CN107440916A

CN107440916A - A kind of Wet preserving sterilizing infant is with activated carbon shower cream and preparation method thereof

Info

Publication number: CN107440916A
Application number: CN201710746428.4A
Authority: CN
Inventors: 不公告发明人
Original assignee: Changsha Small Amperex Technology Ltd
Current assignee: Changsha Small Amperex Technology Ltd
Priority date: 2017-08-27
Filing date: 2017-08-27
Publication date: 2017-12-08

Abstract

The invention discloses a kind of Wet preserving sterilizing infant with activated carbon shower cream.It is made up of the raw material below according to parts by weight：5 25 parts of honeysuckle, 6 18 parts of the shell of areca nut, 2 18 parts of rhizoma atractylodis, 6 22 parts of radix bardanae, 2 18 parts of Pogostemon cablin, 3 17 parts of honewort, 4 16 parts of mulberry leaf, 19 parts of japanese galangal flower, 2 12 parts of radix scrophulariae, 15 parts of double imidazolidinyl urea, 5 15 parts of glycerine, 2 18 parts of lauryl sodium sulfate, 37 parts of polypropylene glycol, 15 parts of allantoin, 28 parts of chamomile extract, 5 25 parts of antioxidant, 3 17 parts of modified activated carbon, 5 35 parts of deionized water.The present invention has the advantages that moistening effect is good, sterilization is thorough and easy to use.

Description

A kind of Wet preserving sterilizing infant is with activated carbon shower cream and preparation method thereof

Technical field

The present invention relates to detergents and cosmetic articles for use field, more particularly to a kind of Wet preserving sterilizing infant with activated carbon shower cream and Its preparation method.

Background technology

At present, as the improvement of people's living standards, requirement of the people to quality of the life also more and more higher, modern people exist Shower cream would generally be used during shower, shower cream is widely used as a kind of liquid cleaner by people, and uses shower cream energy Enough effective dirts for removing human skin's residual, the effect of sterilization can be played, it is well known that adult and infant Skin roughness is different, and the skin of infant is more tender and lovely, therefore, it is necessary to can not in shower cream during using shower cream The stronger material of excitant enough be present, and because infant is weaker to the resistance of germ, in daily life contact, due to disease The infection of bacterium, it is easy to cause infant sick ill symptomses occur, therefore the shower cream that people use for infant will The effect with sterilization is sought, and there can be the effect of moisturizing, is prevented because dry weather causes infant situation about peeling occur, But existing shower cream on the market does not have the scheme for solving this problem.

Absorbent charcoal material is by the amorphous carbon obtained by working process, has very big specific surface area, to gas, solution In inorganic or organic substance and colloidal solid etc. have good adsorption capacity.Absorbent charcoal material mainly includes activated carbon and work Property Carbon fibe etc., absorbent charcoal material has unique absorption surface mainly due to it as a kind of adsorbent of function admirable What architectural characteristic and surface chemistry were determined.The chemical property of absorbent charcoal material is stable, high mechanical strength, acidproof, alkaline-resisting, It is heat-resisting, not soluble in water and organic solvent, use can be regenerated, have been widely used for chemical industry, environmental protection, food processing, metallurgy, The every field such as medicine is refined, military chemistry protection.At present, modified active Carbon Materials are widely used in sewage disposal, air dirt The fields such as dye preventing and treating, curbing environmental pollution, aspect increasingly shows its tempting rosy prospect, and activated carbon is by being containing charcoal Main material makees raw material, through hydrophobic adsorbent made from high temperature carbonization and activation.Activated carbon contains a large amount of micropores, has huge Incomparable surface area, colourity, stink can be effectively removed, can remove most organic pollutants and some inorganic in secondary effluent Thing.

The content of the invention

The defects of in order to overcome above-mentioned prior art, it is an object of the invention to provide a kind of Wet preserving sterilizing infant activity Charcoal shower cream and preparation method thereof.

The present invention takes following technical scheme to realize：A kind of Wet preserving sterilizing infant with activated carbon shower cream, by Formed below according to the raw material of parts by weight：Honeysuckle 5-25 parts, shell of areca nut 6-18 parts, rhizoma atractylodis 2-18 parts, radix bardanae 6-22 parts, Pogostemon cablin 2-18 parts, honewort 3-17 parts, mulberry leaf 4-16 parts, japanese galangal flower 1-9 parts, radix scrophulariae 2-12 parts, double imidazolidinyl urea 1-5 Part, glycerine 5-15 parts, lauryl sodium sulfate 2-18 parts, polypropylene glycol 3-7 parts, allantoin 1-5 parts, chamomile extract 2-8 Part, antioxidant 5-25 parts, modified activated carbon 3-17 parts, deionized water 5-35 parts.

The antioxidant is tertiary butyl hydroxy-methylbenzene 1-7 parts, tertiary butyl hydroxyl fennel seeds brain 1-7 parts, gallic acid third Fat 2-8 parts, butylated hydroxy anisole 2-8 parts, 2,6- di-tert-butyl-4-methy phenol 3-7 parts.

The preparation method of the modified activated carbon is as follows：

(1) activated carbon is put into reducing mechanism and carries out pulverization process, grinding time 180min, by the activity after crushing Charcoal crosses 50 mesh sieves, obtains crushed material；

(2) crushed material obtained in step 1 is put into 2%-10% potassium hydroxide solution and soaked, at 100-140 DEG C It is stirred under temperature conditionss, mixing time 60min, is washed after the completion of stirring by deionized water, adjust it PH value is 7；

(3) material obtained in step 2 is placed in wet grinding mill, regulation grinder rotating speed is 2500-3000r/ Min, 6-9h is ground, it is heated after the completion of grinding, heating-up temperature is 90-120 DEG C, heat time 2-4h, is obtained To modified activated carbon.

A kind of above-mentioned Wet preserving sterilizing infant is with activated carbon shower cream, it is characterised in that by below according to parts by weight Raw material composition：15 parts of honeysuckle, 12 parts of the shell of areca nut, 10 parts of rhizoma atractylodis, 14 parts of radix bardanae, 10 parts of Pogostemon cablin, 10 parts of honewort, 10 parts of mulberry leaf, 5 parts of japanese galangal flower, 7 parts of radix scrophulariae, 6 parts of double imidazolidinyl urea, 10 parts of glycerine, 10 parts of lauryl sodium sulfate, poly- the third two 5 parts of alcohol, 3 parts of allantoin, 5 parts of chamomile extract, 10 parts of modified activated carbon, 4 parts of tertiary butyl hydroxy-methylbenzene, tertiary butyl hydroxyl 4 parts of fennel seeds brain, 5 parts of gallic acid third lipoprotein, 5 parts of butylated hydroxy anisole, 5 parts of 2,6- di-tert-butyl-4-methy phenols, go 20 parts of ionized water.

A kind of above-mentioned Wet preserving sterilizing infant is comprised the steps of with the preparation method of activated carbon shower cream：

(1) the weight composition number of above-mentioned each material is weighed, by honeysuckle, the shell of areca nut, rhizoma atractylodis, radix bardanae, Pogostemon cablin, mill Disk grass, mulberry leaf, japanese galangal flower and radix scrophulariae add water to cook, and for the first time plus water is 6-10 times of material gross weight, decocting time 1.5- 3.5h, for the second time plus water is 5-9 times, decocting time 1.5-3.5h of material gross weight, merges first time and obtains for the second time Decocting liquid and add ethanol solution, carry out concentration, obtain relative density be 1.1-1.2 medicinal extract；

(2) by double imidazolidinyl urea, glycerine, lauryl sodium sulfate, polypropylene glycol, allantoin, chamomile extract, change Property activated carbon, tertiary butyl hydroxy-methylbenzene, tertiary butyl hydroxyl fennel seeds brain, gallic acid third lipoprotein, butylated hydroxy anisole and 2,6- Di-tert-butyl-4-methy phenol is put into agitating device and is stirred, and heating-up temperature is 60-80 DEG C, and mixing time is 40min；

(3) by the material obtained in step 1 and step 2 mix, be stirred simultaneously, mixing speed be 60 turns/ Min, mixing time 70min, heating-up temperature are 55-75 DEG C, 40 DEG C are cooled to after the completion of stirring, you can obtain finished product.

In summary the invention has the advantages that：The present invention is with moistening effect is good, sterilization is thorough and uses The advantages that facilitating, the Chinese medical extract added in the shower cream can play a part of moist infant's skin, for normal The infant's skin disease seen has preferable therapeutic effect, and not only acts as preventive effect for bite by mosquitos, simultaneously for Damaged skin can accelerate its healing, facilitate the long-term use of infant；There is the modified activated carbon specific activity charcoal to compare surface The long-pending bigger and excellent characteristics such as hole increases, therefore can effectively be inhaled by the modified activated carbon particle of addition in shower cream Dirt caused by attached human skin, the purpose of itself is cleaned so as to reach；And the double imidazolidinyl urea added can drop The viscosity of low shower cream, the flushing being convenient for people to, and the smoothness of skin is added, it can be played preferably for germs such as moulds Bactericidal effect, be adapted to infant use；The combination of the glycerine and polypropylene glycol can make shower cream have preferably guarantor Wet performance, in the season that weather is more dry, wherein glycerine and polypropylene glycol have high activity and the characteristic such as anti-oxidant, prevent Human skin because water loss and caused by peel situation, make infant skin be maintained at moistening health state；Institute Moisture in skin can effectively be kept by stating the combination of chamomile extract and allantoin, and the allantoin being capable of promotion organization Growth, cell metabolism and cutin-softening layer albumen, it is not only non-stimulated, while the skin screen of infant can be strengthened Barrier, protects it from the infringement of germ；The chamomile extract also can further strengthen the resistance of skin, and for eczema There is preferable improvement Deng sensitive；The antioxidant tertiary butyl hydroxy-methylbenzene, tertiary butyl hydroxyl fennel seeds brain, Gallic acid third lipoprotein, butylated hydroxy anisole and 2,6- di-tert-butyl-4-methy phenol have preferable inoxidizability, add In shower cream, as infant in use, the antioxidant is adhered to skin surface, avoid because of sunlight direct irradiation or extraneous dirty Dye damages to infant's skin, can reduce the generation of human free radical, reaches the purpose of protection skin, and the modification Activated carbon has more outstanding dispersiveness, so that active ingredient is more uniformly spread in shower cream, so that it is used Effect is more preferable.

In addition to objects, features and advantages described above, the present invention also has other objects, features and advantages. Below, the present invention is further detailed explanation.

Embodiment

Embodiments of the invention are described in detail with reference to embodiments, but the present invention can be according to claim Limit and the multitude of different ways of covering is implemented.

Embodiment 1

The preparation method of modified activated carbon

(3) material obtained in step 2 is placed in wet grinding mill, regulation grinder rotating speed is 2500-3000r/ Min, 6-9h is ground, it is heated after the completion of grinding, heating-up temperature is 90-120 DEG C, heat time 2-4h, is obtained To modified activated carbon

Embodiment 2

The weight composition number of each material is weighed, by 5 parts of honeysuckle, 6 parts of the shell of areca nut, 2 parts of rhizoma atractylodis, 6 parts of radix bardanae, the wide leaves of pulse plants Fragrant 2 parts, 3 parts of honewort, 4 parts of mulberry leaf, 1 part of japanese galangal flower, 2 parts of radix scrophulariae add water to cook, and add the 6- that water is material gross weight for the first time 10 times, decocting time 1.5-3.5h, for the second time plus water is 5-9 times, decocting time 1.5-3.5h of material gross weight, is merged First time and the decocting liquid obtained for the second time simultaneously add ethanol solution, carry out concentration, obtain the leaching that relative density is 1.1-1.2 Cream；By 2 parts of double imidazolidinyl urea, 5 parts of glycerine, 2 parts of lauryl sodium sulfate, 3 parts of polypropylene glycol, 1 part of allantoin, chamomile extraction Take 2 parts of thing, 3 parts of modified activated carbon, 1 part of tertiary butyl hydroxy-methylbenzene, 1 part of tertiary butyl hydroxyl fennel seeds brain, gallic acid third lipoprotein 2 Part, 2 parts of butylated hydroxy anisole and 3 parts of 2,6- di-tert-butyl-4-methy phenol are put into agitating device and are stirred, Heating-up temperature is 60-80 DEG C, mixing time 40min；The material obtained in step 1 and step 2 is mixed, is stirred simultaneously Processing, mixing speed are 60 turns/min, and mixing time 70min, heating-up temperature is 55-75 DEG C, and 40 are cooled to after the completion of stirring DEG C, you can obtain finished product.

Embodiment 3

Weigh each material weight composition number, by 15 parts of honeysuckle, 12 parts of the shell of areca nut, 10 parts of rhizoma atractylodis, 14 parts of radix bardanae, 10 parts of Pogostemon cablin, 10 parts of honewort, 10 parts of mulberry leaf, 5 parts of japanese galangal flower, 7 parts of radix scrophulariae add water to cook, and for the first time plus water is that material is total 6-10 times of weight, decocting time 1.5-3.5h, for the second time plus water is 5-9 times of material gross weight, decocting time 1.5- 3.5h, merge the decocting liquid obtained for the first time and for the second time and add ethanol solution, carry out concentration, obtaining relative density is 1.1-1.2 medicinal extract；By 6 parts of double imidazolidinyl urea, 10 parts of glycerine, 10 parts of lauryl sodium sulfate, 5 parts of polypropylene glycol, allantois Element 3 parts, 5 parts of chamomile extract, 10 parts of modified activated carbon, 4 parts of tertiary butyl hydroxy-methylbenzene, 4 parts of tertiary butyl hydroxyl fennel seeds brain, 5 parts of gallic acid third lipoprotein, 5 parts of butylated hydroxy anisole and 5 parts of 2,6- di-tert-butyl-4-methy phenol are put into agitating device It is stirred, heating-up temperature is 60-80 DEG C, mixing time 40min；The material obtained in step 1 and step 2 is mixed Close, be stirred simultaneously, mixing speed is 60 turns/min, and mixing time 70min, heating-up temperature is 55-75 DEG C, stirring After the completion of be cooled to 40 DEG C, you can obtain finished product.

Embodiment 4

Weigh each material weight composition number, by 25 parts of honeysuckle, 18 parts of the shell of areca nut, 18 parts of rhizoma atractylodis, 22 parts of radix bardanae, 18 parts of Pogostemon cablin, 17 parts of honewort, 16 parts of mulberry leaf, 9 parts of japanese galangal flower, 12 parts of radix scrophulariae add water to cook, and for the first time plus water is that material is total 6-10 times of weight, decocting time 1.5-3.5h, for the second time plus water is 5-9 times of material gross weight, decocting time 1.5- 3.5h, merge the decocting liquid obtained for the first time and for the second time and add ethanol solution, carry out concentration, obtaining relative density is 1.1-1.2 medicinal extract；By 5 parts of double imidazolidinyl urea, 15 parts of glycerine, 18 parts of lauryl sodium sulfate, 7 parts of polypropylene glycol, allantois 5 parts of element, 8 parts of chamomile extract, 17 parts of modified activated carbon, 7 parts of tertiary butyl hydroxy-methylbenzene, tertiary butyl hydroxyl fennel seeds brain 7 Part, 8 parts of gallic acid third lipoprotein, 8 parts of butylated hydroxy anisole and 7 parts of 2,6- di-tert-butyl-4-methy phenol are put into agitating device In be stirred, heating-up temperature be 60-80 DEG C, mixing time 40min；The material that will be obtained in step 1 and step 2 Mixing, is stirred simultaneously, and mixing speed is 60 turns/min, and mixing time 70min, heating-up temperature is 55-75 DEG C, is stirred 40 DEG C are cooled to after the completion of mixing, you can obtain finished product.

Comparative example 1

The weight composition number of each material is weighed, by 5 parts of honeysuckle, 6 parts of the shell of areca nut, 2 parts of rhizoma atractylodis, 6 parts of radix bardanae, the wide leaves of pulse plants Fragrant 2 parts, 3 parts of honewort, 4 parts of mulberry leaf, 1 part of japanese galangal flower, 2 parts of radix scrophulariae add water to cook, and add the 6- that water is material gross weight for the first time 10 times, decocting time 1.5-3.5h, for the second time plus water is 5-9 times, decocting time 1.5-3.5h of material gross weight, is merged First time and the decocting liquid obtained for the second time simultaneously add ethanol solution, carry out concentration, obtain the leaching that relative density is 1.1-1.2 Cream；5 parts of glycerine, 3 parts of polypropylene glycol, 1 part of allantoin, 2 parts of chamomile extract, 2 parts of gallic acid third lipoprotein are put into stirring dress It is stirred in putting, heating-up temperature is 60-80 DEG C, mixing time 40min；The material that will be obtained in step 1 and step 2 Mixing, is stirred simultaneously, and mixing speed is 60 turns/min, and mixing time 70min, heating-up temperature is 55-75 DEG C, 40 DEG C are cooled to after the completion of stirring, you can obtain finished product.

Comparative example 2

Weigh each material weight composition number, by 15 parts of honeysuckle, 12 parts of the shell of areca nut, 10 parts of rhizoma atractylodis, 14 parts of radix bardanae, 10 parts of Pogostemon cablin, 10 parts of honewort, 10 parts of mulberry leaf, 5 parts of japanese galangal flower, 7 parts of radix scrophulariae add water to cook, and for the first time plus water is that material is total 6-10 times of weight, decocting time 1.5-3.5h, for the second time plus water is 5-9 times of material gross weight, decocting time 1.5- 3.5h, merge the decocting liquid obtained for the first time and for the second time and add ethanol solution, carry out concentration, obtaining relative density is 1.1-1.2 medicinal extract；By 10 parts of glycerine, 5 parts of polypropylene glycol, 3 parts of allantoin, 5 parts of chamomile extract, gallic acid third lipoprotein 5 Part, which is put into agitating device, to be stirred, and heating-up temperature is 60-80 DEG C, mixing time 40min；By step 1 and step 2 In obtained material mixing, be stirred simultaneously, mixing speed be 60 turns/min, mixing time 70min, and heating is warm Spend for 55-75 DEG C, 40 DEG C are cooled to after the completion of stirring, you can obtain finished product.

Comparative example 3

Weigh each material weight composition number, by 25 parts of honeysuckle, 18 parts of the shell of areca nut, 18 parts of rhizoma atractylodis, 22 parts of radix bardanae, 18 parts of Pogostemon cablin, 17 parts of honewort, 16 parts of mulberry leaf, 9 parts of japanese galangal flower, 12 parts of radix scrophulariae add water to cook, and for the first time plus water is that material is total 6-10 times of weight, decocting time 1.5-3.5h, for the second time plus water is 5-9 times of material gross weight, decocting time 1.5- 3.5h, merge the decocting liquid obtained for the first time and for the second time and add ethanol solution, carry out concentration, obtaining relative density is 1.1-1.2 medicinal extract；By 15 parts of glycerine, 7 parts of polypropylene glycol, 5 parts of allantoin, 8 parts of chamomile extract, gallic acid third lipoprotein 8 Part, which is put into agitating device, to be stirred, and heating-up temperature is 60-80 DEG C, mixing time 40min；By step 1 and step The material mixing obtained in 2, is stirred simultaneously, and mixing speed is 60 turns/min, mixing time 70min, and heating is warm Spend for 55-75 DEG C, 40 DEG C are cooled to after the completion of stirring, you can obtain finished product.

Experimental method

The infant of selection 60 6-12 months, 30 men, 30 female are divided into A groups and B groups, wherein A groups for 15 men with 15 female, B groups are 15 men and 15 female, the shower cream in embodiment 2-4 are used for A groups infant, for B group infants Use the shower cream in comparative example 1-3, experimental result such as following table：

By experimental data, embodiment 2-4 and comparative example 1-3 contrast can using shower cream produced by the present invention With the purpose for effectively improving infant's moisture content of skin and reaching elimination germ.

Described above is embodiments of the invention, therefore all construction, feature and principle institutes according to described in the present patent application scope The equivalent change or modification done, is included in the range of present patent application.

Claims

1. a kind of Wet preserving sterilizing infant is with activated carbon shower cream, it is characterised in that by below according to the raw material group of parts by weight Into：Honeysuckle 5-25 parts, shell of areca nut 6-18 parts, rhizoma atractylodis 2-18 parts, radix bardanae 6-22 parts, Pogostemon cablin 2-18 parts, honewort 3-17 Part, mulberry leaf 4-16 parts, japanese galangal flower 1-9 parts, radix scrophulariae 2-12 parts, double imidazolidinyl urea 1-5 parts, glycerine 5-15 parts, dodecyl sulphur Sour sodium 2-18 parts, polypropylene glycol 3-7 parts, allantoin 1-5 parts, chamomile extract 2-8 parts, antioxidant 5-25 parts, modified work Property charcoal 3-17 parts, deionized water 5-35 parts.

The antioxidant is tertiary butyl hydroxy-methylbenzene 1-7 parts, tertiary butyl hydroxyl fennel seeds brain 1-7 parts, gallic acid third lipoprotein 2-8 Part, butylated hydroxy anisole 2-8 parts, 2,6- di-tert-butyl-4-methy phenol 3-7 parts.

The preparation method of the modified activated carbon is as follows：

(1) activated carbon is put into reducing mechanism and carries out pulverization process, grinding time 180min, by the activated carbon mistake after crushing 50 mesh sieves, obtain crushed material；

(2) crushed material obtained in step 1 is put into 2%-10% potassium hydroxide solution and soaked, in 100-140 DEG C of temperature Under the conditions of be stirred, mixing time 60min, washed after the completion of stirring by deionized water, adjust its pH value For 7；

(3) material obtained in step 2 being placed in wet grinding mill, regulation grinder rotating speed is 2500-3000r/min, 6-9h is ground, it is heated after the completion of grinding, heating-up temperature is 90-120 DEG C, heat time 2-4h, is changed Property activated carbon.

2. a kind of Wet preserving sterilizing infant according to claim 1 is with activated carbon shower cream, it is characterised in that by pressing below Formed according to the raw material of parts by weight：15 parts of honeysuckle, 12 parts of the shell of areca nut, 10 parts of rhizoma atractylodis, 14 parts of radix bardanae, 10 parts of Pogostemon cablin, mill 10 parts of disk grass, 10 parts of mulberry leaf, 5 parts of japanese galangal flower, 7 parts of radix scrophulariae, 6 parts of double imidazolidinyl urea, 10 parts of glycerine, lauryl sodium sulfate 10 Part, 5 parts of polypropylene glycol, 3 parts of allantoin, 5 parts of chamomile extract, 10 parts of modified activated carbon, 4 parts of tertiary butyl hydroxy-methylbenzene, spy 4 parts of butylhydroxy fennel seeds brain, 5 parts of gallic acid third lipoprotein, 5 parts of butylated hydroxy anisole, 2,6- di-tert-butyl-4-methy phenols 5 parts, 20 parts of deionized water.

3. according to a kind of any described Wet preserving sterilizing infants of claim 1-2 with the preparation method of activated carbon shower cream, its It is characterised by, comprises the steps of：

(1) the weight composition number of each material in claim 1 or 2 is weighed, by the honeysuckle, shell of areca nut, rhizoma atractylodis, radix bardanae, wide Wrinkled giant hyssop, honewort, mulberry leaf, japanese galangal flower and radix scrophulariae add water to cook, and for the first time plus water is 6-10 times of material gross weight, decocting time For 1.5-3.5h, for the second time plus water is 5-9 times, decocting time 1.5-3.5h of material gross weight, merges first time and second Secondary obtained decocting liquid simultaneously adds ethanol solution, carries out concentration, obtains the medicinal extract that relative density is 1.1-1.2；

(2) by double imidazolidinyl urea, glycerine, lauryl sodium sulfate, polypropylene glycol, allantoin, chamomile extract, modified work Property charcoal, tertiary butyl hydroxy-methylbenzene, tertiary butyl hydroxyl fennel seeds brain, gallic acid third lipoprotein, butylated hydroxy anisole and 2, the uncles of 6- bis- Butyl -4- methylphenols, which are put into agitating device, to be stirred, and heating-up temperature is 60-80 DEG C, mixing time 40min；

(3) material obtained in step 1 and step 2 is mixed, be stirred simultaneously, mixing speed is 60 turns/min, is stirred It is 70min to mix the time, and heating-up temperature is 55-75 DEG C, 40 DEG C is cooled to after the completion of stirring, you can obtain finished product.