CN108004066A - It is a kind of suitable for soap of sensitiveness skin and preparation method thereof - Google Patents
It is a kind of suitable for soap of sensitiveness skin and preparation method thereof Download PDFInfo
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- CN108004066A CN108004066A CN201711251469.2A CN201711251469A CN108004066A CN 108004066 A CN108004066 A CN 108004066A CN 201711251469 A CN201711251469 A CN 201711251469A CN 108004066 A CN108004066 A CN 108004066A
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- Prior art keywords
- soap
- parts
- preparation
- fish oil
- sodium hydroxide
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of suitable for soap of sensitiveness skin and preparation method thereof, comprise the following steps：Comprise the following steps：（1）Fish oil and sodium hydroxide solution are subjected to 1 8h of saponification, then successively saltouts and is analysed with alkali, obtains pure soap base of the content of fatty acid more than 60%；（2）Deionized water is added when stirring soap base, when temperature reaches 70 80 DEG C, sequentially adds alkyl-glucoside, glycerine and stearic acid, it is 67 to adjust pH value of solution；（3）Trehalose and plants essential oil are eventually adding, after stirring 1 10h, is stood up to the soap.The present invention effectively removes oil stain and spot, easily rinsing using natural fish oil as emulsifying agent, gentle non-stimulated, and raw materials used nontoxicity, and production process is environmentally protective, has extensive market value.
Description
Technical field
The present invention relates to daily chemical product processing technique field, more particularly, to a kind of fertilizer suitable for sensitiveness skin
Soap and preparation method thereof.
Background technology
In recent years, with the prosperity and development of modern industry, oil, printing and dyeing, chemical industry, agricultural and the production of mankind's everyday life
Raw amount of pollutants increases sharply, and the hazard weather such as haze, sandstorm just increasingly encroaches on the tender and lovely skin of people, with skin
Patient's group's accounting is growing.Sensitiveness skin is a kind of skin being at any time in high alert, and skin allergy can cause skin
Skin is dried, decortication, rubescent, greasy or even sensitive shouting pain.Common soap is the surfactant with chemical synthesis mostly on the market
What saponification obtained, such soap pH value is higher, and human skin is in faintly acid, therefore can destroy the tender and lovely guarantor of skin surface
Barrier is protected, aggravates skin allergy.
Up to the present, existing many refines grease from natural materials and makes soap as emulsifying agent in the prior art
Relevant report, such as：
The Chinese patent of Application No. CN201510238587.4 discloses a kind of wild fragrant fruit liquid soap manufacture method, by open country
It is prepared by raw natural perfume fruit oil, liquid sodium hydroxide, cocounut oil acyl, fatty alcohol polyoxyethylene ether, sodium chloride, glycerine and deionized water
Form；In the inventive solutions, main raw material(s) is oily for the fragrant fruit of the wild fragrant fruit refining of Gaoligong Shan Mountain, Baoshan City Tengchong
County, Longyang District, Longling County and Changning County are the main producing regions of wild fragrant fruit oil plant, and periphery Dehong prefecture Luxi City, Yingjiang County also have
Distribution, belongs to renewable resource, has strong dirt-removing power, easily foaming abundancy, rinsing, power saving, province using the liquid soap of its production
Water, antistatic, feel is submissive, the performance of energy-saving and environmental protection.The invention is not added with essence, keeps wild fragrant fruit ecosystem fragrant.
The Chinese patent of Application No. CN201510918857.6 discloses a kind of preparation method of pollution-free soap of refreshing oneself,
Belong to soap preparing technical field.The present invention is using peppermint, borneol, lilac, gardenia, essence, Schisandra chinensis as raw material, by powder
After broken addition aloe extract, stir evenly, add vitamin mixtures, finally by saponification and injection molding, so as to obtain
A kind of pollution-free soap of refreshing oneself.Example proves that the method for the present invention is unique novel, the obtained pollution-free soap not only operative employee that refreshes oneself
Skill is simple and practicable, is produced without any sewage, and the preparing raw material of soap is of low cost, significant effect of refreshing oneself after use.
Application No. CN201010107594.8 Chinese patents disclose a kind of by Kazak's conventional soap-black soap
Preparation method is combined with modern soapmaking technology, prepares a kind of natural soap, its raw material includes plant ass, animal and plant fat and food
Salt etc., natural soap of the present invention in the trace element of health, have environmentally protective rich in multiple beneficial, and formula is simple, and cost is low
It is honest and clean, many advantages, such as finished product impurity is few, and color and luster is light, and preparation skin disease to a variety of soap and local disease have good treat
Effect.
The Chinese patent of Application No. CN201610144529.X disclose a kind of disposable luffa energy-saving soap and its
Preparation method.The present invention is softened by luffa, luffa heat treatment, makes luffa soft easy to sizing, Ran Houtong
Cross and be mixed and made into soap with soap lye.The present invention soap have lightweight, dosage does not waste, is small, intensity is good, it is easy to process and
The features such as packaging；The present invention is also non-breakable with soap body when washing one's hands at the same time, and common fertilizer is brought in function and visually
The characteristics of soap does not possess, is especially suitable for carrying with during travel in holiday.
Emulsifying agent used is often prepared by chemistry is artificial synthesized in the prior art, is irritating to the skin, or by natural
Extracted in fruits and vegetables, manufacturing cost is high.
The content of the invention
The present invention is in order to overcome emulsifying agent used in the above-mentioned prior art to be often prepared by chemistry is artificial synthesized, to skin
The problem of skin has stimulation, or by being extracted in natural fruit and vegetables, and manufacturing cost is high, there is provided a kind of soap suitable for sensitiveness skin and
Its preparation method, using natural fish oil as emulsifying agent, having soap, component is simple, the performance such as effective decontamination and health environment-friendly.
To achieve these goals, the present invention uses following technical scheme：
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight：
25-30 parts of fish oil
5-10 parts of sodium hydroxide
1-3 parts of alkyl-glucoside
1-3 parts of trehalose
0.5-2 parts of plants essential oil
1-5 parts of glycerine
1-3 parts of stearic acid
55-60 parts of deionized water；
Raw material employed in the present invention is environmentally protective, nontoxic, non-stimulated to skin.
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps：（1）By fish oil and sodium hydroxide
Solution carries out saponification 1-8h, then successively saltouts and analysed with alkali, obtains pure soap base of the content of fatty acid more than 60%；
（2）Add deionized water when stirring soap base, when temperature reaches 70-80 DEG C, sequentially add alkyl-glucoside, glycerine and
Stearic acid, adjusting pH value of solution are 6-7；（3）Trehalose and plants essential oil are eventually adding, after stirring 1-10h, is stood up to the fertilizer
Soap.Saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed and once arrange by alkali twice and obtain fat
Pure soap base of the fat acid content more than 60%, uses the soap that technical solution of the present invention is prepared to be used as emulsification using natural fish oil
Agent, by the selection and optimization of component, effectively removes oil stain and spot, easily rinsing, gentle non-stimulated and raw materials used nontoxic
Property, production process is environmentally protective, has extensive market value.
Preferably, step（1）Described in sodium hydroxide solution pH be 8-10, fish oil and sodium hydroxide solution weight
Than for 1：2-10.
Preferably, step（1）Described in saponification carried out in the reaction pot equipped with steam openings.
Preferably, step（2）In, the ionized water added into soap base is the 60-90% of required deionization total Water, remaining
Under be used for adjust solution ph.
Preferably, step（2）In, the ionized water added into soap base carries out under the conditions of steam is turned over and boiled.
Preferably, the fish oil is refined to obtain by band fish pomace.It is environmentally protective using the leftover bits and pieces refinement fish oil of fish,
Belong to regenerative resource.
Therefore, the present invention has the advantages that：（1）Using natural fish oil as emulsifying agent, oil stain and dirt are effectively removed
Stain；（2）Easily rinsing, it is gentle non-stimulated；（3）Raw materials used nontoxicity, production process is environmentally protective, has extensive market price
Value.
Embodiment
Technical solution of the present invention is further described with reference to embodiment.
Embodiment 1：
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight：
25 parts of fish oil, 5 parts of sodium hydroxide, 1 part of alkyl-glucoside, 3 parts of trehalose, 2 parts of plants essential oil, 5 parts of glycerine are stearic
3 parts of acid, 60 parts of deionized water；
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps：By fish oil be provided with blender and
It is open in the reaction pot of steam and the sodium hydroxide solution progress saponification that pH is 8, the weight of fish oil and sodium hydroxide solution
Than for 1：2, saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed by alkali twice and once arranged
To pure soap base of the content of fatty acid more than 60%, deionized water is added in the case where steam is turned over and boiled with turn on agitator, is added
Water stops when reaching required total Water 80% plus water, treats that temperature reaches 70 DEG C and keeps, sequentially adds alkyl grape while stirring
Glucosides, glycerine, stearic acid, it is 7 to adjust pH value of solution, is eventually adding trehalose, plants essential oil, after stirring 1h, is stood up to institute
State soap.Under normal temperature and pressure, the cloth 30min of lard is infected with this product immersion, frequency is washed by rubbing with the hands and is maintained at 60 times/min, only
It is 20.8% to wash rate, and the pH of finished product is 7 in addition, and human skin is faintly acid, is not stimulated gently.
Embodiment 2：
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight：
30 parts of fish oil, 10 parts of sodium hydroxide, 3 parts of alkyl-glucoside, 1 part of trehalose, 0.5 part of plants essential oil, 1 part of glycerine,
1 part of stearic acid, 55 parts of deionized water；
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps：By fish oil be provided with blender and
It is open in the reaction pot of steam and the sodium hydroxide solution progress saponification that pH is 10, the weight of fish oil and sodium hydroxide solution
Than for 1：10, saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed by alkali twice and once arranged
Pure soap base of the content of fatty acid more than 60% is obtained, deionized water is added in the case where steam is turned over and boiled with turn on agitator,
Amount of water stops when reaching required total Water 90% plus water, treats that temperature reaches 80 DEG C and keeps, sequentially adds alkyl Portugal while stirring
Polyglycoside, glycerine, stearic acid, it is 6 to adjust pH value of solution, is eventually adding trehalose, plants essential oil, after stirring 10h, is stood to obtain the final product
The soap.The cloth 30min of lard is infected with this product immersion, frequency is washed by rubbing with the hands and is maintained at 60 times/min, washing rate is
25.3%, the pH of finished product is 6 in addition, and human skin is faintly acid, is not stimulated gently.
Embodiment 3：
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight：
27 parts of fish oil, 8 parts of sodium hydroxide, 2 parts of alkyl-glucoside, 2 parts of trehalose, 1 part of plants essential oil, 3 parts of glycerine are stearic
2 parts of acid, 57 parts of deionized water；
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps：By fish oil be provided with blender and
It is open in the reaction pot of steam and the sodium hydroxide solution progress saponification that pH is 9, the weight of fish oil and sodium hydroxide solution
Than for 1：6, saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed by alkali twice and once arranged
To pure soap base of the content of fatty acid more than 60%, deionized water is added in the case where steam is turned over and boiled with turn on agitator, is added
Water stops when reaching required total Water 60% plus water, treats that temperature reaches 75 DEG C and keeps, sequentially adds alkyl grape while stirring
Glucosides, glycerine, stearic acid, it is 6.5 to adjust pH value of solution, is eventually adding trehalose, plants essential oil, after stirring 5h, is stood to obtain the final product
The soap.The cloth 30min of lard is infected with this product immersion, frequency is washed by rubbing with the hands and is maintained at 60 times/min, washing rate is
23.5%, the pH of finished product is 6.5 in addition, and human skin is faintly acid, is not stimulated gently.
Claims (7)
1. a kind of soap suitable for sensitiveness skin, it is characterised in that be made from the following raw materials in parts by weight：
25-30 parts of fish oil
5-10 parts of sodium hydroxide
1-3 parts of alkyl-glucoside
1-3 parts of trehalose
0.5-2 parts of plants essential oil
1-5 parts of glycerine
1-3 parts of stearic acid
55-60 parts of deionized water.
A kind of 2. preparation method of soap suitable for sensitiveness skin according to claim 1, it is characterised in that including
Following steps：（1）Fish oil and sodium hydroxide solution are subjected to saponification 1-8h, then successively saltouts and is analysed with alkali, obtains fat
Pure soap base of the fat acid content more than 60%；（2）Deionized water is added when stirring soap base, when temperature reaches 70-80 DEG C,
Alkyl-glucoside, glycerine and stearic acid are sequentially added, adjusting pH value of solution is 6-7；（3）It is eventually adding trehalose and plant essence
Oil, after stirring 1-10h, stands up to the soap.
A kind of 3. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step
（1）Described in the pH of sodium hydroxide solution be 8-10, the weight ratio of fish oil and sodium hydroxide solution is 1：2-10.
A kind of 4. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step
（1）Described in saponification carried out in the reaction pot equipped with steam openings.
A kind of 5. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step
（2）In, the ionized water added into soap base is the 60-90% of required deionization total Water, remaining to be used to adjust solution ph.
A kind of 6. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step
（2）In, the ionized water added into soap base carries out under the conditions of steam is turned over and boiled.
7. a kind of preparation method of soap suitable for sensitiveness skin according to claim 1-6 any one, it is special
Sign is that the fish oil is refined to obtain by band fish pomace.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711251469.2A CN108004066A (en) | 2017-12-01 | 2017-12-01 | It is a kind of suitable for soap of sensitiveness skin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711251469.2A CN108004066A (en) | 2017-12-01 | 2017-12-01 | It is a kind of suitable for soap of sensitiveness skin and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108004066A true CN108004066A (en) | 2018-05-08 |
Family
ID=62056302
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711251469.2A Pending CN108004066A (en) | 2017-12-01 | 2017-12-01 | It is a kind of suitable for soap of sensitiveness skin and preparation method thereof |
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| CN (1) | CN108004066A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110577864A (en) * | 2019-08-13 | 2019-12-17 | 安徽天祥粮油食品有限公司 | Skin-moistening soap prepared by taking fish oil as animal fat |
| CN114717063A (en) * | 2022-01-13 | 2022-07-08 | 郑州工业应用技术学院 | Refining of tea seed oil soap base and preparation method of detergent thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1078258A (en) * | 1992-03-20 | 1993-11-10 | 普罗格特-甘布尔公司 | The neutral pH cleaning soap |
| CN104862131A (en) * | 2015-06-05 | 2015-08-26 | 浙江海洋学院 | Fruit and vegetable tableware detergent based on marine fish oil and preparation method thereof |
| CN104962408A (en) * | 2015-07-01 | 2015-10-07 | 浙江海洋学院 | Marine fish oil washing product and preparation method thereof |
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
| CN106318724A (en) * | 2016-08-19 | 2017-01-11 | 跨越生物科技（滁州）有限公司 | Moisturizing and toxin expelling congealed fat essential oil handmade soap |
-
2017
- 2017-12-01 CN CN201711251469.2A patent/CN108004066A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1078258A (en) * | 1992-03-20 | 1993-11-10 | 普罗格特-甘布尔公司 | The neutral pH cleaning soap |
| CN104862131A (en) * | 2015-06-05 | 2015-08-26 | 浙江海洋学院 | Fruit and vegetable tableware detergent based on marine fish oil and preparation method thereof |
| CN104962408A (en) * | 2015-07-01 | 2015-10-07 | 浙江海洋学院 | Marine fish oil washing product and preparation method thereof |
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
| CN106318724A (en) * | 2016-08-19 | 2017-01-11 | 跨越生物科技（滁州）有限公司 | Moisturizing and toxin expelling congealed fat essential oil handmade soap |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110577864A (en) * | 2019-08-13 | 2019-12-17 | 安徽天祥粮油食品有限公司 | Skin-moistening soap prepared by taking fish oil as animal fat |
| CN110577864B (en) * | 2019-08-13 | 2021-03-16 | 安徽天祥粮油食品有限公司 | Skin-moistening soap prepared by taking fish oil as animal fat |
| CN114717063A (en) * | 2022-01-13 | 2022-07-08 | 郑州工业应用技术学院 | Refining of tea seed oil soap base and preparation method of detergent thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180508 |