.12%.
A kind of preparation method of naturally black composition for hair dying, includes the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 280r/
Min, time 25min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value is controlled in 8.0 ranges
It is interior, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 1.6-5 with phosphoric acid, control mixing speed in 250-300r/min, temperature is maintained at room temperature；Continue to stir
After mixing reaction 2h, pH value is measured, pH value controls within the scope of 1.6-5, as finished product.
Embodiment 3
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 1.5%, compound amino acid 0.85%, EDTA-2 sodium 0.2%, p-phenylenediamine 1.4%, isophthalic
Diphenol 0.2%, vitamin C 4.5%, sodium sulfite 0.3%, triethanolamine 4.5%, ethanol amine 0.4%, stripe aloe vera extract
Object 0.5%, ginseng extract 0.1%, cockscomb flower extract 0.5%, great Ye Pu'er tea 0.5%, polyquaternium -7
1%, DMDM hydantoin 0.4%, phosphoric acid 0.5%, potassium hydroxide 2.5%, stripe aloe vera essential oil 0.5%, deionized water
79.65%；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose 1.5% goes back virgin rubber 0.3%, mistake
Hydrogen oxide 12%, sodium benzoate/sodium salicylate/resorcinol 0.15%, potassium hydroxide 0.8%, phosphoric acid 0.6%, deionized water
84.65%.
A kind of preparation method of naturally black composition for hair dying, includes the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 270r/
Min, time 28min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value is controlled in 9.0 ranges
It is interior, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 3.0 with phosphoric acid, control mixing speed in 280r/min, temperature is maintained at room temperature；Continue to be stirred to react
After 2h, pH value is measured, pH value controls in 3.0 ranges, as finished product.
Embodiment 4
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 2%, compound amino acid 2%, EDTA-2 sodium 0.1%, p-phenylenediamine 0.05%, resorcinol
0.1%, vitamin C 0.1%, sodium sulfite 0.1%, triethanolamine 15%, ethanol amine 0.1%, stripe aloe vera extract
0.1%, ginseng extract 0.01%, cockscomb flower extract 0.1%, great Ye Pu'er tea 0.1%, polyquaternium -7
0.1%, benzoic acid/sodium benzoate 0.01%, phosphatase 11 0%, potassium hydroxide 0.1%, Lavender 0.01%, deionized water
69.92%；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose 2% goes back virgin rubber 0.1%, peroxide
Change hydrogen 20%, sodium benzoate/sodium salicylate/resorcinol 0.01%, potassium hydroxide 0.1%, phosphoric acid 0.1%, deionized water
77.69%.
A kind of preparation method of naturally black composition for hair dying, includes the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 280r/
Min, time 25min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value is controlled in 9.0 ranges
It is interior, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 2.0 with phosphoric acid, control mixing speed in 280r/min, temperature is maintained at room temperature；Continue to be stirred to react
After 2h, pH value is measured, pH value controls in 2.0 ranges, as finished product.
Embodiment 5
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 5%, compound amino acid 0.1%, EDTA-2 sodium 0.01%, p-phenylenediamine 0.01%, isophthalic two
Phenol 0.01%, vitamin C 0.1%, sodium sulfite 0.1%, triethanolamine 0.1%, ethanol amine 0.1%, stripe aloe vera extract
0.1%, ginseng extract 10%, cockscomb flower extract 0.5%, great Ye Pu'er tea 0.1%, polyquaternium -7
0.1%, methylisothiazolinone 0.01%, phosphoric acid 0.1%, potassium hydroxide 15%, menthol 0.01%, Lavender
0.01%, deionized water 68.54%；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose 1% is gone back
The western fourth 0.3% of virgin rubber 5%, hydrogen peroxide 7%, non-sodium, phosphoric acid 0.3%, disodium hydrogen phosphate 0.4%, potassium hydroxide 4%, phosphoric acid
3%, deionized water 79%.
A kind of preparation method of naturally black composition for hair dying, includes the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 300r/
Min, time 20min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value is controlled in 10.0 ranges
It is interior, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 3.0 with phosphoric acid, control mixing speed in 300r/min, temperature is maintained at room temperature；Continue to be stirred to react
After 2h, pH value is measured, pH value controls in 3.0 ranges, as finished product.
Embodiment 6
A kind of naturally black composition for hair dying, including A composition and composition B, the A composition include following weight percent
The raw material of ratio: hydroxyethyl cellulose 0.1%, compound amino acid 0.1%, EDTA-2 sodium 0.01%, p-phenylenediamine 0.01%, isophthalic
Diphenol 0.01%, vitamin C 15%, sodium sulfite 1%, triethanolamine 0.1%, ethanol amine 2%, stripe aloe vera extract 1%,
Ginseng extract 0.1%, cockscomb flower extract 1%, great Ye Pu'er tea 0.5%, polyquaternium -7 0.1%, methyl are different
Thiazolinone/methylchloroisothiazandnone 0.01%, phosphoric acid 0.1%, potassium hydroxide 0.1%, vanillic aldehyde 0.005%, speckle reed
Luxuriant growth essential oil 0.005%, deionized water 78.75%；The composition B includes the raw material of following weight percent: hydroxy propyl cellulose
Element 0.1% goes back the western fourth 0.05% of virgin rubber 2%, hydrogen peroxide 6%, non-sodium, potassium hydroxide 2%, phosphatase 11 0%, deionized water
79.85%.
A kind of preparation method of naturally black composition for hair dying, includes the following steps:
(1) prepared by A composition:
A, p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb are mentioned by weight
Object, stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH is taken to sequentially add at room temperature suitable
It is dissolved in amount deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl second after 10 times of deionized water wetting and dispersings is added
Base cellulose is stirred；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 300r/
Min, time 20min, temperature are maintained at room temperature；Continuing after being stirred to react 2 hours, measures pH value, pH value controls in 11 ranges,
As finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added to dissolve in appropriate amount of deionized water at room temperature and are uniformly mixed
Afterwards；It is added with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and goes back virgin rubber, adjust pH value to 7.2 with potassium hydroxide
Then thickening adjusts PH to 5.0 with phosphoric acid, control mixing speed in 300r/min, temperature is maintained at room temperature；Continue to be stirred to react
After 2h, pH value is measured, pH value controls in 5.0 ranges, as finished product.
Experimental result
1. experimenter: for the hair dyeing effect for proving the invention patent composition for hair dying, random continuous extracts 60 people, respectively
The naturally black composition for hair dying and commercially available hair dye for selecting 1-6 of embodiment of the present invention preparation carry out hair dyeing experiment as a control group,
Wherein each 30 people of men and women, 30 years old or less 10 people, 30-40 years old 10 people, 40-50 years old 20 people, 50-60 years old 20 people.
2. experimental result:
1 dyeing time of table and effect
2 staining conditions of table
Table 3 dyes the retention time
From experimental data as can be seen that composition for hair dying provided by the invention, safe, fast, efficient, clear water is had hair dyed (no
Viscous scalp does not glue clothing), no allergy and other side effects, the color dyed were not faded through 90 days, color lasting stability, and were applicable in
In hairdressing place, beauty parlor and individual use at home.
The above are present pre-ferred embodiments, it is only applicable to the principle for helping to understand the embodiment of the present invention；Meanwhile for this
The those skilled in the art in field, according to the present embodiment, there will be changes in terms of specific embodiments and scope of application, comprehensive
Upper described, the contents of this specification are not to be construed as limiting the invention.
Claims (6)
1. a kind of naturally black composition for hair dying, including A composition and composition B, it is characterised in that: the A composition includes such as
The raw material of lower weight percent: hydroxyethyl cellulose 0.1%-10%, compound amino acid 0.1%-10%, EDTA-2 sodium
0.01%-2%, p-phenylenediamine 0.01%-2%, resorcinol 0.01%-1.25%, vitamin C 0.1%-15%, sulfurous acid
Sodium 0.1%-10%, triethanolamine 0.1%-15%, ethanol amine 0.1%-10%, speckle stripe aloe vera extract 0.1%-
10%, ginseng extract 0.01%-10%, cockscomb flower extract 0.1%-10%, great Ye Pu'er tea 0.1%-10%,
Polyquaternium -70.1%-10%, anticorrosive composite 0.01%-2%, phosphoric acid 0.1%-10%, potassium hydroxide 0.1%-15%,
Essence 0.01%-2%, balance deionized water；The composition B includes the raw material of following weight percent: hydroxypropyl cellulose
0.1%-10%, virgin rubber 0.1%-5%, hydrogen peroxide 6%-20%, hydrogen peroxide stabilizers composition 0.01%-1%, hydrogen-oxygen are gone back
Change potassium 0.1%-10%, phosphoric acid 0.1%-10%, balance deionized water.
2. naturally black composition for hair dying according to claim 1, it is characterised in that: the A composition includes following weight
The raw material of percentage: hydroxyethyl cellulose 1.5%, compound amino acid 0.85%, EDTA-2 sodium 0.2%, p-phenylenediamine 1.4%,
Resorcinol 0.2%, vitamin C 4.5%, sodium sulfite 0.3%, triethanolamine 4.5%, ethanol amine 0.4%, speckle speckle reed
Luxuriant growth extract 0.5%, ginseng extract 0.1%, cockscomb flower extract 0.5%, great Ye Pu'er tea 0.5%, polyquaternary amine
Salt -7 1%, DMDM hydantoin 0.4%, phosphoric acid 0.5%, potassium hydroxide 2.5%, essence 0.5%, balance deionized water；Institute
State the raw material that composition B includes following weight percent: hydroxypropyl cellulose 1.5%, go back virgin rubber 0.3%, hydrogen peroxide 12%,
Hydrogen peroxide stabilizers composition 0.15%, potassium hydroxide 0.8%, phosphoric acid 0.6%, balance deionized water.
3. naturally black composition for hair dying according to claim 1 or 2, it is characterised in that: the anticorrosive composite is DMDM
Hydantoins, bis- (methylol) imidazoles gastral cavity base ureas/iodine propyl alcohol butyl mephenesin Carbamate, sorbic acid/potassium sorbate, benzoic acid/benzene
Sodium formate, methylisothiazolinone, methylisothiazolinone/methylchloroisothiazandnone a combination of one or more
Object.
4. naturally black composition for hair dying according to claim 1 or 2, it is characterised in that: the essence is menthol, chinese cymbidium
The a combination of one or more object of element, stripe aloe vera essential oil, Lavender.
5. naturally black composition for hair dying according to claim 1 or 2, it is characterised in that: the hydrogen peroxide stabilizers combination
Object is benzoic acid/sodium benzoate, the western fourth of non-sodium, phosphoric acid, disodium hydrogen phosphate, Sodium Acid Pyrophosphate, sodium benzoate/salicylic acid
Sodium/resorcinol a combination of one or more object.
6. a kind of preparation method of naturally black composition for hair dying of any of claims 1 or 2, it is characterised in that: including walking as follows
It is rapid:
(1) prepared by A composition:
A, it is extracted by weight by p-phenylenediamine, resorcinol, EDTA-2 sodium, compound amino acid, ginseng extract, cockscomb
Object, speckle stripe aloe vera extract, great Ye Pu'er tea, sodium sulfite, Vc, triethanolamine, KOH are sequentially added at room temperature
It is dissolved in appropriate amount of deionized water；After ethanol amine or phosphoric acid adjustment pH value, the hydroxyl after 10 times of deionized water wetting and dispersings is added
Ethyl cellulose is uniformly mixed；
B, remaining ingredient is added in the mixture in step (1), and stirring is uniformly mixed to dissolving, mixing speed 250-300r/
Min, time 20-30min, temperature are maintained at room temperature；Continue after being stirred to react 2 hours, measure pH value, pH value is controlled in 7.0-
In 11.0 ranges, as finished product；
(2) prepared by composition B:
C, hydrogen peroxide, hydrogen peroxide stabilizers composition are added in appropriate amount of deionized water dissolve after mixing at room temperature；Add
Enter with the hydroxyethyl cellulose after 10 times of deionized water wetting and dispersings and go back virgin rubber, is viscosified with potassium hydroxide adjustment pH value to 7.2,
Then PH to 1.6-5.0 is adjusted with phosphoric acid, controls mixing speed in 250-300r/min, temperature is maintained at room temperature；Continue to stir
After reacting 2h, pH value is measured, pH value controls within the scope of 1.6-5.0, as finished product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910074293.0A CN109646377A (en) | 2019-01-25 | 2019-01-25 | A kind of naturally black composition for hair dying and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910074293.0A CN109646377A (en) | 2019-01-25 | 2019-01-25 | A kind of naturally black composition for hair dying and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112515983A (en) * | 2019-09-17 | 2021-03-19 | 澳集商贸(荆门)有限公司 | Traditional Chinese medicine hair dyeing agent and using method thereof |
| CN113509430A (en) * | 2021-08-18 | 2021-10-19 | 广东芊悦药业有限公司 | Natural black folium artemisiae argyi hair dye |
| CN115043761A (en) * | 2022-07-06 | 2022-09-13 | 湖南丽臣奥威实业有限公司 | Production method of alkyl sulfate triethanolamine salt product |
-
2019
- 2019-01-25 CN CN201910074293.0A patent/CN109646377A/en not_active Withdrawn
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112515983A (en) * | 2019-09-17 | 2021-03-19 | 澳集商贸(荆门)有限公司 | Traditional Chinese medicine hair dyeing agent and using method thereof |
| CN112515983B (en) * | 2019-09-17 | 2024-02-23 | 澳集商贸(荆门)有限公司 | Traditional Chinese medicine hair-blackening agent and application method thereof |
| CN113509430A (en) * | 2021-08-18 | 2021-10-19 | 广东芊悦药业有限公司 | Natural black folium artemisiae argyi hair dye |
| CN115043761A (en) * | 2022-07-06 | 2022-09-13 | 湖南丽臣奥威实业有限公司 | Production method of alkyl sulfate triethanolamine salt product |
| CN115043761B (en) * | 2022-07-06 | 2024-03-19 | 湖南丽臣奥威实业有限公司 | Process for producing triethanolamine alkyl sulfate |
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