CN108606297A - A kind of industrial production process of composite sweetener - Google Patents
A kind of industrial production process of composite sweetener Download PDFInfo
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- CN108606297A CN108606297A CN201810372509.7A CN201810372509A CN108606297A CN 108606297 A CN108606297 A CN 108606297A CN 201810372509 A CN201810372509 A CN 201810372509A CN 108606297 A CN108606297 A CN 108606297A
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- composite sweetener
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- 235000003599 food sweetener Nutrition 0.000 title claims abstract description 57
- 239000003765 sweetening agent Substances 0.000 title claims abstract description 57
- 239000002131 composite material Substances 0.000 title claims abstract description 47
- 238000009776 industrial production Methods 0.000 title claims abstract description 18
- 235000019202 steviosides Nutrition 0.000 claims abstract description 30
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 claims abstract description 27
- 241000544066 Stevia Species 0.000 claims abstract description 26
- 239000004383 Steviol glycoside Substances 0.000 claims abstract description 25
- 235000019411 steviol glycoside Nutrition 0.000 claims abstract description 25
- 229930182488 steviol glycoside Natural products 0.000 claims abstract description 25
- 150000008144 steviol glycosides Chemical class 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000000605 extraction Methods 0.000 claims abstract description 17
- 241001409321 Siraitia grosvenorii Species 0.000 claims abstract description 14
- 235000011171 Thladiantha grosvenorii Nutrition 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 14
- 230000002411 adverse Effects 0.000 claims abstract description 13
- 239000000284 extract Substances 0.000 claims abstract description 12
- 239000012530 fluid Substances 0.000 claims abstract description 12
- TWCMVXMQHSVIOJ-UHFFFAOYSA-N Aglycone of yadanzioside D Natural products COC(=O)C12OCC34C(CC5C(=CC(O)C(O)C5(C)C3C(O)C1O)C)OC(=O)C(OC(=O)C)C24 TWCMVXMQHSVIOJ-UHFFFAOYSA-N 0.000 claims abstract description 10
- PLMKQQMDOMTZGG-UHFFFAOYSA-N Astrantiagenin E-methylester Natural products CC12CCC(O)C(C)(CO)C1CCC1(C)C2CC=C2C3CC(C)(C)CCC3(C(=O)OC)CCC21C PLMKQQMDOMTZGG-UHFFFAOYSA-N 0.000 claims abstract description 10
- PFOARMALXZGCHY-UHFFFAOYSA-N homoegonol Natural products C1=C(OC)C(OC)=CC=C1C1=CC2=CC(CCCO)=CC(OC)=C2O1 PFOARMALXZGCHY-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000011347 resin Substances 0.000 claims abstract description 10
- 229920005989 resin Polymers 0.000 claims abstract description 10
- 238000010612 desalination reaction Methods 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 238000001694 spray drying Methods 0.000 claims abstract description 7
- 238000005189 flocculation Methods 0.000 claims abstract description 6
- 230000016615 flocculation Effects 0.000 claims abstract description 6
- 238000001179 sorption measurement Methods 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 34
- 239000007864 aqueous solution Substances 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 11
- 235000009508 confectionery Nutrition 0.000 claims description 9
- 244000269722 Thea sinensis Species 0.000 claims description 8
- 229930182470 glycoside Natural products 0.000 claims description 8
- 150000002338 glycosides Chemical class 0.000 claims description 8
- 230000002745 absorbent Effects 0.000 claims description 5
- 239000002250 absorbent Substances 0.000 claims description 5
- 229940037003 alum Drugs 0.000 claims description 5
- 229920006395 saturated elastomer Polymers 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 2
- 239000003957 anion exchange resin Substances 0.000 claims description 2
- 239000003729 cation exchange resin Substances 0.000 claims description 2
- 238000009991 scouring Methods 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 238000003809 water extraction Methods 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims 1
- 229930189775 mogroside Natural products 0.000 abstract description 17
- 239000002245 particle Substances 0.000 abstract description 6
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 abstract description 5
- 238000013329 compounding Methods 0.000 abstract description 5
- 229940013618 stevioside Drugs 0.000 abstract description 5
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 abstract description 5
- 238000011109 contamination Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 230000000813 microbial effect Effects 0.000 abstract description 3
- 239000000428 dust Substances 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 244000228451 Stevia rebaudiana Species 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 7
- 229930006000 Sucrose Natural products 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 238000002835 absorbance Methods 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 235000019441 ethanol Nutrition 0.000 description 4
- 239000005720 sucrose Substances 0.000 description 4
- 229930182478 glucoside Natural products 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- -1 Diterpenes glucosides Chemical class 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229930004069 diterpene Natural products 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/12—Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a kind of industrial production process of composite sweetener, the described method comprises the following steps：（1）Stevia rebaudian leaf crushes, and counter-flow water extracts to obtain extracting solution；（2）Fresh fructus momordicae is broken, uses step（1）The extracting solution adverse current extraction Siraitia grosvenorii of middle extraction stevia rebaudian leaf, obtains the extracting solution containing stevioside and mogroside；（3）By step（2）In extracting solution flocculation, filtering, obtain filtered fluid；（4）By step（3）Middle filtered fluid crosses macroporous resin adsorption, washes, parsing；（5）By step（4）Middle desorbed solution desalination, decoloration, concentration, spray drying obtain steviol glycoside and Momordia grosvenori aglycone composite sweetener.The method of the present invention directly can control product proportion by material rate, and the composite sweetener of preparation is more uniform, and mouthfeel is more preferable；Solve the problems, such as between single sweetener compounding there are density, color, particle size differences, product is uneven, compounding generates dust, increases microbial contamination risk.
Description
Technical field
The invention belongs to technical field of plant extraction, more particularly to a kind of industrial production process of composite sweetener.
Background technology
Steviol glycoside is a kind of sweetener extracted from stevia rebaudian leaf, and mogroside is the one kind extracted from Siraitia grosvenorii
Sweetener.Steviol glycoside is Diterpenes glucosides, and mogroside is triterpenes glucosides.Steviol glycoside and mogroside are all nothings
The food additives of heat, Momordia grosvenori aglycone and steviol glycoside collocation increase palatability using the rear bitter taste that can reduce steviol glycoside.
Two kinds of products of the Momordia grosvenori aglycone of report more than document and steviol glycoside carry out the side that compounding prepares composite sweetener at present
Method.There are density, color, particle size differences between single sweetener, and there are compound product problem of non-uniform, and compound generation powder
Dirt increases microbial contamination risk.And steviol glycoside is extracted with mogroside, purifying process is similar, the present invention will contain sweet tea
The extracting solution of synanthrin glycosides extracts Siraitia grosvenorii and can simultaneously be prepared containing there are two types of the extracting solutions of substance to purify together containing stevia rebaudianum again
Glucosides and mogroside composite sweetener.Through this technique prepare composite sweetener, can two kinds of products share it is a set of production set
Standby, production performance greatly improves；Energy consumption is low together for two kinds of products, can also solve the problems, such as that water consumption is big, alleviates at sewage
Reason.The product of the method production does not have to allotment, directly can control product proportion by material rate.The product solution of the method production
The existing density of two kinds of products compounding of having determined, color, granularity disunity problem, the composite sweetener that the method is directly prepared are more equal
One, mouthfeel is more preferable.
Invention content
The technical problem to be solved in the present invention is to provide a kind of industrial production process of composite sweetener.
In order to solve the above technical problems, the technical solution adopted by the present invention is：A kind of industrially prepared side of composite sweetener
Method the described method comprises the following steps：
（1）Stevia rebaudian leaf crushes, and counter-flow water extracts to obtain extracting solution；
（2）Fresh fructus momordicae is broken, uses step（1）Middle extracting solution adverse current extraction Siraitia grosvenorii, obtains containing steviol glycoside and sweet Momordica grosvenori
The extracting solution of glycosides；
（3）By step（2）In containing the extracting solution of stevioside and mogroside flocculate, filtering, obtain filtered fluid；
（4）By step（3）Middle filtered fluid crosses macroporous resin adsorption, washes, parsing；
（5）By step（4）Middle desorbed solution desalination, decoloration, concentration, spray drying obtain steviol glycoside and Momordia grosvenori aglycone composite sweetening
Agent.
Step of the present invention（1）It is pure water that middle stevia rebaudian leaf, which is crushed to 2-10 mesh, extraction with water,.
Step of the present invention（1）The temperature of middle counter-flow water extraction stevia rebaudian leaf is 40-70 DEG C.
Step of the present invention（1）Middle single-stage stevia rebaudian leaf and water quality ratio are 1:18-25, adverse current series are 4 grades, that is, are extracted
4 times.
Step of the present invention（2）Middle fresh fructus momordicae is broken to be referred to only by peel crushing.
Step of the present invention（2）The temperature of middle adverse current extraction Siraitia grosvenorii is 70-90 DEG C.
Step of the present invention（2）Middle fresh fructus momordicae and step（1）Middle stevia rebaudian leaf mass ratio is 1:1-20, adverse current extraction 4
Time, that is, it extracts 4 times.
Step of the present invention（3）Middle flocculant is alum saturated aqueous solution, and dosage is the 0.5- of extracting solution quality
1%；Flocculation temperature is 60-90 DEG C, flocculation time 30-60min；Filtering 300-500 keevil frames.
Step of the present invention（4）Middle macroreticular resin is any one in DA201, DM30, D941 or D860；The step
Suddenly（5）Middle desalination selects cation exchange resin 001*7, decoloration that anion exchange resin D151, destainer is selected to be concentrated into solid
Content 20-50%, spray drying obtain steviol glycoside and Momordia grosvenori aglycone composite sweetener.
Step of the present invention（4）Middle macroporous absorbent resin water scouring water is pure water, and dosage 0-3BV parses solvent
It is 60-80% ethanol solutions for 2-3BV mass fractions.
Composite sweetener product inspection method reference of the present invention：Steviol glycoside detection is with reference to GB 8270-2014《Food is pacified
National family's standard food additive steviol glycoside》, Momordia grosvenori aglycone detection method is with reference to GB188677-2016《Food security state
Family's standard mogroside》.
It is using advantageous effect caused by above-mentioned technical proposal：1, the present invention by the extracting solution containing steviol glycoside again
Extracting Siraitia grosvenorii can simultaneously prepare containing there are two types of the extracting solutions of substance to purify together containing steviol glycoside and mogroside
Composite sweetener.2, the method for the present invention prepares composite sweetener, can two kinds of products share a set of production equipment, total equipment investment
Few, production performance greatly improves；Energy consumption is low together for two kinds of products, can also solve the problems, such as that water consumption is big, alleviates at sewage
Reason.3, the product of the method for the present invention production does not have to allotment, directly can control product proportion, the compound sweet tea of preparation by material rate
Taste agent is more uniform, and mouthfeel is more preferable.4, the present invention compounds existing color, particle size differences between solving single sweetener, and product is not
Uniformly, the problem of compounding generation dust, increase microbial contamination risk.Product of the present invention, each measured value are detected with color difference meter
Unanimously, and two kinds of each measured values of commerieal sugar compound product have differences.5, the present invention meet in sweetener steviol glycoside and
Mogroside total content yield respectively reaches 98% and 97% or more.The composite sweetener includes stevioside sweet tea glycosides and Siraitia grosvenorii
Two kinds of sweeteners of sweet tea glycosides, composite sweetener sugariness are 200 times of sucrose or more, 0.1%（W/V）Aqueous solution is heated to 50 DEG C of energy
It is completely dissolved, insoluble matter presence, the composite sweetener 0.1% is there will not be after cooling（W/V）The absorbance of aqueous solution（460nm）
Less than 0.3.
Specific implementation mode
With reference to specific embodiment, the present invention will be further described in detail.
Embodiment 1
A kind of industrial production process of composite sweetener of the present embodiment, includes the following steps：
It is the stevia rebaudian leaf of 10 mesh to take 100kg grinding particle sizes, and 40 DEG C of Extracting temperature, single-stage stevia rebaudian leaf and water quality ratio are 1:18, it is inverse
4 grades of stream extraction, obtains stevia rebaudianum leaf extract；
The 100kg Siraitia grosvenoriis being crushed are extracted with stevia rebaudianum leaf extract, Extracting temperature is 70 DEG C, and adverse current extraction 4 times obtains
Compound extracted solution；
The alum saturated aqueous solution of extracting solution quality 0.5% is added into compound extracted solution, flocculate 30min under the conditions of 60 DEG C；
Filtered fluid is obtained with 500 mesh plate-frame filterings；
Filtered fluid crosses macroporous absorbent resin DA201, is washed with 3BV, the parsing of 60% ethyl alcohol of 3BV；Desorbed solution crosses desalination, decoloration, dense
It is reduced to solid content 50%, spray drying obtains steviol glycoside, mogroside composite sweetener.The composite sweetener includes stevia rebaudianum
Two kinds of sweeteners of sugared sweet tea glycosides 9.85kg and mogroside 0.52kg, steviol glycoside and mogroside total content yield are respectively
98.7% and 99.2%.The wherein described composite sweetener sugariness is 288 times of sucrose, 0.1%（W/V）Aqueous solution is heated to 50 DEG C
It can be completely dissolved, also exist without insoluble matter after cooling, the composite sweetener 0.1%（W/V）The absorbance of aqueous solution（460nm）
0.18。
Embodiment 2
A kind of industrial production process of composite sweetener of the present embodiment, includes the following steps：
It is the stevia rebaudian leaf of 2 mesh to take 100kg grinding particle sizes, and 70 DEG C of Extracting temperature, single-stage stevia rebaudian leaf and water quality ratio are 1:25, adverse current
4 grades of extraction, obtains stevia rebaudianum leaf extract；
The 300kg Siraitia grosvenoriis being crushed are extracted with stevia rebaudianum leaf extract, Extracting temperature is 90 DEG C, and adverse current extraction 4 times obtains
Compound extracted solution；
The alum saturated aqueous solution of extracting solution quality 0.8% is added into compound extracted solution, flocculate 30min under the conditions of 90 DEG C；
Filtered fluid is obtained with 300 mesh plate-frame filterings；
Filtered fluid crosses macroporous absorbent resin DM30, is washed with 3BV, the parsing of 80% ethyl alcohol of 2BV；Desorbed solution crosses desalination, decoloration, concentration
Steviol glycoside, Momordia grosvenori aglycone composite sweetener are obtained to solid content 20%, spray drying.
The composite sweetener includes stevioside two kinds of sweeteners of sweet tea glycosides 9.93kg and mogroside 1.48kg, steviol glycoside
It is respectively 99.7% and 98.9% with mogroside total content yield.Composite sweetener sugariness is 302 times of sucrose, 0.1%
（W/V）Aqueous solution, being heated to 50 DEG C can be completely dissolved, and also exist without insoluble matter after cooling, the composite sweetener 0.1%（W/V）Water
The absorbance of solution（460nm）0.21.
Embodiment 3
A kind of industrial production process of composite sweetener of the present embodiment, includes the following steps：
It is the stevia rebaudian leaf of 10 mesh to take 100kg grinding particle sizes, and 40 DEG C of Extracting temperature, single-stage stevia rebaudian leaf and water quality ratio are 1:25, it is inverse
4 grades of stream extraction, obtains stevia rebaudianum leaf extract；
2 tons of broken Siraitia grosvenoriis are extracted with stevia rebaudianum leaf extract, Extracting temperature is 70 DEG C, and adverse current extraction 4 times is answered
Close extracting solution；
The alum saturated aqueous solution of extracting solution quality 1.0% is added into compound extracted solution, flocculate 60min under the conditions of 60 DEG C；
Filtered fluid is obtained with 500 mesh plate-frame filterings；
Filtered fluid crosses macroporous absorbent resin D941, is washed with 0BV, the parsing of 60% ethyl alcohol of 2BV；Desorbed solution crosses desalination, decoloration, concentration
Steviol glycoside, Momordia grosvenori aglycone composite sweetener are obtained to solid content 40%, spray drying.
The composite sweetener includes stevioside two kinds of sweeteners of sweet tea glycosides 9.80kg and mogroside 9.53kg, steviol glycoside
It is respectively 99.6% and 97.5% with mogroside total content yield.The composite sweetener sugariness is 298 times of sucrose,
0.1%（W/V）Aqueous solution, being heated to 50 DEG C can be completely dissolved, and also exist without insoluble matter after cooling, the composite sweetener 0.1%（W/
V）The absorbance of aqueous solution（460nm）0.15.
Upper embodiment is only used to illustrate and not limit the technical solutions of the present invention, although in conjunction with above-described embodiment to the present invention
It is described in detail, it will be understood by those of ordinary skill in the art that：It can still modify to the present invention or equivalent
It replaces, without departing from the spirit or scope of the invention, or any substitutions, the right in the present invention should all be covered
In claimed range.
Claims (10)
1. a kind of industrial production process of composite sweetener, which is characterized in that the described method comprises the following steps：
（1）Stevia rebaudian leaf crushes, and counter-flow water extracts to obtain extracting solution；
（2）Fresh fructus momordicae is broken, uses step（1）In extracting solution adverse current extraction Siraitia grosvenorii, obtain contain steviol glycoside and Siraitia grosvenorii
The extracting solution of sweet tea glycosides；
（3）By step（2）In extracting solution flocculation, filtering, obtain filtered fluid；
（4）By step（3）Middle filtered fluid crosses macroporous resin adsorption, washes, parsing；
（5）By step（4）Middle desorbed solution desalination, decoloration, concentration, spray drying obtain steviol glycoside and Momordia grosvenori aglycone composite sweetening
Agent.
2. a kind of industrial production process of composite sweetener according to claim 1, which is characterized in that the step（1）
It is pure water that middle stevia rebaudian leaf, which is crushed to 2-10 mesh, extraction with water,.
3. a kind of industrial production process of composite sweetener according to claim 1, which is characterized in that the step（1）
The temperature of middle counter-flow water extraction stevia rebaudian leaf is 40-70 DEG C.
4. a kind of industrial production process of composite sweetener according to claim 1, which is characterized in that the step（1）
Middle single-stage stevia rebaudian leaf and water quality ratio are 1:18-25, adverse current series are 4 grades, that is, are extracted 4 times.
5. a kind of industrial production process of composite sweetener according to any one of claims 1-4, which is characterized in that institute
State step（2）Middle fresh fructus momordicae is broken to be referred to only by peel crushing.
6. a kind of industrial production process of composite sweetener according to any one of claims 1-4, which is characterized in that institute
State step（2）The temperature of middle adverse current extraction Siraitia grosvenorii is 70-90 DEG C.
7. a kind of industrial production process of composite sweetener according to any one of claims 1-4, which is characterized in that institute
State step（2）Middle fresh fructus momordicae and step（1）Middle stevia rebaudian leaf mass ratio is 1:1-20, adverse current extraction 4 times, that is, extract 4 times.
8. a kind of industrial production process of composite sweetener according to any one of claims 1-4, which is characterized in that institute
State step（3）Middle flocculant is alum saturated aqueous solution, and dosage is the 0.5-1% of extracting solution quality；Flocculation temperature is 60-
90 DEG C, flocculation time 30-60min；Filtering 300-500 keevil frames.
9. a kind of industrial production process of composite sweetener according to any one of claims 1-4, which is characterized in that institute
State step（4）Middle macroreticular resin is any one in DA201, DM30, D941 or D860；The step（5）Middle desalination is selected
Cation exchange resin 001*7, decoloration select anion exchange resin D151, destainer to be concentrated into solid content 20-50%, spraying
It is dried to obtain steviol glycoside and Momordia grosvenori aglycone composite sweetener.
10. a kind of industrial production process of composite sweetener according to any one of claims 1-4, which is characterized in that
The step（4）Middle macroporous absorbent resin water scouring water is pure water, and dosage 0-3BV, parsing solvent is 2-3BV mass fractions
For 60-80% ethanol solutions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810372509.7A CN108606297A (en) | 2018-04-24 | 2018-04-24 | A kind of industrial production process of composite sweetener |
Applications Claiming Priority (1)
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111938126A (en) * | 2019-05-17 | 2020-11-17 | 清馨(北京)科技有限公司 | Preparation method of compound sweetener |
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| CN106666634A (en) * | 2016-12-11 | 2017-05-17 | 周益铭 | Preparation method of natural compound sweetener |
| CN107156445A (en) * | 2017-05-17 | 2017-09-15 | 麦仑(漳州)生物科技有限公司 | A kind of preparation technology of feed sweetener |
| CN107722083A (en) * | 2017-11-29 | 2018-02-23 | 晨光生物科技集团股份有限公司 | A kind of high-efficient production technology of stevioside |
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| CN106432393A (en) * | 2016-09-23 | 2017-02-22 | 桂林电子科技大学 | Method of extracting and detecting mogrosides IV and V from momordica grosvenori of 55 days in fruiting age |
| CN106666634A (en) * | 2016-12-11 | 2017-05-17 | 周益铭 | Preparation method of natural compound sweetener |
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