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CN107745231A - A kind of preparation method of high-precision titanium copper composite bar - Google Patents

A kind of preparation method of high-precision titanium copper composite bar Download PDF

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Publication number
CN107745231A
CN107745231A CN201710942660.5A CN201710942660A CN107745231A CN 107745231 A CN107745231 A CN 107745231A CN 201710942660 A CN201710942660 A CN 201710942660A CN 107745231 A CN107745231 A CN 107745231A
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CN
China
Prior art keywords
titanium
titanium copper
preparation
composite bar
copper
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710942660.5A
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Chinese (zh)
Inventor
陈炳豊
王荣生
马宝全
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BAOJI YONGSHENGTAI TITANIUM INDUSTRY Co Ltd
Original Assignee
BAOJI YONGSHENGTAI TITANIUM INDUSTRY Co Ltd
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Publication date
Application filed by BAOJI YONGSHENGTAI TITANIUM INDUSTRY Co Ltd filed Critical BAOJI YONGSHENGTAI TITANIUM INDUSTRY Co Ltd
Priority to CN201710942660.5A priority Critical patent/CN107745231A/en
Publication of CN107745231A publication Critical patent/CN107745231A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23PMETAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
    • B23P15/00Making specific metal objects by operations not covered by a single other subclass or a group in this subclass

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Metal Extraction Processes (AREA)

Abstract

The invention discloses a kind of preparation method of high-precision titanium copper composite bar, prepared by sorting, poling, coating, heating, drawing, finishing, the several steps of polishing, sorting is chosen according to strict standard, control the temperature and time heated, polishing is roughly ground and refined using polishing equipment, ensures the combination property of titanium and copper composite bar.The titanium and copper composite bar manufactured using the inventive method, section is uniform, and titanium layer is bonded firmly with layers of copper, and surface accuracy is high, and roughness is good.

Description

A kind of preparation method of high-precision titanium copper composite bar
Technical field
The invention belongs to metal material processing technical field, is related to a kind of preparation method of high-precision titanium copper composite bar.
Background technology
The manufacture method of titanium and copper composite bar is mainly using being the manufacture methods such as explosion composite method, hot extrusion method at present, titanium copper The standard GB/T of compound bar/T 12769-2003 are exactly that a diameter of 20-60mm circles titanium is manufactured using above-mentioned manufacture method Copper compound bar, 20mm small-dimension titanium and copper composite bar is less than for diameter, China there is no corresponding national standard, technology not into Ripe and prepared titanium and copper composite bar precision is not high.
The surface treatment of titanium tube, there are three different technologies at present:When annealing and pickling, the heat-treatment of annealing after cold rolling, then Hydrofluoric acid and nitric acid acidwashing are carried out, allows its surface to lose silvery white gloss;Second, vacuum annealing, carries out vacuum annealing after cold rolling Processing, and after being straightened, make its surface that there is metallic luster;Third, decorative pattern extrudes, on the basis of annealing and pickling, machinery is utilized The mode of extrusion molding, the tangible decorative pattern of various bumps is formed in tube surfaces.Current so-called mirror finish, there is polishing, electricity Two kinds of solution polishing, polishing are with the sand paper on polishing wheel, tube surfaces is formed minute surface, this method at a high speed on polishing mechanical Waste time and energy, and surface roughness is very high, more than 8 μm, minute surface is relatively fuzzy;Electrobrightening is to be carried out on the basis of polishing at electrolysis Reason, can form glossy surface in the short time, single pair large area part, to realize that uniform mirror finish is hardly formed, because titanium is easy Oxidation, it is therefore necessary to apply high pressure, electrolyte can form oxide-film in moment in addition, and relatively hazardous, so typically seldom adding Work sector application.
The content of the invention
It is an object of the invention to provide a kind of preparation method of high-precision titanium copper composite bar, solves titanium and copper composite bar material The problem of surface accurate degree is low, roughness is insufficient.
The technical solution adopted in the present invention is a kind of preparation method of high-precision titanium copper composite bar, specifically according to Lower step is implemented:
Step 1, from meet the titanium tube of standard requirement, red copper bar is as blank;
Step 2, copper rod is through in titanium tube;
Step 3, graphite is uniformly applied to titanium tube outer wall and dried;
Step 4, titanium copper rod is put into electric furnace and heated, temperature is ensured between 700 DEG C -800 DEG C, is incubated 1 hour, supporting Suitable mould carries out drawing;
Step 5, burr, the crackle for removing titanium copper rod surface, cut off the position of titanium copper two end face out-of-flatnesses of rod;
Step 6, polishing processing is carried out, until the surface roughness of titanium copper rod is 8 μm or so.
The features of the present invention also resides in:
Equadag coating thickness is 0.2-0.4mm;
Drawing passes sizing reduction is 1.4-1.8mm;
Polishing processing is that bar is roughly ground and refined using grinding machine, reaches finished size requirement.
The beneficial effects of the invention are as follows by the titanium tube surface of titanium and copper composite bar coat graphite linings, in titanium and copper composite bar table Face forms layer oxide film, can improve the combination property of tubing, by strictly choosing blank, titanium and copper composite bar outer surface is entered The operations such as row heats, finishing and polishing processing, obtained titanium and copper composite bar precision is high, and roughness is good, up to 0.8 μm with Under.
Embodiment
With reference to embodiment, the present invention is described in detail.
A kind of preparation method of high precision titanium alloy composite bar of the present invention, specifically implements according to following steps:
Step 1, from meet the titanium tube of standard requirement, red copper bar is as blank;
Step 2, copper rod is through in titanium tube;
Step 3, graphite is uniformly applied to titanium tube outer wall and dried;
Step 4, titanium copper rod is put into electric furnace and heated, temperature is ensured between 700 DEG C -800 DEG C, is incubated 1 hour, supporting Suitable mould carries out drawing;
Step 5, burr, the crackle for removing titanium copper rod surface, cut off the position of titanium copper two end face out-of-flatnesses of rod;
Step 6, polishing processing is carried out, until the surface roughness of titanium copper rod is less than 8 μm.
Embodiment 1
From ISO5832-2 standards, trade mark TA1 is met, specification is 10 × 9200mm titanium tubes and meets GB4423, specification For 8 × Lmm red copper bar;Secondly titanium tube inwall is cleaned, red copper bar outer surface is cleared up, removes flash removed, is reached Circularity is uniform, and then red copper bar is through in titanium tube;Titanium tube surface is uniformly coated with aquadag, thickness 0.2mm, dried;By titanium Copper rod is placed in heating furnace, 700 DEG C of heating-up temperature, is incubated 1 hour;Supporting suitable mould progress drawing is compound, controls drawing Passage sizing reduction 1.4mm;The position of titanium copper rod both ends out-of-flatness is cut off, burr, the crackle on titanium copper rod surface is removed, is ground Light processing, trimmed size are 8.0 × 12000mm, and surface roughness is 0.75 μm.
Embodiment 2
From ISO5832-2 standards, trade mark TA1 is met, specification is 15 × 8500mm titanium tubes and meets GB4423, specification For 12 × Lmm red copper bar;Secondly titanium tube inwall is cleaned, red copper bar outer surface is cleared up, removes flash removed, is reached Circularity is uniform, and then red copper bar is through in titanium tube;Titanium tube surface is uniformly coated with aquadag, thickness 0.2mm, dried;By titanium Copper rod is placed in heating furnace, 720 DEG C of heating-up temperature, is incubated 1 hour;Supporting suitable mould progress drawing is compound, controls drawing Passage sizing reduction 1.5mm;The position of titanium copper rod both ends out-of-flatness is cut off, burr, the crackle on titanium copper rod surface is removed, is ground Light processing, trimmed size are 12.0 × 9600mm, and surface roughness is 0.7 μm.
Embodiment 3
From ISO5832-2 standards, trade mark TA1 is met, specification is 18 × 9230mm titanium tubes and meets GB4423, specification For 16 × Lmm red copper bar;Secondly titanium tube inwall is cleaned, red copper bar outer surface is cleared up, removes flash removed, is reached Circularity is uniform, and then red copper bar is through in titanium tube;Titanium tube surface is uniformly coated with aquadag, thickness 0.3mm, dried;By titanium Copper rod is placed in heating furnace, 750 DEG C of heating-up temperature, is incubated 1 hour;Supporting suitable mould progress drawing is compound, controls drawing Passage sizing reduction 1.6mm;The position of titanium copper rod both ends out-of-flatness is cut off, burr, the crackle on titanium copper rod surface is removed, is ground Light processing, trimmed size are 16.0 × 12300mm, and surface roughness is 0.75 μm.
Embodiment 4
From ISO5832-2 standards, trade mark TA1 is met, specification is 18 × 9230mm titanium tubes and meets GB4423, specification For 16 × Lmm red copper bar;Secondly titanium tube inwall is cleaned, red copper bar outer surface is cleared up, removes flash removed, is reached Circularity is uniform, and then red copper bar is through in titanium tube;Titanium tube surface is uniformly coated with aquadag, thickness 0.4mm, dried;By titanium Copper rod is placed in heating furnace, 780 DEG C of heating-up temperature, is incubated 1 hour;Supporting suitable mould progress drawing is compound, controls drawing Passage sizing reduction 1.8mm;The position of titanium copper rod both ends out-of-flatness is cut off, burr, the crackle on titanium copper rod surface is removed, is ground Light processing, trimmed size are 16.0 × 12300mm, and surface roughness is 0.7 μm.
Embodiment 5
From ISO5832-2 standards, trade mark TA1 is met, specification is 20 × 8500mm titanium tubes and meets GB4423, specification For 18 × Lmm red copper bar;Secondly titanium tube inwall is cleaned, red copper bar outer surface is cleared up, removes flash removed, is reached Circularity is uniform, and then red copper bar is through in titanium tube;Titanium tube surface is uniformly coated with aquadag, thickness 0.3mm, dried;By titanium Copper rod is placed in heating furnace, 800 DEG C of heating-up temperature, is incubated 1 hour;Supporting suitable mould progress drawing is compound, controls drawing Passage sizing reduction 1.4mm;The position of titanium copper rod both ends out-of-flatness is cut off, burr, the crackle on titanium copper rod surface is removed, is ground Light processing, trimmed size are 18.0 × 9500mm, and surface roughness is 0.75 μm.

Claims (4)

1. a kind of preparation method of high-precision titanium copper composite bar, it is characterised in that specifically implement according to following steps:
Step 1, from meet the titanium tube of standard requirement, red copper bar is as blank;
Step 2, copper rod is through in titanium tube;
Step 3, graphite is uniformly applied to titanium tube outer wall and dried;
Step 4, titanium copper rod is put into electric furnace and heated, temperature is ensured between 700 DEG C -800 DEG C, is incubated 1 hour, supporting suitable Mould carry out drawing;
Step 5, burr, the crackle for removing titanium copper rod surface, cut off the position of titanium copper two end face out-of-flatnesses of rod;
Step 6, polishing processing is carried out, until the surface roughness of titanium copper rod is less than 8 μm.
A kind of 2. preparation method of high-precision titanium copper composite bar according to claim 1, it is characterised in that the step 3 In equadag coating thickness be 0.2-0.4mm.
A kind of 3. preparation method of high-precision titanium copper composite bar according to claim 1, it is characterised in that the step 4 Middle drawing passes sizing reduction is 1.4-1.8mm.
A kind of 4. preparation method of high-precision titanium copper composite bar according to claim 1, it is characterised in that the step 6 Middle polishing processing is that bar is roughly ground and refined using grinding machine, reaches finished size requirement.
CN201710942660.5A 2017-10-11 2017-10-11 A kind of preparation method of high-precision titanium copper composite bar Pending CN107745231A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710942660.5A CN107745231A (en) 2017-10-11 2017-10-11 A kind of preparation method of high-precision titanium copper composite bar

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109013742A (en) * 2018-07-06 2018-12-18 苏州市金翔钛设备有限公司 A kind of processing technology of copper composite ti pipe material
CN113787311A (en) * 2021-09-14 2021-12-14 南通市荣泰电化学设备制造有限公司 Preparation process of titanium polar plate with firmly-adhered coating

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201030659Y (en) * 2007-04-05 2008-03-05 宝鸡市巨成钛业有限责任公司 Titanium copper composite rod
CN101138769A (en) * 2007-10-19 2008-03-12 宝鸡市英耐特医用钛有限公司 Method of preparing small-dimension titanium and copper composite bar
CN101698206A (en) * 2009-10-27 2010-04-28 宝鸡市巨成钛业有限责任公司 Technique for producing titanium-copper compound wire
CN102211270A (en) * 2011-04-06 2011-10-12 宝鸡鑫泽钛镍有限公司 Process for manufacturing high-precision titanium and titanium alloy tube
JP2015030910A (en) * 2013-08-06 2015-02-16 株式会社徳力本店 Composite wire material and production method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201030659Y (en) * 2007-04-05 2008-03-05 宝鸡市巨成钛业有限责任公司 Titanium copper composite rod
CN101138769A (en) * 2007-10-19 2008-03-12 宝鸡市英耐特医用钛有限公司 Method of preparing small-dimension titanium and copper composite bar
CN101698206A (en) * 2009-10-27 2010-04-28 宝鸡市巨成钛业有限责任公司 Technique for producing titanium-copper compound wire
CN102211270A (en) * 2011-04-06 2011-10-12 宝鸡鑫泽钛镍有限公司 Process for manufacturing high-precision titanium and titanium alloy tube
JP2015030910A (en) * 2013-08-06 2015-02-16 株式会社徳力本店 Composite wire material and production method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109013742A (en) * 2018-07-06 2018-12-18 苏州市金翔钛设备有限公司 A kind of processing technology of copper composite ti pipe material
CN113787311A (en) * 2021-09-14 2021-12-14 南通市荣泰电化学设备制造有限公司 Preparation process of titanium polar plate with firmly-adhered coating
CN113787311B (en) * 2021-09-14 2022-03-18 南通市荣泰电化学设备制造有限公司 Preparation process of titanium polar plate with firmly-adhered coating

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