CN108426530A - The device and measurement method that a kind of film thickness measures simultaneously with refractive index - Google Patents
The device and measurement method that a kind of film thickness measures simultaneously with refractive index Download PDFInfo
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Abstract
Description
技术领域technical field
本发明设计属于光学测量领域,具体涉及到了一种薄膜厚度与折射率同时测量的装置及测量方法。The design of the invention belongs to the field of optical measurement, and in particular relates to a device and a measurement method for simultaneously measuring film thickness and refractive index.
背景技术Background technique
随着材料科学与技术的蓬勃发展,为满足微电子、光电子、新能量等领域的迫切需求,薄膜在光学工程、机械工程、通讯工程、生物工程、航空航天工程、化学工程、医学工程等领域被广泛应用。薄膜的厚度不仅是薄膜生产中关键的决参数之一,更定着薄膜在力学、电磁、光电和光学等场景中的应用性能。对薄膜厚度的精确测量一直是薄膜生产以及应用中重要的环节之一。With the vigorous development of material science and technology, in order to meet the urgent needs of microelectronics, optoelectronics, new energy and other fields, thin films are widely used in optical engineering, mechanical engineering, communication engineering, biological engineering, aerospace engineering, chemical engineering, medical engineering and other fields. is widely used. The thickness of the film is not only one of the key parameters in film production, but also determines the application performance of the film in mechanical, electromagnetic, optoelectronic and optical scenarios. Accurate measurement of film thickness has always been one of the most important links in film production and application.
1941年,N.Schwartz等人提出了一种利用高精度机械触针在物体表面运动来感知表面轮廓的变化的接触探针法(N.Schwartz,R.Brown,“A Stylus Method for Evaluatingthe Thickness of Thin Films and Substrate Surface Roughness,”in Transactionsof the Eighth Vacuum Symposium and Second International Congress(Pergamon,NewYork,1941),pp.834–845.),该方法具有稳定性好,分辨力高,测量范围大等优点;但由于探针法中包含基于机械运动的探针,对薄膜测量时需要进行二次加工,此外探针在薄膜表面的移动,也会给薄膜造成一定的损害。因此非接触测量法便很快的取代了接触测量法对薄膜的厚度进行测量。In 1941, N. Schwartz and others proposed a contact probe method that uses high-precision mechanical stylus to move on the surface of an object to sense changes in surface contours (N. Schwartz, R. Brown, "A Stylus Method for Evaluating the Thickness of Thin Films and Substrate Surface Roughness,” in Transactions of the Eighth Vacuum Symposium and Second International Congress (Pergamon, New York, 1941), pp.834–845.), this method has the advantages of good stability, high resolution, and large measurement range ; However, since the probe method includes a probe based on mechanical motion, secondary processing is required when measuring the thin film. In addition, the movement of the probe on the surface of the thin film will also cause certain damage to the thin film. Therefore, the non-contact measurement method quickly replaced the contact measurement method to measure the thickness of the film.
2013年,南京航空航天大学的马希直等人公开了一种超声膜厚测量仪及其测量方法(中国专利申请号:201310198294.9),该方法发射超声脉冲入射到油膜的表面发生谐振,再通过测量反射脉冲的相关特性对油膜的厚度进行测量;但是该方法只适用于液态模的测量,且对于不同厚度范围的薄膜需建立不同的模型,解调难度较大。In 2013, Ma Xizhi and others from Nanjing University of Aeronautics and Astronautics disclosed an ultrasonic film thickness measuring instrument and its measurement method (Chinese patent application number: 201310198294.9). The thickness of the oil film is measured by measuring the correlation characteristics of the reflected pulse; however, this method is only suitable for the measurement of the liquid model, and different models need to be established for films with different thickness ranges, and the demodulation is difficult.
光学测量法具有着高精度的优势,在薄膜厚度测量方面开始逐渐广泛的应用起来。2012年,北京京东方光电科技有限公司的曲连杰等人公开了一种膜厚装置及方法(中国专利申请号:201210080754.2),该方法采用空间光路与光纤光路结合的方式,通过棱镜对彩色光源进行分光处理照射在薄膜的表面,通过测量不同反射光的特性对薄膜的厚度进行测量。该方法扩大了薄膜厚度测量的装置取样点的频谱范围,提高了分辨率。The optical measurement method has the advantage of high precision, and it has gradually been widely used in the measurement of film thickness. In 2012, Qu Lianjie and others from Beijing BOE Optoelectronics Technology Co., Ltd. disclosed a film thickness device and method (Chinese patent application number: 201210080754.2). Spectroscopic treatment is performed to irradiate the surface of the film, and the thickness of the film is measured by measuring the characteristics of different reflected light. The method expands the spectrum range of the sampling point of the device for measuring the film thickness and improves the resolution.
作为光学测量法的一部分,白光干涉法由于具有着绝对量的测量优势,在膜厚测量领域逐渐开始发展起来。白光干涉法的基本原理是:在白光干涉仪的一臂末端接上扫描镜作为传感臂,另一臂长度固定作为参考臂,通过移动扫描镜来改变传感臂长度,当传感臂中传输光的光程与参考臂中传输光的光程实现匹配时,出现的干涉峰值最大,通过识别峰值的位置实现相关参数的测量。2008年,美国Zygo公司的Peter J.de Groot等人公开了一种用于薄膜厚度和表面测量的扫描干涉法(Scanning interferometry for thin filmthickness and surface measurements,US Patent 7448799),该方法采用白光干涉原理的薄膜厚度测量方法,利用傅里叶变换方法从干涉光强图中提取两个峰值,该方法不受薄膜厚度的影响,既适用于测量厚度大于光源相干长度的薄膜,又适用于测量厚度小于光源相干长度的薄膜。2014年,山东大学的贾传武等人公开了一种宽谱光干涉法测量薄膜厚度的系统(中国专利申请号:201410290494.1),该系统在反射镜与准直镜之间形成的法布里波罗干涉仪,通过测量在反射镜下放置待测薄膜前后的法布里波罗腔长进行测量可得到待测薄膜的厚度,该方法结构简单,测量精度较高,但是由于需要将待测薄膜放置在反射镜的下方,容易对薄膜表面的形态产生破坏。As a part of the optical measurement method, white light interferometry has gradually begun to develop in the field of film thickness measurement due to its absolute measurement advantages. The basic principle of white light interferometry is: a scanning mirror is connected to the end of one arm of the white light interferometer as the sensing arm, the length of the other arm is fixed as the reference arm, and the length of the sensing arm is changed by moving the scanning mirror. When the optical path of the transmitted light matches the optical path of the transmitted light in the reference arm, the maximum interference peak appears, and the measurement of related parameters is realized by identifying the position of the peak. In 2008, Peter J.de Groot et al. of Zygo Company of the United States disclosed a scanning interferometry for thin film thickness and surface measurements (Scanning interferometry for thin film thickness and surface measurements, US Patent 7448799), which uses the principle of white light interference The film thickness measurement method uses the Fourier transform method to extract two peaks from the interference light intensity map. This method is not affected by the film thickness. The light source coherence length of the thin film. In 2014, Jia Chuanwu of Shandong University and others disclosed a system for measuring film thickness by wide-spectrum optical interferometry (Chinese patent application number: 201410290494.1). Interferometer, the thickness of the film to be tested can be obtained by measuring the length of the Fabry Perot cavity before and after placing the film to be tested under the mirror. This method has a simple structure and high measurement accuracy. Under the mirror, it is easy to damage the morphology of the film surface.
2017年,本发明申请人所在课题组提出一种共光路自校准薄膜厚度测量装置及测量方法(中国专利申请号CN201710277954.0),该方法利用共光路的宽谱光干涉仪与激光干涉仪实现薄膜厚度的测量,具有共光路,不需要标定器件等优点,但是该方法无法消除激光透射光的影响,造成激光干涉信号的裂化,影响厚度测量精度;同年,本发明申请人所在课题组提出了偏振复用的共光路自校准薄膜厚度测量装装置及测量方法(中国专利申请号CN201710277939.6),该方法在原有优势的基础上可进一步消除透射光对测量结果的影响,但是装置搭建较为复杂。In 2017, the research group of the applicant of the present invention proposed a common optical path self-calibration film thickness measurement device and measurement method (Chinese patent application number CN201710277954.0), which is realized by using a common optical path wide-spectrum optical interferometer and laser interferometer The measurement of film thickness has the advantages of common optical path and no need to calibrate the device, but this method cannot eliminate the influence of laser transmitted light, resulting in cracking of laser interference signals and affecting the accuracy of thickness measurement; in the same year, the research group of the applicant of the present invention proposed Polarization multiplexing common optical path self-calibration film thickness measurement device and measurement method (Chinese patent application number CN201710277939.6), this method can further eliminate the influence of transmitted light on the measurement results on the basis of the original advantages, but the device construction is relatively complicated .
本发明提供了一种薄膜厚度与折射率同时测量的装置及测量方法,能够同时实现薄膜厚度及折射率的非接触测量。膜厚测量探头模块中差分结构的设计减小了膜厚测量探头受外界环境的影响,本发明将窄线宽激光输出模块的输出信号直接输入到解调干涉仪模块中,满足干涉信号共光路的同时避免了膜厚测量探头模块中激光透射光以及激光多次反射光对干涉信号质量的影响,提高了薄膜厚度溯源的精度;通过控制膜厚测量探头尾纤的长度避免了膜厚测量探头模块中宽谱光透射光对特征信号峰的干扰,提高了特征信号识别的准确性。本发明可广泛用于薄膜生产以及其他需对薄膜的厚度进行高精度测量的领域。The invention provides a device and a measuring method for simultaneously measuring film thickness and refractive index, which can simultaneously realize non-contact measurement of film thickness and refractive index. The design of the differential structure in the film thickness measurement probe module reduces the influence of the external environment on the film thickness measurement probe. The present invention directly inputs the output signal of the narrow linewidth laser output module into the demodulation interferometer module to meet the common optical path of the interference signal. At the same time, it avoids the influence of laser transmitted light and laser multiple reflection light in the film thickness measurement probe module on the quality of the interference signal, and improves the accuracy of film thickness traceability; by controlling the length of the film thickness measurement probe pigtail, the film thickness measurement probe is avoided. The interference of the wide-spectrum light transmitted light in the module on the characteristic signal peak improves the accuracy of characteristic signal identification. The invention can be widely used in thin film production and other fields where the thickness of the thin film needs to be measured with high precision.
发明内容Contents of the invention
本发明目的在于提供不需标定样品标定即可对薄膜的厚度以及折射率进行测量,具有自校准、测量结果可溯源、稳定性高、抗干扰能力强、特征信号识别简单的一种薄膜厚度与折射率同时测量的装置及测量方法。The purpose of the present invention is to provide a film thickness and refractive index that can be measured without calibration of samples, and has self-calibration, traceable measurement results, high stability, strong anti-interference ability, and simple identification of characteristic signals. Device and method for simultaneous measurement of refractive index.
本发明的目的通过如下技术方案来实现:The purpose of the present invention is achieved through the following technical solutions:
一种薄膜厚度与折射率同时测量的装置,由宽谱光输出模块1、窄线宽激光输出模块2、膜厚测量探头模块3、解调干涉仪模块4以及采集与控制模块5五部分组成;各模块的组成分别是:A device for simultaneous measurement of film thickness and refractive index, consisting of five parts: a wide-spectrum light output module 1, a narrow linewidth laser output module 2, a film thickness measurement probe module 3, a demodulation interferometer module 4, and an acquisition and control module 5 ; The components of each module are:
宽谱光输出模块1由宽谱光源101、第1隔离器102所组成。The broadband light output module 1 is composed of a broadband light source 101 and a first isolator 102 .
窄线宽激光输出模块2由窄线宽激光光源201、第2隔离器202所组成。The narrow linewidth laser output module 2 is composed of a narrow linewidth laser light source 201 and a second isolator 202 .
膜厚测量探头模块3第1测量探头301以及第2测量探头302所组成。The film thickness measuring probe module 3 is composed of a first measuring probe 301 and a second measuring probe 302 .
解调干涉仪模块4由解调干涉仪模块4由第1法拉第反射镜401,第2法拉第反射镜402,第1准直镜403,第2准直镜404,第3准直镜405,第4准直镜406,第1解调干涉仪耦合器407,光程扫描装置408,第2解调干涉仪耦合器409,第5准直镜410,第6准直镜411,第7准直镜412,第8准直镜413,第3法拉第反射镜414以及第4法拉第反射镜415所组成。The demodulation interferometer module 4 is composed of the first Faraday reflector 401, the second Faraday reflector 402, the first collimator 403, the second collimator 404, the 3rd collimator 405, and the 3rd collimator 404. 4 collimator mirror 406, the first demodulation interferometer coupler 407, the optical path scanning device 408, the second demodulation interferometer coupler 409, the fifth collimator mirror 410, the sixth collimator mirror 411, the seventh collimator mirror 412, the eighth collimating mirror 413, the third Faraday mirror 414 and the fourth Faraday mirror 415.
采集与控制模块5由计算机501,数据采集卡502,第1光电探测器503,第2光电探测器504,第3光电探测器505以及第4光电探测器506所组成。The acquisition and control module 5 is composed of a computer 501 , a data acquisition card 502 , a first photodetector 503 , a second photodetector 504 , a third photodetector 505 and a fourth photodetector 506 .
宽谱光输出模块1输出光通过第1分束耦合器6被分为两路分别通过第1环形器10、第2环形器13进入膜厚测量探头模块3的第1测量探头301和第2测量探头302中进行相关参数的测量;经由第1测量探头301和第2测量探头302的返回光通过第1环形器10、第2环形器13进入第1波分复用器8和第2波分复用器9的相关波长输入端;窄线宽激光输出模块2的输出光通过第2分束耦合器7被分为两路分别进入第1波分复用器8和第2波分复用器9的相关波长输入端;经过第1波分复用器8和第2波分复用器9分别合束后的两束光输入到解调干涉仪模块4中,通过解调干涉仪模块4中的第1解调干涉仪4A与第2解调干涉仪4B的扫描分别实现光程匹配;通过第3波分复用器11和第4波分复用器12将不同波长的干涉信号分离后输入到采集与控制模块5中。The output light of the wide-spectrum light output module 1 is divided into two paths through the first beam splitter coupler 6 and enters the first measuring probe 301 and the second measuring probe 301 of the film thickness measuring probe module 3 through the first circulator 10 and the second circulator 13 respectively. Carry out the measurement of relevant parameter in the measurement probe 302; The return light of the 1st measurement probe 301 and the 2nd measurement probe 302 enters the 1st wavelength division multiplexer 8 and the 2nd wavelength through the 1st circulator 10, the 2nd circulator 13 The relevant wavelength input end of the division multiplexer 9; the output light of the narrow linewidth laser output module 2 is divided into two paths through the second beam splitter coupler 7 and enters the first wavelength division multiplexer 8 and the second wavelength division multiplexer respectively. The relevant wavelength input end of the multiplier 9; the two beams of light combined by the first wavelength division multiplexer 8 and the second wavelength division multiplexer 9 are respectively input into the demodulation interferometer module 4, and passed through the demodulation interferometer The scanning of the first demodulation interferometer 4A and the second demodulation interferometer 4B in the module 4 realizes optical path matching respectively; After the signal is separated, it is input into the acquisition and control module 5 .
宽谱光输出模块1中的宽谱光源101的半谱宽度大于45nm,出纤功率大于2mW;窄线宽激光输出模块2中的窄线宽激光光源201的半谱宽度小于1pm,出纤功率大于2mW;宽谱光源101与窄线宽激光光源201具有不同的中心波长,且二者的频谱在半谱宽度内没有重叠的部分;The half-spectrum width of the wide-spectrum light source 101 in the wide-spectrum light output module 1 is greater than 45nm, and the output power is greater than 2mW; the half-spectrum width of the narrow-linewidth laser source 201 in the narrow-linewidth laser output module 2 is less than 1pm, and the output power is Greater than 2mW; the wide-spectrum light source 101 and the narrow-linewidth laser light source 201 have different central wavelengths, and the spectra of the two do not overlap within the half-spectrum width;
膜厚测量探头模块3中的第1测量探头301与第2测量探头302能够同时实现对传输光线的透射和反射,传输光线的反射率在20%~80%之间;第1测量探头301与第2测量探头302的出射光线互相重合;待测器件放置测量时,分别与第1测量探头301和第2测量探头302的出射光线垂直;第1测量探头301第1环形器10的输出端10c相连接,第2测量探头302与第2环形器13输出端13c相连接;The first measuring probe 301 and the second measuring probe 302 in the film thickness measuring probe module 3 can realize the transmission and reflection of the transmitted light at the same time, and the reflectivity of the transmitted light is between 20% and 80%; the first measuring probe 301 and the The outgoing rays of the second measuring probe 302 coincide with each other; when the device under test is placed for measurement, they are perpendicular to the outgoing rays of the first measuring probe 301 and the second measuring probe 302 respectively; the output end 10c of the first measuring probe 301 and the first circulator 10 connected, the second measuring probe 302 is connected to the output end 13c of the second circulator 13;
膜厚测量探头模块3中的第1测量探头301和第2测量探头302尾纤的长度差值大于解调干涉仪模块4中光程扫描装置408的光程扫描范围;The length difference between the first measuring probe 301 and the second measuring probe 302 in the film thickness measuring probe module 3 is greater than the optical path scanning range of the optical path scanning device 408 in the demodulation interferometer module 4;
解调干涉仪模块4中的第1波分复用器5的输出端5c与第1解调干涉仪耦合器407的4a输入端相连接,第1解调干涉仪耦合器407的4c输出端与第1准直镜403相连接,第2准直镜404与第1法拉第反射镜401相连接,第1解调干涉仪耦合器407的4d输出端与第5准直镜410相连接,第6准直镜411与第3法拉第反射镜414相连接;第2波分复用器9的9c输出端与第2解调干涉仪耦合器409的4g输入端相连接,第2解调干涉仪耦合器409的4e输出端与第4准直镜406相连接,第3准直镜405与第2法拉第反射镜402相连接,第2解调干涉仪耦合器409的4f输出端第8准直镜413相连接,第7准直镜412与第4法拉第反射镜415相连接;第1解调干涉仪耦合器407、第1准直镜403、第2准直镜404、第1法拉第反射镜401、第1正向可移动光学反射镜408a、第1反向可移动光学反射镜408b、第5准直镜410、第6准直镜411、第3法拉第反射镜414构成第1解调干涉仪4A;第2解调干涉仪耦合器409、第3准直镜405、第4准直镜406、第2法拉第反射镜402、第2正向可移动光学反射镜408c、第2反向可移动光学反射镜408d、第7准直镜412、第8准直镜413、第4法拉第反射镜415构成第2解调干涉仪4B;第1准直镜403、第2准直镜404、第3准直镜405、第4准直镜406、第5准直镜410、第6准直镜411、第7准直镜412、第8准直镜413的光学参数相一致;第1法拉第反射镜401、第2法拉第反射镜402、第3法拉第反射镜414、第4法拉第反射镜415的光学参数相一致;The output end 5c of the first wavelength division multiplexer 5 in the demodulation interferometer module 4 is connected with the 4a input end of the first demodulation interferometer coupler 407, and the 4c output end of the first demodulation interferometer coupler 407 Connect with the first collimator mirror 403, the second collimator mirror 404 is connected with the first Faraday reflector 401, the 4d output end of the first demodulation interferometer coupler 407 is connected with the 5th collimator mirror 410, the first 6. The collimating mirror 411 is connected with the 3rd Faraday reflector 414; the 9c output terminal of the 2nd wavelength division multiplexer 9 is connected with the 4g input terminal of the 2nd demodulation interferometer coupler 409, and the 2nd demodulation interferometer The 4e output end of the coupler 409 is connected with the 4th collimator mirror 406, the 3rd collimator mirror 405 is connected with the 2nd Faraday reflector 402, the 4f output end of the 2nd demodulation interferometer coupler 409 collimates the 8th Mirror 413 is connected, and the 7th collimating mirror 412 is connected with the 4th Faraday reflector 415; The first demodulation interferometer coupler 407, the first collimating mirror 403, the second collimating mirror 404, the first Faraday reflector 401, the first forward movable optical mirror 408a, the first reverse movable optical mirror 408b, the fifth collimator mirror 410, the sixth collimator mirror 411, and the third Faraday mirror 414 constitute the first demodulation interference Instrument 4A; the second demodulation interferometer coupler 409, the third collimating mirror 405, the fourth collimating mirror 406, the second Faraday mirror 402, the second forward movable optical mirror 408c, the second reverse movable The moving optical mirror 408d, the 7th collimating mirror 412, the 8th collimating mirror 413, and the 4th Faraday mirror 415 constitute the second demodulation interferometer 4B; the 1st collimating mirror 403, the 2nd collimating mirror 404, the The optical parameters of the 3 collimating mirror 405, the 4th collimating mirror 406, the 5th collimating mirror 410, the 6th collimating mirror 411, the 7th collimating mirror 412, and the 8th collimating mirror 413 are consistent; the first Faraday reflection The optical parameters of mirror 401, the 2nd Faraday reflector 402, the 3rd Faraday reflector 414, and the 4th Faraday reflector 415 are consistent;
解调干涉仪模块4中的光程扫描装置中408的第1正向可移动光学反射镜408a、第2正向可移动光学反射镜408b、第1反向可移动光学反射镜408c、第2反向可移动光学反射镜408d的光学参数相一致;位置扫描装置408台面的扫描范围L能够满足膜厚测量探头模块不插入待测薄膜时,第1解调干涉仪4A与第2解调干涉仪4B均能实现由不同探头透镜表面反射光的光程匹配;第1解调干涉仪4A与第2解调干涉仪4B共用同一位置扫描装置408;当第1正向可移动光学反射镜408a与第2正向可移动光学反射镜408c位于零点位置时,第1反向可移动光学反射镜408b与第2反向可移动光学反射镜408d具有最大位移L,第1反向可移动光学反射镜408b与第2反向可移动光学反射镜408d位于零点位置时,第1正向可移动光学反射镜408a与第2正向可移动光学反射镜408c具有最大位移L;扫描过程中,第1正向可移动光学反射镜408a、第2正向可移动光学反射镜408b、第1反向可移动光学反射镜408c、第2反向光学反射镜408d具有相同的位移;The first forward movable optical reflector 408a, the second forward movable optical reflector 408b, the first reverse movable optical reflector 408c, the second The optical parameters of the reverse movable optical mirror 408d are consistent; the scanning range L of the table top of the position scanning device 408 can meet the requirements of the first demodulation interferometer 4A and the second demodulation interferometer when the film thickness measurement probe module is not inserted into the film to be measured. Both instruments 4B can realize optical path matching of light reflected by different probe lens surfaces; the first demodulation interferometer 4A and the second demodulation interferometer 4B share the same position scanning device 408; when the first forward movable optical mirror 408a When the second forward movable optical reflector 408c is at the zero position, the first reverse movable optical reflector 408b and the second reverse movable optical reflector 408d have a maximum displacement L, and the first reverse movable optical reflector 408d has a maximum displacement L. When the mirror 408b and the second reverse movable optical reflector 408d are at the zero position, the first forward movable optical reflector 408a and the second forward movable optical reflector 408c have a maximum displacement L; during the scanning process, the first The forward movable optical reflector 408a, the second forward movable optical reflector 408b, the first reverse movable optical reflector 408c, and the second reverse optical reflector 408d have the same displacement;
采集与控制模块5中第1光电探测器503与第3波分复用器11的11a输出端连接,第2光电探测器504与第2波分复用器11的11b输出端连接;第3光电探测器505与第3波分复用器12的12a输出端连接,第4光电探测器506与第3波分复用器12的12b输出端连接。光电探测器将采集到的信号通过数据采集卡502输送给计算机501,另外,计算机501同时负责位置扫描装置408的驱动以完成光程扫描。The first photodetector 503 is connected with the 11a output end of the 3rd wavelength division multiplexer 11 in the acquisition and control module 5, and the 2nd photodetector 504 is connected with the 11b output end of the 2nd wavelength division multiplexer 11; The photodetector 505 is connected to the output terminal 12 a of the third wavelength division multiplexer 12 , and the fourth photodetector 506 is connected to the output terminal 12 b of the third wavelength division multiplexer 12 . The photodetector transmits the collected signal to the computer 501 through the data acquisition card 502. In addition, the computer 501 is also responsible for driving the position scanning device 408 to complete the optical path scanning.
光学干涉测量方法是当前精度最高的距离测量方法,但是由于激光光源相干长度较长,激光干涉测量方法无法实现绝对量的测量。白光干涉测量方法使用的是低相干的宽谱光源。由于低相干光源的相干长度非常小,干涉后输出的干涉条纹的形状是由高斯包络所调制的正弦振荡,该条纹具有一个主极大值,它对应着干涉仪两臂光程差为零的位置。由于对干涉仪两臂光程差的苛刻要求,中心条纹的位置就为物理量的测量提供了一个优质的参考位置,根据中心条纹位置的变化可获得被测物理量变化的绝对量。因此,在白光干涉测量系统中对物理量的测量就转化成对干涉信号的中心条纹的位置变化进行测量。本发明采用双光源的设计,如图5所示,在位置扫描装置扫描的过程中,同时记录白光干涉信号与激光干涉信号,通过对激光干涉信号条纹数目的读取,可以对位置扫描装置的移动实际距离进行高精度标定。Optical interferometry is currently the most accurate distance measurement method, but due to the long coherence length of the laser light source, laser interferometry cannot achieve absolute measurement. White-light interferometry methods use low-coherence, broad-spectrum light sources. Since the coherence length of the low-coherence light source is very small, the shape of the output interference fringe after interference is a sinusoidal oscillation modulated by a Gaussian envelope. The fringe has a main maximum value, which corresponds to zero optical path difference between the two arms of the interferometer. s position. Due to the strict requirements on the optical path difference between the two arms of the interferometer, the position of the central fringe provides a high-quality reference position for the measurement of physical quantities, and the absolute amount of the change of the measured physical quantity can be obtained according to the change of the position of the central fringe. Therefore, the measurement of the physical quantity in the white light interferometry system is transformed into the measurement of the position change of the central fringe of the interference signal. The present invention adopts the design of dual light sources, as shown in Figure 5, during the scanning process of the position scanning device, the white light interference signal and the laser interference signal are recorded simultaneously, and by reading the number of fringes of the laser interference signal, the position of the position scanning device can be Move the actual distance for high-precision calibration.
一种薄膜厚度与折射率同时测量的装置及测量方法,以不插入待测薄膜时,第1测量探头301返回光测量两探头间距为例说明本发明所使用的距离测量方法:A device and measurement method for simultaneous measurement of film thickness and refractive index. When the film to be measured is not inserted, the first measurement probe 301 returns light to measure the distance between the two probes as an example to illustrate the distance measurement method used in the present invention:
第1测量探头301内部反射光311和第2测量探头302外表面反射光312被第1解调干涉仪耦合器407分为两路:一路进入到由第1准直镜403、第1正向可移动反射镜408a、第2准直镜404以及第1法拉第反射镜401组成的反射系统中,产生311’和312’反射光;一路进入到由第5准直镜410、第1反向可移动反射镜408b、第6准直镜411以及第3法拉第反射镜414组成的反射系统中,产生311”和312”反射光。在计算机501的控制下,位置扫描装置408带动第1正向可移动反射镜408a与第1反向可移动反射镜408b进行光程扫描,如图6所示,宽谱光干涉信号产生过程为:The internal reflected light 311 of the first measurement probe 301 and the external surface reflected light 312 of the second measurement probe 302 are divided into two paths by the first demodulation interferometer coupler 407: one path enters into the first collimating mirror 403, the first positive direction In the reflective system that movable reflector 408a, the 2nd collimating mirror 404 and the 1st Faraday reflector 401 form, produce 311 ' and 312 ' reflection light; In the reflection system composed of the moving mirror 408b, the sixth collimating mirror 411 and the third Faraday mirror 414, 311" and 312" reflected lights are generated. Under the control of the computer 501, the position scanning device 408 drives the first forward movable mirror 408a and the first reverse movable mirror 408b to scan the optical path, as shown in Figure 6, the generation process of the wide-spectrum optical interference signal is :
(1)当两臂光程差等于2H时,扫描臂中光311’与固定臂中光312”发生匹配,则产生第1次极大白光干涉信号331。(1) When the optical path difference between the two arms is equal to 2H, the light 311' in the scanning arm matches the light 312" in the fixed arm, and the first maximum white light interference signal 331 is generated.
(2)当两臂光程差等于0时,扫描臂与固定臂中,光311’与光311”、光312’与光312”发生匹配,则产生主极大白光干涉信号332。(2) When the optical path difference between the two arms is equal to 0, in the scanning arm and the fixed arm, the light 311' and the light 311", and the light 312' and the light 312" are matched, and the main maximum white light interference signal 332 is generated.
(3)当两臂光程差等于-2H时,扫描臂中光312’与固定臂中光312”发生匹配,则产生第2次极大白光干涉信号333。(3) When the optical path difference between the two arms is equal to -2H, the light 312' in the scanning arm matches the light 312" in the fixed arm, and the second maximum white light interference signal 333 is generated.
(4)通过对白光干涉信号中心条纹位置的提取,利用激光干涉信号的溯源特性获得主极大与次极大之间的扫描距离绝对差值,进而获得第1测量探头301与第2测量探头302之间的绝对光程。(4) By extracting the position of the central fringe of the white light interference signal, using the traceability characteristics of the laser interference signal to obtain the absolute difference in scanning distance between the main maximum and the secondary maximum, and then obtain the first measuring probe 301 and the second measuring probe The absolute optical path between 302.
基于上以宽谱光干涉测量方法的不透明待测薄膜303的厚度测量方法为:The thickness measurement method of the opaque film to be measured 303 based on the above broadband light interferometry method is:
(1)在不插入不透明待测薄膜303时,驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光311与第1测量探头301出射光在第2测量探头302外表面反射光312进行光程匹配、第2测量探头302内部反射光321与第2测量探头302出射光在第1测量探头301外表面反射光322进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,获得两测量探头之间的光程H;(1) When the opaque film 303 to be measured is not inserted, the optical path position scanning device 408 is driven to scan the optical path, so that the internal reflected light 311 of the first measuring probe 301 and the outgoing light of the first measuring probe 301 are outside the second measuring probe 302 The surface reflected light 312 performs optical path matching, and the second measuring probe 302 internally reflected light 321 and the second measuring probe 302 outgoing light perform optical path matching on the first measuring probe 301 outer surface reflected light 322; through the acquisition and control module 5 pairs of correlation The parameters are demodulated and recorded to obtain the optical path H between the two measuring probes;
(2)将不透明待测薄膜303插入第1测量探头301与第2测量探头302中间,使不透明待测薄膜303与第1测量探头301与第2测量探头302的出射光线垂直;驱动光程位置扫描装置408进行光程扫描,使由第1测量探头301内部反射光413与第1测量探头301出射光在不透明待测薄膜前表面303a反射光314进行光程匹配、第2测量探头302内部反射光323与第2测量探头302出射光在不透明待测薄膜后表面303b反射光324进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,分别获得第1测量探头301与不透明待测薄膜前表面303a的光程二倍H1、第2测量探头302与不透明待测薄膜前表面303b的二倍光程H2;(2) Insert the opaque film to be measured 303 into the middle of the first measuring probe 301 and the second measuring probe 302, so that the opaque film to be measured 303 is perpendicular to the outgoing rays of the first measuring probe 301 and the second measuring probe 302; drive the optical path position The scanning device 408 scans the optical path, so that the internal reflection light 413 of the first measurement probe 301 and the light emitted by the first measurement probe 301 are reflected on the front surface 303a of the opaque film to be measured for optical path matching, and the internal reflection of the second measurement probe 302 The light 323 and the light emitted by the second measurement probe 302 perform optical path matching on the back surface 303b of the opaque film to be tested; Measuring the double optical path H1 of the front surface 303a of the film, the double optical path H2 of the second measuring probe 302 and the opaque film front surface 303b to be measured;
(3)不透明待测薄膜303厚度d1可由上述的两次测量值所决定,(3) The thickness d1 of the opaque film to be measured 303 can be determined by the above two measured values,
透明待测薄膜304的厚度及折射率测量方法为:The thickness of the transparent film to be measured 304 and the method for measuring the refractive index are:
(1)在不插入透明待测薄膜304时,驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光311与第1测量探头301出射光在第2测量探头302外表面反射光312进行光程匹配、第2测量探头302内部反射光321与第2测量探头302出射光在第1测量探头301外表面反射光322进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,获得两测量探头之间的二倍光程H;(1) When the transparent film 304 to be measured is not inserted, the optical path position scanning device 408 is driven to scan the optical path, so that the reflected light 311 inside the first measuring probe 301 and the outgoing light of the first measuring probe 301 are outside the second measuring probe 302 The surface reflected light 312 performs optical path matching, and the second measuring probe 302 internally reflected light 321 and the second measuring probe 302 outgoing light perform optical path matching on the first measuring probe 301 outer surface reflected light 322; through the acquisition and control module 5 pairs of correlation The parameters are demodulated and recorded to obtain the double optical path H between the two measuring probes;
(2)将透明待测薄膜304插入第1测量探头301与第2测量探头302中间,透明待测薄膜304与第1测量探头301与第2测量探头302的出射光线垂直;驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光315、第1测量探头301出射光在透明待测薄膜前表面304a反射光316、第1测量探头301出射光在透明待测薄膜后表面304b反射光317分别进行光程匹配,使第2测量探头302内部反射光325、第2测量探头302出射光在透明待测薄膜后表面304b反射光326、第2测量探头302出射光在透明待测薄膜前表面304a反射光327分别进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,分别获得第1测量探头301与透明待测薄膜前表面304a的二倍光程H3、第1测量探头301与透明待测薄膜后表面304b的二倍光程H4、第2测量探头302与透明待测薄膜后表面304b的二倍光程H5、第2测量探头302与透明待测薄膜前表面304a的二倍光程H6;(2) Insert the transparent film to be measured 304 into the middle of the first measuring probe 301 and the second measuring probe 302, the transparent film to be measured 304 is perpendicular to the outgoing rays of the first measuring probe 301 and the second measuring probe 302; drive optical path position scanning The device 408 scans the optical path, so that the internal reflection light 315 of the first measuring probe 301, the outgoing light of the first measuring probe 301 reflects the light 316 on the front surface 304a of the transparent film to be measured, and the outgoing light of the first measuring probe 301 is behind the transparent film to be measured The reflected light 317 of the surface 304b carries out optical path matching respectively, so that the internal reflected light 325 of the second measuring probe 302, the outgoing light of the second measuring probe 302 are reflected on the back surface 304b of the transparent film to be measured 326, and the outgoing light of the second measuring probe 302 is in the transparent The reflected light 327 on the front surface 304a of the film to be tested is respectively matched to the optical path; the relevant parameters are demodulated and recorded by the acquisition and control module 5, and the double optical path length H3 of the first measuring probe 301 and the transparent front surface 304a of the film to be tested are respectively obtained , the double optical path H4 between the first measuring probe 301 and the back surface 304b of the transparent film to be measured, the double optical path H5 between the second measuring probe 302 and the back surface 304b of the transparent film to be measured, the second measuring probe 302 and the transparent film to be measured Double the optical path H6 of the film front surface 304a;
(3)透明待测薄膜304厚度d2可由上述的两次测量值所决定,即d2=1/2[H-(H3+H5)];空气折射率为1时,透明待测薄膜304的折射率n可由上述的两次测量值所决定,(3) The thickness d2 of the transparent film to be measured 304 can be determined by the above-mentioned two measurements, i.e. d2=1/2[H-(H3+H5)]; The rate n can be determined by the above two measurements,
即 which is
本发明的有益效果在于:The beneficial effects of the present invention are:
本发明直接将窄线宽激光光源输入到解调干涉仪中,进一步避免了激光透射光以及激光多次反射对干涉信号质量的影响,提高了薄膜厚度溯源的精度;The invention directly inputs the narrow-linewidth laser light source into the demodulation interferometer, further avoids the influence of laser transmitted light and multiple laser reflections on the quality of the interference signal, and improves the accuracy of film thickness traceability;
本发明过控制膜厚测量探头尾纤的长度避免了膜厚测量探头模块中宽谱光透射光对特征信号峰识别的干扰,降低了识别的难度,进一步提高了特征信号识别的准确性。By controlling the length of the tail fiber of the film thickness measuring probe, the present invention avoids the interference of the broad-spectrum light transmitted light in the film thickness measuring probe module on the recognition of the characteristic signal peak, reduces the difficulty of recognition, and further improves the accuracy of characteristic signal recognition.
本发明采用双探头的设计,能够同时非接触的测量薄膜的厚度以及薄膜的折射率;The present invention adopts the design of double probes, which can simultaneously measure the thickness of the film and the refractive index of the film without contact;
本发明双光源共光路以及差分的光路结构设计能够进一步减小外界环境扰动对膜厚测量结果的影响;The dual-light source common optical path and differential optical path structure design of the present invention can further reduce the influence of external environment disturbance on the film thickness measurement result;
附图说明Description of drawings
图1是一种薄膜厚度与折射率同时测量的装置示意图;Fig. 1 is a schematic diagram of a device for simultaneous measurement of film thickness and refractive index;
图2是未加载待测薄膜时测量探头模块内部光路图;Figure 2 is a diagram of the internal optical path of the measuring probe module when the film to be measured is not loaded;
图3是加载待测不透明待测薄膜时测量探头模块内部光路图;Fig. 3 is a diagram of the internal optical path of the measuring probe module when the opaque film to be tested is loaded;
图4是加载待测透明待测薄膜时测量探头模块内部光路图;Fig. 4 is the internal optical path diagram of the measuring probe module when loading the transparent film to be tested;
图5是激光干涉信号溯源原理示意图;Fig. 5 is a schematic diagram of the principle of laser interference signal traceability;
图6是未加载待测薄膜时基于白光干涉原理的距离测量方法示意图。Fig. 6 is a schematic diagram of a distance measurement method based on the principle of white light interference when the film to be tested is not loaded.
具体实施方式Detailed ways
下面结合附图对本发明的具体实施方式作进一步说明:The specific embodiment of the present invention will be further described below in conjunction with accompanying drawing:
实施例一:Embodiment one:
本发明总体技术方案如图1所示。宽谱光输出模块1由中心波长为1310nm的宽谱光源101、工作波长为1310nm的第1隔离器102所组成,宽谱光源101作为测量光源,主要用于实现薄膜厚度的绝对测量;窄线宽激光输出模块由波长1550nm的窄线宽激光光源201、工作波长为1550nm的第2隔离器202所组成,窄线宽稳频激光光源103作为光路校正光源,主要用于实现薄膜厚度测量的溯源。宽谱光源101发出的光分别经过第1隔离器102进入到分光比为3dB的分束耦合器2中被等分成两路分别通过工作波长为1310nm的第1环形器11和工作波长为1310nm的第2环形器13进入到膜厚测量探头模块3中;第1测量探头301与第2测量探头302透镜端面反射率与透射率的比为50:50,从第1测量探头401与第2测量探头402返回的测量光再分别经过工作波长为1310nm的第1环形器11和工作波长为1310nm第2环形器13进入到工作波长为1310nm和1550nm第1波分复用器8和工作波长为1310nm和1550nm第2波分复用器9的相关波长输入端;波长为1550nm的窄线宽激光输出模块2的输出光通过第2分束耦合器7被分为两路分别进入工作波长为1310nm和1550nm第1波分复用器8和工作波长为1310nm和1550nm第2波分复用器9的相关波长输入端;经过工作波长为1310nm和1550nm第1波分复用器8和工作波长为1310nm和1550nm第2波分复用器9分别合束后的两束光输入到解调干涉仪模块4中,通过解调干涉仪模块4中的第1解调干涉仪4A与第2解调干涉仪4B的扫描分别实现光程匹配;通过工作波长为1310nm和1550nm第3波分复用器11和工作波长为1310nm和1550nm第4波分复用器12将中心波长为1310nm的白光测量光束和波长为1550nm激光校正光束分离后被第1光电探测器503、第2光电探测器504、第3光电探测器505、第4光电探测器506所获取。光电探测器将收集到的信号通过数据采集卡502传输到计算机501中进行解调处理,计算机501同时负责对位置扫描装置408进行驱动。The overall technical scheme of the present invention is shown in Figure 1. The wide-spectrum light output module 1 is composed of a wide-spectrum light source 101 with a center wavelength of 1310nm and a first isolator 102 with an operating wavelength of 1310nm. The wide-spectrum light source 101 is used as a measurement light source and is mainly used to achieve absolute measurement of film thickness; The wide laser output module is composed of a narrow linewidth laser light source 201 with a wavelength of 1550nm and a second isolator 202 with an operating wavelength of 1550nm. The narrow linewidth frequency-stabilized laser light source 103 is used as the optical path correction light source, mainly used to realize the traceability of film thickness measurement . The light emitted by the wide-spectrum light source 101 enters the beam-splitting coupler 2 with a splitting ratio of 3dB through the first isolator 102, and is divided into two paths, passing through the first circulator 11 with a working wavelength of 1310nm and the circulator with a working wavelength of 1310nm respectively. The second circulator 13 enters in the film thickness measuring probe module 3; the ratio of the first measuring probe 301 and the second measuring probe 302 lens end face reflectivity to the transmittance is 50:50, from the first measuring probe 401 and the second measuring The measurement light returned by the probe 402 passes through the first circulator 11 with a working wavelength of 1310nm and the second circulator 13 with a working wavelength of 1310nm and enters the first wavelength division multiplexer 8 with a working wavelength of 1310nm and 1550nm and a working wavelength of 1310nm respectively. and the relevant wavelength input end of the second wavelength division multiplexer 9 at 1550nm; the output light of the narrow-linewidth laser output module 2 with a wavelength of 1550nm is divided into two paths by the second beam splitting coupler 7 and enters the working wavelength at 1310nm and The first wavelength division multiplexer 8 at 1550nm and the relevant wavelength input ports of the second wavelength division multiplexer 9 at 1310nm and 1550nm at operating wavelength; the first wavelength division multiplexer 8 at 1310nm and 1550nm at working wavelength and 1310nm at the operating wavelength The two beams combined with the 1550nm second wavelength division multiplexer 9 are respectively input into the demodulation interferometer module 4, and the first demodulation interferometer 4A in the demodulation interferometer module 4 interferes with the second demodulation interferometer The scanning of the instrument 4B realizes optical path matching respectively; the 1310nm and 1550nm 3rd wavelength division multiplexer 11 and the 1310nm and 1550nm 4th wavelength division multiplexer 12 will be the white light measurement beam with the center wavelength of 1310nm and The laser correction beam with a wavelength of 1550nm is separated and acquired by the first photodetector 503 , the second photodetector 504 , the third photodetector 505 and the fourth photodetector 506 . The photoelectric detector transmits the collected signal to the computer 501 for demodulation processing through the data acquisition card 502 , and the computer 501 is responsible for driving the position scanning device 408 at the same time.
当待测薄膜没有插入时,宽谱光输出模块1输出光被分光比为3dB的第1分束耦合器6分束,光线分别经过工作波长为1310nm的第1环形器11和工作波长为1310nm的第2环形器13进入到膜厚测量探头模块3中。如图2所示,由第1测量探头301自身透镜内表面反射光束311、第2测量探头302透镜的外表面反射光束312通过工作波长为1310nm的第1环形器11进入到工作波长为1310nm和1550nm第1波分复用器8相关波长输入端;由第2测量探头302自身透镜内反射光束321、第1测量探头301透镜的外表面反射光束322通过工作波长为1310nm的第2环形器13输入到工作波长为1310nm和1550nm第2波分复用器9相关波长输入端;窄线宽激光输出模块2输出光被分光比为3dB的第2分束耦合器7分束后分别输入到工作波长为1310nm和1550nm的第1波分复用器8和工作波长为1310nm和1550nm的第2波分复用器9的相关波长输入端;经过工作波长为1310nm和1550nm第1波分复用器8合束后光信号输入到第1解调干涉仪4A中;经过工作波长为1310nm和1550nm第2波分复用器9合束后光信号输入到第2解调干涉仪4B中;光束在第1解调干涉仪4A中传输方式为:工作波长为1310nm和1550nm第1波分复用器8将光信号输入到分光比为3dB的第1解调干涉仪耦合器407中分为两束:一束经过第1正向可移动反射镜408a的传输、第1法拉第反射镜401反射,另一束经过第1反向可移动反射镜408b传输、第3法拉第反射镜414反射,当第1正向光学扫描反射镜408a与第1反向可移动光学反射镜408b移动时,反射光411与反射光412发生光程完全匹配,在第1光电探测器503上形成宽谱光干涉条纹,在第2光电探测器504上形成激光干涉条纹;光束在第2解调干涉仪6B中传输方式为:工作波长为1310nm和1550nm第2波分复用器9将光信号输入到分光比为3dB的第2解调干涉仪耦合器409中分为两束:一束经过第2正向可移动反射镜408c的传输、第2法拉第反射镜402反射,另一束经过第2反向可移动反射镜408d的传输、第4法拉第反射镜415反射,当第2正向光学扫描反射镜408c与第2反向可移动光学反射镜408d移动时,反射光321与反射光322发生光程完全匹配,在第3光电探测器505上形成宽谱光干涉条纹,在第4光电探测器506上形成激光干涉条纹,经过对白光干涉信号的解调可以得到两测量探头之间的二倍光程H。When the film to be tested is not inserted, the output light of the wide-spectrum optical output module 1 is split by the first beam-splitting coupler 6 with a splitting ratio of 3dB, and the light passes through the first circulator 11 with a working wavelength of 1310nm and the first circulator 11 with a working wavelength of 1310nm respectively. The second circulator 13 enters into the film thickness measuring probe module 3 . As shown in Figure 2, the reflected light beam 311 from the inner surface of the lens of the first measurement probe 301 and the reflected light beam 312 from the outer surface of the lens of the second measurement probe 302 pass through the first circulator 11 with a working wavelength of 1310nm and enter into a working wavelength of 1310nm and 1310nm. 1550nm 1st wavelength division multiplexer 8 related wavelength input end; the light beam 321 internally reflected by the lens of the second measuring probe 302 and the external surface reflected light beam 322 of the lens of the first measuring probe 301 pass through the second circulator 13 with an operating wavelength of 1310nm Input to the relevant wavelength input ports of the second wavelength division multiplexer 9 with working wavelengths of 1310nm and 1550nm; the output light of the narrow linewidth laser output module 2 is split by the second beam splitting coupler 7 with a splitting ratio of 3dB and then respectively input to the working The first wavelength division multiplexer 8 with a wavelength of 1310nm and 1550nm and the relevant wavelength input end of the second wavelength division multiplexer 9 with an operating wavelength of 1310nm and 1550nm; through the first wavelength division multiplexer with an operating wavelength of 1310nm and 1550nm 8. After beam combining, the optical signal is input to the first demodulation interferometer 4A; after passing through the second wavelength division multiplexer 9 with operating wavelengths of 1310nm and 1550nm, the optical signal is input to the second demodulation interferometer 4B; The transmission mode in the first demodulation interferometer 4A is: the working wavelength is 1310nm and 1550nm. The first wavelength division multiplexer 8 inputs the optical signal to the first demodulation interferometer coupler 407 with a splitting ratio of 3dB and divides it into two beams. : one beam is transmitted through the first forward movable reflector 408a, reflected by the first Faraday reflector 401, and the other beam is transmitted through the first reverse movable reflector 408b, reflected by the third Faraday reflector 414, when the first When the forward optical scanning mirror 408a and the first reverse movable optical mirror 408b move, the optical paths of the reflected light 411 and the reflected light 412 are completely matched, and wide-spectrum optical interference fringes are formed on the first photodetector 503, and the Laser interference fringes are formed on the 2nd photodetector 504; the transmission mode of the light beam in the 2nd demodulation interferometer 6B is: the working wavelength is 1310nm and 1550nm, and the 2nd wavelength division multiplexer 9 inputs the optical signal to the optical signal with a splitting ratio of 3dB. The second demodulation interferometer coupler 409 is divided into two beams: one beam is transmitted through the second forward movable mirror 408c, reflected by the second Faraday mirror 402, and the other beam is passed through the second reverse movable mirror The transmission of 408d, the reflection of the 4th Faraday reflector 415, when the 2nd forward optical scanning reflector 408c and the 2nd reverse movable optical reflector 408d move, the optical paths of the reflected light 321 and the reflected light 322 completely match, in Broad-spectrum light interference fringes are formed on the third photodetector 505, and laser interference fringes are formed on the fourth photodetector 506. After demodulating the white light interference signal, the double optical path H between the two measuring probes can be obtained.
不透明待测薄膜303进行测量时,如图3所示,由第1测量探头301透镜内表面反射光束313、不透明待测薄膜前表面303a反射光束314输入到第1解调干涉仪6A中;由第2测量探头302透镜内表面反射光束323、待测薄膜后表面303b反射光束324输入到第2解调干涉仪6B中。光束在第1解调干涉仪6A中传输方式为:由工作波长为1310nm和1550nm第1波分复用器8将光信号输入到分光比为3dB的第1解调干涉仪耦合器407中分为两束,一束经过第1正向可移动反射镜408a的传输、第1法拉第反射镜401反射,另一束经过第1反向可移动反射镜408b传输、第3法拉第反射镜414反射,当第1正向光学扫描反射镜408a与第1反向可移动光学反射镜408b移动时,反射光313与反射光314发生光程完全匹配,在第1光电探测器703上形成宽谱光干涉条纹,在第2光电探测器704上形成激光干涉条纹;光束在第2解调干涉仪6B中传输方式为:由工作波长为1310nm和1550nm第2波分复用器9将光信号输入到分光比为3dB的第2解调干涉仪耦合器409中分为两束,一束经过第2正向可移动反射镜408c的传输、第2法拉第反射镜402反射,另一束经过第2反向可移动反射镜408d的传输、第4法拉第反射镜415反射,当第2正向光学扫描反射镜408c与第2反向可移动光学反射镜408d移动时,反射光323与反射光324发生光程完全匹配,在第3光电探测器505上形成宽谱光干涉条纹,在第4光电探测器506上形成激光干涉条纹。通过对宽谱光干涉信号和窄线宽激光干涉信号的解调,分别获得第1测量探头301与不透明待测薄膜前表面303a的二倍光程H1、第2测量探头302与不透明待测薄膜后表面303b的二倍光程H2。因此,不透明薄膜厚度d1就被上述两次测量值所决定,即 When the opaque film to be measured 303 is measured, as shown in FIG. 3 , the reflected light beam 313 from the inner surface of the lens of the first measuring probe 301 and the reflected light beam 314 from the front surface 303a of the opaque film to be measured are input into the first demodulation interferometer 6A; The light beam 323 reflected by the lens inner surface of the second measurement probe 302 and the light beam 324 reflected by the rear surface 303b of the film to be measured are input into the second demodulation interferometer 6B. The light beam is transmitted in the first demodulation interferometer 6A in the following way: the optical signal is input to the first demodulation interferometer coupler 407 with a splitting ratio of 3dB by the first wavelength division multiplexer 8 with operating wavelengths of 1310nm and 1550nm. There are two beams, one beam is transmitted by the first forward movable mirror 408a, reflected by the first Faraday mirror 401, and the other beam is transmitted by the first reverse movable mirror 408b and reflected by the third Faraday mirror 414, When the first forward optical scanning mirror 408a and the first reverse movable optical mirror 408b move, the optical paths of the reflected light 313 and the reflected light 314 are completely matched, and wide-spectrum optical interference is formed on the first photodetector 703 fringes, forming laser interference fringes on the second photodetector 704; the light beam is transmitted in the second demodulation interferometer 6B in the following way: the optical signal is input to the light splitter by the second wavelength division multiplexer 9 with operating wavelengths of 1310nm and 1550nm The second demodulation interferometer coupler 409 with a ratio of 3dB is divided into two beams, one beam is transmitted through the second forward movable reflector 408c, reflected by the second Faraday reflector 402, and the other beam is passed through the second reverse direction The transmission of the movable reflector 408d and the reflection of the fourth Faraday reflector 415, when the second forward optical scanning reflector 408c and the second reverse movable optical reflector 408d move, the reflected light 323 and the reflected light 324 have an optical path Completely matched, wide-spectrum light interference fringes are formed on the third photodetector 505 , and laser interference fringes are formed on the fourth photodetector 506 . By demodulating the wide-spectrum optical interference signal and the narrow-linewidth laser interference signal, the double optical path H1 of the first measuring probe 301 and the front surface 303a of the opaque film to be tested, the second measuring probe 302 and the opaque film to be tested are respectively obtained Double the optical path length H2 of the rear surface 303b. Therefore, the opaque film thickness d1 is determined by the above two measured values, namely
透明待测薄膜304测量时,如图4所示,由第1测量探头301透镜内表面反射光束315、透明待测薄膜前表面304a反射光束316、透明待测薄膜后表面304b反射光束317输入到第1解调干涉仪6A中;由第2测量探头302透镜内表面反射光束325、透明待测薄膜后表面304b反射光束326、透明待测薄膜前表面304a反射光束327输入到第2解调干涉仪6B中。光束在第1解调干涉仪6A中传输方式为:由工作波长为1310nm和1550nm第1波分复用器8将光信号输入到分光比为3dB的第1解调干涉仪耦合器407中分为两束,一束经过第1正向可移动反射镜408a的传输、第1法拉第反射镜401反射,另一束经过第1反向可移动反射镜408b传输、第3法拉第反射镜414反射,当第1正向光学扫描反射镜408a与第1反向可移动光学反射镜408b移动时,反射光315、反射光316、反射光317分别发生光程完全匹配,在第1光电探测器503上形成宽谱光干涉条纹,在第2光电探测器504上形成激光干涉条纹;光束在第2解调干涉仪6B中传输方式为:由工作波长为1310nm和1550nm第2波分复用器9将光信号输入到分光比为3dB的第2解调干涉仪耦合器409中分为两束,一束经过第2正向可移动反射镜408c的传输、第2法拉第反射镜402反射,另一束经过第2反向可移动反射镜408d的传输、第4法拉第反射镜415反射,当第2正向光学扫描反射镜408c与第2反向可移动光学反射镜408d移动时,反射光325、反射光326、反射光327分别发生光程完全匹配,在第3光电探测器505上形成宽谱光干涉条纹,在第4光电探测器506上形成激光干涉条纹。通过对宽谱光干涉信号和窄线宽激光干涉信号的解调,分别获得第1测量探头301与透明待测薄膜前表面304a的二倍光程H3、第1测量探头301与透明待测薄膜后表面304b的二倍光程H4、第2测量探头302与透明待测薄膜后表面304b的二倍光程H5、第2测量探头302与透明待测薄膜前表面304a的二倍光程H6;透明待测薄膜(304)厚度d2可由上述的两次测量值所决定,即空气折射率为1时,透明待测薄膜(304)的折射率n可由上述的两次测量值所决定,When the transparent film to be measured 304 is measured, as shown in Figure 4, the reflected light beam 315 from the inner surface of the lens of the first measurement probe 301, the reflected light beam 316 from the front surface 304a of the transparent film to be measured, and the reflected light beam 317 from the rear surface 304b of the transparent film to be measured are input to In the first demodulation interferometer 6A; the reflected light beam 325 from the inner surface of the lens of the second measurement probe 302, the reflected light beam 326 from the rear surface 304b of the transparent film to be measured, and the reflected light beam 327 from the front surface 304a of the transparent film to be measured are input to the second demodulation interference Instrument 6B. The light beam is transmitted in the first demodulation interferometer 6A in the following way: the optical signal is input to the first demodulation interferometer coupler 407 with a splitting ratio of 3dB by the first wavelength division multiplexer 8 with operating wavelengths of 1310nm and 1550nm. There are two beams, one beam is transmitted by the first forward movable mirror 408a, reflected by the first Faraday mirror 401, and the other beam is transmitted by the first reverse movable mirror 408b and reflected by the third Faraday mirror 414, When the first forward optical scanning mirror 408a and the first reverse movable optical mirror 408b move, the reflected light 315, the reflected light 316, and the reflected light 317 are completely matched in optical path respectively, and on the first photodetector 503 Broad-spectrum light interference fringes are formed, and laser interference fringes are formed on the second photodetector 504; the transmission mode of the light beam in the second demodulation interferometer 6B is: the working wavelength is 1310nm and the second wavelength division multiplexer 9 of 1550nm The optical signal is input into the second demodulation interferometer coupler 409 with a splitting ratio of 3dB and divided into two beams, one beam is transmitted through the second forward movable mirror 408c, reflected by the second Faraday mirror 402, and the other beam After the transmission of the second reverse movable reflector 408d and the reflection by the fourth Faraday reflector 415, when the second forward optical scanning reflector 408c and the second reverse movable optical reflector 408d move, the reflected light 325, reflected The optical paths of the light 326 and the reflected light 327 are completely matched respectively, and wide-spectrum light interference fringes are formed on the third photodetector 505 , and laser interference fringes are formed on the fourth photodetector 506 . By demodulating the wide-spectrum optical interference signal and the narrow-linewidth laser interference signal, the double optical path H3 of the first measuring probe 301 and the front surface 304a of the transparent film to be measured, the first measuring probe 301 and the transparent film to be measured are respectively obtained The double optical path H4 of the back surface 304b, the double optical path H5 of the second measuring probe 302 and the back surface 304b of the transparent film to be measured, the double optical path H6 of the second measuring probe 302 and the front surface 304a of the transparent film to be tested; The thickness d2 of the transparent film to be measured (304) can be determined by the above two measured values, namely When the refractive index of air is 1, the refractive index n of the transparent film to be measured (304) can be determined by the above two measured values,
即 which is
实施例二:Embodiment two:
一种薄膜厚度与折射率同时测量的装置由宽谱光输出模块1、窄线宽激光输出模块2、膜厚测量探头模块3、解调干涉仪模块4以及采集与控制模块5等五部分组成;A device for simultaneous measurement of film thickness and refractive index consists of five parts: a wide-spectrum light output module 1, a narrow linewidth laser output module 2, a film thickness measurement probe module 3, a demodulation interferometer module 4, and an acquisition and control module 5. ;
宽谱光输出模块1输出光通过第1分束耦合器6被分为两路分别通过第1环形器10、第2环形器13进入膜厚测量探头模块3的第1测量探头301和第2测量探头302中;经由第1测量探头301和第2测量探头302的返回光通过第1环形器10、第2环形器11分别进入第1波分复用器8和第2波分复用器9的相关波长输入端;The output light of the wide-spectrum light output module 1 is divided into two paths through the first beam splitter coupler 6 and enters the first measuring probe 301 and the second measuring probe 301 of the film thickness measuring probe module 3 through the first circulator 10 and the second circulator 13 respectively. In the measuring probe 302; the return light via the first measuring probe 301 and the second measuring probe 302 enters the first wavelength division multiplexer 8 and the second wavelength division multiplexer respectively through the first circulator 10 and the second circulator 11 9 relevant wavelength input terminals;
窄线宽激光输出模块2的输出光通过第2分束耦合器7被分为两路分别进入第1波分复用器8和第2波分复用器9的相关波长输入端;经过第1波分复用器8和第2波分复用器9分别合束后的两束光输入到解调干涉仪模块4中,通过解调干涉仪模块4中的第1解调干涉仪4A与第2解调干涉仪4B;通过第3波分复用器11和第4波分复用器12的不同波长的干涉信号分离后输入到采集与控制模块5中。The output light of the narrow-linewidth laser output module 2 is divided into two paths through the second beam-splitting coupler 7 and enters the relevant wavelength input ports of the first wavelength division multiplexer 8 and the second wavelength division multiplexer 9 respectively; The two beams of light combined by the first wavelength division multiplexer 8 and the second wavelength division multiplexer 9 are respectively input into the demodulation interferometer module 4, and pass through the first demodulation interferometer 4A in the demodulation interferometer module 4 and the second demodulation interferometer 4B; the interference signals of different wavelengths passed through the third wavelength division multiplexer 11 and the fourth wavelength division multiplexer 12 are separated and input to the acquisition and control module 5 .
所述的宽谱光输出模块1和窄线宽激光输出模块2中光源的特征为:宽谱光源101的半谱宽度大于45nm,出纤功率大于2mW;窄线宽激光光源201的半谱宽度小于1pm,出纤功率大于2mW;宽谱光源101与窄线宽激光光源201具有不同的中心波长,且二者的频谱在半谱宽度内没有重叠的部分。The characteristics of the light source in the wide-spectrum light output module 1 and the narrow-linewidth laser output module 2 are: the half-spectrum width of the wide-spectrum light source 101 is greater than 45nm, and the fiber output power is greater than 2mW; the half-spectrum width of the narrow-linewidth laser light source 201 The fiber output power is less than 1pm, and the fiber output power is greater than 2mW; the wide-spectrum light source 101 and the narrow-linewidth laser light source 201 have different central wavelengths, and the spectra of the two have no overlap within the half-spectrum width.
所述的膜厚测量探头模块3由第1测量探头301和第2测量探头302所组成;第1测量探头301与第2测量探头302能够同时实现对传输光线的透射和反射,传输光线的反射率在20%~80%之间;第1测量探头301与第2测量探头302的出射光线互相重合;待测器件放置测量时,分别与第1测量探头301和第2测量探头302的出射光线垂直;第1测量探头301与第1环形器10的输出端10c相连接,第2测量探头302与第2环形器13输出端13c相连接。The film thickness measuring probe module 3 is composed of a first measuring probe 301 and a second measuring probe 302; the first measuring probe 301 and the second measuring probe 302 can simultaneously realize the transmission and reflection of the transmitted light, and the reflection of the transmitted light rate is between 20% and 80%; the outgoing rays of the first measuring probe 301 and the second measuring probe 302 coincide with each other; Vertical; the first measurement probe 301 is connected to the output end 10c of the first circulator 10, and the second measurement probe 302 is connected to the output end 13c of the second circulator 13.
所述的膜厚测量探头模块3中膜厚测量探头尾纤长度的特征为:第1测量探头301和第2测量探头302尾纤的长度差值大于解调干涉仪模块4中光程扫描装置408的光程扫描范围。The feature of the length of the tail fiber of the film thickness measurement probe in the film thickness measurement probe module 3 is that the length difference between the first measurement probe 301 and the second measurement probe 302 is greater than that of the optical path scanning device in the demodulation interferometer module 4 408 optical path scanning range.
所述的解调干涉仪模块4由第1法拉第反射镜401,第2法拉第反射镜402,第1准直镜403,第2准直镜404,第3准直镜405,第4准直镜406,第1解调干涉仪耦合器407,光程扫描装置408,第2解调干涉仪耦合器409,第5准直镜410,第6准直镜411,第7准直镜412,第8准直镜413,第3法拉第反射镜414以及第4法拉第反射镜415所组成;第1波分复用器8的输出端8c与第1解调干涉仪耦合器407的4a输入端相连接,第1解调干涉仪耦合器407的4c输出端与第1准直镜403相连接,第2准直镜404与第1法拉第反射镜401相连接,第1解调干涉仪耦合器407的4d输出端第5准直镜410相连接,第6准直镜411与第3法拉第反射镜414相连接;第2波分复用器9的9c输出端与第2解调干涉仪耦合器409的4g输入端相连接,第2解调干涉仪耦合器409的4e输出端与第4准直镜406相连接,第3准直镜405与第2法拉第反射镜402相连接,第2解调干涉仪耦合器409的4h输出端第8准直镜413相连接,第7准直镜412与第4法拉第反射镜415相连接;第1解调干涉仪耦合器407、第1准直镜403、第2准直镜404、第1法拉第反射镜401、第1正向可移动光学反射镜408a、第1反向可移动光学反射镜408b、第5准直镜410、第6准直镜411、第3法拉第反射镜414和构成第1解调干涉仪4A;第2解调干涉仪耦合器409、第3准直镜405、第4准直镜406、第2法拉第反射镜402、第2正向可移动光学反射镜408c、第2反向可移动光学反射镜408d、第7准直镜412、第8准直镜413、第4法拉第反射镜415和构成第2解调干涉仪4B;第1准直镜403、第2准直镜404、第3准直镜405、第4准直镜406、第5准直镜410、第6准直镜411、第7准直镜412、第8准直镜413的光学参数相一致;第1法拉第反射镜401、第2法拉第反射镜402、第3法拉第反射镜414、第4法拉第反射镜415的光学参数相一致。Described demodulation interferometer module 4 is by the 1st Faraday reflector 401, the 2nd Faraday reflector 402, the 1st collimating mirror 403, the 2nd collimating mirror 404, the 3rd collimating mirror 405, the 4th collimating mirror 406, the first demodulation interferometer coupler 407, the optical path scanning device 408, the second demodulation interferometer coupler 409, the fifth collimating mirror 410, the sixth collimating mirror 411, the seventh collimating mirror 412, the first 8 collimating mirror 413, the third Faraday mirror 414 and the fourth Faraday mirror 415; the output end 8c of the first wavelength division multiplexer 8 is connected to the input end 4a of the first demodulation interferometer coupler 407 , the 4c output end of the first demodulation interferometer coupler 407 is connected with the first collimator mirror 403, the second collimator mirror 404 is connected with the first Faraday reflector 401, the first demodulation interferometer coupler 407 The 4d output end is connected to the fifth collimating mirror 410, and the sixth collimating mirror 411 is connected to the third Faraday reflector 414; the 9c output end of the second wavelength division multiplexer 9 is connected to the second demodulation interferometer coupler 409 The 4g input terminal of the 2nd demodulation interferometer coupler 409 is connected with the 4th collimating mirror 406, the 3rd collimating mirror 405 is connected with the 2nd Faraday mirror 402, the 2nd demodulation The 4h output end of the interferometer coupler 409 is connected to the 8th collimator mirror 413, and the 7th collimator mirror 412 is connected to the 4th Faraday reflector 415; the first demodulation interferometer coupler 407, the first collimator mirror 403 , the second collimating mirror 404, the first Faraday mirror 401, the first forward movable optical mirror 408a, the first reverse movable optical mirror 408b, the fifth collimating mirror 410, the sixth collimating mirror 411 , the third Faraday mirror 414 and the first demodulation interferometer 4A; the second demodulation interferometer coupler 409, the third collimator mirror 405, the fourth collimator mirror 406, the second Faraday mirror 402, the second Forward movable optical mirror 408c, the second reverse movable optical mirror 408d, the seventh collimator mirror 412, the eighth collimator mirror 413, the fourth Faraday mirror 415 and the second demodulation interferometer 4B; The first collimating mirror 403, the second collimating mirror 404, the third collimating mirror 405, the fourth collimating mirror 406, the fifth collimating mirror 410, the sixth collimating mirror 411, the seventh collimating mirror 412, the 8 The optical parameters of the collimating mirror 413 are consistent; the optical parameters of the first Faraday mirror 401, the second Faraday mirror 402, the third Faraday mirror 414, and the fourth Faraday mirror 415 are consistent.
所述的解调干涉仪模块4中的光程扫描装装置408的特征是:第1正向可移动光学反射镜408a,第2正向可移动光学反射镜408b,第1反向可移动光学反射镜408c,第2反向可移动光学反射镜408d的光学参数相一致;位置扫描装置408的光程扫描范围L能够满足膜厚测量探头模块4不插入待测薄膜时,第1解调干涉仪4A与第2解调干涉仪4B均能实现由不同探头透镜表面反射光的光程匹配;第1解调干涉仪4A与第2解调干涉仪4B共用同一位置扫描装置408;当第1正向可移动光学反射镜408a与第2正向可移动光学反射镜408c位于零点位置时,第1反向可移动光学反射镜408b与第2反向可移动光学反射镜408d具有最大位移L,第1反向可移动光学反射镜408b与第2反向可移动光学反射镜408d位于零点位置时,第1正向可移动光学反射镜408a与第2正向可移动光学反射镜408c具有最大位移L;扫描过程中,第1正向可移动光学反射镜408a、第2正向可移动光学反射镜408b、第1反向可移动光学反射镜408c、第2反向光学反射镜408d具有相同的位移。The feature of the optical path scanning device 408 in the described demodulation interferometer module 4 is: the 1st forward movable optical reflector 408a, the 2nd forward movable optical reflector 408b, the 1st reverse movable optical reflector The optical parameters of the mirror 408c and the second reverse movable optical mirror 408d are consistent; the optical path scanning range L of the position scanning device 408 can meet the requirements of the first demodulation interference when the film thickness measurement probe module 4 is not inserted into the film to be measured. Both the instrument 4A and the second demodulation interferometer 4B can realize the optical path matching of the reflected light from different probe lens surfaces; the first demodulation interferometer 4A and the second demodulation interferometer 4B share the same position scanning device 408; when the first When the forward movable optical reflector 408a and the second forward movable optical reflector 408c are at the zero position, the first reverse movable optical reflector 408b and the second reverse movable optical reflector 408d have a maximum displacement L, When the first reverse movable optical reflector 408b and the second reverse movable optical reflector 408d are at the zero position, the first forward movable optical reflector 408a and the second forward movable optical reflector 408c have the maximum displacement L; in the scanning process, the 1st forward movable optical reflector 408a, the 2nd forward movable optical reflector 408b, the 1st reverse movable optical reflector 408c, the 2nd reverse optical reflector 408d have the same displacement.
所述的不透明薄膜厚度测量方法为:The method for measuring the thickness of the opaque film is:
(1)在不插入不透明待测薄膜303时,驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光311与第1测量探头301出射光在第2测量探头302外表面反射光312进行光程匹配、第2测量探头302内部反射光321与第2测量302探头出射光第1测量探头301外表面反射光322进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,获得两测量探头之间的二倍光程H;(1) When the opaque film 303 to be measured is not inserted, the optical path position scanning device 408 is driven to scan the optical path, so that the internal reflected light 311 of the first measuring probe 301 and the outgoing light of the first measuring probe 301 are outside the second measuring probe 302 The optical path matching is performed on the surface reflected light 312, and the optical path matching is performed on the internal reflected light 321 of the second measuring probe 302 and the emitted light of the second measuring probe 302, and the reflected light 322 on the outer surface of the first measuring probe 301; through the collection and control module 5 pairs of related parameters Perform demodulation and recording to obtain the double optical path H between the two measuring probes;
(2)将不透明待测薄膜303插入第1测量探头301与第2测量探头302中间,使不透明待测薄膜303与第1测量探头301与第2测量探头302的出射光线垂直;驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光313与第1测量探头301出射光在不透明待测薄膜前表面303a反射光314进行光程匹配、第2测量探头302内部反射光323与第2测量探头302出射光在不透明待测薄膜后表面303b反射光324进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,分别获得第1测量探头301与不透明待测薄膜前表面303a的二倍光程H1、第2测量探头302与不透明待测薄膜前表面303b的二倍光程H2;(2) Insert the opaque film to be measured 303 into the middle of the first measuring probe 301 and the second measuring probe 302, so that the opaque film to be measured 303 is perpendicular to the outgoing rays of the first measuring probe 301 and the second measuring probe 302; drive the optical path position The scanning device 408 performs optical path scanning, so that the internal reflected light 313 of the first measuring probe 301 and the emitted light of the first measuring probe 301 are matched in optical path with the reflected light 314 on the front surface 303a of the opaque film to be measured, and the internal reflected light of the second measuring probe 302 323 and the light emitted by the second measuring probe 302 perform optical path matching on the back surface 303b of the opaque film to be measured; the relevant parameters are demodulated and recorded by the acquisition and control module 5, and the first measuring probe 301 and the opaque film to be tested are obtained respectively. The double optical path H1 of the front surface 303a of the film, the double optical path H2 of the second measuring probe 302 and the front surface 303b of the opaque film to be measured;
(3)不透明待测薄膜303厚度d1可由上述的两次测量值所决定,(3) The thickness d1 of the opaque film to be measured 303 can be determined by the above two measured values,
即 which is
一种薄膜厚度与折射率同时测量的装置及测量方法,包括以下步骤:A device and method for simultaneously measuring film thickness and refractive index, comprising the following steps:
(1)在不插入透明待测薄膜304时,驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光311与第1测量探头301出射光在第2测量探头302外表面反射光312进行光程匹配、第2测量探头302内部反射光321与第2测量探头302出射光在第1测量探头301外表面反射光322进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,获得两测量探头之间的二倍光程H;(1) When the transparent film 304 to be measured is not inserted, the optical path position scanning device 408 is driven to scan the optical path, so that the reflected light 311 inside the first measuring probe 301 and the outgoing light of the first measuring probe 301 are outside the second measuring probe 302 The surface reflected light 312 performs optical path matching, and the second measuring probe 302 internally reflected light 321 and the second measuring probe 302 outgoing light perform optical path matching on the first measuring probe 301 outer surface reflected light 322; through the acquisition and control module 5 pairs of correlation The parameters are demodulated and recorded to obtain the double optical path H between the two measuring probes;
(2)将透明待测薄膜304插入第1测量探头301与第2测量探头302中间,使透明待测薄膜304与第1测量探头301与第2测量探头302的出射光线垂直;驱动光程位置扫描装置408进行光程扫描,使第1测量探头301内部反射光315、第1测量探头301出射光在透明待测薄膜前表面304a反射光316、第1测量探头301出射光在透明待测薄膜后表面304b反射光317分别进行光程匹配,使第2测量探头302内部反射光325、第2测量探头302出射光在透明待测薄膜后表面304b反射光326、第2测量探头302出射光在透明待测薄膜前表面304a反射光327分别进行光程匹配;通过采集与控制模块5对相关参数进行解调记录,分别获得第1测量探头301与透明待测薄膜前表面304a的二倍光程H3、第1测量探头301与透明待测薄膜后表面304b的二倍光程H4、第2测量探头302与透明待测薄膜后表面304b的二倍光程H5、第2测量探头302与透明待测薄膜前表面30ab的二倍光程H6;(2) Insert the transparent film 304 to be measured into the middle of the first measuring probe 301 and the second measuring probe 302, so that the transparent film 304 to be measured is perpendicular to the outgoing rays of the first measuring probe 301 and the second measuring probe 302; drive the optical path position The scanning device 408 scans the optical path, so that the internal reflection light 315 of the first measuring probe 301, the light emitted by the first measuring probe 301 is reflected on the front surface 304a of the transparent film to be measured, and the light 316 emitted by the first measuring probe 301 is reflected on the transparent film to be measured. The reflected light 317 of the back surface 304b is respectively carried out optical path matching, so that the reflected light 325 inside the second measuring probe 302 and the outgoing light of the second measuring probe 302 are reflected on the back surface 304b of the transparent film to be measured 326, and the outgoing light of the second measuring probe 302 is in the The reflected light 327 on the front surface 304a of the transparent film to be tested is matched with the optical path respectively; the relevant parameters are demodulated and recorded by the acquisition and control module 5, and the optical path lengths of the first measuring probe 301 and the front surface 304a of the transparent film to be tested are obtained respectively H3, the first measurement probe 301 and the double optical path H4 of the transparent film back surface 304b to be measured, the second measurement probe 302 and the double light path H5 of the transparent film back surface 304b to be measured, the second measurement probe 302 and the transparent film to be tested Measure the double optical path H6 of 30ab on the front surface of the film;
(3)空气折射率为1时,透明待测薄膜304厚度d2可由上述的两次测量值所决定,(3) When the refractive index of air is 1, the thickness d2 of the transparent film to be measured 304 can be determined by the above two measured values,
以上所述仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and changes. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included within the protection scope of the present invention.
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