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CN109109411B - Double-sided sound-absorbing rubber plate and preparation method thereof - Google Patents

Double-sided sound-absorbing rubber plate and preparation method thereof Download PDF

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Publication number
CN109109411B
CN109109411B CN201810918151.3A CN201810918151A CN109109411B CN 109109411 B CN109109411 B CN 109109411B CN 201810918151 A CN201810918151 A CN 201810918151A CN 109109411 B CN109109411 B CN 109109411B
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layer
rubber
fabric layer
middle fabric
groove
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CN109109411A (en
Inventor
李俊
毛旺龙
张文强
李斌商
赵旭
袁良鹏
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Anhui Weiwei Environmental Science And Technology Co ltd
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Anhui Weiwei Environmental Science And Technology Co ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B25/00—Layered products comprising a layer of natural or synthetic rubber
    • B32B25/10—Layered products comprising a layer of natural or synthetic rubber next to a fibrous or filamentary layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B25/00—Layered products comprising a layer of natural or synthetic rubber
    • B32B25/16—Layered products comprising a layer of natural or synthetic rubber comprising polydienes homopolymers or poly-halodienes homopolymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B3/00—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form
    • B32B3/26—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer
    • B32B3/28—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer characterised by a layer comprising a deformed thin sheet, i.e. the layer having its entire thickness deformed out of the plane, e.g. corrugated, crumpled
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/06—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the heating method
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
    • B32B5/08—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer the fibres or filaments of a layer being of different substances, e.g. conjugate fibres, mixture of different fibres
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L9/00—Compositions of homopolymers or copolymers of conjugated diene hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/02—Synthetic macromolecular fibres
    • B32B2262/0253—Polyolefin fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/02—Synthetic macromolecular fibres
    • B32B2262/0261—Polyamide fibres
    • B32B2262/0269—Aromatic polyamide fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/10—Inorganic fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/10—Inorganic fibres
    • B32B2262/101—Glass fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/10—Inorganic fibres
    • B32B2262/106—Carbon fibres, e.g. graphite fibres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/14—Mixture of at least two fibres made of different materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure

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  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Laminated Bodies (AREA)
  • Soundproofing, Sound Blocking, And Sound Damping (AREA)

Abstract

The invention discloses a double-sided sound-absorbing rubber plate and a preparation method thereof, and belongs to the field of rubber materials. The fabric comprises a middle fabric layer, wherein a first groove and a second groove are formed in the upper end and the lower end of the middle fabric layer respectively, the first groove and the second groove are arc-shaped grooves, the first groove and the second groove are identical in size and shape, the second groove is formed between the two adjacent first grooves respectively, the upper end and the lower end of the middle fabric layer are provided with a rubber base layer respectively, the lower end of the rubber base layer on the upper end of the middle fabric layer is provided with a first lug matched with the first groove, the upper end of the rubber base layer on the lower end of the middle fabric layer is provided with a second lug matched with the second groove, and a fiber net. The double-sided sound-absorbing rubber plate disclosed by the invention has the advantages of excellent sound-absorbing performance, same sound-absorbing effect, good wear resistance, cold resistance and heat resistance.

Description

Double-sided sound-absorbing rubber plate and preparation method thereof
Technical Field
The invention belongs to the field of rubber materials, and particularly relates to a double-sided sound-absorbing rubber plate and a preparation method thereof.
Background
The rubber is a high-elasticity polymer material with reversible deformation, is rich in elasticity at room temperature, can generate large deformation under the action of small external force, and can recover the original shape after the external force is removed. The rubber belongs to a completely amorphous polymer, and has low glass transition temperature and large molecular weight which is more than hundreds of thousands. Early rubbers were latex from plants such as hevea brasiliensis, etc. processed to make elastic, insulative, impermeable to water and air. Is a high-elasticity polymer compound. The rubber is divided into natural rubber and synthetic rubber. The natural rubber is prepared by extracting colloid from plants such as rubber tree and rubber grass and processing; synthetic rubbers are obtained by polymerization of various monomers. Rubber products are widely used in industry or in various aspects of life. With the continuous development of economy, rubber is applied to various aspects such as automobile tires, sealing strips and the like. However, noise pollution is more and more serious in the society at present, sound-absorbing materials have a large development space, no sound-absorbing material of rubber products exists in the market, and if the rubber material with the sound-absorbing function is used, troubles caused by the noise pollution can be greatly reduced.
Disclosure of Invention
The invention aims to provide a double-sided sound-absorbing rubber plate and a preparation method thereof.
In order to achieve the purpose, the invention provides the following technical scheme:
the utility model provides a two-sided sound rubber slab of inhaling, includes middle fabric layer, middle fabric layer upper end and lower extreme are equipped with recess one and recess two respectively, recess one is the arc recess with recess two, recess one is the same with the big or small shape of recess two, recess two sets up respectively between two adjacent recess one, middle fabric layer upper end and lower extreme are equipped with rubber substrate respectively, middle fabric layer upper end rubber substrate's lower extreme is equipped with the lug one with a recess looks adaptation, middle fabric layer lower extreme rubber substrate's upper end is equipped with the lug two with recess two phase adaptation, evenly be equipped with the fibre web layer in the rubber substrate.
Preferably, the middle fabric layer comprises ultrahigh molecular weight polyethylene fibers and aramid fibers, and the mass ratio of the ultrahigh molecular weight polyethylene fibers to the aramid fibers is 1: 3.
Preferably, the rubber base layer is composed of the following raw materials in parts by weight: 100-120 parts of butadiene rubber, 80-95 parts of isoprene rubber, 20-25 parts of hollow glass beads, 12-17 parts of ceramic powder silicon carbide, 20-34 parts of vermiculite powder and 30-47 parts of carbon nano tubes.
Preferably, the fiber net layer comprises glass fibers and carbon fibers, and the mass ratio of the glass fibers to the carbon fibers is 1: 2.
Preferably, the thickness of the middle fabric layer is 0.2-0.5mm, the maximum thickness of the rubber base layer is 5-20mm, and the thickness of the fiber net layer is 0.10-0.2 mm.
Preferably, the distance between two adjacent fiber web layers in the rubber substrate is 0.5-1 mm.
Preferably, the preparation method of the double-sided sound absorption rubber plate comprises the following steps:
(1) preparing a middle fabric layer: uniformly mixing the raw materials of the middle fabric layer, sending the mixture into an opener for opening, sending the opened mixture into a carding device for carding, then making a criss-cross fiber web by a lapping machine, then carrying out stitch-bonding reinforcement by a stitch-bonding machine, and finally pressing and molding by a hot press to obtain the middle fabric layer, wherein the average pore diameter of the middle fabric layer is 5-35 mu m;
(2) preparing a fiber web layer: mixing, opening, carding and lapping the raw materials of the fiber net layer to form a fiber net;
(3) preparing a rubber base layer: sequentially adding raw materials of a rubber base layer into an open mill, mixing uniformly, performing heat treatment, after the heat treatment is finished, cooling to room temperature, placing a mixed product for 24 hours, compounding a fiber mesh layer on the mixed product, laminating the fiber mesh layer and the rubber base layer through a calender to obtain a substrate, vulcanizing a plurality of substrates through a flat vulcanizing machine after laminating to prepare rubber, and finally performing compression molding through a hot press to prepare the rubber base layer with the fiber mesh layer;
(4) hot-press molding: and respectively compounding rubber base layers with fiber net layers at the upper end and the lower end of the middle fabric layer, and performing hot-press forming to obtain the double-sided sound-absorbing rubber plate.
Compared with the prior art, the invention has the beneficial effects that:
1) the rubber base layer takes the butadiene rubber and the isoprene rubber as main materials, so that the wear resistance, the cold resistance and the heat resistance of a finished product are improved, the hollow glass beads, the carbon nano tubes and the vermiculite powder have excellent sound absorption effects, and the ceramic powder silicon carbide has high temperature resistance, high bending strength, excellent oxidation resistance, good corrosion resistance and high abrasion resistance.
2) The middle fabric layer has excellent sound absorption performance, and the sound absorption coefficient of a finished product can be improved by combining the special undulating structure with the rubber base layer.
3) And a plurality of fiber net layers are arranged in the rubber base layer, so that the sound absorption coefficient of a finished product is greatly improved.
4) The double sides of the rubber have excellent sound absorption effect, and the sound absorption effect of the double sides of the rubber is the same through the special structure of the middle fabric layer.
Drawings
FIG. 1 is a first schematic structural view of a double-sided sound-absorbing rubber sheet according to an embodiment of the present invention;
FIG. 2 is a second schematic structural view of a double-sided sound-absorbing rubber sheet according to an embodiment of the present invention;
in the figure, 1, a middle fabric layer, 2, first grooves, 3, second grooves, 4, a rubber base layer, 5, first bumps, 6, second bumps, 7 and a fiber net layer.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
As shown in fig. 1-2, the double-sided sound-absorbing rubber plate in this embodiment includes a middle fabric layer 1, the upper end and the lower end of the middle fabric layer 1 are respectively provided with a first groove 2 and a second groove 3, the first groove 2 and the second groove 3 are both arc-shaped grooves, the first groove 2 and the second groove 3 have the same size and shape, the second groove 3 is respectively disposed between two adjacent first grooves 2, the upper end and the lower end of the middle fabric layer 1 are respectively provided with a rubber base layer 4, the lower end of the rubber base layer 4 at the upper end of the middle fabric layer 4 is provided with a first projection 5 adapted to the first groove 2, the upper end of the rubber base layer 4 at the lower end of the middle fabric layer 1 is provided with a second projection 6 adapted to the second groove 3, and a fiber mesh layer 7 is uniformly disposed in.
The middle fabric layer comprises ultrahigh molecular weight polyethylene fibers and aramid fibers, and the mass ratio of the ultrahigh molecular weight polyethylene fibers to the aramid fibers is 1: 3; the rubber base layer is composed of the following raw materials in parts by weight: 100 parts of butadiene rubber, 80 parts of isoprene rubber, 20 parts of hollow glass beads, 12 parts of ceramic powder silicon carbide, 20 parts of vermiculite powder and 30 parts of carbon nano tubes; the fiber mesh layer comprises glass fibers and carbon fibers, and the mass ratio of the glass fibers to the carbon fibers is 1: 2; the thickness of the middle fabric layer is 0.2mm, the maximum thickness of the rubber base layer is 5mm, and the thickness of the fiber net layer is 0.10 mm; the distance between two adjacent fiber net layers in the rubber base layer is 0.5 mm.
A preparation method of a double-sided sound absorption rubber plate comprises the following steps:
(1) preparing a middle fabric layer: uniformly mixing the raw materials of the middle fabric layer, sending the mixture into an opener for opening, sending the opened mixture into a carding device for carding, then making a criss-cross fiber web by a lapping machine, then carrying out stitch-bonding reinforcement by a stitch-bonding machine, and finally pressing and molding by a hot press to obtain the middle fabric layer, wherein the average pore diameter of the middle fabric layer is 5 mu m;
(2) preparing a fiber web layer: mixing, opening, carding and lapping the raw materials of the fiber net layer to form a fiber net;
(3) preparing a rubber base layer: sequentially adding raw materials of a rubber base layer into an open mill, mixing uniformly, performing heat treatment, after the heat treatment is finished, cooling to room temperature, placing a mixed product for 24 hours, compounding a fiber mesh layer on the mixed product, laminating the fiber mesh layer and the rubber base layer through a calender to obtain a substrate, vulcanizing a plurality of substrates through a flat vulcanizing machine after laminating to prepare rubber, and finally performing compression molding through a hot press to prepare the rubber base layer with the fiber mesh layer;
(4) hot-press molding: and respectively compounding rubber base layers with fiber net layers at the upper end and the lower end of the middle fabric layer, and performing hot-press forming to obtain the double-sided sound-absorbing rubber plate.
Example 2
In this embodiment, a two-sided sound absorption rubber slab, including middle fabric layer, middle fabric layer upper end and lower extreme are equipped with recess one and recess two respectively, recess one and recess two are the arc recess, recess one is the same with the big or small shape of recess two, recess two sets up respectively between two adjacent recess one, middle fabric layer upper end and lower extreme are equipped with the rubber substrate respectively, the lower extreme of middle fabric layer upper end rubber substrate is equipped with the lug one with a recess looks adaptation, the upper end of middle fabric layer lower extreme rubber substrate is equipped with the lug two with recess looks adaptation, evenly be equipped with the fibre web layer in the rubber substrate.
The middle fabric layer comprises ultrahigh molecular weight polyethylene fibers and aramid fibers, and the mass ratio of the ultrahigh molecular weight polyethylene fibers to the aramid fibers is 1: 3; the rubber base layer is composed of the following raw materials in parts by weight: 110 parts of butadiene rubber, 87 parts of isoprene rubber, 23 parts of hollow glass beads, 14 parts of ceramic powder silicon carbide, 28 parts of vermiculite powder and 38 parts of carbon nano tubes; the fiber mesh layer comprises glass fibers and carbon fibers, and the mass ratio of the glass fibers to the carbon fibers is 1: 2; the thickness of the middle fabric layer is 0.35mm, the maximum thickness of the rubber base layer is 12mm, and the thickness of the fiber net layer is 0.15 mm; the distance between two adjacent fiber net layers in the rubber base layer is 0.7 mm.
A preparation method of a double-sided sound absorption rubber plate comprises the following steps:
(1) preparing a middle fabric layer: uniformly mixing the raw materials of the middle fabric layer, sending the mixture into an opener for opening, sending the opened mixture into a carding device for carding, then making a criss-cross fiber web by a lapping machine, then carrying out stitch-bonding reinforcement by a stitch-bonding machine, and finally pressing and molding by a hot press to obtain the middle fabric layer, wherein the average pore diameter of the middle fabric layer is 20 microns;
(2) preparing a fiber web layer: mixing, opening, carding and lapping the raw materials of the fiber net layer to form a fiber net;
(3) preparing a rubber base layer: sequentially adding raw materials of a rubber base layer into an open mill, mixing uniformly, performing heat treatment, after the heat treatment is finished, cooling to room temperature, placing a mixed product for 24 hours, compounding a fiber mesh layer on the mixed product, laminating the fiber mesh layer and the rubber base layer through a calender to obtain a substrate, vulcanizing a plurality of substrates through a flat vulcanizing machine after laminating to prepare rubber, and finally performing compression molding through a hot press to prepare the rubber base layer with the fiber mesh layer;
(4) hot-press molding: and respectively compounding rubber base layers with fiber net layers at the upper end and the lower end of the middle fabric layer, and performing hot-press forming to obtain the double-sided sound-absorbing rubber plate.
Example 3
In this embodiment, a two-sided sound absorption rubber slab, including middle fabric layer, middle fabric layer upper end and lower extreme are equipped with recess one and recess two respectively, recess one and recess two are the arc recess, recess one is the same with the big or small shape of recess two, recess two sets up respectively between two adjacent recess one, middle fabric layer upper end and lower extreme are equipped with the rubber substrate respectively, the lower extreme of middle fabric layer upper end rubber substrate is equipped with the lug one with a recess looks adaptation, the upper end of middle fabric layer lower extreme rubber substrate is equipped with the lug two with recess looks adaptation, evenly be equipped with the fibre web layer in the rubber substrate.
The middle fabric layer comprises ultrahigh molecular weight polyethylene fibers and aramid fibers, and the mass ratio of the ultrahigh molecular weight polyethylene fibers to the aramid fibers is 1: 3; the rubber base layer is composed of the following raw materials in parts by weight: 120 parts of butadiene rubber, 95 parts of isoprene rubber, 25 parts of hollow glass beads, 17 parts of ceramic powder silicon carbide, 34 parts of vermiculite powder and 47 parts of carbon nano tubes; the fiber mesh layer comprises glass fibers and carbon fibers, and the mass ratio of the glass fibers to the carbon fibers is 1: 2; the thickness of the middle fabric layer is 0.5mm, the maximum thickness of the rubber base layer is 20mm, and the thickness of the fiber net layer is 0.2 mm; the distance between two adjacent fiber net layers in the rubber base layer is 1 mm.
A preparation method of a double-sided sound absorption rubber plate comprises the following steps:
(1) preparing a middle fabric layer: uniformly mixing the raw materials of the middle fabric layer, sending the mixture into an opener for opening, sending the opened mixture into a carding device for carding, then making a criss-cross fiber web by a lapping machine, then carrying out stitch-bonding reinforcement by a stitch-bonding machine, and finally pressing and molding by a hot press to obtain the middle fabric layer, wherein the average pore diameter of the middle fabric layer is 35 mu m;
(2) preparing a fiber web layer: mixing, opening, carding and lapping the raw materials of the fiber net layer to form a fiber net;
(3) preparing a rubber base layer: sequentially adding raw materials of a rubber base layer into an open mill, mixing uniformly, performing heat treatment, after the heat treatment is finished, cooling to room temperature, placing a mixed product for 24 hours, compounding a fiber mesh layer on the mixed product, laminating the fiber mesh layer and the rubber base layer through a calender to obtain a substrate, vulcanizing a plurality of substrates through a flat vulcanizing machine after laminating to prepare rubber, and finally performing compression molding through a hot press to prepare the rubber base layer with the fiber mesh layer;
(4) hot-press molding: and respectively compounding rubber base layers with fiber net layers at the upper end and the lower end of the middle fabric layer, and performing hot-press forming to obtain the double-sided sound-absorbing rubber plate.
Comparative example 1
The double-sided sound-absorbing rubber plate in the embodiment comprises a middle fabric layer, wherein rubber base layers are respectively arranged at the upper end and the lower end of the middle fabric layer, and fiber mesh layers are uniformly arranged in the rubber base layers.
The comparative example is the same as the example 2 in the composition of each raw material component and the preparation method, and is different in the shape of the middle fabric layer and the rubber base layer, and the cross sections of the high-density fabric layer and the rubber base layer are planar in the example.
Comparative example 2
In this embodiment, the double-sided sound-absorbing rubber plate comprises a middle fabric layer, the upper end and the lower end of the middle fabric layer are respectively provided with a first groove and a second groove, the first groove and the second groove are square grooves, the first groove and the second groove are identical in size and shape, the second groove is respectively arranged between the first two adjacent grooves, the upper end and the lower end of the middle fabric layer are respectively provided with a rubber base layer, the lower end of the rubber base layer on the upper end of the middle fabric layer is provided with a first protruding block matched with the first groove, the upper end of the rubber base layer on the lower end of the middle fabric layer is provided with a second protruding block matched with the second groove, and a fiber.
The comparative example is the same as the raw material components and preparation method in example 2, except that the first groove and the second groove of the middle fabric layer in the example are both square grooves, and the first bump and the second bump of the rubber base layer are both square bumps.
Comparative example 3
In this embodiment the two-sided sound rubber slab of inhaling, including middle fabric layer, middle fabric layer upper end and lower extreme are equipped with recess one and recess two respectively, recess one is square groove with recess two, recess one is the same with the big or small shape of recess two, recess two sets up respectively between two adjacent recess one, middle fabric layer upper end and lower extreme are equipped with rubber substrate respectively, middle fabric layer upper end rubber substrate's lower extreme be equipped with the lug one of a recess looks adaptation, middle fabric layer lower extreme rubber substrate's upper end be equipped with the lug two of recess two phase adaptation.
This comparative example differs from example 2 in that: this embodiment lacks a fiber web layer.
Comparative example 4
This comparative example differs from example 2 in that: the rubber base layer in the embodiment comprises, by weight, 215 parts of butadiene rubber, 25 parts of hollow glass beads, 17 parts of ceramic powder silicon carbide, 34 parts of vermiculite powder and 47 parts of carbon nanotubes.
Comparative example 5
This comparative example differs from example 2 in that: the rubber base layer in the embodiment comprises, by weight, 215 parts of isoprene rubber, 25 parts of hollow glass beads, 17 parts of ceramic powder silicon carbide, 34 parts of vermiculite powder and 47 parts of carbon nanotubes.
In order to verify the sound absorption properties of the materials obtained in accordance with the present invention, sound absorption coefficient measurements were carried out on the materials obtained in examples 1 to 3 and comparative examples 1 to 5, and the following results were obtained:
TABLE 1 Sound absorption coefficient measurement results
Item 125Hz 250Hz 500Hz 1000Hz 2000Hz
Example 1 0.53 0.62 0.75 0.89 0.92
Example 2 0.67 0.75 0.86 0.93 0.97
Example 3 0.58 0.71 0.80 0.89 0.94
Comparative example 1 0.45 0.53 0.66 0.70 0.73
Comparative example 2 0.63 0.72 0.81 0.89 0.91
Comparative example 3 0.32 0.41 0.55 0.59 0.63
Comparative example 4 0.51 0.58 0.68 0.75 0.83
Comparative example 5 0.53 0.61 0.75 0.81 0.88
As can be seen from the results of table 1, the double-sided sound-absorbing rubber sheet prepared according to the present invention has excellent sound-absorbing effect.
The foregoing is illustrative and explanatory only and is intended to be exemplary of the invention, as various modifications, additions and substitutions for the specific embodiments described may be made by those skilled in the art without departing from the scope of the invention or exceeding the scope of the invention as defined in the claims.

Claims (4)

1. The utility model provides a two-sided sound absorption rubber slab which characterized in that: the fabric comprises a middle fabric layer, wherein a first groove and a second groove are respectively arranged at the upper end and the lower end of the middle fabric layer, the first groove and the second groove are arc-shaped grooves, the first groove and the second groove are same in size and shape, the second groove is respectively arranged between two adjacent first grooves, a rubber base layer is respectively arranged at the upper end and the lower end of the middle fabric layer, a first projection matched with the first groove is arranged at the lower end of the rubber base layer at the upper end of the middle fabric layer, a second projection matched with the second groove is arranged at the upper end of the rubber base layer at the lower end of the middle fabric layer, fiber mesh layers are uniformly arranged in the rubber base layers, the distance between two adjacent fiber mesh layers in the rubber base layers is 0.5-1mm, the middle fabric layer comprises ultrahigh molecular weight polyethylene fibers and aramid fibers, the mass ratio of the ultrahigh molecular weight, the rubber base layer comprises, by weight, 120 parts of polybutadiene rubber 100, 80-95 parts of isoprene rubber, 20-25 parts of hollow glass beads, 12-17 parts of ceramic powder silicon carbide, 20-34 parts of vermiculite powder and 30-47 parts of carbon nanotubes.
2. The double-sided sound-absorbing rubber sheet according to claim 1, wherein: the fiber net layer comprises glass fibers and carbon fibers, and the mass ratio of the glass fibers to the carbon fibers is 1: 2.
3. The double-sided sound-absorbing rubber sheet according to claim 1, wherein: the thickness of the middle fabric layer is 0.2-0.5mm, the maximum thickness of the rubber base layer is 5-20mm, and the thickness of the fiber net layer is 0.10-0.2 mm.
4. The method for preparing a double-sided sound-absorbing rubber sheet according to any one of claims 1 to 3, comprising the steps of:
(1) preparing a middle fabric layer: uniformly mixing the raw materials of the middle fabric layer, sending the mixture into an opener for opening, sending the opened mixture into a carding device for carding, then making a criss-cross fiber web by a lapping machine, then carrying out stitch-bonding reinforcement by a stitch-bonding machine, and finally pressing and molding by a hot press to obtain the middle fabric layer, wherein the average pore diameter of the middle fabric layer is 5-35 mu m;
(2) preparing a fiber web layer: mixing, opening, carding and lapping the raw materials of the fiber net layer to form a fiber net;
(3) preparing a rubber base layer: sequentially adding raw materials of a rubber base layer into an open mill, mixing uniformly, performing heat treatment, after the heat treatment is finished, cooling to room temperature, placing a mixed product for 24 hours, compounding a fiber mesh layer on the mixed product, laminating the fiber mesh layer and the rubber base layer through a calender to obtain a substrate, vulcanizing a plurality of substrates through a flat vulcanizing machine after laminating to prepare rubber, and finally performing compression molding through a hot press to prepare the rubber base layer with the fiber mesh layer;
(4) hot-press molding: and respectively compounding rubber base layers with fiber net layers at the upper end and the lower end of the middle fabric layer, and performing hot-press forming to obtain the double-sided sound-absorbing rubber plate.
CN201810918151.3A 2018-08-13 2018-08-13 Double-sided sound-absorbing rubber plate and preparation method thereof Active CN109109411B (en)

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