CN109157421A - Green and healthy toothpaste cream of microvesicle washing function and the preparation method and application thereof - Google Patents
Green and healthy toothpaste cream of microvesicle washing function and the preparation method and application thereof Download PDFInfo
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- CN109157421A CN109157421A CN201810876422.3A CN201810876422A CN109157421A CN 109157421 A CN109157421 A CN 109157421A CN 201810876422 A CN201810876422 A CN 201810876422A CN 109157421 A CN109157421 A CN 109157421A
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- microvesicle
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
- C11D17/0017—Multi-phase liquid compositions
- C11D17/0021—Aqueous microemulsions
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- Oral & Maxillofacial Surgery (AREA)
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Abstract
The present invention relates to green and healthy toothpaste creams of microvesicle washing function and the preparation method and application thereof.Multi-purpose toothpaste cream with microvesicle washing function, the ingredient based on toothpaste increase solvent, uniformly mix, and viscosity is 10000~200000mPas, and the time completely dissolved in water under microvesicle environment is not more than 30 seconds.The present invention is with toothpaste milky product as main component, it can be not only used for daily oral care, it is also particularly suitable for the article washing process as detergent use in microvesicle environment, the toothpaste cream dissolution rapidly under the conditions of microvesicle, it is not only able to replace conventional chemical detergent, and there is far-reaching significance with environmentally protective to care health.
Description
Technical field
The present invention relates to green and healthy toothpaste creams of microvesicle washing function and the preparation method and application thereof, belong to daily life
Product technical field.
Background technique
Toothpaste is common cleaning supplies in daily life, there is long history.With the continuous development of science and technology,
Technological equipment continuously improve and it is perfect, various types of toothpaste are come out one after another, and the quality and grade of product is continuously improved, now
Toothpaste variety by single clean type toothpaste, develops into great variety of goods, vdiverse in function, the Mobyneb tooth of a brands up to a hundred
Cream meets the needs of the different levels level of consumption.
Detergent (Detergent) is the product for being used to clean particular formulation by wash clean process.Main component is usual
It is made of surfactant, builder and additive etc..There are many type of detergent, according to the type for removing dirt, can be divided into
Heavy duty detergent and light-duty detergent；It is more that powdery, bulk, paste, pulpous state and liquid etc. can be divided into according to the shape of product
Kind form.It is broadly divided into according to it using scope: detergent for household use and industrial detergent.Wherein, detergent for household use is mainly answered
For the washing of fabric, there was only anionic surfactant and nonionic surface active agent in the washing of fabric, to fabric
Decontamination can be played the role of positive effective.Therefore both surfactants become the main material of laundry detergent compositions.
Currently there are rich and varied detergent products, such as washing powder, liquid detergent, laundry soap etc., still
Due in above-mentioned detergent product anionic surfactant and nonionic surface active agent be use chemical industry synthesis
Product, leads to it all and can generate the skin of people certain injury also to human body if being strayed into body by other approach
Certain harm is caused, and severe environmental pollution situation can not be changed so far.There are no one kind to reach currently on the market
The detergent product of grade-safe environmental protection.
Chinese patent literature CN102995348A (application number 201210563570.2) discloses a kind of water circle device, packet
Shell is included, at the top of shell water flow variation lid is provided with, the interior of shell is provided with rotation water wheels, the rotation water wheels and institute
The coaxial arrangement of water flow variation lid is stated, the rotation water wheels are rotated clockwise and rotated counterclockwise alternately；The rotation water wheels include
Axis and the multiple lodicules being fixedly installed on axis；It is covered in the water flow variation and is provided with multipair flow guiding slit, it is described every
It include two groups of flow guiding slits of radial symmetric setting to flow guiding slit, the water conservancy diversion direction of two groups of symmetrically arranged flow guiding slits is identical；Phase
The water conservancy diversion of two groups of flow guiding slits of adjacent arrangement is contrary.Invention additionally discloses a kind of water circulation faults hand washing apparatus of laundry and its works
Make method.The present invention revolves water wheels by motor driven, carries out alternately suction to water flow, make water it is described wash wash in container formed it is suitable
The circulating water flow of middle dynamics, and the curve water flow of netted high speed is formed in the top of the water flow variation lid.Make the washing of clothing
Process is truly realized zero abrasion.Above-mentioned apparatus is freely formed stable pressure during Actual laundering fabric, based on interior of shell
Under the action of power (0.25~0.35MPa), a large amount of microvesicles are produced, cooperate detergent product, the thorough clear of fabric may be implemented
It is clean, but there is no a green and healthy detergent products for being really suitble to above-mentioned microvesicle washing currently on the market.
Chinese patent literature CN105007987A (application number 201380074583.6), which discloses to be used to prepare, can be used as gargling
The method without the liquid, aqueous dentifrice composition of alcohol of saliva, the liquid tooth paste are the emulsion oil-in-water with clarification appearance.
But the product is not particularly suited for microvesicle washing.
Summary of the invention
In view of the deficiencies of the prior art, the present invention provides green and healthy toothpaste creams of microvesicle washing function and preparation method thereof
With application.
Term explanation
Microvesicle environment: the microvesicle density 10 in water3~105A/ml, 15~50 μm of microbubble diameter, water flow initial velocity is produced
Raw pressure is 0.25~0.35MPa；The microvesicle environment is by Chinese patent literature CN102995348A (application number
201210563570.2) a kind of water circle device disclosed in is produced when revolving 500 turns/min or more of water wheels revolving speed.
Technical solution of the present invention is as follows:
The green and healthy toothpaste cream of microvesicle washing function, the ingredient based on toothpaste increase solvent, uniformly mix, 20 DEG C of items
Viscosity under part is 10000~200000mPas, and the time completely dissolved in water under microvesicle environment is not more than 30 seconds.
It is preferred according to the present invention, the microvesicle environment are as follows: the microvesicle density 10 in water3~105A/ml, microbubble diameter 15
~50 μm, pressure caused by water flow initial velocity is 0.25~0.35MPa；It is further preferred that the microvesicle environment is in
A kind of water circle device disclosed in state patent document CN102995348A (application number 201210563570.2) turns in rotation water wheels
It is generated when 500 turns/min or more of speed.
Preferred according to the present invention, the toothpaste is the toothpaste for meeting GB8372-2008.
Preferred according to the present invention, the solvent is water.
According to the present invention it is further preferred that the green and healthy toothpaste cream of the microvesicle washing function, moisture content 30%
~60%, viscosity is 30000~150000mPas.
It is furthermore preferred that the moisture content be 30%, 31%, 32%, 33%, 34%, 35%, 36%, 37%, 38%,
39%, 40%, 41%, 42%, 43%, 44%, 45%, 46%, 47%, 48%, 49%, 50%, 51%, 52%, 53%,
54%, 55%, 56%, 57%, 58%, 59%, 60% and any combination between the two.
It is furthermore preferred that the viscosity be 10000mPas, 20000mPas, 30000mPas, 40000mPas,
50000mPa·s、60000mPa·s、70000mPa·s、80000mPa·s、90000mPa·s、100000mPa·s、
110000mPa·s、120000mPa·s、130000mPa·s、140000mPa·s、150000mPa·s、160000mPa·
S, 170000mPas, 180000mPas, 190000mPas, 200000mPas and any combination between the two.
The preparation method of the green and healthy toothpaste cream of above-mentioned microvesicle washing function, steps are as follows:
Ingredient based on toothpaste increases solvent, uniformly mixes, the multi-purpose tooth of 10000~200000mPas of viscosity is made
Cream cream.
The above-mentioned multi-purpose toothpaste cream with microvesicle washing function washes the application in shield in oral cavity.
The green and healthy toothpaste cream of above-mentioned microvesicle washing function is under microvesicle environment as the application of detergent.
Above-mentioned application, the specific steps are as follows:
(1) multi-purpose toothpaste cream is added according to the every 1.5 kilograms usage amounts to 10~20g of washing articles, then according to every 1.5
Kilogram to 10~15 liters of washing articles of water consumption, 10~30min of washing is carried out under microvesicle environment；
(2) by the article after step (1) washing through rinsing.
It is preferred according to the present invention, it is fabric to washing articles in the step (1)；It is further preferred that the fabric
For wool material.
It is preferred according to the present invention, in the step (2), rinse as twice, each water consumption is every 1.5 kilograms wait wash
Article 13L.
Beneficial effect
1, the present invention is also special to can be not only used for daily oral care with toothpaste milky product as main component
It is not suitable as washing process of the detergent use in microvesicle environment, the toothpaste cream dissolution rapidly under the conditions of microvesicle can not only
Replace conventional detergent, and green and healthy is easy to rinse；
2, multi-purpose toothpaste cream of the present invention can dissolve rapidly, water flow under conditions of microbubble generator acts on
It will form milk shape microvesicle group's explosion washing clothing, detergent can be replaced, achieve the effect that the decontamination to clothing is cleaned；And
Since its effective component is ingredient used in daily toothpaste, human body will not be damaged, the water after washing to environment not yet
It will cause pollution, be a kind of safe, green, health detergent product.
Detailed description of the invention
Fig. 1 is that experimental group 1 is mostly used microvesicle water flow photo when toothpaste cream uses in experimental example；
Fig. 2 is microvesicle water flow photo when 6 washing powder of experimental group uses in experimental example；
Fig. 3 is to remain on the photo on washing articles after the washing of 4 toothpaste of experimental group in experimental example；
Fig. 4 is to remain on the photo on chamber wall after the washing of 4 toothpaste of experimental group in experimental example；
Fig. 5 is the photo for remaining on container bottom in experimental example after the washing of 4 toothpaste of experimental group；
Fig. 6 is that 3 toothpaste cream of experimental group is adhered to the photo on toothbrush bristle in experimental example；
Specific embodiment
Technical solution of the present invention is described in detail below with reference to embodiment, but the embodiment is not intended to this
The real protection scope of invention constitutes any type of restriction.
Raw material sources
Toothpaste used in embodiment is that lion trump stain takes off dual-purpose toothpaste, and manufacturer is that lion king daily-use chemical industry (Qingdao) has
Limit company, ordinary commercial products.
Washing powder is that China Household Electrical Appliances Research Institute's test is dedicated, according to IEC60456ed4 annex F A* cleaning ingredients.
Washing facility is purchased from the clean Science and Technology Ltd. of Qingdao Hai Yuan, product type XQS-01.The equipment can produce microvesicle
Wash environment.
Examination criteria
Clean ratio: it is tested according to test method as defined in GB/T 4288-2008 annex E, the clean ratio of the program is answered
Meet 5.15 requirements.
It cleans the uniformity: being tested according to test method as defined in GB/T 4288-2008 annex E, which cleans
The uniformity should meet 5.15 requirements.
Rinsing performance: being tested according to test method as defined in GB/T 4288-2008 appendix C, the program it is rinsability
It can should meet 5.5 requirements.
Embodiment 1
The preparation method of the green and healthy toothpaste cream of microvesicle washing function, steps are as follows:
It toothpaste and water is mixed in 2:1 ratio, is uniformly mixed, moisture content 45%, viscosity 85000mPas is made
Multi-purpose toothpaste cream.
Embodiment 2
The preparation method of the green and healthy toothpaste cream of microvesicle washing function, steps are as follows:
Toothpaste and water are mixed in 10:1 ratio, is uniformly mixed, moisture content 30%, viscosity 200000mPas is made
Multi-purpose toothpaste cream.
Embodiment 3
The preparation method of the green and healthy toothpaste cream of microvesicle washing function, steps are as follows:
It toothpaste and water is mixed in 1:1 ratio, is uniformly mixed, moisture content 60%, viscosity 10000mPas is made
Multi-purpose toothpaste cream.
Comparative example 1
Toothpaste, through detecting, moisture content 21%, (opposite) viscosity is infinitely great.
Comparative example 2
By the preparation method of embodiment 1, the difference is that, toothpaste and water are mixed in 0.8:1 ratio, are stirred
It is even, moisture content 65%, viscosity 8000mPas is made.
Experimental example
It is washed using above-described embodiment 1~3, comparative example 1~2 and washing powder, is respectively labeled as experimental group 1~6, so
It handles in accordance with the following steps afterwards:
(1) Examples 1 to 3, comparative example 1~2 and washing powder are added according to one kilogram of usage amount to washing articles 15g,
Then the water consumption of 13 liters of cloth of the load according to per kilogram with carbon black oil pollution cloth, carries out washing 12min under microvesicle environment；
(2) by the article after step (1) washing through rinsing twice.
Through detecting, the related washing data of experimental group 1~6 is as shown in table 1:
Table 1
It is found by Actual laundering, under microbubble generator effect, toothpaste cream, washing powder can dissolve rapidly (30
Second), the microvesicle group of milky milk shape is formed, the microvesicle group of toothpaste cream is more tiny, fine and close compared with microvesicle group's microvesicle of washing powder,
Water flow photo when toothpaste cream uses is as shown in Figure 1, water flow photo when washing powder uses is as shown in Figure 2；The difference results in
Toothpaste cream washing effect under microbubble generator effect is better than washing powder.
But in the case where microbubble generator acts on, toothpaste causes aliquots of toothpaste lotion that can not dissolve since viscosity is excessively high, thus
It is attached on washing clothing and washing chamber wall, to affect clean and rinsing performance, as seen in figures 3-5.
Experimental example 2
Embodiment 3 is subjected to relevant toothpaste cream using testing, respectively by the tooth of embodiment 3 and comparative example 2 to comparative example 2
Cream cream squeezes on toothbrush, and the toothpaste cream of embodiment 3 can be attached in bristles, is not in quick trickling, and comparative example 2
Toothpaste cream can not be attached in bristles；As a result such as Fig. 6.
Claims (10)
1. the green and healthy toothpaste cream of microvesicle washing function, which is characterized in that the green and healthy toothpaste cream of microvesicle washing function,
Solvent is added on the basis of toothpaste, the viscosity under the conditions of 20 DEG C is 10000~200000mPas, completely molten under microvesicle environment
Time in Xie Yushui is not more than 30 seconds.
2. multi-purpose toothpaste cream as described in claim 1, which is characterized in that the microvesicle environment are as follows: the microvesicle density 10 in water3
~105A/ml, 15~50 μm of microbubble diameter, pressure caused by water flow initial velocity is 0.25~0.35MPa；It is further excellent
Choosing, a kind of microvesicle environment water circle device as disclosed in Chinese patent literature CN102995348A is in rotation water wheels revolving speed
It is generated when 500 turns/min or more.
3. multi-purpose toothpaste cream as described in claim 1, which is characterized in that the toothpaste is the toothpaste for meeting GB8372-2008；
Preferably, the solvent is water.
4. multi-purpose toothpaste cream as claimed in claim 3, which is characterized in that the green and healthy toothpaste of the microvesicle washing function
Cream, moisture content are 30%~60%, and viscosity is 30000~150000mPas.
5. multi-purpose toothpaste cream as claimed in claim 4, which is characterized in that the moisture content is 30%, 31%, 32%, 33%,
34%, 35%, 36%, 37%, 38%, 39%, 40%, 41%, 42%, 43%, 44%, 45%, 46%, 47%, 48%,
49%, 50%, 51%, 52%, 53%, 54%, 55%, 56%, 57%, 58%, 59%, 60% and any between the two
Combination；
It is furthermore preferred that the viscosity be 10000mPas, 20000mPas, 30000mPas, 40000mPas,
50000mPa·s、60000mPa·s、70000mPa·s、80000mPa·s、90000mPa·s、100000mPa·s、
110000mPa·s、120000mPa·s、130000mPa·s、140000mPa·s、150000mPa·s、160000mPa·
S, 170000mPas, 180000mPas, 190000mPas, 200000mPas and any combination between the two.
6. the preparation method of the green and healthy toothpaste cream of microvesicle washing function described in claim 1, which is characterized in that step is such as
Under:
Ingredient based on toothpaste increases solvent, uniformly mixes, and the multi-purpose toothpaste cream of 10000~200000mPas of viscosity is made.
7. the multi-purpose toothpaste cream with microvesicle washing function washes the application in shield in oral cavity as described in claim 1.
8. the answering as detergent under microvesicle environment of the multi-purpose toothpaste cream with microvesicle washing function as described in claim 1
With.
9. application as claimed in claim 8, which is characterized in that specific step is as follows:
(1) multi-purpose toothpaste cream is added according to the every 1.5 kilograms usage amounts to 10~20g of washing articles, then according to every 1.5 kilograms
To 10~15 liters of water consumption of washing articles, 10~30min of washing is carried out under microvesicle environment；
(2) by the article after step (1) washing through rinsing.
10. application as claimed in claim 9, which is characterized in that be fabric to washing articles in the step (1)；Further
Preferably, the fabric is wool material；
Preferably, it in the step (2), rinses as twice, each water consumption is that per kilogram waits for washing articles 13L.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810876422.3A CN109157421A (en) | 2018-08-03 | 2018-08-03 | Green and healthy toothpaste cream of microvesicle washing function and the preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810876422.3A CN109157421A (en) | 2018-08-03 | 2018-08-03 | Green and healthy toothpaste cream of microvesicle washing function and the preparation method and application thereof |
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| Publication Number | Publication Date |
|---|---|
| CN109157421A true CN109157421A (en) | 2019-01-08 |
Family
ID=64898808
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810876422.3A Pending CN109157421A (en) | 2018-08-03 | 2018-08-03 | Green and healthy toothpaste cream of microvesicle washing function and the preparation method and application thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1747709A (en) * | 2003-02-05 | 2006-03-15 | Fmc有限公司 | Toothpaste compositions with reduced abrasivity |
| CN101564360A (en) * | 2008-04-23 | 2009-10-28 | 东和酵素株式会社 | Micro-bubble washing composition, micro-bubble washing method and micro-bubble washing equipment |
| CN103276561A (en) * | 2012-11-30 | 2013-09-04 | 李守林 | Water circulating device for low temperature fast dissolving of detergent and efficient washing of roller washing machine and working method thereof |
| CN105147583A (en) * | 2015-09-30 | 2015-12-16 | 福建春辉生物工程有限公司 | Special camellia-saponin-contained toothpaste for child and preparation method thereof |
| CN105792798A (en) * | 2013-12-11 | 2016-07-20 | 高露洁-棕榄公司 | High salt toothpaste with stable viscosity |
-
2018
- 2018-08-03 CN CN201810876422.3A patent/CN109157421A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1747709A (en) * | 2003-02-05 | 2006-03-15 | Fmc有限公司 | Toothpaste compositions with reduced abrasivity |
| CN101564360A (en) * | 2008-04-23 | 2009-10-28 | 东和酵素株式会社 | Micro-bubble washing composition, micro-bubble washing method and micro-bubble washing equipment |
| CN103276561A (en) * | 2012-11-30 | 2013-09-04 | 李守林 | Water circulating device for low temperature fast dissolving of detergent and efficient washing of roller washing machine and working method thereof |
| CN105792798A (en) * | 2013-12-11 | 2016-07-20 | 高露洁-棕榄公司 | High salt toothpaste with stable viscosity |
| CN105147583A (en) * | 2015-09-30 | 2015-12-16 | 福建春辉生物工程有限公司 | Special camellia-saponin-contained toothpaste for child and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 顾勇: "牙膏巧洗衣服", 《聪明过日子：幸福生活的5000个技巧》 * |
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Application publication date: 20190108 |