CN109431909A - A kind of cosmetic composition containing plant component, cosmetics and its preparation method and application - Google Patents
A kind of cosmetic composition containing plant component, cosmetics and its preparation method and application Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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Abstract
The present invention relates to a kind of cosmetic compositions containing plant component, cosmetics and its preparation method and application.The cosmetic composition containing plant component, is grouped as by the group of following parts by weight: sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed oil, chamber Thallus Laminariae (Thallus Eckloniae) extract, woaded blue root extract, European pear berry extract, big red tangerine peel oil.The inventors of the present invention discovered through researches that, the collaboration whitening function of each component can be played by the composition that sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed oil, chamber Thallus Laminariae (Thallus Eckloniae) extract, woaded blue root extract, European pear berry extract and big red tangerine peel oil are mixed to get, the dosage with the chemical synthesis preparation of whitening function can significantly reduced by being applied in cosmetics, whitening effect is good, irritation is small, clearly, not sticky, and also there is anti-inflammatory, moisturizing, remove free radical, stablize oxidation resistant effect.
Description
Technical field
The invention belongs to cosmetic fields, and in particular, to a kind of cosmetic composition containing plant component, cosmetics and
Preparation method and application.
Background technique
Peach and cream, moist skin are always what women was pursued, whitening, it is anti-oxidant also be always cosmetics city
The theme of field.Whitening class cosmetics are currently on the market to add arbutin, quinhydrones, kojic acid, BHT, vitamin C and its derivative
Based on the chemical synthesis substance with whitening, anti-oxidation efficacy.Although these chemical synthesis effect compound effects are significant,
The problems such as irritation is big, unstable, effect is single is gradually exposed in use.So exploitation security level height, more function
Effect, stability is good, cosmetic material from natural plant active constituent, becomes cosmetics research and development institution and production in recent years
The hot spot of enterprises pay attention.
The applicating history of plant component is long, and already there are many plant, Chinese herbal medicine achievement incense drug grass etc. are extracted in ancient times
Application, the effect of retaining plant ingredient and its activity.
Plant it is many kinds of, there is certain effect curative effect mostly, and side effect is smaller.
Therefore, the extraction to active components of plants, the novel formula containing plant component of reasonable development, avoiding how to be utilized
The irritation for learning synthesising preparation, especially antioxidant BHT etc. further increases the whitening, oxidation resistant of natural plant component
Multiple efficacies have important meaning for the development of good stability cosmetics.
Summary of the invention
It is an object of the invention to overcome in the prior art chemical synthesis preparation irritation it is strong, it is unstable, act on single
Defect or deficiency provide a kind of cosmetic composition containing plant component.Cosmetic composition provided by the invention contains naturally
Plant component, not only clearly, it is not sticky, also have preferable whitening, anti-inflammatory, moisturizing, remove free radical, stablize oxidation resistant effect
Fruit, whitening agent dosage can be reduced by being applied in cosmetics.
Another object of the present invention is to provide the preparation methods of above-mentioned cosmetic composition.
Another object of the present invention is to provide above-mentioned cosmetic compositions to prepare the application in cosmetics.
Another object of the present invention is to provide a kind of cosmetics.
For achieving the above object, the present invention adopts the following technical scheme:
A kind of cosmetic composition containing plant component, is grouped as by the group of following parts by weight:
Sharp 0.1~4.0 part of face cream fruit oil,
0.1~4.0 part of spinach leaf extract,
0.1~3.0 part of Australia indigo plant cedar wood oil,
0.1~2.0 part of coriander seed oil,
0.1~6.0 part of chamber Thallus Laminariae (Thallus Eckloniae) extract,
0.1~3.0 part of woaded blue root extract,
0.1~7.0 part of European pear berry extract,
Big 0.1~3.0 part of peel oil of red tangerine.
Chamber Thallus Laminariae (Thallus Eckloniae) extract: a kind of edible brown alga and a kind of perennial plant are distributed near Liaodong Peninsula more
Sea area.The Multiple components such as the phytic acid tannin, the polyphenol that are extracted in chamber thallus laminariae, including inoxidizability, anti-inflammatory, radioactive protection and anti-sugar
Urine disease activity.Chamber Thallus Laminariae (Thallus Eckloniae) extract has skin brightening effect, prevents pigmentation.The extract also has uvioresistant, resists
Acne effect, anti-inflammatory effect and oxidation resistant effect.
Sharp face cream fruit oil is the essential oil extracted from face cream fruit beans wood, vegetable formal name:
MYROCARPUSFASTIGIATUS originates in Brazil, and Paraguay, Chile and Argentina are northern, and sharp face cream fruit beans wood is a height
Big akee, high one, 12-15 rice very wooden hard, the growth of pole humidity and mould.Sharp face cream fruit oil, it can be helped
Healing of wound, ulcer are helped, and avoids the generation of scar.It is also used to treatment chilly, coughs, flu.It is a kind of preservative,
Cicarisantia.Sometimes it is used to improve arthritis；Present invention discover that it dispels in light spot yellow has functions that synergy.
The beneficiating ingredients such as carrotene rich in spinach, vitamin C, calcium, phosphorus and a certain amount of iron, vitamin E,
And it is the solvent microwave abstracting mixed by water and glycerol that such spinach, which mentions leaf to take object, remains the battalion in spinach to greatest extent
It forms point, 75% effective plant essence is about remained after concentration, promote the effect of culture cell Proliferation, anti-aging but also can not only increase
The effect of strong youthful vigor, the substances such as the folic acid and vitamin c class of the inside, there are also Whitening, spots.
Australia indigo plant cedar wood oil: Australia indigo plant cypress original is grown in Australian Northern territories, and Western Australia is northern, York angle
And Queensland state northeast, it is grown in from close to sea level to 900 meters of height above sea level of region, is generally grown in sparse woods, but can also
To be found at heath forest, spinney, monsoon rainforest and rainforest edge.Its is wooden with characteristic fragrance and with the effect of termite-proof
Fruit.Australia indigo plant cypress Pterostyrax is in medium-sized to large-scale tree, and 15 to 45 meters of height, the age of tree was up to 200 years.Australia indigo plant cedar wood oil is by indigo plant
Cypress sprig and blue cypress are obtained by long-term steam distillation process, and main component is guaiol, different guaiaci lignum
Alcohol, eudesmol, selinene, guaiene, refined olive indigo plant alkene, Eucaulen, german chamomile Austria etc. ingredient.Australia indigo plant cedar wood oil has
Anti-inflammatory, antiviral, moisturizing effect, while the present inventors have additionally discovered that it dispels in burn treating, reparation, light trace yellow has certain effect
Fruit.
The yellow that coriander seed oil is obtained by steam distillation by the seed of coriander maturation is to brown color liquid.It has
The distinctive fragrance of coriander, main component are linalool, phellandrene, certain herbaceous plants with big flowers aldehyde, borneol, geraniol, firpene and geranyl acetate etc.
Equal ingredients.It is generally used in the tax perfume of food, cigarette, wine, mainly assigns fragrant, antibacterial with it in the present invention and Huangping weighing apparatus of dispelling
The effect of the colour of skin.
Woaded blue root extract: woaded blue root is the dry root of cruciferae isatis, the effective component of woaded blue root extract
Mainly there are fast indigo glycosides, isatin, indigo, woaded blue glycosides B, uridine, uracil, secondary Huang, salicylic acid, Qingdainone, daucosterol, β-paddy steroid
Alcohol, Radix Isatidis B prime etc. also contain vegetable protein, resin-like object, carbohydrate, Myronate Potassium, a variety of amino acid and microelement.Have
The effect of clearing heat and detoxicating, antibacterial, antiviral, cool blood relieving sore-throat.Present invention discover that the extract is preventing light aging and pigmentation
The effect that aspect has collaboration to promote.
Western the operatic circle mainly contain moisturizing polysaccharide (pectin), vitamin C, citric acid, minerals and amino acid (alanine,
Arginine, cystine, glycine).The fragrance of solarization pear is pure and fresh pleasant, sweet and dilitious.European pear berry extract is suitable as
Emulsifiable paste, lotion, shampoo and conditioner, bath product, salubrious, convergence wheaten food additive, have anti-oxidant, moisturizing, releive
Skin and dispel yellow whitening the effect of.
Big red tangerine peel oil is extracted from big red tangerine pericarp, cold pressing and full refining extraction technique through big red tangerine pericarp and obtain
?.The natural oily Alphalin etc. containing high-content, it is effective to treatment acne and heavy wool skin.Big red tangerine peel oil is in fragrance
There is the ability of releive completely pressure and anxiety in therapy.In cosmetic product, the sweet taste of big red tangerine peel oil is special with it
Smell energy sensation, effect of also releiving while moist.Present invention discover that it has certain effect to dispel Huang, antibacterial and oil-control
Fruit.
The inventors of the present invention discovered through researches that by sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed
The composition that oil, chamber Thallus Laminariae (Thallus Eckloniae) extract, woaded blue root extract, European pear berry extract and big red tangerine peel oil are mixed to get can be with
The collaboration whitening function for playing each component, the chemical synthesis with whitening function can significantly reduced by being applied in cosmetics
The dosage of preparation, whitening effect is good, and irritation is small, clearly, not sticky, and also has anti-inflammatory, moisturizing, removes free radical, stabilization
Oxidation resistant effect.
Preferably, the cosmetic composition is grouped as by the group of following parts by weight:
Sharp 1.0~3.0 parts of face cream fruit oil,
0.5~2.0 part of spinach leaf extract,
0.8~1.8 part of Australia indigo plant cedar wood oil,
0.2~1.0 part of coriander seed oil,
1.0~4.0 parts of chamber Thallus Laminariae (Thallus Eckloniae) extract,
0.5~2.0 part of woaded blue root extract,
1.0~3.0 parts of European pear berry extract,
Big 0.5~2.0 part of peel oil of red tangerine.
It is further preferable that the cosmetic composition containing plant component is grouped as by the group of following parts by weight:
Sharp 2 parts of face cream fruit oil,
1 part of spinach leaf extract,
1.2 parts of Australia indigo plant cedar wood oil,
0.5 part of coriander seed oil,
3 parts of chamber Thallus Laminariae (Thallus Eckloniae) extract,
1 part of woaded blue root extract,
1.5 parts of European pear berry extract,
Big 1 part of peel oil of red tangerine.
The preparation method of above-mentioned cosmetic composition, includes the following steps:
S1: by the core position of sharp face cream fruit tree, pass through the isolated sharp face cream fruit oil of steam distillation；
S2: it by the leaf harvesting of spinach, cleaning and crushes, spinach leaf extract is obtained by microwave abstracting；
S3: by the bark and core of Australia indigo plant cypress, pass through the isolated Australia indigo plant cedar wood oil of steam distillation；
S4: after the fruit of coriander is dried, pass through the isolated coriander seed oil of steam distillation；
S5: the frond of chamber thallus laminariae is passed through into the isolated chamber Thallus Laminariae (Thallus Eckloniae) extract of extraction；
S6: after the dried roots of woaded blue are crushed, woaded blue root extract is obtained by microwave abstracting；
S7: after the fruit position of European pear is crushed, pass through the isolated European pear berry extract of microwave extraction method；
S8: by the pericarp of bright red orange, pass through the isolated big red tangerine peel oil of extraction；
S9: by sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed oil pocket Thallus Laminariae (Thallus Eckloniae) extract, woaded blue root
Extract, European pear berry extract and big red tangerine peel oil mix up to the cosmetic composition containing plant component.
Said extracted object is extracted by microwave extraction method, extractant be water and propylene glycol mixed solution or water with
Glycerol mixed solution.
Above-mentioned cosmetic composition prepare in cosmetics application it is also within the scope of the present invention.
A kind of cosmetics are grouped as by the group of following mass fraction:
Above-mentioned cosmetic composition 1.0~32.0%,
Chemical whitening agent 4.0~10.0%,
Emulsifier 0.5~3.0%,
Thickener 0.1~0.8%,
Auxiliary agent TO100%.
Above-mentioned cosmetic composition is added in cosmetics, the change with whitening and antioxidant effect can significantly reduced
The dosage of synthetic is learned, whitening effect is good, and irritation is small, clearly, not sticky, and also has anti-inflammatory, moisturizing, removes freely
Base stablizes oxidation resistant effect.
Preferably, the cosmetics are grouped as by the group of following mass fraction:
Cosmetic composition 4.0~19.0%,
Chemical whitening agent 5.0~8.0%,
Emulsifier 0.8~2.0%,
Thickener 0.2~0.6%,
Auxiliary agent TO100%.
It is further preferable that the cosmetics are grouped as by the group of following mass fraction:
Cosmetic composition 11.2%,
Chemical whitening agent 6.6%,
Emulsifier 1%,
Thickener 0.5%,
Auxiliary agent TO100%.
Chemical whitening agent, emulsifier, thickener and the auxiliary agent of this field routine are used equally in the present invention.
Preferably, chemical whitening agent is alpha-arbutin, niacinamide, ethylascorbyl, Symwhite-337,1- methyl
One or more of hydantoins -2- acid imide or tranexamic acid.
Preferably, emulsifier is double-PEG/PPG-16/16PEG/PPG-16/16 dimethyl silicone polymers, polysorbate
One or more of ester -60 or cocoyl glucoside.
Preferably, thickener be one of xanthan gum, carbomer or ammonium acryloyl taurate/VP copolymer or
It is several；
Preferably, auxiliary agent be water, it is glycerol, butanediol, allantoin, dipotassium glycyrrhizinate, Sodium Hyaluronate, bisabolol, different
One or more of the different nonyl ester of n-nonanoic acid, reed fragrant plant oil, sodium pyrosulfite, hexylene glycol or Phenoxyethanol.
Cosmetics provided by the invention can be used in the spraying mode of inhalator jar or pump head.
Cosmetics provided by the invention are suitable for keratin fiber and are dyed, especially human hair.
Compared with prior art, the invention has the following beneficial effects:
Cosmetic composition provided by the invention contains natural plant composition, not only clearly, it is not sticky, also have it is preferable
Whitening, moisturizing, removes free radical, stablizes oxidation resistant effect at anti-inflammatory, and whitening agent use can be reduced by being applied in cosmetics
Amount.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.These embodiments are retouched to typical case of the invention
It states, however, the present invention is not limited thereto.Test method as used in the following examples unless otherwise specified, is conventional method, is made
Raw material, reagent etc. are unless otherwise specified the raw materials and reagents that can be obtained from commercial sources such as conventional markets.
Embodiment 1
The present embodiment provides a kind of cosmetic compositions containing plant component, by sharp face cream fruit oil 20g, spinach leaf extract
10g, Australia indigo plant cedar wood oil 12g, coriander seed oil 5g, chamber Thallus Laminariae (Thallus Eckloniae) extract 30g, woaded blue root extract 10g, European pear berry extract
15g and big red tangerine peel oil 10g composition.
The cosmetic composition containing plant component is prepared via a method which to obtain:
The preparation of sharp face cream fruit oil: fragrant by the isolated point of steam distillation by the core position of sharp face cream fruit tree
Rouge fruit oil；
The preparation of spinach leaf extract: it by the leaf harvesting of spinach, cleaning and crushes, the leaf of spinach is obtained by microwave abstracting
Extract；
The preparation of Australia indigo plant cedar wood oil: isolated by steam distillation by the bark and core of Australia indigo plant cypress
Australia indigo plant cedar wood oil；
The preparation of coriander seed oil: after the fruit of coriander is dried, pass through the isolated coriander seed oil of steam distillation；
The preparation of chamber Thallus Laminariae (Thallus Eckloniae) extract: the frond of chamber thallus laminariae is passed through into the isolated chamber Thallus Laminariae (Thallus Eckloniae) extract of extraction；
The preparation of woaded blue root extract: after the dried roots of woaded blue are crushed, woaded blue root is obtained by microwave abstracting and is extracted
Object；
The preparation of European pear berry extract: isolated by microwave extraction method after the fruit position of European pear is crushed
European pear berry extract；
The preparation of big red tangerine peel oil: by the pericarp of bright red orange, pass through the isolated big red tangerine peel oil of extraction；
Sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed oil pocket Thallus Laminariae (Thallus Eckloniae) extract, woaded blue root are mentioned
It takes object, European pear berry extract and big red tangerine peel oil to mix up to the cosmetic composition containing plant component, is denoted as 1# containing plant
The cosmetic composition of object ingredient.
Embodiment 2
The present embodiment provides a kind of cosmetic composition containing plant component, sharp face cream fruit oil 40g, spinach leaf extract
40g, Australia indigo plant cedar wood oil 30g, coriander seed oil 20g, chamber Thallus Laminariae (Thallus Eckloniae) extract 1g, woaded blue root extract 1g, European pear berry extract
1g and big red tangerine peel oil 1g composition.
Preparation method and embodiment 1 are consistent, are denoted as cosmetic composition of the 2# containing plant component.
Embodiment 3
The present embodiment provides a kind of cosmetic compositions containing plant component, by sharp face cream fruit oil 1g, spinach leaf extract
1g, Australia indigo plant cedar wood oil 1g, coriander seed oil 1g, chamber Thallus Laminariae (Thallus Eckloniae) extract 60g, woaded blue root extract 30g, European pear berry extract
70g and big red tangerine peel oil 30g composition.
Preparation method and embodiment 1 are consistent, are denoted as cosmetic composition of the 3# containing plant component.
Embodiment 4
The present embodiment provides a kind of cosmetic composition containing plant component, sharp face cream fruit oil 30g, spinach leaf extract
5g, Australia indigo plant cedar wood oil 18g, coriander seed oil 2g, chamber Thallus Laminariae (Thallus Eckloniae) extract 40g, woaded blue root extract 5g, European pear berry extract
30g and big red tangerine peel oil 5g composition.
Preparation method and embodiment 1 are consistent, are denoted as cosmetic composition of the 4# containing plant component.
Embodiment 5
The present embodiment provides a kind of cosmetic compositions containing plant component, by sharp face cream fruit oil 10g, spinach leaf extract
20g, Australia indigo plant cedar wood oil 8g, coriander seed oil 10g, chamber Thallus Laminariae (Thallus Eckloniae) extract 10g, woaded blue root extract 20g, European pear berry extract
10g and big red tangerine peel oil 20g composition.
Preparation method and embodiment 1 are consistent, are denoted as cosmetic composition of the 5# containing plant component.
In addition, the sharp face cream fruit oil in embodiment 1 is replaced with isononyl isononanoate, object is closed as a control group, is denoted as 1*
Cosmetic composition containing plant component；Australia indigo plant cedar wood oil in embodiment 1 is replaced with into isononyl isononanoate, as control
Composition is denoted as cosmetic composition of the 2* containing plant component；It is different that woaded blue root extract in embodiment 1 is replaced with into isononanoic acid
Nonyl ester, closes object as a control group, is denoted as cosmetic composition of the 3* containing plant component.By the big red tangerine peel oil in embodiment 1
Isononyl isononanoate is replaced with, closes object as a control group, is denoted as cosmetic composition of the 4* containing plant component
Embodiment 6~14 and reference examples 1~5
Table 1,2 and 3 is respectively that the formula of the cosmetics of embodiment 6~10, embodiment 11~14 and reference examples 1~5 is (single
Position: wt%).
The chemical whitening agent of embodiment 6~14 and reference examples 1~5 is alpha-arbutin, niacinamide, ethylascorbyl；It is real
The emulsifier for applying example 6~14 and reference examples 1~5 is double-PEG/PPG-16/16PEG/PPG-16/16 dimethyl silicone polymers, gathers
Sorbitol ester -60；The thickener of embodiment 6~14 and reference examples 1~5 is xanthan gum, ammonium acryloyldime-thyltaurate/VP is total
Polymers；
The auxiliary agent of embodiment 6~14 and reference examples 1~5 be water, glycerol, allantoin, Sodium Hyaluronate, dipotassium glycyrrhizinate,
Bisabolol, isononyl isononanoate, reed fragrant plant oil, sodium pyrosulfite, hexylene glycol.
Reference examples 5 do not add plant component make-up composition.
The formula (wt%) for the cosmetics that 1 embodiment 6~10 of table provides
The formula for the cosmetics that 1 embodiment 11~14 of table provides
The formula (wt%) for the cosmetics that 3 reference examples 1~5 of table provide
The following performance for the cosmetics that embodiment 6~14 and reference examples 1~5 provide is tested:
(1) tyrosinase inhibits test: tyrosinase is the key enzyme of melanin production, it controls the formation of melanin
Its level of activity of process plays a major role to the deposition of pigment.Current market sales of many whitening products are all to inhibit junket
Propylhomoserin enzyme reaches whitening function, therefore is to evaluate one of the main indicator of skin-lightening cosmetic to the power of tyrosinase inhibitory action,
The specific test method is as follows:
Sample system is added: preparing the phosphate buffer (PBS) of pH=6.8；Concentration is the tyrosinase phosphoric acid of 200U/mL
Buffer solution (is operated in ice-water bath, is saved)；Concentration is the l-tyrosine buffer solution of 2.5mmol/L；Take 1.5mL L- junket
Propylhomoserin buffer solution, 1.5mLPBS solution, the sample of 1mL above-described embodiment or reference examples, mixing are kept the temperature in 37 DEG C of water-baths
1mL tyrosinase phosphate buffer solution is added in 10min, reacts 10min, and light absorption value is measured at 475nm.
It is not loaded product system: preparing the phosphate buffer (PBS) of pH=6.8；Concentration is the tyrosinase phosphoric acid of 200U/mL
Buffer solution (is operated in ice-water bath, is saved)；Concentration is the l-tyrosine buffer solution of 2.5mmol/L；Take 1.5mL L- junket
Propylhomoserin buffer solution, 1.5mLPBS solution, 1mL deionized water, mixing keep the temperature 10min in 37 DEG C of water-baths, and 1mL junket ammonia is added
Sour enzyme phosphate buffer solution reacts 10min, and light absorption value is measured at 475nm.
The inhibiting rate of tyrosinase is calculated as follows:
Inhibiting rate=(A-B)/A × 100%
Wherein, A is the absorbance value for not being loaded product system, and B is the absorbance value of system after sample is added.Test result is shown in
Table 4.
(2) it removes the test of DPPH free radical: evaluating the antioxidation in vitro performance of sample with the method for removing DPPH free radical,
Its ethanol solution has absorption maximum at wavelength 517nm, purple.In the presence of having free radical scavenger, and its electron pairing,
UV absorption remitted its fury is set even to disappear, and to it to receive electron amount directly proportional for fading extent.Therefore, it can be inhaled by measurement
Light value changes to evaluate the antioxidant activity of sample.Specific step is as follows: taking three PE pipes, the deionization of an addition 3mL
Water, another two each prepare liquids that 3mL is added, is respectively labeled as 1,2,3, sequentially adds the DPPH solution of 3mL into 1 and 2 pipes, and 3
3mL dehydrated alcohol is added in pipe, is uniformly mixed, is protected from light and stands 40min, with ultraviolet specrophotometer at 517nm wavelength, successively
Measure its absorbance.Clearance rate calculation formula are as follows:
Clearance rate (%)=[1- (A2-A3)/A1] × 100%,
In formula: A1For the absorbance of DPPH ethanol solution；A2The absorbance of free radical is removed for prepare liquid；A3For prepare liquid
Absorbance.Test result is shown in Table 4.
(3) stability test is tested
A. heat resistance.By embodiment and reference examples after 48 DEG C are stored 30 days, visual observations find itself and the property before test
Whether shape and color generate notable difference, and whether there is or not layerings, oil slick phenomenon, if no significant difference, show embodiment or reference examples
Sample heat resistance is preferable.
B. cold resistance.By embodiment and reference examples after -10 DEG C are stored 30 days, visual observations find itself and the property before test
Whether shape and color generate notable difference, and whether there is or not layering, oil slick phenomenons to show that embodiment or reference examples are resistance to if no significant difference
It is cold preferable.
C. cold cycling.Alternately experiment (is placed on high/low temperature cold cycling to test through cold cycling for embodiment and reference examples
In case, one day temperature difference is 0-40 DEG C) after 90 days, visual observations find its with before test character and color whether generate it is obvious poor
Different, whether there is or not layering, oil slick phenomenons to show that embodiment or reference examples cold cycling stability are preferable if no significant difference.
Test result is shown in Table 5.
(4) in-service evaluation is tested
Using effect evaluation is primarily referred to as the aspiration trier by 20 Jing Guo professional training, and the sample of 80ul is applied to hand
Back mildly circle round with another hand and is smeared 8 times, and the texture of sample, spreadability, soft is then successively evaluated in a manner of marking
Soft, absorbability, with rear pleasant feeling；Evaluation criterion: very good (8-10), good (6-8), general (4-6), poor (2-4), poor
(0-2), the scoring highest of properties are divided into 10 points, and minimum to be divided into 0 point, score is higher, and the performance for representing the product is better, always
It is divided into 50 points, numerical value is higher, and effect is better.
Tyrosinase inhibits and removes DPPH free radical test result such as table 4.
4 tyrosinase of table inhibits and removes DPPH free radical test result
| Sample | Tyrosinase inhibits | Remove DPPH free radical |
| Embodiment 6 | 85.6% | 74.8% |
| Embodiment 7 | 83.8% | 72.1% |
| Embodiment 8 | 84.2% | 74.2% |
| Embodiment 9 | 83.6% | 71.3% |
| Embodiment 10 | 82.9% | 70.8% |
| Embodiment 11 | 83.0% | 69.8% |
| Embodiment 12 | 83.7% | 73.2% |
| Embodiment 13 | 82.4% | 71.1% |
| Embodiment 14 | 84.1% | 72.6% |
| Reference examples 1 | 78.2% | 66.3% |
| Reference examples 2 | 79.8% | 65.8% |
| Reference examples 3 | 78.6% | 66.2% |
| Reference examples 4 | 79.2% | 65.3% |
| Reference examples 5 | 84.2% | 63.2% |
As can be known from the results of Table 4, in embodiment 6~14 and reference examples 1~5, the tyrosinase inhibition rate of embodiment 6 with
It is all optimal for removing the effect of DPPH free radical rate.Embodiment 6 is compared with reference examples 1~5, because reference examples 5 add excess
Chemical whitening agent close to embodiment 6, that is, proves the vegetalization so its tyrosinase inhibition rate is higher than reference examples 1~4
Cosmetic compositions help to promote tyrosinase inhibition rate and remove the ability of DPPH free radical, there is whitening and oxidation resistant function
Effect.
Stability test test result such as table 5.
Test result is tested in 5 stability test of table
As can be known from the results of Table 5, embodiment 6~14 is added to plant cosmetic composition ingredient pair compared with reference examples 5
The stability of product is helpful；Reference examples 5 are the dosages of the chemical whitening agent of increase without adding plant cosmetic composition, therefore right
5 heat-resistant stability and cold cycling stability are worst as usual.
Using effect evaluation such as table 6.
The evaluation of 6 using effect of table
| Sample | Texture | Spreadability | Flexibility | Absorbability | With rear pleasant feeling | Comprehensive statistics |
| Embodiment 6 | 9.4 | 9.3 | 9.3 | 9.2 | 9.3 | 46.5 |
| Embodiment 7 | 9.3 | 9.2 | 9.2 | 9.1 | 9.2 | 46.0 |
| Embodiment 8 | 9.4 | 9.2 | 9.3 | 9.2 | 9.3 | 46.4 |
| Embodiment 9 | 9.2 | 9.2 | 9.2 | 9.1 | 9.2 | 45.9 |
| Embodiment 10 | 9.3 | 9.1 | 9.2 | 9.1 | 9.1 | 45.8 |
| Embodiment 11 | 9.0 | 9.1 | 9.2 | 9.3 | 9.0 | 45.6 |
| Embodiment 12 | 9.4 | 9.2 | 9.1 | 9.2 | 9.2 | 46.1 |
| Embodiment 13 | 9.1 | 9.1 | 9.1 | 9.1 | 9.1 | 45.5 |
| Embodiment 14 | 9.3 | 9.1 | 9.2 | 9.2 | 9.2 | 46.0 |
| Reference examples 1 | 9.0 | 9.0 | 8.9 | 8.9 | 9.0 | 44.8 |
| Reference examples 2 | 9.1 | 9.0 | 9.0 | 8.9 | 8.9 | 44.9 |
| Reference examples 3 | 9.0 | 9.1 | 8.8 | 8.9 | 9.0 | 44.8 |
| Reference examples 4 | 8.9 | 9.1 | 8.9 | 9.0 | 8.9 | 44.8 |
| Reference examples 5 | 8.7 | 8.6 | 8.5 | 8.5 | 8.4 | 42.7 |
As can be known from the results of Table 6, from the point of view of in-service evaluation, in embodiment 6~14, the synthesis in-service evaluation of embodiment 6 is most
It is excellent；Embodiment 6 is compared with reference examples 1~5, and as a result and the using effect of embodiment 6 is optimal.That is the plant cosmetics group
Closing object helps to promote the usability and skin sense of product.
In summary it can be seen that by sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed oil, chamber thallus laminariae
The composition that extract, woaded blue root extract, European pear berry extract and big red tangerine peel oil are mixed to get can play each group
The collaboration whitening function divided, the use with the chemical synthesis preparation of whitening function can significantly reduced by being applied in cosmetics
Amount, whitening effect is good, and irritation is small, clearly, not sticky, and also have anti-inflammatory, moisturizing, remove free radical, stablize it is oxidation resistant
Effect.
Above-described specific embodiment has carried out further the purpose of the present invention, technical scheme and beneficial effects
It is described in detail, it should be understood that being not intended to limit the present invention the foregoing is merely a specific embodiment of the invention
Protection scope, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should all include
Within protection scope of the present invention.
Claims (10)
1. a kind of cosmetic composition containing plant component, which is characterized in that be grouped as by the group of following parts by weight:
Sharp 0.1 ~ 4.0 part of face cream fruit oil,
0.1 ~ 4.0 part of spinach leaf extract,
0.1 ~ 3.0 part of Australia indigo plant cedar wood oil,
0.1 ~ 2.0 part of coriander seed oil,
0.1 ~ 6.0 part of chamber Thallus Laminariae (Thallus Eckloniae) extract,
0.1 ~ 3.0 part of woaded blue root extract,
0.1 ~ 7.0 part of European pear berry extract,
Big 0.1 ~ 3.0 part of peel oil of red tangerine.
2. cosmetic composition according to claim 1, which is characterized in that the cosmetic composition is by following parts by weight
Group be grouped as:
Sharp 1.0 ~ 3.0 parts of face cream fruit oil,
0.5 ~ 2.0 part of spinach leaf extract,
0.8 ~ 1.8 part of Australia indigo plant cedar wood oil,
0.2 ~ 1.0 part of coriander seed oil,
1.0 ~ 4.0 parts of chamber Thallus Laminariae (Thallus Eckloniae) extract,
0.5 ~ 2.0 part of woaded blue root extract,
1.0 ~ 3.0 parts of European pear berry extract,
Big 0.5 ~ 2.0 part of peel oil of red tangerine.
3. according to claim 2 containing the cosmetic composition of plant component, which is characterized in that the change containing plant component
Cosmetic compositions are grouped as by the group of following parts by weight:
Sharp 2 parts of face cream fruit oil,
1 part of spinach leaf extract,
1.2 parts of Australia indigo plant cedar wood oil,
0.5 part of coriander seed oil,
3 parts of chamber Thallus Laminariae (Thallus Eckloniae) extract,
1 part of woaded blue root extract,
1.5 parts of European pear berry extract,
Big 1 part of peel oil of red tangerine.
4. the preparation method of any cosmetic composition of claim 1 ~ 3, which comprises the steps of:
S1: by the core position of sharp face cream fruit tree, pass through the isolated sharp face cream fruit oil of steam distillation；
S2: it by the leaf harvesting of spinach, cleaning and crushes, spinach leaf extract is obtained by microwave abstracting；
S3: by the bark and core of Australia indigo plant cypress, pass through the isolated Australia indigo plant cedar wood oil of steam distillation；
S4: after the fruit of coriander is dried, pass through the isolated coriander seed oil of steam distillation；
S5: the frond of chamber thallus laminariae is passed through into the isolated chamber Thallus Laminariae (Thallus Eckloniae) extract of extraction；
S6: after the dried roots of woaded blue are crushed, woaded blue root extract is obtained by microwave abstracting；
S7: after the fruit position of European pear is crushed, pass through the isolated European pear berry extract of microwave extraction method；
S8: by the pericarp of bright red orange, pass through the isolated big red tangerine peel oil of extraction；
S9: sharp face cream fruit oil, spinach leaf extract, Australia indigo plant cedar wood oil, coriander seed oil, chamber Thallus Laminariae (Thallus Eckloniae) extract, woaded blue root are mentioned
Object, European pear berry extract and big red tangerine peel oil is taken to mix up to the cosmetic composition containing plant component.
5. preparation method according to claim 4, which is characterized in that the solvent of microwave abstracting is molten for the mixing of water and propylene glycol
Liquid or water and glycerol mixed solution.
6. any cosmetic composition of claim 1 ~ 3 is preparing the application in cosmetics.
7. a kind of cosmetics, which is characterized in that be grouped as by the group of following mass fraction:
Any cosmetic composition 1.0 ~ 32.0% of claim 1 ~ 3,
Chemical whitening agent 4.0 ~ 10.0%,
Emulsifier 0.5 ~ 3.0%,
Thickener 0.1 ~ 0.8%,
Auxiliary agent TO100%.
8. cosmetics according to claim 7, which is characterized in that the cosmetics are grouped as by the group of following mass fraction:
Cosmetic composition 4.0 ~ 19.0%,
Chemical whitening agent 5.0 ~ 8.0%,
Emulsifier 0.8 ~ 2.0%,
Thickener 0.2 ~ 0.6%,
Auxiliary agent TO100%.
9. cosmetics according to claim 8, which is characterized in that the cosmetics are grouped as by the group of following mass fraction:
Cosmetic composition 11.2%,
Chemical whitening agent 6.6%,
Emulsifier 1%,
Thickener 0.5%,
Auxiliary agent TO100%.
10. cosmetics according to claim 7, which is characterized in that the chemistry whitening agent is arbutin, niacinamide, ethyl
One or more of ascorbic acid, Symwhite-337,1- methyl hydantoin -2- acid imide or tranexamic acid；The cream
Agent is double-PEG/PPG-16/16 PEG/PPG-16/16 dimethyl silicone polymers, polysorbate -60 or cocoyl glucose
One or more of glycosides；The thickener is in xanthan gum, carbomer or ammonium acryloyldime-thyltaurate/VP copolymer
One or more；The auxiliary agent be water, glycerol, butanediol, allantoin, dipotassium glycyrrhizinate, Sodium Hyaluronate, bisabolol,
The one or more of isononyl isononanoate, reed fragrant plant oil, sodium pyrosulfite, hexylene glycol or Phenoxyethanol.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113730314A (en) * | 2021-10-22 | 2021-12-03 | 广州市胜梅化妆品有限公司 | Anti-aging and relieving composition and application thereof |
| CN115554208A (en) * | 2022-11-07 | 2023-01-03 | 广州德亿化妆品有限公司 | Antioxidant whitening composition containing American pear flower extract, tea polyphenol and peptides and preparation method thereof |
| CN116869864A (en) * | 2023-07-20 | 2023-10-13 | 广州市华侬化妆品股份有限公司 | Composition containing camellia seed oil, preparation method and application thereof |
-
2018
- 2018-12-26 CN CN201811603636.XA patent/CN109431909A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113730314A (en) * | 2021-10-22 | 2021-12-03 | 广州市胜梅化妆品有限公司 | Anti-aging and relieving composition and application thereof |
| CN115554208A (en) * | 2022-11-07 | 2023-01-03 | 广州德亿化妆品有限公司 | Antioxidant whitening composition containing American pear flower extract, tea polyphenol and peptides and preparation method thereof |
| CN116869864A (en) * | 2023-07-20 | 2023-10-13 | 广州市华侬化妆品股份有限公司 | Composition containing camellia seed oil, preparation method and application thereof |
| CN116869864B (en) * | 2023-07-20 | 2024-01-30 | 广州市华侬化妆品股份有限公司 | Composition containing camellia seed oil, preparation method and application thereof |
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Application publication date: 20190308 |