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CN108130155A - Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil - Google Patents

Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil Download PDF

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Publication number
CN108130155A
CN108130155A CN201711297430.4A CN201711297430A CN108130155A CN 108130155 A CN108130155 A CN 108130155A CN 201711297430 A CN201711297430 A CN 201711297430A CN 108130155 A CN108130155 A CN 108130155A
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CN
China
Prior art keywords
oil
composition
modified
polyalphaolefin
gutter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711297430.4A
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Chinese (zh)
Inventor
高平
刘维民
冯大鹏
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Lanzhou Institute of Chemical Physics LICP of CAS
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Lanzhou Institute of Chemical Physics LICP of CAS
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Priority to CN201711297430.4A priority Critical patent/CN108130155A/en
Publication of CN108130155A publication Critical patent/CN108130155A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/08—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing oxygen
    • C10M105/32—Esters
    • C10M105/38—Esters of polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/06—Well-defined aromatic compounds
    • C10M2203/065—Well-defined aromatic compounds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/283—Esters of polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/401—Fatty vegetable or animal oils used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
    • C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
    • C10M2219/066—Thiocarbamic type compounds
    • C10M2219/068—Thiocarbamate metal salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/04—Groups 2 or 12
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/10—Groups 5 or 15
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/08—Hydraulic fluids, e.g. brake-fluids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of modified swill-cooked dirty oil prepare lubricant oil composite, the composition on the basis of composition gross weight, comprising component and mass percent be：Detersive 0.01 ~ 0.1%, anti emulsifier 0.01 ~ 0.1%, 0.5 ~ 1.0 % of antiwear additive, antioxidant 0.05 ~ 0.5%, antirust agent 0.01 ~ 0.1%, antifoaming agent 0.001 ~ 0.01% and surplus base oil；Base oil is modified gutter oil, alkyl tetrahydro naphthalene and polyalphaolefin；Modified gutter oil is polyalcohol modified gutter oil.Composition of the present invention can be used for the lubrication of hydraulic system.Modified swill-cooked dirty oil is selected in the base oil part of lubricant oil composite of the present invention, realizes the effective recycling of waste.

Description

Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil
Technical field
The invention belongs to technical field of lubricating oil, are related to lubricant oil composite prepared by a kind of modified swill-cooked dirty oil.The combination Object can be used for the lubrication of hydraulic system.
Background technology
Gutter oil refers to all kinds of abandoned oils, poor oil present in life, by some people possessed with a lust for gain by processing The dining table of people is gone on after refinement, is done great harm to human body；Being allowed to discharge also can seriously polluted-water and soil.Therefore, rationally Ground recycles gutter oil, in addition to direct economic benefit, also very big social benefit.
The main chemical compositions of gutter oil are higher fatty acid fat, and common method of comprehensive utilization is to urge gutter oil Change is decomposed into higher fatty acids and glycerine, further prepares industrial oleic acid, stearic acid, fatty acid mixed and commercial grease etc. (CN103172851A；CN103214366A；CN103214375A)；The gutter oil research on utilization of document report further includes gutter oil Prepare biodiesel, macromolecular plasticizer, transformer insulation oil, nicotine cream preparation, lubricant for drilling fluids, biological alkane and Biological plastics, oil-soluble organic rare earth compounds and rubber interleaving agent, lube base oil, biology base rolling mill compound etc. (CN103146488A；CN103193933A, CN103012840A；CN103131524A；CN103299991A； CN103013464A, CN103045183A；The country will build first waste grease alkene project, petroleum refining and chemical industry, and 2015, 46（7）：94-94；Britain research waste cooking oils biological plastics, Shanghai chemical industry, 2012,37（10）：49-49. bangs Steel, Liu Rende, gutter oil prepare organic rare earth compounds and its tribological Properties, China rare earth journal, and 2015,33（3）： 355-362；Qingdao University of Science and Technology utilizes " gutter oil " to develop new type rubber interleaving agent, modern rubber technology, and 2014（2）：46； CN103275812B；CN104726183B).
Invention content
The present invention is intended to provide lubricant oil composite prepared by a kind of modified swill-cooked dirty oil, can simply and efficiently realize trench The utilization of oil.
Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil, it is characterised in that the composition is using composition gross weight as base Standard, comprising component and mass percent be：Detersive 0.01 ~ 0.1%, anti emulsifier 0.01 ~ 0.1%, antiwear additive 0.5 ~ 1.0 %, antioxidant 0.05 ~ 0.5%, antirust agent 0.01 ~ 0.1%, antifoaming agent 0.001 ~ 0.01% and surplus base oil；It is described Base oil is modified gutter oil, alkyl tetrahydro naphthalene and polyalphaolefin (PAO)；The gutter oil of the modification is polyalcohol modifiedly Ditch oil.
The detersive is alkyl benzene calcium sulfonate；The anti emulsifier is amine and ethylene oxide condensate (T1001)；It is described Antiwear additive is N- normal-butyl-N- n-octyl antimony dithiocarbamates；The antioxidant is 3.5- di-tert-butyl-4-hydroxyl benzyls Acetic acid esters；The antirust agent is dinonyl naphthalene sulfonate barium (T705)；The antifoaming agent is dimethicone (T901).
The alkyl tetrahydro naphthalene is one or more of octyl group naphthane, decyl naphthane and dodecyl naphthane.
The polyalphaolefin is one or more of PAO2, PAO4 and PAO6.
The mass ratio of modified gutter oil, alkyl tetrahydro naphthalene and polyalphaolefin is 3 in the base oil:1:1.
Lubricant oil composite of the present invention, base oil part select modified swill-cooked dirty oil, had both realized the effective of waste It recycles, and can reduce with oily cost.The lubricant oil composite can be used for the lubrication of hydraulic system, can also be according to making Equipment, the additives such as addition waterproof, metal deactivator.
Specific embodiment
Embodiment 1
Lubricant oil composite I
59.434g modified swill-cooked dirty oils；19.812g octyl group naphthane；19.812g PAO4；0.02g alkyl benzene calcium sulfonates；0.02g T1001；0.6g N- normal-butyl-N- n-octyl antimony dithiocarbamates；0.1g 3.5- di-tert-butyl-4-hydroxyl benzyl acetic acid Ester；0.02gT705；0.002gT901.Performance is listed in table 1.
Lubricant oil composite II
59.597g modified swill-cooked dirty oils, 19.865g decyl naphthanes, 19.865g PAO6,0.03g alkyl benzene calcium sulfonates, 0.03g T1001,0.5g N- normal-butyl-N- n-octyl antimony dithiocarbamates, 0.08g 3.5- di-tert-butyl-4-hydroxyl benzyl second Acid esters, 0.03gT705,0.003gT901.Performance is listed in table 1.
Lubricant oil composite III
59.570g modified swill-cooked dirty oils；19.857g dodecyl naphthane；16.857g PAO4；3g PAO2；0.01g alkylbenzenes Sulfoacid calcium；0.01g T1001；0.6g N- normal-butyl-N- n-octyl antimony dithiocarbamates；0.08g 3.5- di-t-butyls- 4- hydroxybenzyl acetic acid esters；0.01gT705；0.006gT901.Performance is listed in table 1.
Lubricant oil composite IV
59.550g modified swill-cooked dirty oils；10.849g octyl group naphthanes, 5g decyl naphthanes, 4g dodecyl naphthanes；18.849g PAO6,1gPAO2；0.03g alkyl benzene calcium sulfonates；0.03g T1001；0.6g N- normal-butyl-N- n-octyl dithiocarbamates first Sour antimony；0.06g 3.5- di-tert-butyl-4-hydroxyl benzyl acetic acid esters；0.03gT705；0.002gT901.Performance is listed in table 1.
Lubricant oil composite V
59.511g modified swill-cooked dirty oils；10.838g octyl group naphthanes, 9g decyl naphthanes；10.838g PAO4,5g PAO6,4g PAO2；0.02g alkyl benzene calcium sulfonates；0.02g T1001；0.65g N- normal-butyl-N- n-octyl antimony dithiocarbamates； 0.1g 3.5- di-tert-butyl-4-hydroxyl benzyl acetic acid esters；0.02gT705,0.003gT901.Performance is listed in table 1.
Lubricant oil composite VI
59.404g modified swill-cooked dirty oils；10.801g decyl naphthanes, 9g dodecyl naphthanes；19.801g PAO2；0.03g alkane Base benzene sulfonic acid calcium；0.03g T1001；0.7g N- normal-butyl-N- n-octyl antimony dithiocarbamates；Bis- tertiary fourths of 0.2g 3.5- Base -4- hydroxybenzyl acetic acid esters；0.03gT705；0.004gT901.Performance is listed in table 1.
1 lubricating oil composition physical performance of table
。

Claims (5)

1. a kind of lubricant oil composite prepared by modified swill-cooked dirty oil, it is characterised in that the composition on the basis of composition gross weight, Comprising component and mass percent be：Detersive 0.01 ~ 0.1%, anti emulsifier 0.01 ~ 0.1%, antiwear additive 0.5 ~ 1.0 %, antioxidant 0.05 ~ 0.5%, antirust agent 0.01 ~ 0.1%, antifoaming agent 0.001 ~ 0.01% and surplus base oil；The basis Oil is modified gutter oil, alkyl tetrahydro naphthalene and polyalphaolefin；The gutter oil of the modification is polyalcohol modified gutter oil.
2. composition as described in claim 1, it is characterised in that the detersive is alkyl benzene calcium sulfonate；The anti emulsifier For amine and ethylene oxide condensate；The antiwear additive is N- normal-butyl-N- n-octyl antimony dithiocarbamates；The antioxidant For 3.5- di-tert-butyl-4-hydroxyl benzyl acetic acid esters；The antirust agent is dinonyl naphthalene sulfonate barium；The antifoaming agent is dimethyl Silicone oil.
3. composition as described in claim 1, it is characterised in that modified gutter oil in the base oil, alkyl tetrahydro naphthalene and The mass ratio of polyalphaolefin is 3:1:1.
4. the composition as described in claim 1 or 3, it is characterised in that the alkyl tetrahydro naphthalene is octyl group naphthane, decyl four One or more of hydrogen naphthalene and dodecyl naphthane.
5. the composition as described in claim 1 or 3, it is characterised in that the polyalphaolefin is one in PAO2, PAO4 and PAO6 Kind is several.
CN201711297430.4A 2017-12-08 2017-12-08 Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil Pending CN108130155A (en)

Priority Applications (1)

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CN201711297430.4A CN108130155A (en) 2017-12-08 2017-12-08 Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil

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Application Number Priority Date Filing Date Title
CN201711297430.4A CN108130155A (en) 2017-12-08 2017-12-08 Lubricant oil composite prepared by a kind of modified swill-cooked dirty oil

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CN108130155A true CN108130155A (en) 2018-06-08

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112694379A (en) * 2021-01-18 2021-04-23 太原理工大学 Preparation method and application of alkyl tetrahydronaphthalene
CN114907906A (en) * 2022-06-20 2022-08-16 太原理工大学 Lithium-based lubricating grease containing alkyl tetrahydronaphthalene compound and preparation method thereof
CN114907909A (en) * 2022-06-20 2022-08-16 太原理工大学 Lithium-based lubricating grease with alkyl tetrahydronaphthalene compound as blending oil and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102952617A (en) * 2012-11-02 2013-03-06 北京欧陆宝石化产品有限公司 Hydraulic-transmission-braking three-use lubricating oil composition
CN103214366A (en) * 2013-04-13 2013-07-24 齐河县齐翔生物科技有限公司 Method for producing pentaerythrite oleate by utilizing swill-cooked dirty oil
CN103289792A (en) * 2012-02-22 2013-09-11 中国石油化工股份有限公司 Production method for lubricant oil composition
CN104726184A (en) * 2015-02-09 2015-06-24 新疆福克油品股份有限公司 Environment-friendly bio-based gear oil composition
CN106221881A (en) * 2016-07-29 2016-12-14 广西蓝德再生能源有限责任公司 Biodegradable antiwear hydraulic oil compositions

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CN103289792A (en) * 2012-02-22 2013-09-11 中国石油化工股份有限公司 Production method for lubricant oil composition
CN102952617A (en) * 2012-11-02 2013-03-06 北京欧陆宝石化产品有限公司 Hydraulic-transmission-braking three-use lubricating oil composition
CN103214366A (en) * 2013-04-13 2013-07-24 齐河县齐翔生物科技有限公司 Method for producing pentaerythrite oleate by utilizing swill-cooked dirty oil
CN104726184A (en) * 2015-02-09 2015-06-24 新疆福克油品股份有限公司 Environment-friendly bio-based gear oil composition
CN106221881A (en) * 2016-07-29 2016-12-14 广西蓝德再生能源有限责任公司 Biodegradable antiwear hydraulic oil compositions

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112694379A (en) * 2021-01-18 2021-04-23 太原理工大学 Preparation method and application of alkyl tetrahydronaphthalene
CN112694379B (en) * 2021-01-18 2023-07-14 太原理工大学 Preparation method and application of alkyl tetrahydronaphthalene
CN114907906A (en) * 2022-06-20 2022-08-16 太原理工大学 Lithium-based lubricating grease containing alkyl tetrahydronaphthalene compound and preparation method thereof
CN114907909A (en) * 2022-06-20 2022-08-16 太原理工大学 Lithium-based lubricating grease with alkyl tetrahydronaphthalene compound as blending oil and preparation method thereof
CN114907909B (en) * 2022-06-20 2023-04-11 太原理工大学 Lithium-based lubricating grease with alkyl tetrahydronaphthalene compound as blending oil and preparation method thereof

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