CN107651934A - 一种骨瓷坯料 - Google Patents
一种骨瓷坯料 Download PDFInfo
- Publication number
- CN107651934A CN107651934A CN201710808668.2A CN201710808668A CN107651934A CN 107651934 A CN107651934 A CN 107651934A CN 201710808668 A CN201710808668 A CN 201710808668A CN 107651934 A CN107651934 A CN 107651934A
- Authority
- CN
- China
- Prior art keywords
- parts
- powder
- added
- bone china
- modifying agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 210000000988 bone and bone Anatomy 0.000 title claims abstract description 24
- 239000000843 powder Substances 0.000 claims abstract description 56
- 239000000919 ceramic Substances 0.000 claims abstract description 18
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 16
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 16
- 241001330002 Bambuseae Species 0.000 claims abstract description 16
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 16
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 16
- 239000004113 Sepiolite Substances 0.000 claims abstract description 16
- 239000011425 bamboo Substances 0.000 claims abstract description 16
- 239000003610 charcoal Substances 0.000 claims abstract description 16
- 239000010452 phosphate Substances 0.000 claims abstract description 16
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 16
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 16
- 229910052624 sepiolite Inorganic materials 0.000 claims abstract description 16
- 235000019355 sepiolite Nutrition 0.000 claims abstract description 16
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000001913 cellulose Substances 0.000 claims abstract description 15
- 229920002678 cellulose Polymers 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 38
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 28
- 239000000463 material Substances 0.000 claims description 24
- 238000002156 mixing Methods 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 14
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 14
- 235000012424 soybean oil Nutrition 0.000 claims description 14
- 239000003549 soybean oil Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 13
- 239000012188 paraffin wax Substances 0.000 claims description 13
- 239000006004 Quartz sand Substances 0.000 claims description 12
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 12
- 239000005864 Sulphur Substances 0.000 claims description 12
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 12
- 238000009413 insulation Methods 0.000 claims description 12
- 239000004200 microcrystalline wax Substances 0.000 claims description 12
- 229920001592 potato starch Polymers 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 11
- 229910007948 ZrB2 Inorganic materials 0.000 claims description 8
- VWZIXVXBCBBRGP-UHFFFAOYSA-N boron;zirconium Chemical compound B#[Zr]#B VWZIXVXBCBBRGP-UHFFFAOYSA-N 0.000 claims description 8
- 238000000465 moulding Methods 0.000 claims description 8
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- 238000005498 polishing Methods 0.000 claims description 5
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 4
- 229910052796 boron Inorganic materials 0.000 claims description 4
- 239000012752 auxiliary agent Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 abstract description 2
- 229910052573 porcelain Inorganic materials 0.000 description 5
- 238000000498 ball milling Methods 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 230000000149 penetrating effect Effects 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 239000010433 feldspar Substances 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1315—Non-ceramic binders
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3436—Alkaline earth metal silicates, e.g. barium silicate
- C04B2235/3445—Magnesium silicates, e.g. forsterite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/38—Non-oxide ceramic constituents or additives
- C04B2235/3804—Borides
- C04B2235/3813—Refractory metal borides
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
- C04B2235/422—Carbon
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/447—Phosphates or phosphites, e.g. orthophosphate or hypophosphite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5454—Particle size related information expressed by the size of the particles or aggregates thereof nanometer sized, i.e. below 100 nm
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/963—Surface properties, e.g. surface roughness
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dental Preparations (AREA)
- Materials For Medical Uses (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
一种骨瓷坯料，涉及陶瓷制造技术领域，本发明以活性白土为主要原料，再加入竹炭纤维素、海泡石粉，并配合了磷酸盐、水玻璃、纳米陶瓷粉等，并辅以多种助剂，制得的坯料细腻、光滑，具有优异的耐高温性和牢固性等，用于制作的骨瓷细腻、光泽、质感好，品质好。
Description
技术领域：
本发明涉及陶瓷制造技术领域，具体涉及一种骨瓷坯料。
背景技术：
骨瓷最早产生于英国，因其造型独特、简洁明快，质地洁白而细腻，长期以来一直是各国贵族用瓷，是目前唯一世界上公认的高档瓷种。骨质瓷产生于英国的一个高档瓷种，距今已有300多年的历史。因其“薄如纸、透如镜、声如磬、白如玉”，瓷质细腻通透，器型美观典雅，彩面润泽光亮，花面多姿多彩的特点，成就了它洁白的质地和华贵的造型，兼有使用和艺术的双重价值，历史上是宫廷专用品和贵族收藏之珍品。
骨质瓷是以动物的骨炭、粘土、长石和石英为基本原料，经过高温素烧和低温釉烧两次烧制而成的一种瓷器。由于骨瓷是以光亮、细腻、通透为美，因此骨瓷坯料的质量决定骨瓷的质量。
发明内容：
本发明所要解决的技术问题在于提供一种骨瓷坯料。
本发明所要解决的技术问题采用以下的技术方案来实现：
一种骨瓷坯料，由如下重量份数的原料制成：
活性白土25-30份、竹炭纤维素12-15份、海泡石粉10-15份、活性炭8-11份、磷酸盐6-10份、水玻璃5-8份、纳米陶瓷粉5-8份、粘黏剂4-6份、聚丙烯酸钠3-5份、改良剂4-6份、石蜡1-3份，环氧大豆油5-10份，二硼化锆1-2份、水100-150份。
进一步的，上述骨瓷坯料，优选以下重量份数的原料制成：
活性白土28份、竹炭纤维素14份、海泡石粉13份、活性炭9份、磷酸盐8份、水玻璃7份、纳米陶瓷粉6份、粘黏剂5份、聚丙烯酸钠4份、改良剂5份、石蜡2份，环氧大豆油8份，二硼化锆2份、水125份。
进一步的，所述改良剂由以下重量份的组分构成：土豆淀粉5-10份，河蚌壳粉3-6份，珍珠粉2-4份，石英砂1-3份，滑石粉2-4份，硫磺1-3份，微晶蜡2-4份。
进一步的，所述改良剂优选以下重量份的组分构成：土豆淀粉8份，河蚌壳粉5份，珍珠粉3份，石英砂2份，滑石粉3份，硫磺2份，微晶蜡3份。
其制备方法包括如下步骤：
(1)将活性白土、竹炭纤维素、海泡石粉、活性炭、纳米陶瓷粉充分混合，进行搅拌加热，加热至90-100℃保温静置10min，加入环氧大豆油，再继续搅拌加热至120-130℃保温静置5min，即得物料I；
(2)向水中加入磷酸盐、水玻璃、聚丙烯酸钠、石蜡、二硼化锆均匀混合，浸泡30分钟，加热至回流状态保温处理15min，再加入粘黏剂，继续保温处理10min，即得物料II；
(3)向物料I中加入物料II、改良剂，充分混合均匀，加入球磨机中，球磨至细度小于20μm；
(4)将打磨后的混合物加入搅拌机中进行搅拌加热，搅拌速度为600-800r/min，加热温度为120-150度；
(5)将搅拌后的混合物再加入球磨机中，球磨至细度小于10μm，再经过干燥塑形，即形成坯料。
进一步的，所述改良剂的制备方法包括如下步骤：
将土豆淀粉、河蚌壳粉、珍珠粉、石英砂、滑石粉、硫磺、微晶蜡混合，搅拌均匀，进行加热，加热温度为120-150度，加热时间为20-30分钟，将加热好的混合物加入搅拌器中进行保温搅拌，搅拌速度为800-1000r/min,保持温度为100-120度。
本发明的有益效果是：本发明以活性白土为主要原料，再加入竹炭纤维素、海泡石粉，并配合了磷酸盐、水玻璃、纳米陶瓷粉等，并辅以多种助剂，制得的坯料细腻、光滑，具有优异的耐高温性和牢固性等，用于制作的骨瓷细腻、光泽、质感好，品质好。
具体实施方式：
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
实施例1
一种骨瓷坯料，由如下重量份数的原料制成：
活性白土25份、竹炭纤维素12份、海泡石粉10份、活性炭8-份、磷酸盐6份、水玻璃5份、纳米陶瓷粉5份、粘黏剂4份、聚丙烯酸钠3份、改良剂4份、石蜡1份，环氧大豆油5份，二硼化锆1份、水100份。
进一步的，所述改良剂由以下重量份的组分构成：土豆淀粉5份，河蚌壳粉3份，珍珠粉2份，石英砂1份，滑石粉2份，硫磺1份，微晶蜡2份。
其制备方法包括如下步骤：
(1)向水中加入活性白土、活性炭、石蜡、二硼化锆，浸泡30min加热至回流状态保温处理15min，再加入环氧大豆油，继续保温处理10min，即得物料I；
(2)将海泡石粉、水玻璃、纳米陶瓷粉充分混合，再加入竹炭纤维素和磷酸盐，先加热至70-80℃保温混合10min，然后继续加热至120-130℃保温混合5min，即得物料II；
(3)向物料I中加入物料II、粘黏剂、聚丙烯酸钠、改良剂，充分混合均匀，加入球磨机中，球磨至细度小于20μm；
(4)将打磨后的混合物加入搅拌机中进行搅拌加热，搅拌速度为600r/min，加热温度为120度；
(5)将搅拌后的混合物再加入球磨机中，球磨至细度小于10μm，再经过干燥塑形，即形成坯料。；
进一步的，所述改良剂的制备方法包括如下步骤：
将土豆淀粉、河蚌壳粉、珍珠粉、石英砂、滑石粉、硫磺、微晶蜡混合，搅拌均匀，进行加热，加热温度为120度，加热时间为20分钟，将加热好的混合物加入搅拌器中进行保温搅拌，搅拌速度为800r/min,保持温度为100度。
实施例2
一种骨瓷坯料，由如下重量份数的原料制成：
活性白土30份、竹炭纤维素15份、海泡石粉15份、活性炭11份、磷酸盐10份、水玻璃8份、纳米陶瓷粉8份、粘黏剂6份、聚丙烯酸钠5份、改良剂6份、石蜡3份，环氧大豆油10份，二硼化锆2份、水150份。
所述改良剂由以下重量份的组分构成：土豆淀粉10份，河蚌壳粉6份，珍珠粉4份，石英砂3份，滑石粉4份，硫磺3份，微晶蜡4份。
其制备方法包括如下步骤：
(1)向水中加入活性白土、活性炭、石蜡、二硼化锆，浸泡30min加热至回流状态保温处理15min，再加入环氧大豆油，继续保温处理10min，即得物料I；
(2)将海泡石粉、水玻璃、纳米陶瓷粉充分混合，再加入竹炭纤维素和磷酸盐，先加热至80℃保温混合10min，然后继续加热至130℃保温混合5min，即得物料II；
(3)向物料I中加入物料II、粘黏剂、聚丙烯酸钠、改良剂，充分混合均匀，加入球磨机中，球磨至细度小于20μm；
(4)将打磨后的混合物加入搅拌机中进行搅拌加热，搅拌速度为800r/min，加热温度为150度；
(5)将搅拌后的混合物再加入球磨机中，球磨至细度小于10μm，再经过干燥塑形，即形成坯料。
进一步的，所述改良剂的制备方法包括如下步骤：
将土豆淀粉、河蚌壳粉、珍珠粉、石英砂、滑石粉、硫磺、微晶蜡混合，搅拌均匀，进行加热，加热温度为150，加热时间为30分钟，将加热好的混合物加入搅拌器中进行保温搅拌，搅拌速度为1000r/min,保持温度为120度。
对照组1
一种骨瓷坯料，由如下重量份数的原料制成：
活性白土25份、竹炭纤维素12份、海泡石粉10份、活性炭8-份、磷酸盐6份、水玻璃5份、纳米陶瓷粉5份、粘黏剂4份、聚丙烯酸钠3份、石蜡1份，环氧大豆油5份，二硼化锆1份、水100份。
其制备方法包括如下步骤：
(1)向水中加入活性白土、活性炭、石蜡、二硼化锆，浸泡30min加热至回流状态保温处理15min，再加入环氧大豆油，继续保温处理10min，即得物料I；
(2)将海泡石粉、水玻璃、纳米陶瓷粉充分混合，再加入竹炭纤维素和磷酸盐，先加热至70-80℃保温混合10min，然后继续加热至120-130℃保温混合5min，即得物料II；
(3)向物料I中加入物料II、粘黏剂、聚丙烯酸钠，充分混合均匀，加入球磨机中，球磨至细度小于20μm；
(4)将打磨后的混合物加入搅拌机中进行搅拌加热，搅拌速度为600r/min，加热温度为120度；
(5)将搅拌后的混合物再加入球磨机中，球磨至细度小于10μm，再经过干燥塑形，即形成坯料。
对照组2
一种骨瓷坯料，由如下重量份数的原料制成：
活性白土30份、竹炭纤维素15份、海泡石粉15份、活性炭11份、磷酸盐10份、水玻璃8份、纳米陶瓷粉8份、粘黏剂6份、聚丙烯酸钠5份、改良剂6份、石蜡3份，环氧大豆油10份，二硼化锆2份、水150份。
所述改良剂由以下重量份的组分构成：土豆淀粉10份，河蚌壳粉6份，珍珠粉4份，石英砂3份，滑石粉4份，硫磺3份，微晶蜡4份。
其制备方法包括如下步骤：
(1)向水中加入活性白土、活性炭、石蜡、二硼化锆，环氧大豆油，加热至回流状态保温处理15min，即得物料I；
(2)将海泡石粉、水玻璃、纳米陶瓷粉充分混合，再加入竹炭纤维素和磷酸盐，加热至130℃保温混合5min，即得物料II；
(3)向物料I中加入物料II、粘黏剂、聚丙烯酸钠、改良剂，充分混合均匀，加入球磨机中，球磨至细度小于20μm，再经过干燥塑形，即形成坯料。
进一步的，所述改良剂的制备方法包括如下步骤：
将土豆淀粉、河蚌壳粉、珍珠粉、石英砂、滑石粉、硫磺、微晶蜡混合，搅拌均匀，进行加热，加热温度为150，加热时间为30分钟。
表1为本发明与对照组的试验对比结果
本发明生产出来的骨瓷坯料，细腻度高，光滑，耐高温，牢固性强，以此制作的骨瓷细腻、光泽、品质高，是一种优质的骨瓷坯料。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。
Claims (6)
1.一种骨瓷坯料，其特征在于，由如下重量份数的原料制成：活性白土25-30份、竹炭纤维素12-15份、海泡石粉10-15份、活性炭8-11份、磷酸盐6-10份、水玻璃5-8份、纳米陶瓷粉5-8份、粘黏剂4-6份、聚丙烯酸钠3-5份、改良剂4-6份、石蜡1-3份，环氧大豆油5-10份，二硼化锆1-2份、水100-150份。
2.根据权利要求1所述的骨瓷坯料，其特征在于，上述骨瓷坯料，优选以下重量份数的原料制成：活性白土28份、竹炭纤维素14份、海泡石粉13份、活性炭9份、磷酸盐8份、水玻璃7份、纳米陶瓷粉6份、粘黏剂5份、聚丙烯酸钠4份、改良剂5份、石蜡2份，环氧大豆油8份，二硼化锆2份、水125份。
3.根据权利要求1所述的骨瓷坯料，其特征在于，所述改良剂由以下重量份的组分构成：土豆淀粉5-10份，河蚌壳粉3-6份，珍珠粉2-4份，石英砂1-3份，滑石粉2-4份，硫磺1-3份，微晶蜡2-4份。
4.根据权利要求1所述的骨瓷坯料，其特征在于，所述改良剂优选以下重量份的组分构成：土豆淀粉8份，河蚌壳粉5份，珍珠粉3份，石英砂2份，滑石粉3份，硫磺2份，微晶蜡3份。
5.根据权利要求1或2所述的骨瓷坯料，其特征在于，其制备方法包括如下步骤：
(1)将活性白土、竹炭纤维素、海泡石粉、活性炭、纳米陶瓷粉充分混合，进行搅拌加热，加热至90-100℃保温静置10min，加入环氧大豆油，再继续搅拌加热至120-130℃保温静置5min，即得物料I；
(2)向水中加入磷酸盐、水玻璃、聚丙烯酸钠、石蜡、二硼化锆均匀混合，浸泡30分钟，加热至回流状态保温处理15min，再加入粘黏剂，继续保温处理10min，即得物料II；
(3)向物料I中加入物料II、改良剂，充分混合均匀，加入球磨机中，球磨至细度小于20μm；
(4)将打磨后的混合物加入搅拌机中进行搅拌加热，搅拌速度为600-800r/min，加热温度为120-150度；
(5)将搅拌后的混合物再加入球磨机中，球磨至细度小于10μm，再经过干燥塑形，即形成坯料。
6.根据权利要求3或4所述的骨瓷坯料，其特征在于，所述改良剂的制备方法包括如下步骤：将土豆淀粉、河蚌壳粉、珍珠粉、石英砂、滑石粉、硫磺、微晶蜡混合，搅拌均匀，进行加热，加热温度为120-150度，加热时间为20-30分钟，将加热好的混合物加入搅拌器中进行保温搅拌，搅拌速度为800-1000r/min,保持温度为100-120度。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710808668.2A CN107651934A (zh) | 2017-09-09 | 2017-09-09 | 一种骨瓷坯料 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710808668.2A CN107651934A (zh) | 2017-09-09 | 2017-09-09 | 一种骨瓷坯料 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107651934A true CN107651934A (zh) | 2018-02-02 |
Family
ID=61129432
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710808668.2A Pending CN107651934A (zh) | 2017-09-09 | 2017-09-09 | 一种骨瓷坯料 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107651934A (zh) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928132A (zh) * | 2010-06-23 | 2010-12-29 | 平定莹玉陶瓷有限公司 | 一种普细瓷 |
| CN104140235A (zh) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | 一种免烧高韧性环保陶瓷 |
| CN105060859A (zh) * | 2015-07-30 | 2015-11-18 | 叶俊 | 一种遗体骨灰处理方法及其制品 |
| CN105859268A (zh) * | 2016-03-30 | 2016-08-17 | 安徽青花坊瓷业股份有限公司 | 一种骨瓷餐具制作用坯料 |
| CN107140948A (zh) * | 2017-06-12 | 2017-09-08 | 安徽青花坊瓷业股份有限公司 | 一种高白度日用骨灰瓷及其制备方法 |
-
2017
- 2017-09-09 CN CN201710808668.2A patent/CN107651934A/zh active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928132A (zh) * | 2010-06-23 | 2010-12-29 | 平定莹玉陶瓷有限公司 | 一种普细瓷 |
| CN104140235A (zh) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | 一种免烧高韧性环保陶瓷 |
| CN105060859A (zh) * | 2015-07-30 | 2015-11-18 | 叶俊 | 一种遗体骨灰处理方法及其制品 |
| CN105859268A (zh) * | 2016-03-30 | 2016-08-17 | 安徽青花坊瓷业股份有限公司 | 一种骨瓷餐具制作用坯料 |
| CN107140948A (zh) * | 2017-06-12 | 2017-09-08 | 安徽青花坊瓷业股份有限公司 | 一种高白度日用骨灰瓷及其制备方法 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105130378B (zh) | 一种人工彩砂着色剂、使用该着色剂的人工彩砂及制备方法 | |
| CN108358602A (zh) | 一种影青瓷陶瓷制品及其制造工艺 | |
| CN107140948A (zh) | 一种高白度日用骨灰瓷及其制备方法 | |
| CN107021626A (zh) | 一种金斑兰釉 | |
| CN107188528A (zh) | 仿树纹效果的陶瓷制品及其制备工艺 | |
| CN106746659B (zh) | 一种蓝色羽毛状晶花结晶釉釉料及其配置方法 | |
| CN104478482A (zh) | 一种南宋官窑米黄釉料变配方及制作工艺 | |
| CN104843999B (zh) | 青玉黄釉日用陶瓷的制备方法 | |
| CN111592330B (zh) | 一种炻质砖坯料及其制备方法与炻质砖 | |
| CN106565091A (zh) | 一种高温快烧砂晶釉及其制备工艺 | |
| CN107651934A (zh) | 一种骨瓷坯料 | |
| CN104944912A (zh) | 一种环保型节能低温白半瓷的配方及其制备方法 | |
| CN106671556A (zh) | 一种高性能墙纸 | |
| CN103288347B (zh) | 超平高透高亮一次烧成淋抛熔块及其制备和应用方法 | |
| CN106810207A (zh) | 一种高白瓷泥 | |
| CN107573024A (zh) | 一种用于陶瓷餐具的坯料 | |
| CN103992140B (zh) | 一种铜铁色曜变金圈天目釉及用其制作日用瓷的方法 | |
| CN110078375A (zh) | 一种用于玻璃马赛克的裂纹釉及玻璃马赛克的制备工艺 | |
| CN107056060B (zh) | 渐变孔雀蓝釉陶瓷及其制备工艺 | |
| CN113800770A (zh) | 一种中温双层窑变花釉和制作方法 | |
| CN104944906B (zh) | 一种色瓷及其制备方法 | |
| JP2002128577A (ja) | 釉薬組成物及びその製造方法，並びに施釉品 | |
| CN107445485A (zh) | 一种骨瓷光亮釉料 | |
| CN107522472A (zh) | 一种用于陶瓷花盆的坯料 | |
| CN109485383A (zh) | 一种菱形花瓶钧瓷工艺品制作方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180202 |
|
| RJ01 | Rejection of invention patent application after publication |