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CN107794016A - A kind of rejected well drilling liquid harmless treatment process and device - Google Patents

A kind of rejected well drilling liquid harmless treatment process and device Download PDF

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Publication number
CN107794016A
CN107794016A CN201711096481.0A CN201711096481A CN107794016A CN 107794016 A CN107794016 A CN 107794016A CN 201711096481 A CN201711096481 A CN 201711096481A CN 107794016 A CN107794016 A CN 107794016A
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CN
China
Prior art keywords
well drilling
rejected well
drilling liquid
liquid
harmless treatment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711096481.0A
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Chinese (zh)
Inventor
田玉芹
江少波
张雷
唐延彦
刘伟伟
陈雷
赵洪涛
刘巍
郭慧
唐培忠
衣哲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Research Institute of Petroleum Engineering Shengli Co
Original Assignee
China Petroleum and Chemical Corp
Sinopec Research Institute of Petroleum Engineering Shengli Co
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Publication date
Application filed by China Petroleum and Chemical Corp, Sinopec Research Institute of Petroleum Engineering Shengli Co filed Critical China Petroleum and Chemical Corp
Priority to CN201711096481.0A priority Critical patent/CN107794016A/en
Publication of CN107794016A publication Critical patent/CN107794016A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/50Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
    • C09K8/504Compositions based on water or polar solvents
    • C09K8/506Compositions based on water or polar solvents containing organic compounds
    • C09K8/508Compositions based on water or polar solvents containing organic compounds macromolecular compounds
    • C09K8/5086Compositions based on water or polar solvents containing organic compounds macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/50Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
    • C09K8/504Compositions based on water or polar solvents
    • C09K8/506Compositions based on water or polar solvents containing organic compounds
    • C09K8/508Compositions based on water or polar solvents containing organic compounds macromolecular compounds
    • C09K8/512Compositions based on water or polar solvents containing organic compounds macromolecular compounds containing cross-linking agents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/50Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
    • C09K8/504Compositions based on water or polar solvents
    • C09K8/506Compositions based on water or polar solvents containing organic compounds
    • C09K8/508Compositions based on water or polar solvents containing organic compounds macromolecular compounds
    • C09K8/514Compositions based on water or polar solvents containing organic compounds macromolecular compounds of natural origin, e.g. polysaccharides, cellulose
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B21/00Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
    • E21B21/06Arrangements for treating drilling fluids outside the borehole
    • E21B21/062Arrangements for treating drilling fluids outside the borehole by mixing components
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B21/00Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
    • E21B21/06Arrangements for treating drilling fluids outside the borehole
    • E21B21/063Arrangements for treating drilling fluids outside the borehole by separating components
    • E21B21/065Separating solids from drilling fluids

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Fluid Mechanics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention belongs to oilfield exploitation environmental protection treatment technical field, discloses a kind of rejected well drilling liquid harmless treatment process and device.The technique is mixed to prepare blocking agent including being carried out to rejected well drilling liquid except solid processing, and by the rejected well drilling liquid after removing admittedly with auxiliary agent;Described device includes skid and the solid-liquid separation unit being slidably disposed on the skid and mixes unit.Removing for the present invention need not add demulsifier in solid processing step, but with blocking agent injection stratum is directly prepared into after physical method simple process waste liquid, reduce the expense of processing, and can suppresses the water breakthrough of injection water, effectively improves water flooding effectiveness.The device of the present invention is skid structure, detachably, and it is easy to connect rapid, the pretreatment of rejected well drilling liquid can be realized and adjusted and blocked up, reduce the processing cost of rejected well drilling liquid, avoid environmental pollution, the blocking agent made from carries out stifled tune to oil-water well simultaneously, is advantageous to improve recovery ratio.

Description

A kind of rejected well drilling liquid harmless treatment process and device
Technical field
The invention belongs to oilfield exploitation environmental protection treatment technical field, and in particular to a kind of rejected well drilling liquid harmless treatment work Skill and device.
Background technology
Drilling fluid is a kind of circulation of fluid for drilling well, and in drilling well work, it is the blood of drilling well, is to ensure drilling well The indispensable material of normal operation, it, which has, carries suspension landwaste, balancing layer pressure, cooling and lubricating drill bit and drilling tool, clear The effect such as well-flushing bottom, the protection borehole wall and oil-gas Layer and raising bit speed, passing power.
Rejected well drilling liquid is caused pollutant in drilling process, such as:The landwaste discharged in drilling process and a small amount of drilling well The drilling fluid and kill-job for returning discharge when liquid, completion from pit shaft need that lays in be redrilled well liquid.Rejected well drilling liquid is a kind of multiphase Stable colloidal suspension system, main component are clay, weighting material, chemical treatments, sewage, sump oil, drilling cuttings etc., and it, which has, contains Water rate is high, and mobility is strong, and volume is big, extraction and separation wherein poisonous and harmful (heavy metal, acid, alkali, salt, greasy dirt, organic matter etc.) The characteristics such as polluter difficulty.The all places about more than 200 of rejected well drilling liquid caused by the annual drilling well in China oil field, if be stored in for a long time In the drilling fluid pot of well site or inevitable ground contamination surrounding environment and water source are understood in directly discharge, jeopardize the existence of the mankind, or even sternly Heavily contaminated land occupation prevents it to be lain waste from second ploughing.Therefore, caused rejected well drilling liquid need to be located in time in oilfield development process Reason.
The main processing ways of rejected well drilling liquid are complexing, consolidation drilling waste mud at present, averagely per square processing cost 500 Member or so, it is costly, though these methods can effectively handle rejected well drilling liquid, it is not inherently eliminated the hidden of environmental pollution Suffer from, and waste is caused to available resources.Discarded therefore, Chinese patent literature CN205618115U discloses a kind of drilling fluid Thing concentrate environment-friendly treatment method, its be by rejected well drilling liquid by vibratory sieve or respectively through vibratory sieve and deaerator, desander, remove For the solid waste obtained after mud device and centrifuge processing successively after de- steady, the separation of solid and liquid processing of broken glue, solid phase concentrates outward transport, liquid Mutually used after the reverse osmosis advanced processing mechanism processing of filtrate as drilling fluid reclamation liquid.The handling process is employed to discarded brill Demulsifier is added in well liquid, by chemical action, is aided with other separate modes and reaches the de- steady, demulsification of emulsion, realize oil breast point From purpose, but due to adding chemical addition agent, not only increase cost, and the performance meeting of the drilling fluid of recycling Degradation failure is simultaneously abandoned eventually, so as to also bring new environmental problem.If rejected well drilling liquid physical method can simply be located Blocking agent injection stratum is directly prepared into after reason, then had both reduced the expense of processing, does not produce new environmental pollution, and can suppresses injection The water breakthrough of water, water flooding effectiveness is effectively improved, realized " turning waste into wealth ", to promoting the production of oil field green low-carbon that there is weight Want meaning.
The content of the invention
Therefore, the technical problem to be solved in the present invention be to overcome present in existing waste drilling fluids disposal method into Hydraulic performance decline and the defects of pollution environment after this height, recovery, so as to provide a kind of pass through the letter of rejected well drilling liquid physical method Blocking agent is directly prepared into reduce the processing cost of rejected well drilling liquid, improve its performance and environmental pollution can be overcome after single processing Rejected well drilling liquid harmless treatment process and device.
In order to solve the above technical problems, the technical solution adopted by the present invention is as follows:
A kind of blocking agent, its raw material, which forms, includes rejected well drilling liquid and auxiliary agent, the grain of the Solid content in the rejected well drilling liquid Footpath is no more than 500 mesh.
Preferably, the mass ratio of the rejected well drilling liquid and the auxiliary agent is 5~15.
Preferably, the auxiliary agent is one kind in stabilizer, dispersant, suspending agent, crosslinking agent, thickener, retarder It is or a variety of.
Preferably, counted using the quality of the rejected well drilling liquid as 100%, the stabilizer, dispersant, the matter of thickener It is respectively 0.05~1%, 0.05~0.25%, 0.05~0.2% to measure accounting
It is further preferred that
The stabilizer is the one or more such as sodium carbonate, sodium hydroxide, small molecule amine;
The dispersant is lignosulfonates, fluosilicic thinner, the one or more of silicate;
The crosslinking agent is phenolic resin, Lauxite, the one or more of organic amine-lactic acid chromium;
The thickener is high viscous CMC, high adhesive aggregation anionic cellulose, the one or more of starch;
The retarder is citric acid, sodium gluconate, the one or more of carboxymethyl cellulose.
A kind of rejected well drilling liquid harmless treatment process, comprises the following steps:
Rejected well drilling liquid is carried out except solid processing, so that wherein the particle diameter of Solid content is no more than 500 mesh;
Rejected well drilling liquid after removing admittedly is mixed with auxiliary agent, blocking agent is made.
Preferably, the mass ratio of the rejected well drilling liquid and the auxiliary agent is 5~15.
Preferably, the auxiliary agent is the one or more in stabilizer, dispersant, crosslinking agent, thickener, retarder.
Preferably, counted using the quality of the rejected well drilling liquid as 100%, the stabilizer, dispersant, the matter of thickener It is respectively 0.05~1%, 0.05~0.25%, 0.05~0.2% to measure accounting.
It is further preferred that
The stabilizer is the one or more such as sodium carbonate, sodium hydroxide, small molecule amine;
The dispersant is lignosulfonates, fluosilicic thinner, the one or more of silicate;
The crosslinking agent is phenolic resin, Lauxite, the one or more of organic amine-lactic acid chromium;
The thickener is high viscous CMC, high adhesive aggregation anionic cellulose, the one or more of starch;
The retarder is citric acid, sodium gluconate, the one or more of carboxymethyl cellulose.
Preferably, described the step of removing processing admittedly, includes two-stage separation of solid and liquid, wherein liquid obtained by first order separation of solid and liquid The particle diameter of solid content in phase is no more than 50 mesh.
Preferably, in addition to by the solid phase except obtained by solid processing step the step of being used as sealing slug.
A kind of rejected well drilling liquid harmless treatment device, including,
Skid and the solid-liquid separation unit being slidably disposed on the skid and mixing unit, the solid-liquid point Leakage fluid dram from unit is connected with the mixing unit.
Preferably, the solid-liquid separation unit includes at least two-stage vibration sieve, bulky grain holding vessel and waste liquid tank, wherein The solid-phase outlet of primary vibration sieve is connected with the bulky grain holding vessel, liquid-phase outlet and the secondary vibration sieve of primary vibration sieve Charging aperture connects;The solid-phase outlet of the secondary vibration sieve connects the bulky grain holding vessel, the liquid phase of the secondary vibration sieve Outlet connects the waste liquid tank.
Preferably, the sieve aperture of the primary vibration sieve is 50~150 mesh;The sieve aperture of secondary vibration sieve for 500~ 1000 mesh.
Preferably, the solid-liquid separation unit also includes rejected well drilling liquid storage pool and feeding device, the discarded brill Well liquid storage pool is connected by the first Transmission system with the feeding device;The feeding device connects the primary vibration sieve.
Preferably, the unit that mixes includes agitator tank and auxiliary agent adding apparatus that connection is set, the stirring Tank is connected by the second Transmission system with the waste liquid tank.
Preferably, the mixing unit also includes high-pressure water pipe, the agitator tank and the auxiliary agent adding apparatus Connected by the high-pressure water pipe.
Preferably, the discharging opening of the agitator tank is connected by the 3rd Transmission system with well head.
More there is choosing, first Transmission system, the second Transmission system and the 3rd Transmission system are high-pressure pump.
Rejected well drilling liquid harmless treatment process described above or described rejected well drilling liquid harmless treatment device exist Application in rejected well drilling liquid recycling, oilwell water shutoff or drilling leakage blockage.
Technical solution of the present invention, have the following advantages that:
1. rejected well drilling liquid harmless treatment process provided by the invention include by rejected well drilling liquid carry out except solid processing with The particle diameter of wherein Solid content is no more than 500 mesh and the rejected well drilling liquid after removing admittedly is mixed to the step of blocking agent with auxiliary agent Suddenly, except in solid processing step without add demulsifier into rejected well drilling liquid, but with directly being made after physical method simple process Stratum is injected into blocking agent, had both reduced the expense of processing, does not produce new environmental pollution, and can suppresses the water breakthrough of injection water, had Water flooding effectiveness is improved to effect, is realized " turning waste into wealth ", to promoting green low-carbon production in oil field significant.
2. the invention provides the device of waste liquid drilling fluid harmless treatment, described device includes solid-liquid separation unit and mixed Agitating unit is closed, the solid-liquid separation unit carries out physical treatment to rejected well drilling liquid, and solid bulky grain is sent into bulky grain storage Tank, in order to be used as well site sealing slug, fine particle and liquid feeding mixing unit are prepared into blocking agent and pass through pump Inject well head.Described device is skid structure, detachably, and it is easy to connect rapid, it is possible to achieve the pretreatment of rejected well drilling liquid And adjust and block up, reduce the processing cost of rejected well drilling liquid, avoid environmental pollution, while blocking agent made from utilization is entered to oil-water well Row is stifled to be adjusted, and is advantageous to improve recovery ratio.
Brief description of the drawings
, below will be to specific in order to illustrate more clearly of the specific embodiment of the invention or technical scheme of the prior art The required accompanying drawing used is briefly described in embodiment or description of the prior art, it should be apparent that, in describing below Accompanying drawing is some embodiments of the present invention, for those of ordinary skill in the art, before creative work is not paid Put, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the structural representation of rejected well drilling liquid harmless treatment device of the present invention;
Fig. 2 is the well location map for simulating well LPP1-46.
Reference:
1- rejected well drilling liquid storage pools;The Transmission systems of 2- first;3- feeding devices;4- primary vibrations sieve;5- primary vibrations The solid-phase outlet of sieve;The liquid-phase outlet of 6- primary vibrations sieve;7- secondary vibrations are sieved;The solid-phase outlet of 8- secondary vibrations sieve;9- bis- The liquid-phase outlet of level vibratory sieve;10- bulky grain holding vessels;11- waste liquid tanks;The Transmission systems of 12- second;13- agitator tanks;14- is helped Agent feeding device;15- discharging openings;The Transmission systems of 16- the 3rd;17- well heads;18- high-pressure water pipes.
Embodiment
Technical scheme will be clearly and completely described below, it is clear that described embodiment is this hair Bright part of the embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not having There is the every other embodiment made and obtained under the premise of creative work, belong to the scope of protection of the invention.In addition, below As long as it is mutual not form conflict can each other for involved technical characteristic in described different embodiments of the present invention With reference to.
Embodiment 1
A kind of rejected well drilling liquid harmless treatment process, comprises the following steps:
S1, the rejected well drilling liquid being stored in rejected well drilling liquid storage pool 1 enter one after being sent into feeding device 3 by pump 2 Level vibratory sieve 4;The sieve aperture of the primary vibration sieve 4 is 50 mesh, and gained solid is sent into bulky grain holding vessel 10, gained liquid portion Into secondary vibration sieve 7;The sieve aperture of the secondary vibration sieve 7 is 500 mesh, and gained solid is sent into bulky grain holding vessel 10 and is used as envelope Mouth slug, gained liquid portion enter waste liquid tank 9;
Waste liquid in S2, waste liquid tank 9 is sent into agitator tank 13 by pump 12, and auxiliary agent passes through auxiliary agent in the presence of water under high pressure The note agitator tank 13 of feeding device 14, the blocking agent is produced after stirring 20min;
S3, the blocking agent are directly injected into underground by pump 16.
In the present embodiment, the mass ratio of the rejected well drilling liquid and the auxiliary agent is 5:1, the composition of the auxiliary agent is: Na2CO30.05wt%, Na2SiO30.05wt%, phenolic resin 0.08wt%, starch 0.2wt%, sodium gluconate 0.1wt%.
Embodiment 2
A kind of rejected well drilling liquid harmless treatment process, comprises the following steps:
S1, the rejected well drilling liquid being stored in rejected well drilling liquid storage pool 1 enter one after being sent into feeding device 3 by pump 2 Level vibratory sieve 4;The sieve aperture of the primary vibration sieve 4 is 100 mesh, and gained solid is sent into bulky grain holding vessel 10, gained liquid portion Divide and enter secondary vibration sieve 7;The sieve aperture of the secondary vibration sieve 7 is 800 mesh, and gained solid is sent into bulky grain holding vessel 10 and is used as Slug is sealed, gained liquid portion enters waste liquid tank 9;
Waste liquid in S2, waste liquid tank 9 is sent into agitator tank 13 by pump 12, and auxiliary agent passes through auxiliary agent in the presence of water under high pressure The note agitator tank 13 of feeding device 14, the blocking agent is produced after stirring 25min;
S3, the blocking agent are directly injected into underground by pump 16.
In the present embodiment, the mass ratio of the rejected well drilling liquid and the auxiliary agent is 10:1, the composition of the auxiliary agent is: NaOH 0.5wt%, sodium lignin sulfonate 0.1wt%, Lauxite 0.1wt%, sodium carboxymethylcellulose 0.1wt%, citric acid 0.05wt%.
Embodiment 3
A kind of rejected well drilling liquid harmless treatment process, comprises the following steps:
S1, the rejected well drilling liquid being stored in rejected well drilling liquid storage pool 1 enter one after being sent into feeding device 3 by pump 2 Level vibratory sieve 4;The sieve aperture of the primary vibration sieve 4 is 150 mesh, and gained solid is sent into bulky grain holding vessel 10, gained liquid portion Divide and enter secondary vibration sieve 7;The sieve aperture of the secondary vibration sieve 7 is 1000 mesh, and gained solid is sent into bulky grain holding vessel 10 and used Make sealing slug, gained liquid portion enters waste liquid tank 9;
Waste liquid in S2, waste liquid tank 9 is sent into agitator tank 13 by pump 12, and auxiliary agent passes through auxiliary agent in the presence of water under high pressure The note agitator tank 13 of feeding device 14, the blocking agent is produced after stirring 28min;
S3, the blocking agent are directly injected into underground by pump 16.
In the present embodiment, the mass ratio of the rejected well drilling liquid and the auxiliary agent is 15:1, the composition of the auxiliary agent is:1, 2- cyclohexanediamine 0.05wt%, Perfluoropolyether amide sodium sulfonate heavy crude thinner ANF 0.25wt%, phenolic resin 0.08wt%, Polyanion cellulose 0.05wt%, carboxymethyl cellulose 0.1wt%.
Embodiment 4
A kind of rejected well drilling liquid harmless treatment process, comprises the following steps:
S1, the rejected well drilling liquid being stored in rejected well drilling liquid storage pool 1 enter one after being sent into feeding device 3 by pump 2 Level vibratory sieve 4;The sieve aperture of the primary vibration sieve 4 is 150 mesh, and gained solid is sent into bulky grain holding vessel 10, gained liquid portion Divide and enter secondary vibration sieve 7;The sieve aperture of the secondary vibration sieve 7 is 1000 mesh, and gained solid is sent into bulky grain holding vessel 10 and used Make sealing slug, gained liquid portion enters waste liquid tank 9;
Waste liquid in S2, waste liquid tank 9 is sent into agitator tank 13 by pump 12, and auxiliary agent passes through auxiliary agent in the presence of water under high pressure The note agitator tank 13 of feeding device 14, the blocking agent is produced after stirring 22min;
S3, the blocking agent are directly injected into underground by pump 16.
In the present embodiment, the mass ratio of the rejected well drilling liquid and the auxiliary agent is 10:1, the composition of the auxiliary agent is: Na2CO31wt%, potassium silicate 0.2wt%, starch 0.1wt%.
Embodiment 5
Rejected well drilling liquid harmless treatment device as shown in Figure 1, including skid and it is slidably disposed in the skid On solid-liquid separation unit and mix unit.
The solid-liquid separation unit includes rejected well drilling liquid storage pool 1, feeding device 3, primary vibration sieve 4 and secondary vibration Sieve 5, bulky grain holding vessel 10 and waste liquid tank 11, the rejected well drilling liquid storage pool 1 pass through high-pressure pump 2 and the feeding device 3 Connection;The feeding device 3 connects the primary vibration sieve 4;The solid-phase outlet 5 of the primary vibration sieve is stored up with the bulky grain Deposit tank 10 to connect, the liquid-phase outlet 6 of primary vibration sieve is connected with secondary vibration sieve 5;The solid-phase outlet 8 of the secondary vibration sieve connects The bulky grain holding vessel 10 is connect, the liquid-phase outlet 9 of the secondary vibration sieve connects the waste liquid tank 11.
In the present embodiment, the sieve aperture of the primary vibration sieve is 100 mesh, and the sieve aperture of the secondary vibration sieve is 800 mesh.
The unit that mixes includes agitator tank 13, auxiliary agent adding apparatus 14 and high-pressure water pipe 18 that connection is set, institute Agitator tank 13 is stated to connect with the waste liquid tank 11 by the second Transmission system 12;The agitator tank 13 and the auxiliary agent adding apparatus 14 are connected by the pump 18;The discharging opening 15 of the agitator tank 13 is connected by pump 16 with well head 17.
The operation principle of the rejected well drilling liquid harmless treatment device of the present invention is as follows:
Rejected well drilling liquid in the rejected well drilling liquid storage pool 1 is sent into the primary vibration sieve 4 by pump 2.By described The solid bulky grain that primary vibration sieve 4 is separated is sent into the bulky grain holding vessel 10, and remaining is sent into the secondary vibration In sieve 7.The bulky grain holding vessel 10 is equally sent into by the bulky grain after the filtering of secondary vibration sieve 7, in order to as well Field sealing slug is used, and waste liquid and fine particle are sent into the waste liquid tank 11.Waste liquid in the waste liquid tank 11 passes through pump 12 It is pumped into agitator tank 13, various auxiliary agents is added by additive feeding device 14, by under the injection well of pump 16 after stirs.
The rejected well drilling liquid harmless treatment device of the present embodiment is used without adding demulsifier into rejected well drilling liquid Blocking agent injection stratum is directly prepared into after physical method simple process rejected well drilling liquid.
Above-described embodiment is the preferable implementation of the present invention, and in addition, the present invention can be realized with other modes, Such as:Form and connected using the mode such as lock, screw thread, spline between each component of described device or grafting, to realize the device Convenient installation or removal.
The device of the present invention is established according to the demand of Oil Field, is solved annual Shengli Oil Field and is played new well generation The problem of a few all places dumping mud treatment difficulties, discarded slurry pollution surrounding environment, underground water source and shared soil are avoided, together The average processing costs per 500 yuan or so of side of Shi Jieyue, the purposes of " turn waste into wealth " is realized again.Discarded slurry is injected into ground Layer, both reduces processing cost, and and can suppresses injection water water breakthrough, is effectively improved water flooding effectiveness, meets field application demand.
Experimental example 1
Below by taking lonely southern 2-X701 wells rejected well drilling liquid as an example, it is made into blocking agent and applied to LPP1-46 simulation wells, leads to The creation data of the simulation well is crossed to illustrate the rejected well drilling liquid harmless treatment process of the present invention and device in profile control construction Effect.
The solid content of lonely southern 2-X701 wells rejected well drilling liquid is 24.14%, density 1.284g/cm3, pH value is 10.739, viscosity 200mPa.s, 32.1 μm of median grain diameter.LPP1-46 well locations are in facing the unit of disk oil recovery list price one, the sand three of disk 1 Lower mean permeability 204.2 × 10-3um2, 75 DEG C, strata pressure 16.9MPa of prime stratum temperature, formation water salinity 40000-50000mg/L, hypotonic, high salinity reservoir in category, the lower wall top structural map of one block of sand of which disk three is see Fig. 2.
After lonely southern 2-X701 wells finishing drilling, the device that is provided using embodiment 5 and according to the technique described in embodiment 1 to Gu Nan The rejected well drilling liquid of 2-X701 wells is handled, and obtained blocking agent is injected into simulation underground, coarse granule is as sealing slug injection. After the completion of profile control construction, lonely southern 2-X701 well pressures are improved and pressure decline becomes slow, and water content is decreased obviously, and shows Gu Nan The profile control of 2-X701 wells is very effective.
Obviously, above-described embodiment is only intended to clearly illustrate example, and is not the restriction to embodiment.It is right For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or Among changing still in the protection domain of the invention.

Claims (21)

1. a kind of blocking agent, it is characterised in that its raw material, which forms, includes rejected well drilling liquid and auxiliary agent, consolidating in the rejected well drilling liquid The particle diameter of inclusion is no more than 500 mesh.
2. blocking agent according to claim 1, it is characterised in that the mass ratio of the rejected well drilling liquid and the auxiliary agent is 5 ~15.
3. blocking agent according to claim 1 or 2, it is characterised in that the auxiliary agent is stabilizer, dispersant, crosslinking agent, increasing Thick dose, the one or more in retarder.
4. blocking agent according to claim 3, it is characterised in that counted using the quality of the rejected well drilling liquid as 100%, it is described Stabilizer, dispersant, the quality accounting of thickener are respectively 0.05~1%, 0.05~0.25%, 0.05~0.2%.
5. the blocking agent according to claim 3 or 4, it is characterised in that
The stabilizer is the one or more such as sodium carbonate, sodium hydroxide, small molecule amine;
The dispersant is lignosulfonates, fluosilicic thinner, the one or more of silicate;
The crosslinking agent is phenolic resin, Lauxite, the one or more of organic amine-lactic acid chromium;
The thickener is high viscous CMC, high adhesive aggregation anionic cellulose, the one or more of starch;
The retarder is citric acid, sodium gluconate, the one or more of carboxymethyl cellulose.
6. a kind of rejected well drilling liquid harmless treatment process, it is characterised in that comprise the following steps:
Rejected well drilling liquid is carried out except solid processing, so that wherein the particle diameter of Solid content is no more than 500 mesh;
Rejected well drilling liquid after removing admittedly is mixed with auxiliary agent, blocking agent is made.
7. rejected well drilling liquid harmless treatment process according to claim 6, it is characterised in that the rejected well drilling liquid with The mass ratio of the auxiliary agent is 5~15.
8. the rejected well drilling liquid harmless treatment process according to claim 6 or 7, it is characterised in that the auxiliary agent is steady Determine the one or more in agent, dispersant, crosslinking agent, thickener, retarder.
9. rejected well drilling liquid harmless treatment process according to claim 8, it is characterised in that with the rejected well drilling liquid Quality be 100% meter, the stabilizer, dispersant, the quality accounting of thickener be respectively 0.05~1%, 0.05~ 0.25%th, 0.05~0.2%.
10. rejected well drilling liquid harmless treatment process according to claim 8 or claim 9, it is characterised in that
The stabilizer is the one or more such as sodium carbonate, sodium hydroxide, small molecule amine;
The dispersant is lignosulfonates, fluosilicic thinner, the one or more of silicate;
The crosslinking agent is phenolic resin, Lauxite, the one or more of organic amine-lactic acid chromium;
The thickener is high viscous CMC, high adhesive aggregation anionic cellulose, the one or more of starch;
The retarder is citric acid, sodium gluconate, the one or more of carboxymethyl cellulose.
11. according to the rejected well drilling liquid harmless treatment process described in claim any one of 6-10, it is characterised in that described to remove Admittedly the step of processing includes two-stage separation of solid and liquid, the particle diameter of the wherein solid content in liquid phase obtained by first order separation of solid and liquid is no more than 50 mesh.
12. according to the rejected well drilling liquid harmless treatment process described in claim any one of 6-11, it is characterised in that also include The step of solid phase except obtained by solid processing step is used as sealing slug.
A kind of 13. rejected well drilling liquid harmless treatment device, it is characterised in that including,
Skid and the solid-liquid separation unit being slidably disposed on the skid and mixing unit, the separation of solid and liquid list The leakage fluid dram of member is connected with the mixing unit.
14. rejected well drilling liquid harmless treatment device according to claim 13, it is characterised in that the separation of solid and liquid list Member includes the solid-phase outlet (5) of at least two-stage vibration sieve, bulky grain holding vessel (10) and waste liquid tank (11), wherein primary vibration sieve It is connected with the bulky grain holding vessel (10), the liquid-phase outlet (6) of primary vibration sieve is connected with secondary vibration sieve (7);Described two The solid-phase outlet (8) of level vibratory sieve connects the bulky grain holding vessel (10), liquid-phase outlet (9) connection of the secondary vibration sieve The waste liquid tank (11).
15. rejected well drilling liquid harmless treatment device according to claim 14, it is characterised in that the primary vibration sieve Sieve aperture be 50~150 mesh;The sieve aperture of the secondary vibration sieve is 500~1000 mesh.
16. rejected well drilling liquid harmless treatment device according to claim 13, it is characterised in that the separation of solid and liquid list Member also includes rejected well drilling liquid storage pool (1) and feeding device (3), and the rejected well drilling liquid storage pool (1) passes through the first transmission System (2) connects with the feeding device (3);The feeding device (3) connects the primary vibration sieve (4).
17. according to the rejected well drilling liquid harmless treatment device described in claim any one of 13-16, it is characterised in that described Mixing unit includes agitator tank (13) and auxiliary agent adding apparatus (14) that connection is set, and the agitator tank (13) passes through second Transmission system (12) connects with the waste liquid tank (11).
18. rejected well drilling liquid harmless treatment device according to claim 17, it is characterised in that described to mix list Member also includes high-pressure water pipe (18), and the agitator tank (13) passes through the high-pressure water pipe (18) with the auxiliary agent adding apparatus (14) Connection.
19. the rejected well drilling liquid harmless treatment device according to claim 17 or 18, it is characterised in that the agitator tank (13) discharging opening (15) is connected by the 3rd Transmission system (16) with well head (17).
20. according to the rejected well drilling liquid harmless treatment device described in claim any one of 13-19, it is characterised in that described First Transmission system (2), the second Transmission system (12) and the 3rd Transmission system (16) are high-pressure pump.
21. any one of rejected well drilling liquid harmless treatment process or claim 13-20 described in claim any one of 6-12 Described rejected well drilling liquid harmless treatment device answering in rejected well drilling liquid recycling, oilwell water shutoff or drilling leakage blockage With.
CN201711096481.0A 2017-11-09 2017-11-09 A kind of rejected well drilling liquid harmless treatment process and device Pending CN107794016A (en)

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CN110964490B (en) * 2019-10-30 2022-01-21 中国石油化工股份有限公司 Plugging adjusting system containing waste drilling fluid and preparation method thereof

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