CN108852959A - A kind of preparation method of natural multiple-effect lip film - Google Patents
A kind of preparation method of natural multiple-effect lip film Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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Abstract
The invention discloses a kind of preparation methods of natural multiple-effect lip film, including：(1) two kinds of olive oil, grape seed oil oily matters are mixed into oily phase, glycerol and water mixing is used as water phase, and pectin is heated to 70-80 DEG C as emulsifier, stirs evenly, then through high speed shear, the high-pressure homogeneous oil-in-water emulsion for obtaining stable homogeneous；(2) Vitamin E contained micro capsule is prepared by spray drying using chitosan, maltodextrin as wall material；(3) lotion obtained by step (1) is mixed with Vitamin E contained micro capsule, Glycolic acid, honey, chitosan, is stirred evenly；(4) frosting agent is prepared；(5) step (3) products therefrom is sufficiently mixed with frosting agent and is stirred evenly；(6) it sterilizes；(7) cooling packing obtains lip film product.Lip film produced by the present invention has good moisturizing, inoxidizability, antibiotic property and exfoliation.
Description
(1) technical field
The invention belongs to daily chemical products fields, and in particular to a kind of preparation method of natural multiple-effect lip film.
(2) technical background
Lip film is a kind of novel lip treatment products, and the purpose using lip film is to moisten softening, removal old useless cutin, light
Change lip pigementation, provides nutrition and brilliance for lips.Dead skin cutin is not removed, and nutrition cannot be absorbed, thus cannot
Nourish lip skin.And old useless cutin makes pachylosis, and unsmooth, the colour of skin is dim, influences beauty.General lip film does not add
Cutin-softening ingredient directly uses frosting agent to force removal aging cutin, and removal is not enough thoroughly and larger to Mucosa of lip damage, makes
Lip cannot be protected well.
The lip film of a maturation not only will maintain problem in view of lip, it is contemplated that scribble effect and safe and healthy asking
Topic.Traditional lip membrane process is simple, and raw material is ground into a powder and is mixed into paste with water by single effect, spreads on lip.Simple is ground into
Powder can prevent the effective component in raw material from being utilized well, and not salubrious comfortable enough, easily dry and cracked.Lip skin is tender
Fragility, vulnerable, pigment easily deposits, and traditional lip film does not consider pigment deposition problem, cannot fundamentally solve the problems, such as lip color,
Portioned product uses single antioxidant, cannot play good antioxidation, improves lip color and lip microgroove.In addition, very
More lip film products, using many chemical synthesis substances, can make skin of lip be stimulated to obtain effect needed for it, generate
Phenomena such as allergy.
Patent CN107569406A discloses a kind of lip film and preparation method thereof, its key points of the technical solution are that preparing a kind of lip
Film, including following components：Vaseline, beeswax, synthetic wax, polyisobutene, polyethylene, ethylhexyl palmitate, Phenoxyethanol, pyrrole sieve
Gram ketone ethanolamine salt.The patent has the function of moistening and removing aging cutin, but uses chemical component, can stimulate skin and produce
Raw certain harm.Patent CN106880575A discloses a kind of production method of frosted lip film, passes through the system of frosted particle
Make, the dissolution of functional component, mixing sterilizing, the cooling several steps of packing, a kind of frosted lip film is made.The patent passes through frosting agent
Physical action remove cutin, skin surface dead skin can only be removed, can not deeply clear up, and directly be easily caused using frosting agent
Skin of lip is impaired.
(3) summary of the invention
Technical problem to be solved by the invention is to provide a kind of preparation method of natural multiple-effect lip film, which has good
Good moisturizing, inoxidizability, antibiotic property and exfoliation.
In order to solve the above technical problems, the present invention adopts the following technical scheme that：
The present invention provides a kind of preparation methods of natural multiple-effect lip film, include the following steps：
(1) lotion is prepared：By olive oil, two kinds of oily matters of grape seed oil example 3-5 in mass ratio:1.5-2.5 mixing, adds
Heat arrives 80-90 DEG C, stirs evenly, for oily phase；Glycerol and water mixing is used as water phase, pectin as emulsifier, by oily phase, water phase and
Emulsifier mixing, is heated to 70-80 DEG C, stirs evenly, then through high speed shear, the high-pressure homogeneous oil-in-water for obtaining stable homogeneous
Lotion；Wherein, by the gross mass of feeding intake of each component be 100% in terms of, glycerol, water, emulsifier mass percent be respectively 15%-
25%, 30%-40%, 5%-10%, surplus are oily phase；
(2) Vitamin E contained micro capsule is prepared by spray drying using chitosan, maltodextrin as wall material：By vitamin E and cream
Agent mixing, wherein emulsifier is 4 using mass ratio:2 lecithin and gelatin, high shear agitation obtain core material solution, then
Chitosan solution is added in core material solution while stirring, adds maltodextrin solution, then through high speed shear, high-pressure homogeneous
Microcapsules emulsion is obtained, then spray-dried obtains Vitamin E contained micro capsule；With emulsifier, chitosan, maltodextrin and Wei Sheng
The gross mass of plain E is 100% meter, and mass percent shared by each component is as follows：Chitosan 3%-5%, maltodextrin 60%-
70%, vitamin e1 5%-20%, emulsifier 5%-15%；
(3) material mixes：Temperature is controlled at 55 DEG C -65 DEG C, by lotion obtained by step (1) and Vitamin E contained micro capsule, glycol
Acid, honey, chitosan mixing, wherein Vitamin E contained micro capsule, Glycolic acid, honey, chitosan mass ratio be 1-2:0.3-
0.6:2-3:3-4, lotion dosage account for the 80%-95% of material gross mass, stir evenly；
(4) frosting agent is prepared：Using natural frosted particle, the natural frosted particle uses walnut powder, oatmeal, olive
Core powder, the combination of one of almond powder, cherry stone powder or any several arbitrary proportions, using micron disintegrator by frosted particle
It is ground into 150-350 microns of uniform particle, obtains frosting agent；
(5) material mixes：Step (3) products therefrom and the frosting agent of step (4) are sufficiently mixed, frosted in mixture is made
The mass fraction of agent stirs evenly between 3%-5%；
(6) by the control temperature of mixture obtained by step (5) in 60 DEG C of -70 DEG C of sterilizings；
(7) by product cooling (being preferably cooled to 30 DEG C) packing after sterilizing, lip film product is obtained.
Further, in step (1), high speed shear condition is：2- is sheared using 26000rpm-30000rpm high-speed shearing machine
3min；High-pressure homogeneous condition is：Recycled under 70MPa-80MPa pressure using high pressure homogenizer can obtain for homogeneous 5-6 times it is uniform
Stable oil-in-water emulsion.
Further, in step (2), high speed shear condition is：13000r/min-15000r/min, 2-4min；It is high-pressure homogeneous
Condition is：40Mpa-60Mpa, 3-5 times；Spray drying condition is：Spray drying EAT is 170 DEG C -190 DEG C, out wind-warm syndrome
Degree is 80 DEG C -90 DEG C.
Further, in step (6), control temperature 60 DEG C -70 DEG C of holding 0.5-1 hours, largely micro- life can be killed
Object.
In the present invention, in order to obtain better lip film lip care effect, the usage amount for increasing lotion will increase its moisturizing
Property, the usage amount for increasing grape seed oil and vitamin E will increase its inoxidizability, and increasing the usage amount of chitosan, to will increase it anti-
Bacterium property.Therefore in step (1) of the present invention, the mutually preferred 30%-35% of oil, wherein olive oil is 3-4 with grape seed oil optimal proportion:
2-2.5.In step (3) of the present invention, Vitamin E contained micro capsule, Glycolic acid, honey, chitosan mixing mass ratio be preferably 1.5-
2:0.3-0.5:2.5-3:3.5-4, the preferred 90%-95% of lotion dosage.The beneficial effect of advantages of the present invention and generation：
(1) present invention adds a kind of oil-in-water emulsion, and Vitamin E contained micro capsule, honey, chitosan isoreactivity object is added
Matter generates preferably moist, moisturizing, anti-oxidant, fungistatic effect, lip is made to obtain extensive maintenance.
Specifically, common lip film single effect, lip cannot obtain maintenance in all directions.This programme is with olive oil, Portugal
Oil based on grape seed oil is prepared into oil-in-water lotion using naturally occurring emulsifying agent using the method for preparation lotion.In supplement water
While dividing, the absorption of liposoluble substance can be strengthened, skin of lip is made to obtain profound nourishing.Oil-in-water system makes the lip
After film is smeared, lip skin more water moistens gloss, non-greasy and is not easy dry and cracked.
Olive oil is rich in the squalene and essential fatty acid splendid with skin affinity, absorbs rapidly, and moistness is good,
It effectively keeps skin elasticity and moistens.Linolenic acid is fat that is needed by human and cannot synthesizing for human body in grape pip
Acid can resist free radical, anti-aging, prevention melanin deposition, help to absorb vitamin C and E.Vitamin E it is not soluble in water and
It is oxidizable, Vitamin E contained micro capsule is made using microcapsule embedded technology and adds, it can be made more stable in system, makes to tie up
The bioactivity utilization rate of raw element E significantly improves, and improves skin condition.The slow releasing function of microcapsules simultaneously, continues vitamin E
Act on skin of lip.Grape seed oil helps to absorb vitamin E, is able to extend and enhances oxidation resistant effect.Chitosan is by outer
Portion has an effect to somatic cells, and there are positively charged amino in molecular structure, it is easily mutually adsorbed in electronegative thallus,
It can enter inside thallus, by combining with such as protein of ingredient necessary to bacteria live etc., its metabolic balance be destroyed, to produce
Raw antibacterial effect.
(2) present invention uses frosting agent and tartaric acid collective effect, can not only deeply clear up skin, and more effectively removal is old
Change cutin, moreover it is possible to protect lips, keep skin of lip smooth, tender.
Specifically, frosting agent uses natural frosted particle, such as walnut powder, oatmeal, dento liva powder, almond powder, cherry
Frosted particle is ground into 150-350 microns of uniform particle using micron disintegrator by core powder etc., by being mechanically pulverized and airflow screen
Choosing is completed at the same time being crushed and classified for particle, ensure that the uniform particle diameter of frosted particle is suitable for, the excessive friction of particle can excessively produce
Very painful pain, the too small exfoliation of particle are not improved.Frosting agent is to remove cutin by physical action, acts on skin
Outermost layer, frosted particle constantly rub with lip, and the connection of skin and cuticula is stuck up in cutting, achieve the purpose that remove cutin.It is going
While except cutin, frosted particle is constantly slided in lip, is increased friction comfort, is promoted lip blood circulation, is conducive to new
Old metabolism.
The active skull cap components such as tartaric acid are added, tartaric acid is to remove cutin by chemical action, and tartaric acid can destroy cuticula
Intercellular connection interferes the binding force of cell surface to weaken the mutual adhesion of keratinocyte, epidermis angle by iron atom
Matter layer adhesive weakens, and the dead skin accumulated on the skin is made to be fallen off.The penetrating power of high concentration tartaric acid is quite strong, can incite somebody to action
Aging cutin once peels off, but skin of lip is more delicate, and high concentration tartaric acid can cause stronger irritation to skin, it is possible to right
Skin damages.To solve this problem, this programme is used using low concentration Glycolic acid cooperation frosting agent, will not be caused to skin
Any stimulation, Glycolic acid have the smallest chemical structure, only two carbon atoms in tartaric acid；The smallest molecular weight, only
76.05, therefore it is easiest to the surface layer of skin permeation, the effect of absorption is also most obvious, and the Glycolic acid of low concentration can reduce epidermis
Coagulability between horn cell, softening skin old useless cutin destroy the connection between corneocyte, generate caducous cutin
Bits, then the slight friction through frosting agent, can effectively remove lip cutin dead skin.Single frosting agent is also avoided to lip simultaneously
It is damaged caused by portion, protects lips, keep skin of lip smooth, tender.
(4) Detailed description of the invention
Fig. 1 is conventional lip film production process flow chart；
Fig. 2 is lip film production process flow chart of the present invention.
(5) specific implementation method
The present invention is described further combined with specific embodiments below, but protection scope of the present invention is not limited in
This：
Embodiment 1：
(1) lotion is prepared：Example 4 in mass ratio:2.5 mix two kinds of 18.5g olive oil, 11.5g grape seed oil oily matters
It closes, is heated to 85 DEG C, stirs evenly, for oily phase.Glycerol 25g, water 40g mixing are used as water phase, and pectin 5g, will be oily as emulsifier
Phase, water phase and emulsifier mixing, are heated to 80 DEG C, stir evenly, and shear 2min using 26000rpm high-speed shearing machine, use height
Pressure homogenizer recycles the homogeneous 5 times oil-in-water emulsions that can obtain stable homogeneous under 70MPa pressure；
(2) Vitamin E contained micro capsule is prepared：It is micro- that vitamin E is prepared by spray drying using chitosan, maltodextrin as wall material
Capsule, emulsifier are 4 using mass ratio:2 lecithin and gelatin, the quality that feeds intake compare chitosan：Maltodextrin：Vitamin E：Cream
Agent=3%：70%：15%：12%.Vitamin e1 .5g, lecithin 0.8g and gelatin 0.4g are mixed, high shear agitation
(13000r/min, 3min) obtains core material solution, then the chitosan solution 3g that mass concentration is 10% is added to core while stirring
In material solution, add mass concentration be 70% maltodextrin solution 10g, then high shear agitation (13000r/min,
3min), high-pressure homogeneous to obtain microcapsules emulsion (40Mpa, 3 times, 30min), it is finally spray-dried, spray drying EAT
It is 180 DEG C, leaving air temp is 80 DEG C, obtains Vitamin E contained micro capsule；
(3) material mixes：After being cooled to 55 DEG C, by lotion 90g obtained by step (1) and Vitamin E contained micro capsule 1.1g, glycol
Sour 0.4g, honey 2.2g, chitosan 3.3g mixing, Vitamin E contained micro capsule, Glycolic acid, honey, chitosan mixing mass ratio be
1:0.33:2:3, lotion dosage accounts for the 92.8% of material gross mass, stirs evenly；
(4) frosting agent is prepared：Using natural frosted particle, selected from walnut powder, oatmeal, any group of dento liva powder
It closes, frosted particle is ground into 200 microns of uniform particle using micron disintegrator；
(5) material mixes：Step (3) products therefrom 97g and the frosting agent 3g of step (4) are sufficiently mixed, stirred evenly；
(6) it sterilizes：Using low temperature sterilization, temperature control is kept for 1 hour at 60 DEG C, can kill most of microorganism；
(7) cooling packing：To be cooled to 30 DEG C, lip film product can be obtained in packing.
Embodiment 2：
(1) lotion is prepared：Example 3 in mass ratio:2 mix two kinds of 19.2g olive oil, 12.8g grape seed oil oily matters,
90 DEG C are heated to, is stirred evenly, for oily phase.Glycerol 25g, water 35g mixing are used as water phase, pectin 8g as emulsifier, by oily phase,
Water phase and emulsifier mixing, are heated to 80 DEG C, stir evenly, and shear 3min using 30000rpm high-speed shearing machine, use high pressure
Homogenizer recycles the homogeneous 5 times oil-in-water emulsions that can obtain stable homogeneous under 70MPa pressure；
(2) Vitamin E contained micro capsule is prepared：It is micro- that vitamin E is prepared by spray drying using chitosan, maltodextrin as wall material
Capsule, emulsifier are 4 using mass ratio:2 lecithin and gelatin, the quality that feeds intake compare chitosan：Maltodextrin：Vitamin E：Cream
Agent=4%：60%：20%：15%.Vitamin E2 g, lecithin 1g and gelatin 0.5g are mixed, high shear agitation
(14000r/min, 3min) obtains core material solution, then the chitosan solution 5g that mass concentration is 10% is added to core while stirring
In material solution, add mass concentration be 60% maltodextrin solution 10g, then high shear agitation (14000r/min,
3min), high-pressure homogeneous to obtain microcapsules emulsion (50Mpa, 4 times, 25min), it is finally spray-dried, spray drying EAT
It is 185 DEG C, leaving air temp is 85 DEG C, obtains Vitamin E contained micro capsule；
(3) after being cooled to 60 DEG C, by lotion 88g obtained by step (1) and Vitamin E contained micro capsule 1.5g, Glycolic acid 0.5g, bee
Sweet 2.5g, chitosan 3.5g mixing, Vitamin E contained micro capsule, Glycolic acid, honey, chitosan mixing mass ratio be 1.5:0.5:
2.5:3.5, lotion dosage accounts for the 91.7% of material gross mass, stirs evenly；
(4) frosting agent is prepared：Using natural frosted particle, selected from walnut powder, dento liva powder, any group of cherry stone powder
It closes, frosted particle is ground into 350 microns of uniform particle using micron disintegrator；
(5) material mixes：Step (3) products therefrom 96g and the frosting agent 4g of step (4) are sufficiently mixed, stirred evenly；
(6) it sterilizes：Using low temperature sterilization, temperature control is kept for 1 hour at 65 DEG C, can kill most of microorganism；
(7) cooling packing：To be cooled to 30 DEG C, lip film product can be obtained in packing.
Embodiment 3：
(1) lotion is prepared：Example 5 in mass ratio:1.5 mix two kinds of 26.9g olive oil, 8.1g grape seed oil oily matters
It closes, is heated to 75 DEG C, stirs evenly, for oily phase.Glycerol 15g, water 40g mixing are used as water phase, and pectin 10g, will as emulsifier
Oily phase, water phase and emulsifier mixing, are heated to 75 DEG C, stir evenly, and shear 2-3min using 28000rpm high-speed shearing machine, make
The homogeneous 5 times oil-in-water emulsions that can obtain stable homogeneous are recycled under 70MPa pressure with high pressure homogenizer；
(2) Vitamin E contained micro capsule is prepared：It is micro- that vitamin E is prepared by spray drying using chitosan, maltodextrin as wall material
Capsule, emulsifier are 4 using mass ratio:2 lecithin and gelatin, chitosan：Maltodextrin：Vitamin E：Emulsifier=4%：
65%：18%：13%.Vitamin e1 .8g, lecithin 0.9g and gelatin 0.4g are mixed, high shear agitation (15000r/
Min, 3min) core material solution is obtained, then the chitosan solution 4g that mass concentration is 10% is added in core material solution while stirring,
The maltodextrin solution 10g that mass concentration is 65% is added, then high shear agitation (15000r/min, 3min), high pressure
Homogeneous obtains microcapsules emulsion (60Mpa, 5 times, 20min), is finally spray-dried, and spray drying EAT is 180 DEG C, out
Air temperature is 80 DEG C, obtains Vitamin E contained micro capsule；
(3) after being cooled to 65 DEG C, by lotion 85g obtained by step (1) and Vitamin E contained micro capsule 2.1g, Glycolic acid 0.6g, bee
Sweet 3.1g, chitosan 4.2g mixing, Vitamin E contained micro capsule, Glycolic acid, honey, chitosan mixing mass ratio be 2:0.6:3:
4, lotion dosage accounts for the 89.5% of material gross mass, stirs evenly；
(4) frosting agent is prepared：Using natural frosted particle, it is selected from oatmeal, dento liva powder, almond powder, cherry stone powder
Any combination, frosted particle is ground into 150 microns of uniform particle using micron disintegrator；
(5) material mixes：Step (3) products therefrom 95g and the frosting agent 5g of step (4) are sufficiently mixed, stirred evenly；
(6) it sterilizes：Using low temperature sterilization, temperature control is kept for 0.5 hour at 70 DEG C, can kill most of micro- life
Object；
(7) cooling packing：To be cooled to 30 DEG C, lip film product can be obtained in packing.
Experiment effect：
The measurement of moisturizing rate：In order to control humidity, saturated acetic acid potassium is placed in drier, control humidity 60% or so,
For the actual conditions of better simulated skin, selects glass plate (50mm × 100mm) to stick 3M adhesive tape, take 200mg sample equal
Even is applied to tape surface, puts drier into and claims quality after a certain period of time, biodiversity m before placing1, biodiversity after placement
m2, moisturizing rate is calculated as follows：Rm=m2/m1× 100%
Free radical scavenging activity measurement：Using DPPH method, 4mlDPPH solution is sequentially added in 10ml colorimetric cylinder and lip film is dilute
Release liquid 2ml (1:50) dehydrated alcohol constant volume, is reentered, light absorption value is surveyed at 517nm, light absorption value remembers Ai, and 30min is kept in dark place and surveys and inhales
Light value Aj, check experiment only add the ethanol solution of DPPH, and clearance rate is calculated as follows in light absorption value Ac：K (%)=[1- (Ai-
Aj)/Ac] × 100%
Exfoliation measurement：The horn cell that the skin surface before and after the use of lip film is removed with special conducting resinl,
It scans, gets a distinct image in scanning electron microscope, compare horn cell quantity variation before and after the use of lip film.
Antibiotic rate measurement：2g lip film is weighed, it is outstanding to be separately added into 0.2ml Escherichia coli bacteria suspension, staphylococcus aureus bacterium
Liquid, and 17.8ml physiological saline is added in 50ml conical flask, it is fixed on oscillation shaking table, 2h is shaken with 200r/min.It will vibration
Swing front and back sample liquid dilution (1：10) it, is inoculated on culture dish respectively, carries out viable bacteria culture and count.Antibiotic rate is calculated as follows：Suppression
Average colony number before bacterium rate=(average colony number after average colony number-sample oscillation before sample oscillation)/sample oscillation ×
100%.
Lip film properties characterize data is as shown in the table：
Table 1
The experimental results showed that the lip film have good moisturizing, inoxidizability, antibiotic property and exfoliation compared with
It is good.
Claims (8)
1. a kind of preparation method of natural multiple-effect lip film, includes the following steps：
(1) lotion is prepared：By olive oil, two kinds of oily matters of grape seed oil example 3-5 in mass ratio:1.5-2.5 mixing, is heated to
It 80-90 DEG C, stirs evenly, for oily phase；Glycerol and water mixing is used as water phase, and pectin is as emulsifier, by oily phase, water phase and emulsification
Agent mixing, is heated to 70-80 DEG C, stirs evenly, then through high speed shear, the high-pressure homogeneous oil-in-water cream for obtaining stable homogeneous
Liquid；Wherein, by the gross mass of feeding intake of each component be 100% in terms of, glycerol, water, emulsifier mass percent be respectively 15%-
25%, 30%-40%, 5%-10%, surplus are oily phase；
(2) Vitamin E contained micro capsule is prepared by spray drying using chitosan, maltodextrin as wall material：By vitamin E and emulsifier
Mixing, wherein emulsifier is 4 using mass ratio:2 lecithin and gelatin, high shear agitation obtain core material solution, then by shell
Glycan solution is added in core material solution while stirring, adds maltodextrin solution, then through high speed shear, high-pressure homogeneous obtain
Microcapsules emulsion, then spray-dried obtain Vitamin E contained micro capsule；With emulsifier, chitosan, maltodextrin and vitamin E
Gross mass be 100% meter, mass percent shared by each component is as follows：Chitosan 3%-5%, maltodextrin 60%-70%,
Vitamin e1 5%-20%, emulsifier 5%-15%；
(3) material mixes：Temperature is controlled at 55 DEG C -65 DEG C, by lotion obtained by step (1) and Vitamin E contained micro capsule, Glycolic acid,
Honey, chitosan mixing, wherein Vitamin E contained micro capsule, Glycolic acid, honey, chitosan mass ratio be 1-2:0.3-0.6:
2-3:3-4, lotion dosage account for the 80%-95% of material gross mass, stir evenly；
(4) frosting agent is prepared：Using natural frosted particle, the natural frosted particle uses walnut powder, oatmeal, dento liva
Powder, the combination of one of almond powder, cherry stone powder or any several arbitrary proportions, using micron disintegrator by frosted granular powder
It is broken into 150-350 microns of uniform particle, obtains frosting agent；
(5) material mixes：Step (3) products therefrom and the frosting agent of step (4) are sufficiently mixed, frosting agent in mixture is made
Mass fraction stirs evenly between 3%-5%；
(6) by the control temperature of mixture obtained by step (5) in 60 DEG C of -70 DEG C of sterilizings；
(7) by the cooling packing of product after sterilizing, lip film product is obtained.
2. preparation method as described in claim 1, it is characterised in that：In step (1), high speed shear condition is：It uses
26000rpm-30000rpm high-speed shearing machine shears 2-3min；High-pressure homogeneous condition is：Using high pressure homogenizer in 70MPa-
The homogeneous 5-6 times oil-in-water emulsion up to stable homogeneous is recycled under 80MPa pressure.
3. preparation method as described in claim 1, it is characterised in that：In step (2), high speed shear condition is：13000r/
Min-15000r/min, 2-4min；High-pressure homogeneous condition is：40MPa-60MPa, 3-5 times；Spray drying condition is：It is spraying dry
Dry inlet air temperature is 170 DEG C -190 DEG C, and leaving air temp is 80 DEG C -90 DEG C.
4. preparation method as claimed in claim 2, it is characterised in that：In step (2), high speed shear condition is：13000r/
Min-15000r/min, 2-4min；High-pressure homogeneous condition is：40MPa-60MPa, 3-5 times；Spray drying condition is：It is spraying dry
Dry inlet air temperature is 170 DEG C -190 DEG C, and leaving air temp is 80 DEG C -90 DEG C.
5. the preparation method as described in one of Claims 1 to 4, it is characterised in that：In step (1), quality percentage shared by oily phase
Than for 30%-35%, wherein olive oil and the mass ratio of grape seed oil are 3-4:2-2.5.
6. the preparation method as described in one of Claims 1 to 4, it is characterised in that：It is Vitamin E contained micro capsule, sweet in step (3)
Alkyd, honey, chitosan mixing mass ratio be 1.5-2:0.3-0.5:2.5-3:3.5-4, lotion dosage account for material gross mass
90%-95%.
7. the preparation method as described in one of Claims 1 to 4, it is characterised in that：In step (1), quality percentage shared by oily phase
Than for 30%-35%, wherein olive oil and the mass ratio of grape seed oil are 3-4:2-2.5；In step (3), vitamin E is micro-
Capsule, Glycolic acid, honey, chitosan mixing mass ratio be 1.5-2:0.3-0.5:2.5-3:3.5-4, lotion dosage account for material
The 90%-95% of gross mass.
8. the preparation method as described in one of Claims 1 to 4, it is characterised in that：In step (6), temperature is controlled at 60 DEG C -70
DEG C keep 0.5-1 hours.
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| CN201810525588.0A CN108852959B (en) | 2018-05-28 | 2018-05-28 | Preparation method of natural multi-effect lip mask |
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| CN108852959B CN108852959B (en) | 2020-12-25 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111909507A (en) * | 2020-07-02 | 2020-11-10 | 青岛百草新材料股份有限公司 | Radix isatidis modified polyamide masterbatch for superfine fibers |
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| AU6781198A (en) * | 1997-05-09 | 1998-11-27 | Avon Products Inc. | Cosmetic sticks containing microcapsules |
| CN105943432A (en) * | 2016-05-10 | 2016-09-21 | 杭州西顿生物科技有限公司 | Peach gum moisturizing gel mask and preparation method thereof |
| CN107625690A (en) * | 2017-10-18 | 2018-01-26 | 湖南大三湘油茶生态产业有限公司 | Moisten moisturizing camellia oleifera fruit lip gloss and preparation method thereof |
| CN108158918A (en) * | 2018-01-12 | 2018-06-15 | 广州赛莱拉干细胞科技股份有限公司 | Wrap up microcapsules of natural extract and preparation method thereof and microcapsule-type lipstick |
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| WO1994006401A1 (en) * | 1992-09-21 | 1994-03-31 | The Procter & Gamble Company | Moisturizing lipstick compositions |
| AU6781198A (en) * | 1997-05-09 | 1998-11-27 | Avon Products Inc. | Cosmetic sticks containing microcapsules |
| CN105943432A (en) * | 2016-05-10 | 2016-09-21 | 杭州西顿生物科技有限公司 | Peach gum moisturizing gel mask and preparation method thereof |
| CN107625690A (en) * | 2017-10-18 | 2018-01-26 | 湖南大三湘油茶生态产业有限公司 | Moisten moisturizing camellia oleifera fruit lip gloss and preparation method thereof |
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| CN111909507A (en) * | 2020-07-02 | 2020-11-10 | 青岛百草新材料股份有限公司 | Radix isatidis modified polyamide masterbatch for superfine fibers |
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| CN108852959B (en) | 2020-12-25 |
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