CN109437565A - A kind of radix curcumae glaze - Google Patents
A kind of radix curcumae glaze Download PDFInfo
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- CN109437565A CN109437565A CN201811558276.6A CN201811558276A CN109437565A CN 109437565 A CN109437565 A CN 109437565A CN 201811558276 A CN201811558276 A CN 201811558276A CN 109437565 A CN109437565 A CN 109437565A
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- glaze
- overglaze
- coat enamel
- ground coat
- feldspar
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Cosmetics (AREA)
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Abstract
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight: ilmenite 15-25, glass 30-40, spot fossil 5-10, plant ash 10-15, porcelain stone 15-25, calcite 15-20, red feldspar 10-15；The overglaze includes the raw material of following parts by weight: feldspar 35-45, zinc oxide 5-8, quartz 10-15, agate 10-15, phoenix cave temple soil 5-10.The present invention is used in combination using two kinds of glaze of ground coat enamel and overglaze, and pass through optimization method for cooking, reach slow cooling after firing temperature, a kind of novel glaze colours with large stretch of golden spot and golden flow liner on navy blue background color can successfully be burnt out, it is colorful, texture is unique, art with higher and ornamental value.
Description
Technical field
The invention belongs to pottery production technical fields, and in particular to a kind of radix curcumae glaze and preparation method.
Background technique
Chun glaze is one layer of glaze on pottery product mold surface, is generally fired under high temperature reduction flame using copper, iron as colorant
Form, and because kiln temperature, atmosphere variation due to form the transmutation effect that color desktop, lines are peculiar, artistic conception is infinite.Its feature
Mainly glaze thickness, milkiness, colour generation are complicated and changeable.
Chun glaze can generally be divided into transmutation single colour glaze, transmutation variegation glaze and transmutation fancy glaze, when transmutation single colour glaze such as Song Yuan
Bluish white, sky blue, reddish black, the pea green glaze of phase, the sky blue erythema glaze in transmutation variegation glaze such as Song Yuan period, transmutation fancy glaze such as Tang Junhua
Glaze, with the development of the times with the raising of technique, people no longer meet traditional glaze colours, it is therefore desirable to be badly in need of carrying out new glaze colours
Exploitation.
Crystalline glaze is a kind of glaze with unique artistic effect, and the crystalline substance flower of different shape, glaze colours is precipitated on smooth glaze,
With high technological value and ornamental value.The present invention exactly on this basis, passes through optimization of C/C composites and method for cooking success
The chun glaze with large stretch of golden spot crystalline glaze similar with flow liner in a kind of blue is burnt out, to enrich glaze colours kind.
Summary of the invention
The object of the invention is that providing a kind of radix curcumae glaze to solve the deficiencies in the prior art.
The purpose of the present invention is what is realized with following technical proposals:
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 15-25, glass 30-40, spot fossil 5-10, plant ash 10-15, porcelain stone 15-25, calcite 15-20, red feldspar 10-
15；The overglaze includes the raw material of following parts by weight: feldspar 35-45, zinc oxide 5-8, quartz 10-15, agate 10-15, phoenix cave
Temple soil 5-10.
The overglaze andesine includes the Sanmenxia Gorge feldspar of 25-30 parts by weight and Nan Zhao's feldspar of 10-15 parts by weight.
Preferably, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 20, glass 35, spot fossil 7.5, plant ash 12.5, porcelain stone 20, calcite 17.5, red feldspar 12.5；The overglaze packet
Include the raw material of following parts by weight: Sanmenxia Gorge feldspar 27.5, Nan Zhao's feldspar 12.5, zinc oxide 6.5, quartzy 12.5, agate 12.5, phoenix
Cave temple soil 7.5.
The preparation method of radix curcumae glaze as described above, comprising the following steps:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry, overglaze is then applied again；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1020-1080 DEG C by room temperature in 4-6h；
2. reduction phase: being warming up to 1290-1310 DEG C in 3.5-5h；
3. temperature-fall period: being slowly dropped to room temperature in 9-11h.
For the step (2) using leaching glaze method glazing, the ground coat enamel concentration of glaze slip is 30-40 Baume degrees；The overglaze glaze
Slurry concentration is 55-65 Baume degrees.
The present invention is used in combination using two kinds of glaze of ground coat enamel and overglaze, and by optimization method for cooking, reaches firing temperature
Slow cooling afterwards can successfully burn out a kind of novel glaze colours with large stretch of golden spot and golden flow liner on navy blue background color, color
Variegation bright-coloured, texture is unique, art with higher and ornamental value.
Detailed description of the invention
Fig. 1 is the radix curcumae glaze glaze figure that the embodiment of the present invention 2 provides.
Specific embodiment
Embodiment 1
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 15-25, glass 30-40, spot fossil 5-10, plant ash 10-15, porcelain stone 15-25, calcite 15-20, red feldspar 10-
15；The overglaze includes the raw material of following parts by weight: feldspar 35-45, zinc oxide 5-8, quartz 10-15, agate 10-15, phoenix cave
Temple soil 5-10.
The present invention uses ground coat enamel and the compound glaze of overglaze, not only improves the combination in green body, is also beneficial to complicated glaze colours
It generates.Wherein ilmenite, spot fossil, porcelain stone, calcite and red feldspar are all made of the product of Yuzhou in ground coat enamel, wherein red length
Stone, calcite, porcelain stone and plant ash are to commonly use raw material in pottery production, have solvent and strong cosolvent effect；In ilmenite
Containing more than 40 percent titanium oxide, more than 30 percent iron oxide, golden crystallization can be precipitated in sintering process in titanium and iron
Spot, spot fossil are a kind of poor iron ores containing iron oxide of Yuzhou, are equally used for providing ferro element, are used for colour generation.Ground coat enamel
In additionally use larger amount of glass, glaze mobility can be obviously improved, be conducive to form golden flow liner；Expansion can be reduced simultaneously
Coefficient increases the bond strength with green body, is conducive to the attachment of overglaze.Overglaze andesine and quartz are used as solvent and cosolvent,
Feldspar is used in mixed way using Sanmenxia Gorge feldspar and Nan Zhao's feldspar, wherein Sanmenxia Gorge feldspar 25-30 parts by weight, Nan Zhao feldspar 10-15
Parts by weight, Nan Zhao's feldspar is for the red feldspar of Sanmenxia Gorge feldspar and Yuzhou, and aluminium content is higher, by different sources
Feldspar is used in mixed way, and in combination with different sources feldspar ingredient, product is made to obtain better stability.Wind scoop temple soil is to be derived from Ruzhou
The clay substance at wind scoop temple can reinforce overglaze adhesion, a certain amount of agate and zinc oxide are also used in overglaze of the present invention,
It can obviously improve the texture of glaze, reduce enamelled glass sense, and reinforce opaque effect, make glaze jade-like stone profit as beautiful, zinc oxide also helps
It is generated in glaze colours.
Radix curcumae glaze preparation method as described above, it is characterised in that the following steps are included:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry (about 20S), overglaze is then applied again；It is preferred that using leaching
Glaze method glazing, ground coat enamel concentration of glaze slip are 30-40 Baume degrees；The overglaze concentration of glaze slip is 55-65 Baume degrees；Using suitable
Concentration of glaze slip can reduce the defects of contracting glaze, sagging；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1020-1080 DEG C by room temperature in 4-6h；
2. reduction phase: being warming up to 1290-1310 DEG C in 3.5-5h；
3. temperature-fall period: being slowly dropped to room temperature in 9-11h, using the method for slow cooling, be conducive to the precipitation of golden spot.
Under the suitable atmosphere of high temperature, is burnt using bavin burning, coal or gas firing method can successfully burn out radix curcumae glaze, wherein bavin
Burning, coal firing method fire yield rate 30% or so, and gas firing method is 50% or so.
Embodiment 2
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 20, glass 35, spot fossil 7.5, plant ash 12.5, porcelain stone 20, calcite 17.5, red feldspar 12.5；The overglaze packet
Include the raw material of following parts by weight: Sanmenxia Gorge feldspar 27.5, Nan Zhao's feldspar 12.5, zinc oxide 6.5, quartzy 12.5, agate 12.5, phoenix
Cave temple soil 7.5.
Radix curcumae glaze preparation method as described above, it is characterised in that the following steps are included:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry (about 20S), overglaze is then applied again；It is preferred that using leaching
Glaze method glazing, ground coat enamel concentration of glaze slip are 35 Baume degrees；The overglaze concentration of glaze slip is 60 Baume degrees；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1050 DEG C by room temperature in 5h；
2. reduction phase: being warming up to 1300 DEG C in 4h；
3. temperature-fall period: being slowly dropped to room temperature in 10h.
Glaze figure after it is burnt into can reach 52% as shown in Figure 1, burning its yield rate using gas.
Embodiment 3
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 22, glass 34, spot fossil 8, plant ash 12.5, porcelain stone 18, calcite 20, red feldspar 11；The overglaze includes following
The raw material of parts by weight: Sanmenxia Gorge feldspar 29, Nan Zhao's feldspar 10, zinc oxide 6.5, quartzy 15, agate 13, phoenix cave temple soil 6.
Radix curcumae glaze preparation method as described above, it is characterised in that the following steps are included:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry (about 20S), overglaze is then applied again；It is preferred that using leaching
Glaze method glazing, ground coat enamel concentration of glaze slip are 38 Baume degrees；The overglaze concentration of glaze slip is 62 Baume degrees；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1070 DEG C by room temperature in 5h；
2. reduction phase: being warming up to 1300 DEG C in 4.5h；
3. temperature-fall period: being slowly dropped to room temperature in 9-11h.
Embodiment 4
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 19, glass 39, spot fossil 5, plant ash 11, porcelain stone 22, calcite 17.5, red feldspar 12.5；The overglaze include with
The raw material of lower parts by weight: Sanmenxia Gorge feldspar 26, Nan Zhao's feldspar 14, zinc oxide 6, quartzy 11, agate 15, phoenix cave temple soil 9.
Radix curcumae glaze preparation method as described above, it is characterised in that the following steps are included:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry (about 20S), overglaze is then applied again；It is preferred that using leaching
Glaze method glazing, ground coat enamel concentration of glaze slip are 34 Baume degrees；The overglaze concentration of glaze slip is 60 Baume degrees；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1040 DEG C by room temperature in 6h；
2. reduction phase: being warming up to 1310 DEG C in 4.5h；
3. temperature-fall period: being slowly dropped to room temperature in 9h.
Embodiment 5
A kind of radix curcumae glaze, it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes the raw material of following parts by weight:
Ilmenite 21, glass 37, spot fossil 7.5, plant ash 10, porcelain stone 19, calcite 17, red feldspar 13；The overglaze includes following
The raw material of parts by weight: Sanmenxia Gorge feldspar 28, Nan Zhao's feldspar 13, zinc oxide 5, quartzy 10, agate 14, phoenix cave temple soil 8.
Radix curcumae glaze preparation method as described above, it is characterised in that the following steps are included:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry (about 20S), overglaze is then applied again；It is preferred that using leaching
Glaze method glazing, ground coat enamel concentration of glaze slip are 35 Baume degrees；The overglaze concentration of glaze slip is 58 Baume degrees；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1050 DEG C by room temperature in 5h；
2. reduction phase: being warming up to 1290 DEG C in 5h；
3. temperature-fall period: being slowly dropped to room temperature in 11h.
The formula of 6-13 of the embodiment of the present invention is shown in Table 1, remaining is the same as embodiment 2.
Claims (5)
1. a kind of radix curcumae glaze, it is characterised in that it is prepared by two kinds of glaze of ground coat enamel and overglaze, and the ground coat enamel includes following
The raw material of parts by weight: ilmenite 15-25, glass 30-40, spot fossil 5-10, plant ash 10-15, porcelain stone 15-25, calcite 15-
20, red feldspar 10-15；The overglaze includes the raw material of following parts by weight: feldspar 35-45, zinc oxide 5-8, quartz 10-15, Ma
Nao 10-15, phoenix cave temple soil 5-10.
2. radix curcumae glaze as described in claim 1, it is characterised in that the overglaze andesine includes the Sanmenxia Gorge of 25-30 parts by weight
Nan Zhao's feldspar of feldspar and 10-15 parts by weight.
3. radix curcumae glaze as claimed in claim 2, it is characterised in that it is prepared by two kinds of glaze of ground coat enamel and overglaze, described
Ground coat enamel includes the raw material of following parts by weight: ilmenite 20, glass 35, spot fossil 7.5, plant ash 12.5, porcelain stone 20, calcite
17.5, red feldspar 12.5；The overglaze includes the raw material of following parts by weight: Sanmenxia Gorge feldspar 27.5, Nan Zhao's feldspar 12.5, oxidation
Zinc 6.5, quartzy 12.5, agate 12.5, phoenix cave temple soil 7.5.
4. the preparation method of radix curcumae glaze as described in any one of claims 1-3, it is characterised in that the following steps are included:
(1) ground coat enamel and overglaze material are mixed respectively, ball milling obtains ground coat enamel glaze slip and overglaze glaze slip；
(2) ground coat enamel first is applied on the carcass after biscuiting；After ground coat enamel is slightly dry, overglaze is then applied again；
(3) it is burnt into, specifically includes following several stages:
1. oxidation stage: rising to 1020-1080 DEG C by room temperature in 4-6h；
2. reduction phase: being warming up to 1290-1310 DEG C in 3.5-5h；
3. temperature-fall period: being slowly dropped to room temperature in 9-11h.
5. the preparation method of radix curcumae glaze as claimed in claim 4, it is characterised in that the step (2) is applied using leaching glaze method
Glaze, the ground coat enamel concentration of glaze slip are 30-40 Baume degrees；The overglaze concentration of glaze slip is 55-65 Baume degrees.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811558276.6A CN109437565B (en) | 2018-12-19 | 2018-12-19 | Jade and gold glaze |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811558276.6A CN109437565B (en) | 2018-12-19 | 2018-12-19 | Jade and gold glaze |
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| CN109437565B CN109437565B (en) | 2021-10-01 |
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Cited By (3)
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| CN110092579A (en) * | 2019-04-18 | 2019-08-06 | 大宋官窑股份有限公司 | A kind of starry sky glaze glaze, starry sky glaze pottery and preparation method thereof |
| CN111302832A (en) * | 2020-04-09 | 2020-06-19 | 广东皓业青花彩瓷股份有限公司 | Method for forming red substrate golden wafer ceramic product in glaze firing process |
| CN112358184A (en) * | 2020-11-30 | 2021-02-12 | 海南丹之海文化传播有限公司 | High-temperature raw ore red glaze and preparation method and use method thereof |
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| CN111302832A (en) * | 2020-04-09 | 2020-06-19 | 广东皓业青花彩瓷股份有限公司 | Method for forming red substrate golden wafer ceramic product in glaze firing process |
| CN112358184A (en) * | 2020-11-30 | 2021-02-12 | 海南丹之海文化传播有限公司 | High-temperature raw ore red glaze and preparation method and use method thereof |
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