CN108975889A - It is a kind of to dissolve out the ceramic materials of minerals, ceramic component and preparation method thereof - Google Patents
It is a kind of to dissolve out the ceramic materials of minerals, ceramic component and preparation method thereof Download PDFInfo
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- CN108975889A CN108975889A CN201810890890.6A CN201810890890A CN108975889A CN 108975889 A CN108975889 A CN 108975889A CN 201810890890 A CN201810890890 A CN 201810890890A CN 108975889 A CN108975889 A CN 108975889A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
- C04B35/634—Polymers
- C04B35/63404—Polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B35/63424—Polyacrylates; Polymethacrylates
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
- C04B35/636—Polysaccharides or derivatives thereof
- C04B35/6365—Cellulose or derivatives thereof
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
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- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
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Abstract
The invention discloses a kind of ceramic materials for dissolving out minerals, ceramic component and preparation method thereof, the ceramic material of the dissolution minerals includes ceramic major ingredient and ceramic additive, it includes polymethyl methacrylate and sodium carboxymethylcellulose that the ceramics major ingredient, which includes 60~70wt% medical stone, 10~20wt%, six ring stone, 5~11wt% diatomite, 4~14wt% feldspar and 1~5wt% lepidolite, the ceramic additive,.Using ceramic component made of ceramic material of the invention can Fast Stripping several mineral materials, in terms of healthy drinking water with good application prospect.
Description
Technical field
The present invention relates to Material Fields, more particularly, to a kind of ceramic material, ceramic component and its system for dissolving out minerals
Preparation Method.
Background technique
With being constantly progressive for society, water pollution caused by industrial and agricultural development is got worse, for safe drinking water, water process
Field starts the improvement that water is carried out using RO (reverse osmosis) means, eliminate from biological (microorganism, virus etc.), physics (silt,
Iron rust etc.), the threat of chemical (organic matter, chlorine residue etc.) etc..Although RO technology can efficiently solve pollution problem, simultaneously
So that the mineral trace element loss in water is totally, long-term drinking can cause certain damage to human body, under health idea
People often have more demands to minerals, and the material dissolution rate for being furthermore capable of providing minerals in the prior art is low, lead to
Soaking time is often needed just to have result of extraction more than even higher for 24 hours, it is therefore desirable to which finding one kind being capable of a variety of mine of Fast Stripping
The material of substance meets the needs of people.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of ceramic material, ceramic component and its systems for dissolving out minerals
Preparation Method, the ceramic component prepared using the ceramic material can dissolve out several mineral materials within a short period of time.
The technical solution used in the present invention is:
The present invention provides a kind of ceramic material for dissolving out minerals, including ceramic major ingredient and ceramic additive, the ceramics
Major ingredient include 60~70wt% medical stone, 10~20wt%, six ring stone, 5~11wt% diatomite, 4~14wt% feldspar and 1~
5wt% lepidolite, the ceramic additive include polymethyl methacrylate (PMMA) and sodium carboxymethylcellulose (CMC).
Preferably, the additive amount of polymethyl methacrylate accounts for 0.3~1.5wt% of the ceramic major ingredient, carboxymethyl cellulose
Plain sodium accounts for 0.3~1.5wt% of the ceramic major ingredient.
Preferably, the additive amount of polymethyl methacrylate accounts for 0.3~0.9wt% of the ceramic major ingredient.
Preferably, partial size≤13 μm of the polymethyl methacrylate.
The present invention also provides a kind of ceramic components, are made by the ceramic material of above-mentioned dissolution minerals.
Preferably, the ceramic component includes at least one of tea set, drinking utensils, filter core.
The present invention also provides a kind of preparation methods of above-mentioned ceramic component, comprising the following steps: takes the dissolution mineral
The ceramic material of matter is formed and is sintered and is obtained.
Preferably, the temperature of sintering is 850~950 DEG C.
Preferably, the process of sintering uses gradient-heated.
Preferably, the process of sintering specifically: to 500~600 DEG C, heat preservation, then isothermal gradient add first isothermal gradient-heated
Heat is to 850~950 DEG C, heat preservation.
The beneficial effects of the present invention are:
The present invention provides a kind of ceramic material for dissolving out minerals, can dissolve out multiple types with its ceramic utensil prepared
Minerals such as calcium and magnesium potassium sodium silicon etc., meet demand of the people to mineral matter element, at the same dissolution rate it is fast, when very short
Interior that water can just be made to reach alkalescent, heavy metal and nuisance content are low, meet national standard.
Being capable of providing the materials of minerals in the prior art, often sintering temperature is higher during the preparation process, usually 1100
DEG C or more, it is unfavorable for environmental protection, sintering temperature can be greatly lowered using ceramic material of the invention, improves porosity, increases
The amount of dissolution, and improve dissolution rate.
Detailed description of the invention
Attached drawing 1 is the sintering process curve of Ceramic Balls in embodiment 1；
The SEM figure that attached drawing 2 is Ceramic Balls a-g in embodiment 1；
Attached drawing 3 is the bulk density of Ceramic Balls a-g and the relational graph of porosity and additive level in embodiment 1；
The TDS that attached drawing 4 is Ceramic Balls a-g in embodiment 1 is with the change curve of soaking time；
Attached drawing 5 is that Ceramic Balls a-g impregnates water sample pH versus time curve in embodiment 1.
Specific embodiment
It is clearly and completely described below with reference to technical effect of the embodiment to design and generation of the invention, with
It is completely understood by the purpose of the present invention, feature and effect.Obviously, described embodiment is that a part of the invention is implemented
Example, rather than whole embodiments, based on the embodiment of the present invention, those skilled in the art is not before making the creative labor
Other embodiments obtained are put, the scope of protection of the invention is belonged to.
Embodiment 1
Take the Maifanitums of 65 mass parts, six ring stones of 15 mass parts, the diatomite of 8 mass parts, 9 mass parts feldspar
It is mixed to get ceramic major ingredient with the lepidolite of 3 mass parts, is added in the ceramic major ingredient according to component shown in table 1 and additive amount
Ceramic additive is added to obtain ceramic material, wherein the content of ceramic additive is the percentage for accounting for the ceramic major ingredient weight, this
Partial size≤13 μm of polymethyl methacrylate in embodiment.
1 ceramic additive component of table and additive amount (additional wt%)
Ceramic material obtained above is taken, according to ceramic material: deionized water: ZrO2 mill ball quality ratio is 1:2:3 mixing,
The ball milling 18 hours on PMQ2L type omnidirectional planetary ball mill, is placed in DHG-9053A type drying box and dries, after pugging
Be made by handwork ball, is sintered to obtain Ceramic Balls by Fig. 1 sintering process curve using SXL-1400 type chamber type electric resistance furnace.
Ceramic Balls a-g made from above-mentioned sintering is taken, Nova Nano SEM450 type field emission scanning electron microscope is passed through
Microstructure analysis is carried out to sample, analysis result is as shown in Fig. 2, wherein a-g indicates that Ceramic Balls a-g is corresponding sweeps in figure
Electron microscope picture is retouched, it is as can be seen from the figure more simultaneously added with the Ceramic Balls stomata of PMMA and CMC, gas cell distribution is equal
It is even, be conducive to the dissolution of minerals, when the additive amount of PMMA is 0.9wt%, the aperture of Ceramic Balls and hole number reach maximum,
It is preferred that PMMA additive amount is 0.3~0.9wt%.The porosity of sample is measured to above-mentioned ceramics a-g with Archimedes method, it is real
Result is tested as shown in figure 3, wherein abscissa additive level refers to the weight of PMMA and CMC.It can be seen from the figure that comparing
In the Ceramic Balls for not adding PMMA and CMC simultaneously, the Ceramic Balls added with PMMA and CMC while of the invention have higher hole
Gap rate is conducive to the dissolution of minerals, wherein porosity is up to 93.17%, bulk density when the additive amount of PMMA is 0.9wt%
Reach 1.36g/cm3, the additive amount range of preferably PMMA is that (additive amount refers to accounting for ceramic major ingredient 0.3~0.9wt%
Weight percent).
The present embodiment is illustrated by taking Ceramic Balls as an example, can be prepared according to actual needs using ceramic material of the invention
A variety of ceramic components, such as tea set, drinking utensils, filter core ....
Embodiment 2
The Ceramic Balls a-g being prepared in Example 1, with Ceramic Balls: pure water=1:20 ratio is impregnated, and TDS- is utilized
3 TDS, types measure the salinity of sample, as a result as shown in figure 4, dissolution element number determine mineralized water TDS (dissolubility be total
Solid) height, wherein the effect of K+, Na+ are the most obvious, as can be seen from the figure utilize ceramic material formula system of the invention
The Ceramic Balls obtained can dissolve out rapidly minerals within a short period of time.
The mineralized water Element detection that above-mentioned Ceramic Balls a-g impregnates 5h, 30h is carried out respectively, as a result as shown in table 2-3, in table
This detection part mineral matter element is only listed, and measured heavy metal ion is far below national standard, wherein N.D. is indicated
Content is lower than detection limit.Ceramic Balls provided by the invention can dissolve out multi mineral prime element simultaneously as can be seen from the table, and
With the extension of soaking time, the amount of dissolution is also increased with it.
2 Ceramic Balls a-g of table impregnates 5h water sample Element detection (mg/L)
3 Ceramic Balls a-g of table impregnates 30h water sample Element detection (mg/L)
Above-mentioned Ceramic Balls a-g is taken, it is measured and impregnates water sample pH versus time curve as shown in figure 5, can be with from figure
Find out, with the extension of soaking time, pH is increased, and reaches highest in 5h, continues to extend soaking time, pH is in decline
Trend, and be allowed to maintain between 7 to 8, meet demand of the people to drinking water pH.Medical stone mine in ceramic material of the present invention
It is rich in alkali metal element and alkali earth metal between nitride layer, when acting on water, can make solution that higher pH be presented.And when pH is increased
When to a certain extent, the silicic acid that Maifanitum generates after acting on water will ionize in water, generate H+, to reduce mineralising
The pH of water.And chemically angle considers, amphoteric oxide Al contained in Maifanitum2O3In terms of the pH for adjusting water
It plays a crucial role, and the alkalescent that mineralized water can be made to reach healthy drinking water requires.
Claims (10)
1. a kind of ceramic material for dissolving out minerals, which is characterized in that including ceramic major ingredient and ceramic additive, the ceramics are main
Material include 60~70wt% medical stone, 10~20wt%, six ring stone, 5~11wt% diatomite, 4~14wt% feldspar and 1~
5wt% lepidolite, the ceramic additive include polymethyl methacrylate and sodium carboxymethylcellulose.
2. the ceramic material of dissolution minerals according to claim 1, which is characterized in that polymethyl methacrylate adds
Dosage accounts for 0.3~1.5wt% of the ceramic major ingredient, and sodium carboxymethylcellulose accounts for 0.3~1.5wt% of the ceramic major ingredient.
3. the ceramic material of dissolution minerals according to claim 2, which is characterized in that polymethyl methacrylate adds
Dosage accounts for 0.3~0.9wt% of the ceramic major ingredient.
4. the ceramic material of dissolution minerals according to claim 1-3, which is characterized in that the poly- methyl-prop
Partial size≤13 μm of e pioic acid methyl ester.
5. a kind of ceramic component, which is characterized in that by the ceramic material system of the described in any item dissolution minerals of claim 1-4
?.
6. ceramic component according to claim 5, which is characterized in that the ceramic component includes tea set, drinking utensils, in filter core
At least one.
7. the preparation method of ceramic component described in claim 5 or 6, which comprises the following steps: take the dissolution
The ceramic material of minerals is formed and is sintered and is obtained.
8. the preparation method of ceramic component according to claim 7, which is characterized in that the temperature of sintering is 850~950
℃。
9. the preparation method of ceramic component according to claim 7, which is characterized in that the process of sintering is added using gradient
Heat.
10. the preparation method of ceramic component according to claim 8 or claim 9, which is characterized in that the process of sintering specifically:
First isothermal gradient-heated is to 500~600 DEG C, heat preservation, then isothermal gradient-heated is kept the temperature to 850~950 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810890890.6A CN108975889A (en) | 2018-08-07 | 2018-08-07 | It is a kind of to dissolve out the ceramic materials of minerals, ceramic component and preparation method thereof |
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| CN201810890890.6A CN108975889A (en) | 2018-08-07 | 2018-08-07 | It is a kind of to dissolve out the ceramic materials of minerals, ceramic component and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109400136A (en) * | 2018-12-25 | 2019-03-01 | 佛山科学技术学院 | It is a kind of can Fast Stripping minerals ceramic component and preparation method thereof |
| CN112408963A (en) * | 2020-10-27 | 2021-02-26 | 深圳市华诚达精密工业有限公司 | Porous ceramic material with adsorption and ion elution functions and manufacturing method thereof |
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| JPH10182215A (en) * | 1996-12-25 | 1998-07-07 | J G I:Kk | Ceramic product containing medical mineral and its production |
| KR20050051803A (en) * | 2003-11-28 | 2005-06-02 | 주식회사 이엔이텍놀로지 | A process of ceramics having hollow structure |
| CN101503287A (en) * | 2009-03-04 | 2009-08-12 | 陆保华 | Medical stone sintering vessel and preparing process thereof |
| WO2010069097A1 (en) * | 2008-12-15 | 2010-06-24 | Fong King Leung | Ceramic material for purifying and activating water |
| CN104496420A (en) * | 2015-01-13 | 2015-04-08 | 唐山立雄峰汇材料科技有限公司 | Ceramic balls with drinking water purifying function |
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| JPH10182215A (en) * | 1996-12-25 | 1998-07-07 | J G I:Kk | Ceramic product containing medical mineral and its production |
| KR20050051803A (en) * | 2003-11-28 | 2005-06-02 | 주식회사 이엔이텍놀로지 | A process of ceramics having hollow structure |
| WO2010069097A1 (en) * | 2008-12-15 | 2010-06-24 | Fong King Leung | Ceramic material for purifying and activating water |
| CN101503287A (en) * | 2009-03-04 | 2009-08-12 | 陆保华 | Medical stone sintering vessel and preparing process thereof |
| CN104496420A (en) * | 2015-01-13 | 2015-04-08 | 唐山立雄峰汇材料科技有限公司 | Ceramic balls with drinking water purifying function |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109400136A (en) * | 2018-12-25 | 2019-03-01 | 佛山科学技术学院 | It is a kind of can Fast Stripping minerals ceramic component and preparation method thereof |
| CN112408963A (en) * | 2020-10-27 | 2021-02-26 | 深圳市华诚达精密工业有限公司 | Porous ceramic material with adsorption and ion elution functions and manufacturing method thereof |
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