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CN107782882A - The method of inspection of pin hole inside a kind of composite coating - Google Patents

The method of inspection of pin hole inside a kind of composite coating Download PDF

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Publication number
CN107782882A
CN107782882A CN201710940365.6A CN201710940365A CN107782882A CN 107782882 A CN107782882 A CN 107782882A CN 201710940365 A CN201710940365 A CN 201710940365A CN 107782882 A CN107782882 A CN 107782882A
Authority
CN
China
Prior art keywords
composite coating
pin hole
coating
inspection
brassboard
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710940365.6A
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Chinese (zh)
Inventor
徐峥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI 3N CHEMICALS CO Ltd
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SHANGHAI 3N CHEMICALS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANGHAI 3N CHEMICALS CO Ltd filed Critical SHANGHAI 3N CHEMICALS CO Ltd
Priority to CN201710940365.6A priority Critical patent/CN107782882A/en
Publication of CN107782882A publication Critical patent/CN107782882A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/38Concrete; Lime; Mortar; Gypsum; Bricks; Ceramics; Glass
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/04Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
    • G01M3/06Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point by observing bubbles in a liquid pool

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Materials By The Use Of Optical Means Adapted For Particular Applications (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The invention discloses a kind of method of inspection of pin hole inside composite coating, comprise the following steps:S1 the brassboard of composite coating first) is subjected to bound edge processing;S2) and then the brassboard of composite coating is immersed into petrolic solvent to be soaked;S3) in immersion process, if bubble from top layer emerges out, then judge pin hole be present inside composite coating.The method of inspection of pin hole inside composite coating provided by the invention, fast and effeciently judge whether coat inside has pin hole by way of solvent soaking, so as to greatly improve efficiency of the coating research and development engineer in early stage product formula R&D process, satisfactory coating products are quickly filtered out.

Description

The method of inspection of pin hole inside a kind of composite coating
Technical field
The present invention relates to a kind of a kind of inspection of pin hole inside composite coating quality inspection method, more particularly to composite coating Method.
Background technology
In modern coatings industry, the quality of film dry film directly reflects the quality of coating quality, and coating is in work progress In generally have many paint film defects, such as a shrinkage cavity, flake, cracking, sagging, bubble pin hole etc., some defects obviously may be used With the naked eye to judge, it can not be difficult with the naked eye to be identified in other words to also have quite a few defect.Such as bubble pin hole, substantially On can not possibly be by being visually identified, this requires to need the analytical equipment of specialty and instrument is detected, and among these Many methods have they itself the defects of, equipment cost, the problems such as time cost etc..Therefore, it is necessary to provide a kind of quick high The detection means of effect differentiates whether film is defective.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of method of inspection of pin hole inside composite coating, can be quick Effectively judge whether coat inside has pin hole, greatly improve the screening efficiency of qualified coating products, quickly filter out and conform to The coating products asked.
The present invention is to provide pin hole inside a kind of composite coating to solve the technical scheme that above-mentioned technical problem uses The method of inspection, comprise the following steps:S1 the brassboard of composite coating first) is subjected to bound edge processing;S2) and then by composite coating Brassboard immerses petrolic solvent and soaked;S3) in immersion process, if bubble from top layer emerges out, then judge compound Pin hole be present in coat inside.
The method of inspection of pin hole inside above-mentioned composite coating, wherein, the composite coating include prime coat, floating coat and Finish paint figure layer;The step S2) in the 2/3 of the brassboard of composite coating is immersed in petrolic solvent, soak time is 25~35 Minute.
The method of inspection of pin hole inside above-mentioned composite coating, wherein, the step S2) in composite coating brassboard Soak time is 30 minutes.
The method of inspection of pin hole inside above-mentioned composite coating, wherein, the step S2) in be mixed with stone in petrolic solvent Oil solvent oil and ethyl acetate, the mass percent of each component are as follows:No. 92 gasoline 70%, No. 150 solvent naphthas 15%, No. 100 Solvent naphtha 10%, ethyl acetate 5%.
The method of inspection of pin hole inside above-mentioned composite coating, wherein, the prime coat is electrophoretic coating, thickness 18- 22um;The floating coat is polyurethane coating, acrylic acid coatings or epoxy coating, thickness 25-35um;The top coat layer is poly- Urethane coating or acrylic acid coatings, thickness 20-30um.
Present invention contrast prior art has following beneficial effect:The inspection of pin hole inside composite coating provided by the invention Method, fast and effeciently judge whether coat inside has pin hole by way of solvent soaking, so as to greatly improve coating Efficiency of the engineer in early stage product formula R&D process is researched and developed, quickly filters out satisfactory coating products.
Brief description of the drawings
Fig. 1 is the inspection process schematic diagram of pin hole inside composite coating of the present invention.
Embodiment
The invention will be further described with reference to the accompanying drawings and examples.
General complete coating system includes prime coat, floating coat and finish paint figure layer, and the prime coat is electrophoretic coating, film Thickness is 18-22um;The floating coat is polyurethane coating, acrylic acid coatings or epoxy coating, thickness 25-35um;The face Enamelled coating is polyurethane coating or acrylic acid coatings, thickness 20-30um.When outermost surface seems smooth, then can not often lead to Whether cross naked eyes and quickly observe inside figure layer has pin hole (for example sometimes floating coat has pin hole, and finish paint figure layer does not have pin The such case in hole).In order to remove finish paint figure layer, method that the present invention selects boiling water boiling first, with boiling water boiling 2 hours, if There is bubble to emerge out from top layer, then judge pin hole be present inside composite coating.But the method for boiling water boiling compares the consuming time, And waste the energy.
Then the present invention is considered as organic solvent and removes finish paint figure layer, but often dissolved destruction is whole for organic solvent Coating system, it is therefore desirable to prepare a kind of dedicated solvent.Refer to Fig. 1, the inspection of composite coating inside provided by the invention pin hole Proved recipe method, comprises the following steps:
S1 the brassboard of composite coating first) is subjected to bound edge processing.
S2) and then the brassboard of composite coating is immersed into petrolic solvent to be soaked;It is molten that oil is mixed with petrolic solvent Agent oil and ethyl acetate, the mass percent of each component are as follows:No. 92 gasoline 70%, No. 150 solvent naphthas 15%, No. 100 solvents Oil 10%, ethyl acetate 5%.
S3) in immersion process, if bubble from top layer emerges out, then judge pin hole be present inside composite coating.Leaching Preferably the 2/3 of the brassboard of composite coating is immersed in petrolic solvent during bubble, so as to the experiment to invading the front and rear composite coating of bubble Plate is compared;Soak time is 25~35 minutes, preferably 30 minutes.After immersion about 30 minutes, visually observe, if internal When coating has pin hole and covered by topcoat, by immersion, bubble can emerge out from top layer, and directly available naked eyes are distinguished Know.Experiment finishes taking-up test plate (panel), the pin hole that surface can not visually identify, then illustrates coat inside also without pin hole (including middle painting And priming paint), the compactness of coating is relatively good.
The present invention can fast and effectively filter out some undesirable products, greatly improve operating efficiency;Reduce real The time spent in testing the experiment and analysis of room tester, it is not necessary to quick succinct effective using analytical instrument.
Although the present invention is disclosed as above with preferred embodiment, so it is not limited to the present invention, any this area skill Art personnel, without departing from the spirit and scope of the present invention, when a little modification and perfect, therefore the protection model of the present invention can be made Enclose to work as and be defined by what claims were defined.

Claims (5)

1. the method for inspection of pin hole inside a kind of composite coating, it is characterised in that comprise the following steps:
S1 the brassboard of composite coating first) is subjected to bound edge processing;
S2) and then the brassboard of composite coating is immersed into petrolic solvent to be soaked;
S3) in immersion process, if bubble from top layer emerges out, then judge pin hole be present inside composite coating.
2. the method for inspection of pin hole inside composite coating as claimed in claim 1, it is characterised in that the composite coating includes Prime coat, floating coat and finish paint figure layer;The step S2) in the 2/3 of the brassboard of composite coating is immersed in petrolic solvent, leaching It is 25~35 minutes to steep the time.
3. the method for inspection of pin hole inside composite coating as claimed in claim 2, it is characterised in that the step S2) in it is multiple The soak time for closing the brassboard of coating is 30 minutes.
4. the method for inspection of pin hole inside composite coating as claimed in claim 1, it is characterised in that the step S2) in vapour White spirit and ethyl acetate are mixed with oil solvent, the mass percent of each component is as follows:No. 92 gasoline 70%, No. 150 Solvent naphtha 15%, No. 100 solvent naphthas 10%, ethyl acetate 5%.
5. the method for inspection of pin hole inside composite coating as claimed in claim 1, it is characterised in that the prime coat is electrophoresis Coating, thickness 18-22um;The floating coat is polyurethane coating, acrylic acid coatings or epoxy coating, thickness 25-35um; The top coat layer is polyurethane coating or acrylic acid coatings, thickness 20-30um.
CN201710940365.6A 2017-10-11 2017-10-11 The method of inspection of pin hole inside a kind of composite coating Pending CN107782882A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710940365.6A CN107782882A (en) 2017-10-11 2017-10-11 The method of inspection of pin hole inside a kind of composite coating

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710940365.6A CN107782882A (en) 2017-10-11 2017-10-11 The method of inspection of pin hole inside a kind of composite coating

Publications (1)

Publication Number Publication Date
CN107782882A true CN107782882A (en) 2018-03-09

Family

ID=61434366

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710940365.6A Pending CN107782882A (en) 2017-10-11 2017-10-11 The method of inspection of pin hole inside a kind of composite coating

Country Status (1)

Country Link
CN (1) CN107782882A (en)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01276064A (en) * 1988-04-27 1989-11-06 Eagle Ind Co Ltd Detecting device for pin hole of plating
US5963040A (en) * 1997-09-24 1999-10-05 Taiwan Semiconductor Manufacturing Co. Ltd. Method and apparatus for detecting pin-holes in a passivation layer
CN201852681U (en) * 2010-11-18 2011-06-01 沈阳维用精密机械有限公司 Bubble leakage detection device
CN103364381A (en) * 2007-12-17 2013-10-23 生命技术公司 Methods for detecting defects in inorganic-coated polymer surfaces
CN103454297A (en) * 2013-09-02 2013-12-18 武汉钢铁(集团)公司 Method for identifying steel plate coating defect caused by coating liquid bubbles
CN103558338A (en) * 2013-10-12 2014-02-05 奇瑞汽车股份有限公司 Method for detecting pollutant causing contraction cavity on automobile finish
CN103630543A (en) * 2013-10-23 2014-03-12 航天材料及工艺研究所 Judgment method for detecting defects of wave absorption coating by using pulse infrared thermal waves
CN104387816A (en) * 2014-11-28 2015-03-04 佛山市南海万磊建筑涂料有限公司 Multifunctional inorganic diatom ooze coating and preparation method thereof
CN105277319A (en) * 2015-11-30 2016-01-27 四川南格尔生物科技有限公司 Seal head leakage detection device and method
CN105628865A (en) * 2014-11-07 2016-06-01 立邦涂料(中国)有限公司 Method for detecting hidden coating pit in composite coating

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01276064A (en) * 1988-04-27 1989-11-06 Eagle Ind Co Ltd Detecting device for pin hole of plating
US5963040A (en) * 1997-09-24 1999-10-05 Taiwan Semiconductor Manufacturing Co. Ltd. Method and apparatus for detecting pin-holes in a passivation layer
CN103364381A (en) * 2007-12-17 2013-10-23 生命技术公司 Methods for detecting defects in inorganic-coated polymer surfaces
CN201852681U (en) * 2010-11-18 2011-06-01 沈阳维用精密机械有限公司 Bubble leakage detection device
CN103454297A (en) * 2013-09-02 2013-12-18 武汉钢铁(集团)公司 Method for identifying steel plate coating defect caused by coating liquid bubbles
CN103558338A (en) * 2013-10-12 2014-02-05 奇瑞汽车股份有限公司 Method for detecting pollutant causing contraction cavity on automobile finish
CN103630543A (en) * 2013-10-23 2014-03-12 航天材料及工艺研究所 Judgment method for detecting defects of wave absorption coating by using pulse infrared thermal waves
CN105628865A (en) * 2014-11-07 2016-06-01 立邦涂料(中国)有限公司 Method for detecting hidden coating pit in composite coating
CN104387816A (en) * 2014-11-28 2015-03-04 佛山市南海万磊建筑涂料有限公司 Multifunctional inorganic diatom ooze coating and preparation method thereof
CN105277319A (en) * 2015-11-30 2016-01-27 四川南格尔生物科技有限公司 Seal head leakage detection device and method

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Application publication date: 20180309

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