CN108387670A - A method of utilizing the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer - Google Patents
A method of utilizing the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer Download PDFInfo
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- CN108387670A CN108387670A CN201810228039.7A CN201810228039A CN108387670A CN 108387670 A CN108387670 A CN 108387670A CN 201810228039 A CN201810228039 A CN 201810228039A CN 108387670 A CN108387670 A CN 108387670A
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- G—PHYSICS
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
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Abstract
The present invention relates to a kind of methods using the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer, which is characterized in that includes the following steps：1), hot-vibration sifter constitutional diagram is detached according to n-alkane and unidentified compound；2), the spectrogram at the unidentified compound component peak that observation is separated, studies unidentified compound component peak shape state, using the subtle variation of oil in spectrogram, identifies different fluid property layer, that is, distinguishes oil-gas-water layer；3) total peak area for, calculating separately n-alkane and unidentified compound component peak is identifying peak area, unidentified peak area, total peak area, is identifying that peak selects two parameters to draw hot-vibration sifter interpretation chart as horizontal, ordinate than total peak area, unidentified peak than total peak area and in having identified peak than six parameters of unidentified peak area.Fundamentally solve the problems, such as that existing thermal evaporation gas chromatographic technique can not accurately distinguish oil reservoir and oil-water common-layer, good classification effect from composition chromatograph chart.
Description
Technical field
The present invention relates to the methods of identification of hydrocarbon water layer, especially a kind of to utilize the unidentified compound shape of hot-vibration sifter component
The method of state and content identification of hydrocarbon water layer.
Background technology
Thermal evaporation gas chromatographic technique is a kind of logging method detected using hydrocarbon component in rock, due to this technology
With the ability for the hydrocarbon mixture in rock being separated into single component, the identification of reservoir oil property, the interference that decontaminates,
Oil-gas-water layer evaluation etc. played an important role, and effective technological means is provided for In Oil Field Exploration And Development.But due to
Oil reservoir, the thermal evaporation constitutional diagram form of oil-water common-layer are similar, therefore the bad differentiation of oil reservoir, oil-water common-layer, referring to Fig. 1.
Invention content
The purpose of the invention is to provide it is a kind of more it is reasonable effectively utilize the unidentified compound of hot-vibration sifter component
The method of form and content identification of hydrocarbon water layer, fundamentally solving existing thermal evaporation gas chromatographic technique can not be from composition chromatograph chart
In the problem of accurately distinguishing oil reservoir and oil-water common-layer, good classification effect.
The technical scheme is that：
A method of using the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer, feature exists
In including the following steps：
1), hot-vibration sifter constitutional diagram is detached according to n-alkane and unidentified compound；
2), the spectrogram at the unidentified compound component peak that observation is separated, studies unidentified compound component peak shape state,
Using the subtle variation of oil in spectrogram, identifies different fluid property layer, that is, distinguish oil-gas-water layer；
3) total peak area for, calculating separately n-alkane and unidentified compound component peak is identifying peak area, is not knowing
Other peak area, total peak area have identified that peak than total peak area and has identified peak than unidentified peak face than total peak area, unidentified peak
Two parameters are selected to draw hot-vibration sifter interpretation chart as horizontal, ordinate in six parameters of product.
The above-mentioned method using the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer, step 1)
In, using chromatographic work station separating normal alkane and unidentified compound, qualitative and quantitative analysis is carried out to component, wherein qualitative
It is to determine that the title of the compound in component, the content of quantification of each compound of determination calculate all compounds first
Then peak area again calculates identified all n-alkane peak areas, the two is subtracted each other as corresponding unidentified
The peak area of compound, and then obtain the spectrogram of unidentified compound component.
The above-mentioned method using the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer, step 2)
In, the variation that oil is subtle in spectrogram is identified using fingerprinting methodology.
The beneficial effects of the invention are as follows：
This method can efficiently solve that constitutional diagram is similar, the problem of being not easy to judge properties of fluid in bearing stratum, by heat
Evaporated components figure carries out the separation of n-alkane and unidentified compound, then observes the subtle change at unidentified compound component peak
Change, and calculate the total peak area of n-alkane and unidentified compound peaks, and then draw interpretation chart, classify, obtains
Good classifying quality.
Description of the drawings
Fig. 1 is XX well XXm hot-vibration sifter component analyses spectrograms (comparison of oil reservoir and oil-water common-layer)；
Fig. 2 is the unidentified peak spectrogram of hot-vibration sifter group (comparison of oil reservoir and oil-water common-layer) in Fig. 1；
Fig. 3 is the XX well XXm hot-vibration sifter interpretation charts made using the method for the present invention.
Specific implementation mode
This utilizes the method for the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer, and specific steps are such as
Under：
1), hot-vibration sifter constitutional diagram is detached according to n-alkane and unidentified compound；
2), the spectrogram at the unidentified compound component peak that observation is separated, studies unidentified compound component peak shape state,
It using the subtle variation of oil in spectrogram, identifies different fluid property layer, that is, distinguishes oil-gas-water layer, referring in Fig. 2 in drawn circle
Component peaks metamorphosis；
3) total peak area for, calculating separately n-alkane and unidentified compound component peak is identifying peak area, is not knowing
Other peak area, total peak area have identified that peak than total peak area and has identified peak than unidentified peak face than total peak area, unidentified peak
Two parameters are selected to draw hot-vibration sifter interpretation chart as horizontal, ordinate in six parameters of product.
Wherein, in step 1), using chromatographic work station separating normal alkane and unidentified compound, component is carried out qualitative
And quantitative analysis, wherein the title of the qualitative compound being to determine in component, the content of quantification of each compound of determination, first
The peak area of all compounds is calculated, then identified all n-alkane peak areas are calculated again, the two phase
Subtract the peak area as corresponding unidentified compound, and then obtains the spectrogram of unidentified compound component.In step 2), use
The fingerprinting methodology of spectrogram identifies the variation that oil is subtle in spectrogram.
In the present embodiment, using total peak area and peak ratio total peak area, total peak area and the unidentified peak total peak of ratio have been identified
Area draws hot-vibration sifter interpretation chart respectively, as shown in Figure 3.
Claims (3)
1. a kind of method using the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer, feature exists
In including the following steps：
1), hot-vibration sifter constitutional diagram is detached according to n-alkane and unidentified compound；
2), the spectrogram at the unidentified compound component peak that observation is separated, studies unidentified compound component peak shape state, utilizes
The subtle variation of oil in spectrogram, identifies different fluid property layer, that is, distinguishes oil-gas-water layer；
3) total peak area for, calculating separately n-alkane and unidentified compound component peak is identifying peak area, unidentified peak
Area, total peak area have identified that peak than total peak area and has identified peak than unidentified peak area six than total peak area, unidentified peak
Two parameters are selected to draw hot-vibration sifter interpretation chart as horizontal, ordinate in a parameter.
2. according to claim 1 utilize the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer
Method, it is characterised in that：In step 1), using chromatographic work station separating normal alkane and unidentified compound, component is carried out
Qualitative and quantitative analysis, wherein the title of the qualitative compound being to determine in component, the content of quantification of each compound of determination,
The peak area of all compounds is calculated first, then identified all n-alkane peak areas is calculated again, two
Person subtracts each other the peak area as corresponding unidentified compound, and then obtains the spectrogram of unidentified compound component.
3. according to claim 1 utilize the unidentified compound form of hot-vibration sifter component and content identification of hydrocarbon water layer
Method, it is characterised in that：In step 2), the variation that oil is subtle in spectrogram is identified using fingerprinting methodology.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109001355A (en) * | 2018-08-16 | 2018-12-14 | 中海石油（中国）有限公司天津分公司 | Method of discrimination is explained based on the well logging oil gas that hot-vibration sifter gas-chromatography map compares |
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| CN103364427A (en) * | 2012-04-10 | 2013-10-23 | 中国石油化工股份有限公司 | Method for identifying in-place oil display in presence of drilling fluid solid-state fluorescent additive |
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| CN106437691A (en) * | 2016-08-05 | 2017-02-22 | 中国石油集团长城钻探工程有限公司录井公司 | Low gas-oil-ratio oil reservoir gas logging evaluation method |
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2018
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| CN103364427A (en) * | 2012-04-10 | 2013-10-23 | 中国石油化工股份有限公司 | Method for identifying in-place oil display in presence of drilling fluid solid-state fluorescent additive |
| CN106437691A (en) * | 2016-08-05 | 2017-02-22 | 中国石油集团长城钻探工程有限公司录井公司 | Low gas-oil-ratio oil reservoir gas logging evaluation method |
| CN106442757A (en) * | 2016-08-31 | 2017-02-22 | 中国石油集团渤海钻探工程有限公司 | Judgment method for oil-water layer |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109001355A (en) * | 2018-08-16 | 2018-12-14 | 中海石油（中国）有限公司天津分公司 | Method of discrimination is explained based on the well logging oil gas that hot-vibration sifter gas-chromatography map compares |
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