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CN109627065A - A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer and preparation method thereof - Google Patents

A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer and preparation method thereof Download PDF

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Publication number
CN109627065A
CN109627065A CN201811597641.4A CN201811597641A CN109627065A CN 109627065 A CN109627065 A CN 109627065A CN 201811597641 A CN201811597641 A CN 201811597641A CN 109627065 A CN109627065 A CN 109627065A
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parts
fertilizer
seaweed
salt resistance
soil
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孙红瑞
吴国会
侯松青
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Agriculture Co Ltd Harbin
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Agriculture Co Ltd Harbin
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D3/00Calcareous fertilisers
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/22Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/26Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/90Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Molecular Biology (AREA)
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  • Fertilizers (AREA)

Abstract

A kind of salt resistance containing seaweed of disclosure of the invention is alkalized Biocidal compound fertilizer and preparation method thereof, by rice bar, peanut vine, seaweed, sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris, animal wastes, EM bacterium stoste, EM nutrient solution, urease inhibitor, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate by etc. it is selected, grinding, it decocts, it pulverizes, enzymatic hydrolysis, centrifugation, fermentation, the techniques such as mixing are prepared meticulously, it alkalizes with salt resistance, fertile soil fertilizing, the function of Pesticidal and sterilizing can be carried out to soil by promoting soil soil fertility again.

Description

A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer and preparation method thereof
Technical field
The present invention relates to technical field of fertilizer production, especially a kind of salt resistance containing seaweed alkalize Biocidal compound fertilizer and its Preparation method.
Background technique
The whole world 1/5th is accounted for for population, how cultivated area for the China in the insufficient world 9%, ensures that grain is pacified It is significant problem entirely.The existing 1,800,000,000 mu of arable lands of China, to very difficult by increase arable land raising grain yield, then to It is a solution route of grain security that middle-and-low-yielding fields and obstacle soil, which want grain then,.The analysis data of the Chinese Academy of Sciences show, Hebei of Bohai Rim, Shandong, Liaoning, in Tianjin 4 province (city), have more than 4,000 ten thousand mu middle-and-low-yielding fields and more than 1,000 ten thousand mu Saline-alkali wasteland.If the factors such as breakthrough scarcity of fresh water resources and barren soil are saline and alkaline restrict, these middle-and-low-yielding fields increases in grain production are latent Power is huge.Therefore the technology and product that research and development are improved with salinization soil grain production capacity, for promoting China's agricultural can Sustainable development, Ensuring Food Safety are of great significance.
Salt-soda soil is the general designation of the various types soil of various solonchak and alkaline earth and other different degrees of salinization and alkalization. When the basicity that the cumulant of water soluble salt in upper soll layer or subsurface stratum is more than 1-2g/kg or alkalization of soils layer is more than When 5%, soil just belongs to salt-soda soil range.It is counted according to Second National soil survey information, before not including coastal tidal It puts, China's salinized soil area is 34,870,000 hectares, about 5.2 hundred million mu.With the increasingly reduction of China's cultivated area, rationally open Hair, transformation, using salt-soda soil, excavate its productive potentialities, to ensure China's grain security, promote agricultural sustainable development, improve Ecological environment and thrust zone coordinated development of the economy and society are of great significance.Salt-soda soil is mainly characterized by containing more Water soluble salt or alkaline matter.Since salinity is more, alkalinity is big, makes agron by leaching loss, and soil texture is destroyed, Sticked when showing as wet, hard when doing, native table often has a white salinity accumulation, ventilation, permeable bad, it is serious will cause plant wilt, Poisoning and rotten death, so soil improvement must be carried out to salt-soda soil.Salt-soda soil is because its soil salt content is high, the content of organic matter The low, reasons such as nutrient is barren, soil texture is poor, it is difficult to be exploited.Therefore, how to reduce salt-soda soil salt content, improve soil Earth fertility, improvement soil texture are the key that one of alkaline land improvings.Currently, saline and alkali land improvement method is mainly eliminated in soil Excessive Sodium by substitution increases soil with organic matter content to achieve the purpose that reduce soil excess salt to reach improvement The purpose of soil texture increases a large amount of and middle microelement finally by nutrient balance input to reach the mesh of suitable plant growth 's.
Agricultural is the basis of national economy, and fertilizer is an important factor for agricultural production continues stable development, fertilizer variety knot Structure it is reasonable whether, quantity number, quality height be all related to agricultural development.The enforcement period of the seventh five-year plan, country's investment are a large amount of While fund builds up the Large Fertilizer Plants such as middle petrochemical industry, Shan, black petrochemical industry;Every year from more than 2,000 ten thousand tons of external import chemical fertilizer. 19,910,000 tons of nineteen ninety-five import, 18,570,000 tons of import in 1996 becomes world Fertilizer import big country, is used for import chemical fertilizer every year Foreign exchange expenditure be more than 30 hundred million dollars.It, be by the effect of microorganism and the variation ability of soil chemistry after fertilizer applies soil It can be converted into the ionic state fertilizer of crop absorption, currently on the market mostly based on the single chemical fertilizers such as urea, ammonium nitrate, sulphur ammonium;This It meets water after a little incorporation of fertilizerin the soil to dissolve, trans-utilization rate only has 30-40% or so, and fertilizer efficiency period is short can make more nitrogen It can permeate the ground with water, flow into river, river, lake, sea by earth's surface, make the Water Eutrophication in lake region, coastal waters, Yi Fasheng red tide. Also it can make saline Land, desertification that can not cultivate;Some nitrogen gets into the air after evaporation from land, generates nitrogen oxide Etc. harmful substances, influence air quality and also destroy ozone layer.The single chemical fertilizer of another chronic administration, easily aggravates saline Land, It ploughs hardened, utilization rate of fertilizer is low.Urea, ammonium nitrate, ammonium bicarbonate are especially applied for many years, enter underground with water penetration and are dispersed into sky Nitrogen in gas.Make water eutrophication.Organic nitrogen, organic phosphorus severe overweight lead to the red tide of coastal waters occurrence of large-area year after year.Greatly A part of nitrate nitrogen is converted into carcinogenic nitrite while amount applies single nitrogenous fertilizer.According to document announcement, " the fifties are extremely The present, China's cancer morbidity increase 321%, this is had some relations with a large amount of in the recent period using chemical fertilizer and pesticide." " seven flood It is that nearly half section is seriously polluted, some lake eutrophication pollution level aggravations, 50% or more urban groundwater is by dirt Dye, National urban section 70% is contaminated."
Cultural control pest and disease damage and crops institute to fertilize, are mainly mixed with chemicals and toxic pesticides at present, Be manured into soil or crops on, be used for a long time year in year out, a large amount of pesticide and chemical fertilizer, cause pest generate drug resistance, Soil hardening, salinization of soil, soil-borne disease etc. are to lose caused by agricultural production more seriously, are caused to water source soil and crops Pollution, agricultural product quality decline, the physical and mental health and agricultural products in China that excessive pesticide residues seriously affect people are in international market Competitiveness.Thus novel organic fertilizer becomes the emphasis of people's research as the good approach to solve the above problems.
Therefore, be badly in need of in production practices it is a kind of not only can with salt resistance alkalization, fertile soil fertilizing, promote soil soil fertility but also The organic fertilizer of Pesticidal and sterilizing can be carried out to soil.
Summary of the invention
The purpose of the present invention is to provide a kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, by rice bar, peanut vine, Seaweed, sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris, animal wastes, EM bacterium are former Liquid, EM nutrient solution, urease inhibitor, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, yellow corruption Sour potassium by etc. selected, grinding, decoct, pulverize, enzymatic hydrolysis, centrifugation, fermentation, the techniques such as mixing are prepared meticulously, have anti- Salinization of soil, fertile soil fertilizing, promotion soil soil fertility can carry out the function of Pesticidal and sterilizing to soil again.
What the object of the invention was achieved through the following technical solutions:
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, is made: rice bar 50-75 of the raw material of following weight proportion Part, 45-65 parts of peanut vine, 50-70 parts of seaweed, 3-9 parts of sargentodoxa cuneata, 8-12 parts of azedarach, 15-25 parts of frutus cnidii, Wild Carrot Fruit 10- 20 parts, 2-8 parts of asafoetide, 3-15 parts of decomposite leaf violet 2-11 Fen, Common St.Paulswort Herb, 5-15 parts of Prunella vulgaris, 40-60 parts of animal wastes, EM bacterium 1-5 parts of stoste, 1-5 parts of EM nutrient solution, 0.2-0.8 parts of urease inhibitor, 15-25 parts of humic acid silicon fertilizer, 10-15 parts of zinc sulfate, 10-15 parts of magnesium sulfate, 10-20 parts of calcareous fertilisers, 10-20 parts of nitrogenous fertilizer, 15-25 parts of phosphate fertilizer, 20-30 parts of desulfurized gypsum, potassium fulvate 15- 25 parts.
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to match processing system by following preferred weight number by raw material It is made: 50 parts of rice bar, 45 parts of peanut vine, 50 parts of seaweed, 3 parts of sargentodoxa cuneata, 8 parts of azedarach, 15 parts of frutus cnidii, Wild Carrot Fruit 10 Part, 2 parts of asafoetide, 23 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 5 parts of Prunella vulgaris, 40 parts of animal wastes, 1 part of EM bacterium stoste, EM nutrient solution 1 Part, 0.2 part of urease inhibitor, 15 parts of humic acid silicon fertilizer, 10 parts of zinc sulfate, 10 parts of magnesium sulfate, 10 parts of calcareous fertilisers, 10 parts of nitrogenous fertilizer, phosphorus Fertile 15 parts, 20 parts of desulfurized gypsum, 15 parts of potassium fulvate.
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to match processing system by following preferred weight number by raw material It is made: 55 parts of rice bar, 50 parts of peanut vine, 55 parts of seaweed, 4 parts of sargentodoxa cuneata, 9 parts of azedarach, 18 parts of frutus cnidii, Wild Carrot Fruit 12 Part, 3 parts of asafoetide, 55 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 7 parts of Prunella vulgaris, 50 parts of animal wastes, 2 parts of EM bacterium stoste, EM nutrient solution 2 Part, 0.3 part of urease inhibitor, 18 parts of humic acid silicon fertilizer, 10 parts of zinc sulfate, 11 parts of magnesium sulfate, 12 parts of calcareous fertilisers, 12 parts of nitrogenous fertilizer, phosphorus Fertile 18 parts, 22 parts of desulfurized gypsum, 18 parts of potassium fulvate.
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to match processing system by following preferred weight number by raw material It is made: 65 parts of rice bar, 60 parts of peanut vine, 60 parts of seaweed, 5 parts of sargentodoxa cuneata, 10 parts of azedarach, 20 parts of frutus cnidii, Wild Carrot Fruit 15 parts, 5 parts of asafoetide, 10 8 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 8 parts of Prunella vulgaris, 60 parts of animal wastes, 3 parts of EM bacterium stoste, EM nutrition 3 parts of liquid, 0.6 part of urease inhibitor, 20 parts of humic acid silicon fertilizer, 12 parts of zinc sulfate, 12 parts of magnesium sulfate, 15 parts of calcareous fertilisers, 15 parts of nitrogenous fertilizer, 20 parts of phosphate fertilizer, 25 parts of desulfurized gypsum, 20 parts of potassium fulvate.
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to match processing system by following preferred weight number by raw material It is made: 75 parts of rice bar, 65 parts of peanut vine, 70 parts of seaweed, 9 parts of sargentodoxa cuneata, 12 parts of azedarach, 25 parts of frutus cnidii, Wild Carrot Fruit 10-20 parts, 8 parts of asafoetide, 11 15 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 15 parts of Prunella vulgaris, 60 parts of animal wastes, 5 parts of EM bacterium stoste, 5 parts of EM nutrient solution, 0.8 part of urease inhibitor, 25 parts of humic acid silicon fertilizer, 15 parts of zinc sulfate, 15 parts of magnesium sulfate, 20 parts of calcareous fertilisers, nitrogen Fertile 20 parts, 25 parts of phosphate fertilizer, 30 parts of desulfurized gypsum, 25 parts of potassium fulvate.
A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 90~100 DEG C, the time 100 minutes, are then placed in be put into grinder and are ground up, sieved 60-80 mesh, extracting screen underflow;
C, the screenings in step B is immersed in 5 times of pure water after 6-8 hours, decocts 1-2 hours, filter residue and filtrate is obtained by filtration One;Filter residue is continuously added into 5 times of pure water, decocts 0.5-1 hours, filters to obtain the dregs of a decoction and filtrate two;After dregs of a decoction drying, it crushed 100-140 mesh is sieved, Chinese medicine slag is obtained;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 200-300 mesh;Water is added by material-water ratio 1:0.45 into seaweed particle to mix It closes stirring and homogenate is made;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH in gained homogenate Value digests 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH Value digests 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;It will digest At homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, Marine algae powder is obtained, it is spare;
E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and EM bacterium stoste, the EM nutrition of the 0.025%- 0.03% of total weight of the mixture is then added Liquid fermentation, is then cooled to 30-40 DEG C for Chinese medicine liquid obtained in step C, is then uniformly sprayed in fermentation vat, fermentation 15 It, it is primary every 4 days stirrings, obtain fermentation material;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed on In fermentation material;
F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 10-15wt%, crushes, adds step A In weighed humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, be uniformly mixed, stir It mixes uniformly, then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
The beneficial effects of the present invention are: salt resistance alkali long-term stability fertilizer of the invention collects soil improvement and fertilizer in one Body, not only can be to mitigation soil salt damage, but also can improve soil texture and level of increasing soil fertility, and solved soil because salt damage is tight Weight and fertility it is barren and the problem of influence its sustainable use, the present invention is useless by the agricultural such as rice bar, peanut vine, animal wastes Slag, house refuse are recycled, and be also added Chinese herbal medicine and are fermented, and the utility value of raw material is improved, both containing rich Rich active organic principle, can activating soil, and increase beneficial microorganism amount, dramatically increase crop yield, Chinese medicine group Dividing has the function of desinsection, sterilization, and the traditional Chinese medicinal components of the desinsection class of addition while making it have fertilizer function, can also press down The growth of pythium spp processed, rhizoctonia, sickle-like bacteria etc., so that Crop Root maize ear rot is prevented and treated, crops caused by eliminating because of root rot Yield reduces.Meanwhile the effective component of seaweed and the active material contained can provide various nutrition members up to 66 kinds or more for vegetables Plain, a variety of amino acid, polysaccharide, vitamin and basic element of cell division etc. can help vegetables to establish healthy and strong root system, it is right to promote its Soil nutrient, moisture and gas are absorbed and utilized, while can increase stalk vascular bundle cell, accelerate moisture, nutrient has with photosynthetic The transport of machine product, basic element of cell division contained etc. can promote cell division, and delaying cell aging has the effect ground photosynthetic effect of ti high Rate, to reach the raising of yield, quality;Cold-resistant, drought resisting, the raising of disease resistance, in addition, alginic acid, which also has, abolishes soil It is hardened, delay saliferous effect, the main function of desulfurized gypsum is to exchange soil using the calcium ion in gypsum in the fertilizer Replaceability sodium ion on earth colloid, makes sodium ion enter the soil liquid from soil colloid transfer, enters underground water with irrigation water Or drained by drainage ditch;Animal wastes, humic acid silicon fertilizer mainly neutralize surface soil alkalinity, increase the soil organism, improve soil and hand over Change capacity, porosity and soil soil conservation water holding capacity;Chinese herbal medicine and seaweeds mainly improve soil texture, promote robust seedling root, enhancing Crop anti-adversity, increasing both production and income simultaneously improve crop quality;Calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, zinc sulfate, magnesium sulfate, potassium fulvate mainly mention For big, middle and trace element;Urease inhibitor mainly increases the long-acting deliverability of nitrogenous fertilizer, can be with disease-resistant high yield, raising crops Quality, Prunella vulgaris can not only improve nitrogen fertilizer use He Common St.Paulswort Herb can inhibit hydrolysis of urea and inhibit nitrification Rate, additionally it is possible to protect agroecological environment, simple production process of the invention, operation is easy, easy to use, raw material sources are wide General, small investment, convenient for being widely applied.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, the present invention is made below further Detailed description.
Embodiment 1
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, is made: rice bar 50-75 of the raw material of following weight proportion Part, 45-65 parts of peanut vine, 50-70 parts of seaweed, 3-9 parts of sargentodoxa cuneata, 8-12 parts of azedarach, 15-25 parts of frutus cnidii, Wild Carrot Fruit 10- 20 parts, 2-8 parts of asafoetide, 3-15 parts of decomposite leaf violet 2-11 Fen, Common St.Paulswort Herb, 5-15 parts of Prunella vulgaris, 40-60 parts of animal wastes, EM bacterium 1-5 parts of stoste, 1-5 parts of EM nutrient solution, 0.2-0.8 parts of urease inhibitor, 15-25 parts of humic acid silicon fertilizer, 10-15 parts of zinc sulfate, 10-15 parts of magnesium sulfate, 10-20 parts of calcareous fertilisers, 10-20 parts of nitrogenous fertilizer, 15-25 parts of phosphate fertilizer, 20-30 parts of desulfurized gypsum, potassium fulvate 15- 25 parts.
A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 90~100 DEG C, the time 100 minutes, are then placed in be put into grinder and are ground up, sieved 60-80 mesh, extracting screen underflow;
C, the screenings in step B is immersed in 5 times of pure water after 6-8 hours, decocts 1-2 hours, filter residue and filtrate is obtained by filtration One;Filter residue is continuously added into 5 times of pure water, decocts 0.5-1 hours, filters to obtain the dregs of a decoction and filtrate two;After dregs of a decoction drying, it crushed 100-140 mesh is sieved, Chinese medicine slag is obtained;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 200-300 mesh;Water is added by material-water ratio 1:0.45 into seaweed particle to mix It closes stirring and homogenate is made;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH in gained homogenate Value digests 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH Value digests 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;It will digest At homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, Marine algae powder is obtained, it is spare;
E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and EM bacterium stoste, the EM nutrition of the 0.025%- 0.03% of total weight of the mixture is then added Liquid fermentation, is then cooled to 30-40 DEG C for Chinese medicine liquid obtained in step C, is then uniformly sprayed in fermentation vat, fermentation 15 It, it is primary every 4 days stirrings, obtain fermentation material;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed on In fermentation material;
F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 10-15wt%, crushes, adds step A In weighed humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, be uniformly mixed, stir It mixes uniformly, then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
Embodiment 2
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to be manufactured by raw material by following preferred weight number proportion : 50 parts of rice bar, 45 parts of peanut vine, 50 parts of seaweed, 3 parts of sargentodoxa cuneata, 8 parts of azedarach, 15 parts of frutus cnidii, 10 parts of Wild Carrot Fruit, 2 parts of asafoetide, 23 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 5 parts of Prunella vulgaris, 40 parts of animal wastes, 1 part of EM bacterium stoste, 1 part of EM nutrient solution, 0.2 part of urease inhibitor, 15 parts of humic acid silicon fertilizer, 10 parts of zinc sulfate, 10 parts of magnesium sulfate, 10 parts of calcareous fertilisers, 10 parts of nitrogenous fertilizer, phosphate fertilizer 15 Part, 20 parts of desulfurized gypsum, 15 parts of potassium fulvate.
A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 90 DEG C, the time 100 minutes, are then placed in be put into and carry out being ground up, sieved 60-80 in grinder Mesh, extracting screen underflow;
C, the screenings in step B is immersed in 5 times of pure water after 6 hours, decocts 1 hour, filter residue and filtrate one is obtained by filtration;It will Filter residue continuously adds 5 times of pure water, decocts 1 hour, filters to obtain the dregs of a decoction and filtrate two;By the dregs of a decoction it is dry after, pulverize and sieve 100 mesh, Obtain Chinese medicine slag;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 200 mesh;Water mixing is added by material-water ratio 1:0.45 into seaweed particle to stir Mixing is at homogenate;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH value in gained homogenate It is digested 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH value It is digested 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;Enzymatic hydrolysis is completed Homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, obtain It is spare to marine algae powder;
E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and 0.03% EM bacterium stoste, the fermentation of EM nutrient solution of total weight of the mixture is then added, so Chinese medicine liquid obtained in step C is cooled to 40 DEG C afterwards, is then uniformly sprayed in fermentation vat, is fermented 15 days, every 4 days stirrings Once, fermentation material is obtained;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed in fermentation material;
F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 10wt%, crushes, adds in step A and claim Humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, the potassium fulvate taken is uniformly mixed, and stirring is equal It is even, it then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
Embodiment 3
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to be manufactured by raw material by following preferred weight number proportion : 75 parts of rice bar, 65 parts of peanut vine, 70 parts of seaweed, 9 parts of sargentodoxa cuneata, 12 parts of azedarach, 25 parts of frutus cnidii, Wild Carrot Fruit 10-20 Part, 8 parts of asafoetide, 11 15 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 15 parts of Prunella vulgaris, 60 parts of animal wastes, 5 parts of EM bacterium stoste, EM nutrition 5 parts of liquid, 0.8 part of urease inhibitor, 25 parts of humic acid silicon fertilizer, 15 parts of zinc sulfate, 15 parts of magnesium sulfate, 20 parts of calcareous fertilisers, 20 parts of nitrogenous fertilizer, 25 parts of phosphate fertilizer, 30 parts of desulfurized gypsum, 25 parts of potassium fulvate.
A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 95 DEG C, the time 100 minutes, are then placed in be put into and carry out being ground up, sieved 80 mesh in grinder, Extracting screen underflow;
C, the screenings in step B is immersed in 5 times of pure water after 7 hours, decocts 1.5 hours, filter residue and filtrate one is obtained by filtration; Filter residue is continuously added into 5 times of pure water, decocts 0.8 hour, filters to obtain the dregs of a decoction and filtrate two;By the dregs of a decoction it is dry after, pulverize and sieve 140 Mesh obtains Chinese medicine slag;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 300 mesh;Water mixing is added by material-water ratio 1:0.45 into seaweed particle to stir Mixing is at homogenate;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH value in gained homogenate It is digested 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH value It is digested 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;Enzymatic hydrolysis is completed Homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, obtain It is spare to marine algae powder;
E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and 0.025% EM bacterium stoste, the fermentation of EM nutrient solution of total weight of the mixture is then added, so Chinese medicine liquid obtained in step C is cooled to 40 DEG C afterwards, is then uniformly sprayed in fermentation vat, is fermented 15 days, every 4 days stirrings Once, fermentation material is obtained;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed in fermentation material;
F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 12wt%, crushes, adds in step A and claim Humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, the potassium fulvate taken is uniformly mixed, and stirring is equal It is even, it then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
Embodiment 4
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to be manufactured by raw material by following preferred weight number proportion : 65 parts of rice bar, 60 parts of peanut vine, 60 parts of seaweed, 5 parts of sargentodoxa cuneata, 10 parts of azedarach, 20 parts of frutus cnidii, 15 parts of Wild Carrot Fruit, 5 parts of asafoetide, 10 8 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 8 parts of Prunella vulgaris, 60 parts of animal wastes, 3 parts of EM bacterium stoste, EM nutrient solution 3 Part, 0.6 part of urease inhibitor, 20 parts of humic acid silicon fertilizer, 12 parts of zinc sulfate, 12 parts of magnesium sulfate, 15 parts of calcareous fertilisers, 15 parts of nitrogenous fertilizer, phosphorus Fertile 20 parts, 25 parts of desulfurized gypsum, 20 parts of potassium fulvate.
A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 100 DEG C, the time 100 minutes, are then placed in be put into and carry out being ground up, sieved 80 in grinder Mesh, extracting screen underflow;
C, the screenings in step B is immersed in 5 times of pure water after 6 hours, decocts 1 hour, filter residue and filtrate one is obtained by filtration;It will Filter residue continuously adds 5 times of pure water, decocts 1 hour, filters to obtain the dregs of a decoction and filtrate two;By the dregs of a decoction it is dry after, pulverize and sieve 100 mesh, Obtain Chinese medicine slag;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 200 mesh;Water mixing is added by material-water ratio 1:0.45 into seaweed particle to stir Mixing is at homogenate;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH value in gained homogenate It is digested 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH value It is digested 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;Enzymatic hydrolysis is completed Homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, obtain It is spare to marine algae powder;
E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and 0.025% EM bacterium stoste, the fermentation of EM nutrient solution of total weight of the mixture is then added, so Chinese medicine liquid obtained in step C is cooled to 40 DEG C afterwards, is then uniformly sprayed in fermentation vat, is fermented 15 days, every 4 days stirrings Once, fermentation material is obtained;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed in fermentation material;
F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 15wt%, crushes, adds in step A and claim Humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, the potassium fulvate taken is uniformly mixed, and stirring is equal It is even, it then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
Embodiment 5
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer is to be manufactured by raw material by following preferred weight number proportion : 55 parts of rice bar, 50 parts of peanut vine, 55 parts of seaweed, 4 parts of sargentodoxa cuneata, 9 parts of azedarach, 18 parts of frutus cnidii, 12 parts of Wild Carrot Fruit, 3 parts of asafoetide, 55 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 7 parts of Prunella vulgaris, 50 parts of animal wastes, 2 parts of EM bacterium stoste, 2 parts of EM nutrient solution, 0.3 part of urease inhibitor, 18 parts of humic acid silicon fertilizer, 10 parts of zinc sulfate, 11 parts of magnesium sulfate, 12 parts of calcareous fertilisers, 12 parts of nitrogenous fertilizer, phosphate fertilizer 18 Part, 22 parts of desulfurized gypsum, 18 parts of potassium fulvate.
A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 90 DEG C, the time 100 minutes, are then placed in be put into and carry out being ground up, sieved 80 mesh in grinder, Extracting screen underflow;
C, the screenings in step B is immersed in 5 times of pure water after 6 hours, decocts 2 hours, filter residue and filtrate one is obtained by filtration;It will Filter residue continuously adds 5 times of pure water, decocts 1 hour, filters to obtain the dregs of a decoction and filtrate two;By the dregs of a decoction it is dry after, pulverize and sieve 100 mesh, Obtain Chinese medicine slag;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 200-300 mesh;Water is added by material-water ratio 1:0.45 into seaweed particle to mix It closes stirring and homogenate is made;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH in gained homogenate Value digests 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH Value digests 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;It will digest At homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, Marine algae powder is obtained, it is spare;
E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and 0.03% EM bacterium stoste, the fermentation of EM nutrient solution of total weight of the mixture is then added, so Chinese medicine liquid obtained in step C is cooled to 40 DEG C afterwards, is then uniformly sprayed in fermentation vat, is fermented 15 days, every 4 days stirrings Once, fermentation material is obtained;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed in fermentation material;
F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 10wt%, crushes, adds in step A and claim Humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, the potassium fulvate taken is uniformly mixed, and stirring is equal It is even, it then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
Comparative example 1
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, with embodiment 1, the difference is that: desulfurization is free of in the fertilizer Gypsum.
Comparative example 2
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the difference is that: animal wastes are free of in the fertilizer.
Comparative example 3
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the difference is that: seaweed is free of in the fertilizer.
Comparative example 4
A kind of salt resistance containing seaweed is alkalized Biocidal compound fertilizer, the difference is that: be free of in the fertilizer sargentodoxa cuneata, azedarach, Frutus cnidii, Wild Carrot Fruit, asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris.
Comparative example 5
A kind of salt resistance containing seaweed is alkalized Biocidal compound fertilizer, the difference is that: be free of in the fertilizer animal wastes, seaweed, Sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris.
Comparative example 6
A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the difference is that: urease inhibitor is free of in the fertilizer.
Experimental example: application of the alkalization of salt resistance containing the seaweed Biocidal compound fertilizer in corn growth
1, profile test
1.1, test site is located at farm, and soil physico-chemical property is alkaline hydrolysis nitrogen content 26.2mg/kg, available phosphorus content 8.24mg/ Kg, pH 8.55, quick-acting potassium content 192mg/kg, content of organic matter 15.4g/kg, salt content 0.22%, soluble sodium from Sub- content 82.0mg/kg.Test corn variety abundant rich 303.
1.2,7 processing of test setting, respectively 1 (embodiment 1) of processing, handle 2 (comparative examples 1), handle 3 (comparative examples 2) 4 (comparative examples 3), are handled, 5 (comparative examples 4) are handled, handle 6 (comparative examples 5), handle 7 (comparative examples 6), each processing repeats 3 It is secondary, each processing area 50m2.
1.3, test method: every season applies the alkalization Biocidal compound fertilizer 100kg of salt resistance containing seaweed, and corn is sowed June, October harvests;
1.4, measurement item: corn yield, soil soluble sodium content and pH.
2, result and analysis
2.1, influence of the alkalization of salt resistance containing the seaweed Biocidal compound fertilizer to soluble sodium content in crop yield and soil
From table 1 it follows that corn yield is lower than the embodiment of the present invention 2,3,4, soluble sodium in comparative example 1,2,3,4,5,6 Ion concentration and pH are higher than embodiment 2,3,4, illustrate that desulfurized gypsum, animal wastes, seaweed all have significant desalting effect simultaneously Improve soil environment by desalination and improves corn yield;Corn yield and soluble-salt content are high in comparative example 2,3,4 In comparative example 1, illustrate under this experimental condition, the desalting effect and corn yield increasing effect of desulfurized gypsum be higher than animal wastes, Seaweed;Corn yield is lower than example 1 in comparative example 4 and 5, illustrates sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide, decomposite leaf Violet, Common St.Paulswort Herb, Prunella vulgaris collaboration improve corn yield;In comparative example 1 and 5 corn yield lower than example 1 and soluble sodium from Sub- content is higher than example 1, illustrate desulfurized gypsum and animal wastes, seaweed, sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide, It can be cooperateed between decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris and improve corn yield and reduction soluble sodium ion concentration;Comparative example 6 Middle corn yield is lower than example 1, illustrates that urease inhibitor plays remarkable result in the long-acting supply side of fertilizer.
Corn yield, soil soluble sodium content and pH situation of change under the conditions of 1 different disposal of table
Corn yield (kg/ mus) Soluble sodium ion concentration (mg/kg) Soil pH
Embodiment 2 555 25 8.09
Embodiment 3 565 19 7.98
Embodiment 4 573 21 7.65
Comparative example 1 437 44 8.37
Comparative example 2 508 49 8.51
Comparative example 3 490 52 8.41
Comparative example 4 498 43 8.42
Comparative example 5 439 51 8.39
Comparative example 6 472 47 8.33
The experiment of fertilizer product insecticidal effect prepared by fertilizer preparation method of the present invention
Application value in order to further illustrate the present invention implements people for fertility, sunshine, the identical corn trials field 200 in water source Mu is divided into 5 parts, and 40 mu every part, wherein 3 parts use fertilizer of the invention as base manure as experimental group, another is as a control group 1 uses traditional common fertilizer as base manure, it is last it is a as a control group 2 using fertilizer of the present invention but fertilizer be free of sargentodoxa cuneata, Azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material, the weight of fertilizer that every part of experimental plot uses Equal, fertilization time is identical, identical plantation gimmick is used during crop growth, detecting pesticide during corn growth makes With situation and disease and insect situation.
Experimental result is as follows:
2 Pesticide use situation of table and disease and insect situation experimental result
Group Pesticide use situation Disease and insect situation
Embodiment 2 It is less, and can self-healing
Embodiment 3 It is less, it does not influence to produce
Embodiment 4 It is less, and can self-healing
Control group 1 Largely It must use pesticide that could ensure production
Control group 2 It must use pesticide that could ensure production
By being tested above as can be seen that making according to insecticidal fertilizer prepared by production method of the present invention with significant disinsection prophylaxis With sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, asafoetide in raw material, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material mainly rise It is acted on to disinsection prophylaxis.
The above is only a preferred embodiment of the present invention and experimental example, is not intended to restrict the invention, for this field Technical staff for, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made Any modification, equivalent substitution, improvement and etc. should all be included in the protection scope of the present invention.

Claims (6)

  1. The Biocidal compound fertilizer 1. a kind of salt resistance containing seaweed is alkalized, it is characterised in that: it is by the raw material system of following weight proportion At: 50-75 parts of rice bar, 45-65 parts of peanut vine, 50-70 parts of seaweed, 3-9 parts of sargentodoxa cuneata, 8-12 parts of azedarach, frutus cnidii 15- 25 parts, 10-20 parts of Wild Carrot Fruit, 2-8 parts of asafoetide, 3-15 parts of decomposite leaf violet 2-11 Fen, Common St.Paulswort Herb, 5-15 parts of Prunella vulgaris, animal excreta Just 40-60 parts, 1-5 parts of EM bacterium stoste, 1-5 parts of EM nutrient solution, 0.2-0.8 parts of urease inhibitor, 15-25 parts of humic acid silicon fertilizer, 10-15 parts of zinc sulfate, 10-15 parts of magnesium sulfate, 10-20 parts of calcareous fertilisers, 10-20 parts of nitrogenous fertilizer, 15-25 parts of phosphate fertilizer, desulfurized gypsum 20-30 Part, 15-25 parts of potassium fulvate.
  2. The Biocidal compound fertilizer 2. one kind salt resistance containing seaweed according to claim 1 is alkalized, it is characterised in that: be by raw material Manufactured by following preferred weight number proportion: 50 parts of rice bar, 45 parts of peanut vine, 50 parts of seaweed, 3 parts of sargentodoxa cuneata, 8 parts of azedarach, 15 parts of frutus cnidii, 10 parts of Wild Carrot Fruit, 2 parts of asafoetide, 23 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 5 parts of Prunella vulgaris, animal 40 parts of excrement, 1 part of EM bacterium stoste, 1 part of EM nutrient solution, 0.2 part of urease inhibitor, 15 parts of humic acid silicon fertilizer, 10 parts of zinc sulfate, sulphur 10 parts of sour magnesium, calcareous fertilisers 10,10 parts of nitrogenous fertilizer, 15 parts of phosphate fertilizer, 20 parts of desulfurized gypsum, 15 parts of potassium fulvate.
  3. The Biocidal compound fertilizer 3. one kind salt resistance containing seaweed according to claim 1 is alkalized, it is characterised in that: be by raw material Manufactured by following preferred weight number proportion: 55 parts of rice bar, 50 parts of peanut vine, 55 parts of seaweed, 4 parts of sargentodoxa cuneata, 9 parts of azedarach, 18 parts of frutus cnidii, 12 parts of Wild Carrot Fruit, 3 parts of asafoetide, 55 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 7 parts of Prunella vulgaris, animal 50 parts of excrement, 2 parts of EM bacterium stoste, 2 parts of EM nutrient solution, 0.3 part of urease inhibitor, 18 parts of humic acid silicon fertilizer, 10 parts of zinc sulfate, sulphur 11 parts of sour magnesium, 12 parts of calcareous fertilisers, 12 parts of nitrogenous fertilizer, 18 parts of phosphate fertilizer, 22 parts of desulfurized gypsum, 18 parts of potassium fulvate.
  4. The Biocidal compound fertilizer 4. one kind salt resistance containing seaweed according to claim 1 is alkalized, it is characterised in that: be by raw material Manufactured by following preferred weight number proportion: 65 parts of rice bar, 60 parts of peanut vine, 60 parts of seaweed, 5 parts of sargentodoxa cuneata, 10 parts of azedarach, 15 parts of Wild Carrot Fruit, 5 parts of asafoetide, 10 8 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, 8 parts of Prunella vulgaris, moves 20 parts of frutus cnidii 60 parts of object excrement, 3 parts of EM bacterium stoste, 3 parts of EM nutrient solution, 0.6 part of urease inhibitor, 20 parts of humic acid silicon fertilizer, 12 parts of zinc sulfate, 12 parts of magnesium sulfate, 15 parts of calcareous fertilisers, 15 parts of nitrogenous fertilizer, 20 parts of phosphate fertilizer, 25 parts of desulfurized gypsum, 20 parts of potassium fulvate.
  5. The Biocidal compound fertilizer 5. one kind salt resistance containing seaweed according to claim 1 is alkalized, it is characterised in that: be by raw material Manufactured by following preferred weight number proportion: 75 parts of rice bar, 65 parts of peanut vine, 70 parts of seaweed, 9 parts of sargentodoxa cuneata, 12 parts of azedarach, 25 parts of frutus cnidii, 10-20 parts of Wild Carrot Fruit, 8 parts of asafoetide, 11 15 parts of Fen, Common St.Paulswort Herb of decomposite leaf violet, Prunella vulgaris 15 Part, 60 parts of animal wastes, 5 parts of EM bacterium stoste, 5 parts of EM nutrient solution, 0.8 part of urease inhibitor, 25 parts of humic acid silicon fertilizer, zinc sulfate 15 parts, 15 parts of magnesium sulfate, 20 parts of calcareous fertilisers, 20 parts of nitrogenous fertilizer, 25 parts of phosphate fertilizer, 30 parts of desulfurized gypsum, 25 parts of potassium fulvate.
  6. The Biocidal compound fertilizer 6. one kind salt resistance containing seaweed according to claim 1-5 is alkalized, it is characterised in that: A kind of preparation method of the alkalization of salt resistance containing seaweed Biocidal compound fertilizer, the specific steps are as follows:
    A, it is matched by raw material weight number, weighs rice bar, peanut vine, seaweed, humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcium Fertilizer, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, it is spare;Select respectively high-quality sargentodoxa cuneata, azedarach, frutus cnidii, Wild Carrot Fruit, Asafoetide, decomposite leaf violet, Common St.Paulswort Herb, Prunella vulgaris raw material are cleaned, and remove the impurity in various raw materials;
    B, the various Chinese medicine materials that will be obtained after sorting, cleaning, removal of impurities are put into batch mixer mixing, after mixing evenly, are put into Desiccation in drying box, temperature control at 90~100 DEG C, the time 100 minutes, are then placed in be put into grinder and are ground up, sieved 60-80 mesh, extracting screen underflow;
    C, the screenings in step B is immersed in 5 times of pure water after 6-8 hours, decocts 1-2 hours, filter residue and filtrate is obtained by filtration One;Filter residue is continuously added into 5 times of pure water, decocts 0.5-1 hours, filters to obtain the dregs of a decoction and filtrate two;After dregs of a decoction drying, it crushed 100-140 mesh is sieved, Chinese medicine slag is obtained;Merging filtrate one and filtrate two, obtain Chinese medicine liquid, and Chinese medicine slag is spare;
    D, seaweed is handled: air-drying after first cleaning up the new fresh seaweed in step A, air-dried compound seaweed is used ultra micro It is crushed in pulverizer, obtains the seaweed particle that granularity is 200-300 mesh;Water is added by material-water ratio 1:0.45 into seaweed particle to mix It closes stirring and homogenate is made;Circumscribed beta-1,4 glucose enzyme and cellobiohydrolase are firstly added in 40 DEG C, pH in gained homogenate Value digests 4 hours under conditions of being 5, then adds Isosorbide-5-Nitrae-β-mannuronic acid lyases and bromelain in 45 DEG C, pH Value digests 7 hours under conditions of being 5;Carbohydrase is eventually adding to digest 3 hours under conditions of 50 DEG C, pH value are 4;It will digest At homogenate be centrifuged, discard sediment after the completion of centrifugation, by supernatant collection, and be put into dehydration in vacuum freeze drier, Marine algae powder is obtained, it is spare;
    E, rice bar, peanut vine are crushed respectively, is added into fermentation vat, marine algae powder, animal wastes and step C is then added Obtained Chinese medicine slag is uniformly mixed, and EM bacterium stoste, the EM nutrition of the 0.025%- 0.03% of total weight of the mixture is then added Liquid fermentation, is then cooled to 30-40 DEG C for Chinese medicine liquid obtained in step C, is then uniformly sprayed in fermentation vat, fermentation 15 It, it is primary every 4 days stirrings, obtain fermentation material;Urea takes urease inhibitor to be dissolved in the methanol of meltage, is then uniformly sprayed on In fermentation material;
    F, being transferred to drying machine drying to water content by the fermentation material that step E is handled is 10-15wt%, crushes, adds step A In weighed humic acid silicon fertilizer, zinc sulfate, magnesium sulfate, calcareous fertilisers, nitrogenous fertilizer, phosphate fertilizer, desulfurized gypsum, potassium fulvate, be uniformly mixed, stir It mixes uniformly, then, is granulated, is dry, is cooling, screening, packing to obtain the final product.
CN201811597641.4A 2018-12-26 2018-12-26 A kind of alkalization of salt resistance containing seaweed Biocidal compound fertilizer and preparation method thereof Pending CN109627065A (en)

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Application publication date: 20190416