CN107375033A - A kind of osmanthus essential oil shampoo and preparation method thereof - Google Patents
A kind of osmanthus essential oil shampoo and preparation method thereof Download PDFInfo
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- CN107375033A CN107375033A CN201710688677.2A CN201710688677A CN107375033A CN 107375033 A CN107375033 A CN 107375033A CN 201710688677 A CN201710688677 A CN 201710688677A CN 107375033 A CN107375033 A CN 107375033A
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- essential oil
- osmanthus essential
- osmanthus
- surfactant
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 79
- 235000019082 Osmanthus Nutrition 0.000 title claims abstract description 77
- 241000333181 Osmanthus Species 0.000 title claims abstract description 77
- 239000002453 shampoo Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 64
- 229920006317 cationic polymer Polymers 0.000 claims abstract description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000004094 surface-active agent Substances 0.000 claims abstract description 26
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 15
- 229920005573 silicon-containing polymer Polymers 0.000 claims abstract description 15
- 239000008367 deionised water Substances 0.000 claims abstract description 5
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 5
- 208000034530 PLAA-associated neurodevelopmental disease Diseases 0.000 claims abstract description 4
- 229920000747 poly(lactic acid) Polymers 0.000 claims description 19
- 239000004626 polylactic acid Substances 0.000 claims description 19
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 18
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 16
- 210000004209 hair Anatomy 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- 235000019270 ammonium chloride Nutrition 0.000 claims description 9
- 229940063953 ammonium lauryl sulfate Drugs 0.000 claims description 9
- BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 claims description 8
- 239000004310 lactic acid Substances 0.000 claims description 8
- 235000014655 lactic acid Nutrition 0.000 claims description 8
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 6
- 239000003643 water by type Substances 0.000 claims description 6
- -1 poly dimethyl silicon Oxygen alkane Chemical class 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- YQGOWXYZDLJBFL-UHFFFAOYSA-N dimethoxysilane Chemical compound CO[SiH2]OC YQGOWXYZDLJBFL-UHFFFAOYSA-N 0.000 claims description 3
- 238000010008 shearing Methods 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 4
- 244000007835 Cyamopsis tetragonoloba Species 0.000 claims 2
- 125000005233 alkylalcohol group Chemical group 0.000 claims 2
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims 2
- 235000011130 ammonium sulphate Nutrition 0.000 claims 2
- 210000000481 breast Anatomy 0.000 claims 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 18
- 230000000694 effects Effects 0.000 abstract description 15
- 230000001835 salubrious effect Effects 0.000 abstract description 6
- 210000004761 scalp Anatomy 0.000 abstract description 5
- 230000003750 conditioning effect Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 11
- 244000242564 Osmanthus fragrans Species 0.000 description 9
- 235000019083 Osmanthus fragrans Nutrition 0.000 description 9
- 244000303965 Cyamopsis psoralioides Species 0.000 description 7
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 6
- 210000003780 hair follicle Anatomy 0.000 description 5
- 230000002045 lasting effect Effects 0.000 description 5
- CMCBDXRRFKYBDG-UHFFFAOYSA-N 1-dodecoxydodecane Chemical compound CCCCCCCCCCCCOCCCCCCCCCCCC CMCBDXRRFKYBDG-UHFFFAOYSA-N 0.000 description 4
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 235000006708 antioxidants Nutrition 0.000 description 3
- AOLMPVPUFVWGPN-UHFFFAOYSA-N diazanium;1-dodecoxydodecane;sulfate Chemical compound [NH4+].[NH4+].[O-]S([O-])(=O)=O.CCCCCCCCCCCCOCCCCCCCCCCCC AOLMPVPUFVWGPN-UHFFFAOYSA-N 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 230000000975 bioactive effect Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000004456 color vision Effects 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 230000031700 light absorption Effects 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- QPJVMBTYPHYUOC-UHFFFAOYSA-N methyl benzoate Chemical compound COC(=O)C1=CC=CC=C1 QPJVMBTYPHYUOC-UHFFFAOYSA-N 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 229940079877 pyrogallol Drugs 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- QBJWYMFTMJFGOL-UHFFFAOYSA-N 2-hexadecyloxirane Chemical compound CCCCCCCCCCCCCCCCC1CO1 QBJWYMFTMJFGOL-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 241001080929 Zeugopterus punctatus Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 230000009920 chelation Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 210000003128 head Anatomy 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 229940095102 methyl benzoate Drugs 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 210000001541 thymus gland Anatomy 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 235000020795 whole food diet Nutrition 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention relates to a kind of osmanthus essential oil shampoo and preparation method thereof, with salubrious natural fragrance, and fragrance continuation is good, the present invention is by osmanthus essential oil composition, cationic polymer, surfactant, dimethyl silicone polymer, PLA and deionized water composition, the present invention is by handling osmanthus essential oil, slow down the rate of release of osmanthus essential oil, pass through the synergy of extraneous component simultaneously, osmanthus essential oil is set preferably to be absorbed, play protection scalp effect, the osmanthus essential oil shampoo of gained of the invention not only has salubrious natural fragrance, also there is good conditioning effect.
Description
Technical field
The present invention relates to a kind of osmanthus essential oil shampoo and preparation method thereof, belong to field of daily chemicals.
Background technology
Sweet osmanthus has very high value, can both beautify the environment, and can be used for chemical industry and food industry, sweet osmanthus taste giving off a strong fragrance again
Sweet tea, nutrition very abundant, it is referred to as in the world " wholefood ".Total amino acid content is up to 13.78% in sweet osmanthus, wherein
Essential amino acid is 6.26%, accounts for the 45.55% of total amino acid content, the reasonable mixture ratio of amino acid in sweet osmanthus, is a kind of high-quality
Protein, in addition sweet osmanthus contain abundant vitamin and various trace elements, potassium, iron, Zn content is apparently higher than general plant, tool
There are certain beauty treatment whitening, blood circulation promoting and enriching, promote growth in humans's development, improve immunity, reduce blood pressure, promote carbohydate metabolism etc.
Effect, is a kind of preferable health food.
Osmanthus essential oil is the primary bioactive components of sweet osmanthus, the research tool to osmanthus essential oil chemical composition and bioactivity
It is significant.Osmanthus essential oil contains the compositions such as alcohol, ketone, aldehyde, acid, ester, alkane, terpene and its containing oxygen derivative, with esters and
Based on constituents, containing a variety of bioactive ingredients for having application value, 5- vinyl-Niacin Nicitinic Acid methyl esters, to formoxyl
Methyl benzoate, palmitic acid, the carbon diene of 1,21- 22,1,2- epoxy octadecane contents are higher, and osmanthus essential oil has good
Antioxidation activity in vitro, total reducing power and the chelation highly significant to metal ion.
The main component of hair is protein, without any physiological function, more without any self-clean or
The effect of self-regeneration.The long-term exposed dust constantly adsorbed outside in air causes hair contaminated, becomes greasy, has some setbacks
It is sliding, and protein is easily damaged by ultraviolet, becomes the bad phenomenon such as withered and yellow, hair fork, looping.Osmanthus essential oil shampoo is as clear
A kind of cleaning agent of wash my hair, not only there is the sludge that can remove hair, also have unique fragrance, make people salubrious certainly
So, there is last osmanthus essential oil good antioxidation, scalp oxidation aging can be reduced after absorbing, and promote the health hair of hair follicle
Exhibition, fundamentally ensure the health of hair, but osmanthus essential oil volatility is stronger, and adsorptivity is not strong, how by osmanthus essential oil
It is long-term that to reside in hair and scalp be a great problem, the present invention provide one kind with lasting fragrance, with fine repairing hair follicle and
The osmanthus essential oil shampoo of hair.
The content of the invention
To achieve the above object, the present invention provides a kind of lasting fragrance, has the osmanthus of repairing hair follicle and hair effect
Flower essential oil shampoo, embodiment of the present invention are as follows：
A kind of osmanthus essential oil shampoo, by osmanthus essential oil composition, cationic polymer, surfactant, polydimethylsiloxanes
Alkane, PLA and deionized water composition, component ratio are as follows：
Osmanthus essential oil composition 10%-30%
Cationic polymer 1%-3%
Surfactant 5%-10%
Dimethyl silicone polymer 1%-5%
PLA 3%-6%
Water 50%-70%
Aforementioned proportion is weight ratio.
Described osmanthus essential oil composition is made up of osmanthus essential oil, lactic acid, water, according to weight ratio, the ratio of three kinds of components
It is followed successively by 1:1:5.
Described osmanthus essential oil preparation method of composition is as follows：Osmanthus essential oil is uniformly mixed with lactic acid, and water is heated to
50 DEG C, constant temperature stirring, the mixture of osmanthus essential oil and lactic acid is added, is sheared after adding 5-10 minutes, shear rate control exists
10000r/min or more.
Described osmanthus essential oil be it is unique from a kind of fragrance by traditional extraction means, is extracted in sweet osmanthus, mainly
Composition is the material of volatile oil.
Further, described osmanthus essential oil extracting method is as follows：Take sweet osmanthus appropriate, add 3 equivalent to sweet osmanthus weight
Amount water again, extraction backflow, is extracted 3 hours, collection volatile oil, produces osmanthus essential oil.
Described cationic polymer refer to Polyquaternium-10 or guar hydroxypropyltrimonium ammonium chloride one kind or
Two kinds of mixtures.
Preferably, described cationic polymer is Polyquaternium-10 and guar hydroxypropyltrimonium weight ammonium chloride
Than 1:2 mixture.
Described surfactant is one or two kinds of mixed in dodecyl ether sulfate ammonium, ammonium lauryl sulfate
Compound.
Preferably, shown surfactant is dodecyl ether sulfate ammonium and ammonium lauryl sulfate weight ratio is 1:
1 mixture.
For described polylactic acid molecule amount between 5000-15000, preferred molecular weight is 10000 PLA.
Described water is deionized water.
Preferably, described osmanthus essential oil shampoo is made up of following component：
Osmanthus essential oil composition 15%-25%
Cationic polymer 1%-3%
Surfactant 6%-8%
Dimethyl silicone polymer 2%-4%
PLA 4%-6%
Water 55%-65%
Further, described osmanthus essential oil shampoo is made up of following component：
Osmanthus essential oil composition 20%
Cationic polymer 2%
Surfactant 7%
Dimethyl silicone polymer 3%
PLA 5%
Water 63%
Further, a kind of preparation method of described osmanthus essential oil shampoo is as follows：
1）Osmanthus essential oil composition, 70 DEG C of deionized waters are added, stirring is to being completely dissolved
2）Cationic polymer is added, stirring is to being completely dissolved
3）Surfactant, poly- dimethoxy silane and PLA are added, is uniformly mixed, is sheared 5-10 minutes, shearing speed
Spend for 10000r/min or more, you can.
Further, a kind of preparation method of described osmanthus essential oil shampoo is as follows：
1）Osmanthus essential oil composition, 70 DEG C of deionized waters are added, stirring is to being completely dissolved
2）Cationic polymer is added, stirring is to being completely dissolved
3）Surfactant, poly- dimethoxy silane and PLA are added, is uniformly mixed, is sheared 8 minutes, shear rate is
10000r/min, you can.
The invention is characterized in that a kind of osmanthus essential oil shampoo is provided, by osmanthus essential oil composition, cationic polymer, table
Face activating agent, dimethione, PLA and deionized water composition, osmanthus essential oil has anti-oxidant, antifatigue and anti-
Bacterium effect, the present invention carry out preliminary processing to osmanthus essential oil, mixed under certain temperature with lactic acid, lactic acid content hydroxyl and carboxylic
Base, it can not only polymerize with osmanthus essential oil composition, certain polymer can be also thought of as between self-molecules present, osmanthus essential oil is in inclusion
State, prevent it from quickly volatilizing, reach the effect of lasting fragrance, while hydroxyl in lactic acid and carboxyl are dissolved in water, play one
Fixed hydrotropy effect, promote absorption of the scalp to osmanthus essential oil, the hair follicle of protection head root is oxidized, while also acts as antibacterial effect
Fruit.
Another feature of the present invention is that the present invention in addition to osmanthus essential oil is handled, also fills to other components
Divide research, add a certain amount of PLA, there is certain slow release effect, the composition volatilization of protection osmanthus essential oil, while PLA
It can also be combined with the grease of scalp, be easy to oil stain removing, play the effect of synergy cleansing power.
The beneficial effects of the present invention are：
1. the present invention uses simple preparation technology, it is easy to amplification and industrialization, cost is cheap
2. the present invention provides a kind of osmanthus essential oil shampoo, there is lasting fragrance she's effect, moreover it is possible to protect hair follicle
Embodiment
In order to be better understood from main points of the present invention, now foregoing invention is described in further detail by specific embodiment, but under
Embodiment is stated it is not intended that to further limitation of the invention.
Comparative example 1
Osmanthus essential oil 20%
Cationic polymer 2%
Surfactant 8%
Dimethyl silicone polymer 3%
PLA 5%
Water 62%
Cationic polymer is that cationic polymer is Polyquaternium-10 with guar hydroxypropyltrimonium weight ammonium chloride than 1:
2 mixture
Surfactant is：Dodecyl ether sulfate ammonium and ammonium lauryl sulfate weight ratio are 1:1 mixture.
Comparative example 2
Osmanthus essential oil 20%
Cationic polymer 2%
Surfactant 8%
Dimethyl silicone polymer 3%
Water 67%
Comparative example 3
The preparation method of the composition of comparative example 1 is as follows：
1. osmanthus essential oil, 70 DEG C of deionized waters are added, stirring is to being completely dissolved
2. adding cationic polymer, stirring is to being completely dissolved
3. adding surfactant, dimethyl silicone polymer and PLA, it is uniformly mixed, shears 8 minutes, shear rate
For 10000r/min, you can.
The preparation method of the composition of comparative example 2 is as follows：
1. osmanthus essential oil composition, 70 DEG C of deionized waters are added, stirring is to being completely dissolved
2. adding cationic polymer, stirring is to being completely dissolved
3. adding surfactant, dimethyl silicone polymer, it is uniformly mixed, shears 8 minutes, shear rate 10000r/
Min, you can.
Embodiment 1
Osmanthus essential oil composition 20%
Cationic polymer 2%
Surfactant 8%
Dimethyl silicone polymer 3%
PLA 5%
Water 62%
Cationic polymer is that cationic polymer is Polyquaternium-10 with guar hydroxypropyltrimonium weight ammonium chloride than 1:
2 mixture.
Surfactant is：Dodecyl ether sulfate ammonium and ammonium lauryl sulfate weight ratio are 1:1 mixture
Embodiment 2
Osmanthus essential oil composition 10%
Cationic polymer 3%
Surfactant 10%
Dimethyl silicone polymer 5%
PLA 3%
Water 69%
Cationic polymer is that cationic polymer is Polyquaternium-10 with guar hydroxypropyltrimonium weight ammonium chloride than 1:
2 mixture
Surfactant is：Dodecyl ether sulfate ammonium and ammonium lauryl sulfate weight ratio are 1:1 mixture.
Embodiment 3
Osmanthus essential oil composition 30%
Cationic polymer 1%
Surfactant 5%
Dimethyl silicone polymer 1%
PLA 6%
Water 57%
Cationic polymer is that cationic polymer is Polyquaternium-10 with guar hydroxypropyltrimonium weight ammonium chloride than 1:
2 mixture
Surfactant is：Dodecyl ether sulfate ammonium and ammonium lauryl sulfate weight ratio are 1:1 mixture.
Embodiment 4
Osmanthus essential oil composition 20%
Polyquaternium-10 2%
Dodecyl ether sulfate ammonium 7%
Dimethyl silicone polymer 3%
PLA 5%
Water 63%.
Embodiment 5
Osmanthus essential oil composition 20%
Guar hydroxypropyltrimonium ammonium chloride 2%
Ammonium lauryl sulfate 7%
Dimethyl silicone polymer 3%
PLA 5%
Water 63%.
Embodiment 6
Embodiment 1 is as follows to the preparation method of the resulting composition of embodiment 5：
1. osmanthus essential oil composition, 70 DEG C of deionized waters are added, stirring is to being completely dissolved
2. adding cationic polymer, stirring is to being completely dissolved
3. adding surfactant, dimethyl silicone polymer, it is uniformly mixed, shears 8 minutes, shear rate 10000r/
Min, you can
Detect the fragrance of comparative example 1-2 and the resulting composition of embodiment 1 to 5
Take hair appropriate, respectively 7 parts, prick beam, every part of 5g, take comparative example 1-2, each compositions of embodiment 1-5, apply respectively
Cloth adds 10g water into above-mentioned hair weight, and soft wash my hair 5 minutes is clean by flush with foam with water.By five colour visions, smell
Normal adult, the topknot taste income after above-mentioned cleaning is judged, using fragrant and salubrious nature as scale, takes average,
Fraction is higher, and effect is better, and five marking average results are as follows：
The composition fragrance evaluation result table of table 1
Detect the fragrance continuation of comparative example 1-2 and the resulting composition of embodiment 1 to 5
Comparative example 1-2, each 3g of each compositions of embodiment 1-5 are taken, is respectively coated on stainless steel disc, spreading area is
5cm2,, opening placement, 5 colour visions, osmatic female adults are chosen, the fragrance of above-mentioned composition is given a mark, with
Fragrant and salubrious is naturally scale, takes average, and fraction is higher, and effect is better, five marking average result such as following tables：
The composition fragrance continuation evaluation result table of table 2
Remarks "-" is completely without salubrious natural fragrance.
Analyze from the above, osmanthus essential oil shampoo of the invention has good natural fragrance, and fragrance has fine
Continuation.
Detect the oxidation resistance of comparative example 1-2 and the resulting composition of embodiment 1 to 2
The external Ability of antioxygen free radicals of comparative example 1-2 and embodiment 1-2 resulting compositions is detected, using pyrogallol method
Measure, mouse thymus cells can produce O2.16 10ml tool plug test tubes are taken, label No. 1 to No. 16, being separately added into pH value is
8.2 Tris-HC1 cushioning liquid 4.5mL, 20min is preheated in 20 DEG C of water-baths, is added composition according to the amount in table 3 below, is moved
Take 1 mL distilled water and 0.4 mL pyrogallol solution（45mmol）, reacted in 25 DEG C of water-baths, the reaction time such as following table institute
State, after reaction terminates, add（6mmol）HCl solution lmL makes reaction terminating, and its absorbance value A is determined at 420nm wavelengthSample。
Calculate inhibiting rate.Control absorbance A is detected with methodControl。
Inhibiting rate=(AControl-ASample)/AControlX 100%
A in formulaControlThe light absorption value measured for control group；ASampleTo add the reacted light absorption value of extract solution.
The composition of table 3 illustrates table
The test tube number of table 4 and detection time table
Remarks：2 hours, No. 1/5/9/13 test tube antioxidant capacity is detected, other the like.
The anti-oxidant result table of table 5
As a result show that shampoo of the present invention has better effects in terms of antioxygen, also there is significant effect in terms of lasting antioxygen
Fruit.
Above-described embodiment is not to make any formal limitation to the present invention, any those skilled in the art,
In the case of not departing from technical solution of the present invention scope, all technical solution of the present invention is done using the technology contents of the disclosure above
Go out many possible changes and modifications, or be revised as the equivalent embodiment of equivalent variations.Therefore, it is every without departing from the technology of the present invention
The content of scheme, according to the technology of the present invention essence to any simple modifications, equivalents, and modifications made for any of the above embodiments,
It should fall in the range of technical solution of the present invention protection.
Claims (9)
- A kind of 1. osmanthus essential oil shampoo, by osmanthus essential oil composition, cationic polymer, surfactant, poly dimethyl silicon Oxygen alkane, PLA and deionized water composition, it is characterised in that component ratio is as follows：Osmanthus essential oil composition 10%-30%Cationic polymer 1%-3%Surfactant 5%-10%Dimethyl silicone polymer 1%-5%PLA 3%-6%Water 50%-70%Aforementioned proportion is weight ratio.
- A kind of 2. osmanthus essential oil shampoo according to claim 1, it is characterised in that described osmanthus essential oil composition by Osmanthus essential oil, lactic acid, water composition, according to weight ratio, the ratio of three kinds of components is followed successively by 1:1:5.
- A kind of 3. osmanthus essential oil shampoo according to claim 2, it is characterised in that described osmanthus essential oil composition system Preparation Method is as follows：Osmanthus essential oil is uniformly mixed with lactic acid, and water is heated to 50 DEG C, constant temperature stirring, adds osmanthus essential oil and breast The mixture of acid, sheared after adding 5-10 minutes, shear rate is controlled in 10000r/min or more.
- 4. a kind of osmanthus essential oil shampoo according to claim 1, it is characterised in that described cationic polymer refers to One or two kinds of mixture of Polyquaternium-10 or guar hydroxypropyltrimonium ammonium chloride.
- 5. a kind of osmanthus essential oil shampoo according to claim 4, it is characterised in that described cationic polymer is poly- Quaternary ammonium salt -10 is with guar hydroxypropyltrimonium weight ammonium chloride than 1:2 mixture.
- 6. a kind of osmanthus essential oil shampoo according to claim 1, it is characterised in that described surfactant is 12 One or two kinds of mixture in alkyl alcohol ether ammonium sulfate, ammonium lauryl sulfate.
- 7. a kind of osmanthus essential oil shampoo according to claim 6, it is characterised in that shown surfactant is 12 Alkyl alcohol ether ammonium sulfate and ammonium lauryl sulfate weight ratio are 1:1 mixture.
- 8. a kind of osmanthus essential oil shampoo according to claim 1, it is characterised in that described polylactic acid molecule amount exists Between 5000-15000.
- A kind of a kind of 9. osmanthus essential oil shampoo according to claim 1, it is characterised in that described osmanthus essential oil hair washing The preparation method of water is as follows：（1）Osmanthus essential oil composition, 70 DEG C of deionized waters are added, stirring is to being completely dissolved（2）Cationic polymer is added, stirring is to being completely dissolved（3）Surfactant, poly- dimethoxy silane and PLA are added, is uniformly mixed, is sheared 5-10 minutes, shearing speed Spend for 10000r/min or more, you can.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109512757A (en) * | 2018-11-22 | 2019-03-26 | 刘真 | A kind of hair soap and preparation method thereof |
| CN114767577A (en) * | 2022-04-02 | 2022-07-22 | 湖北科技学院 | Lasting fragrance type osmanthus essential oil shampoo and preparation method thereof |
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| CN102772326A (en) * | 2012-07-10 | 2012-11-14 | 江苏天辅星光学材料有限公司 | Hair conditioner |
| CN104248556A (en) * | 2013-06-28 | 2014-12-31 | 青岛康泰鑫环保科技有限公司 | Plant hair conditioner |
| CN104398459A (en) * | 2014-11-27 | 2015-03-11 | 青岛市市南区隆德中医药研究所 | Shampoo with flavor of osmanthus |
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| CN102772326A (en) * | 2012-07-10 | 2012-11-14 | 江苏天辅星光学材料有限公司 | Hair conditioner |
| CN104248556A (en) * | 2013-06-28 | 2014-12-31 | 青岛康泰鑫环保科技有限公司 | Plant hair conditioner |
| CN104398459A (en) * | 2014-11-27 | 2015-03-11 | 青岛市市南区隆德中医药研究所 | Shampoo with flavor of osmanthus |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109512757A (en) * | 2018-11-22 | 2019-03-26 | 刘真 | A kind of hair soap and preparation method thereof |
| CN114767577A (en) * | 2022-04-02 | 2022-07-22 | 湖北科技学院 | Lasting fragrance type osmanthus essential oil shampoo and preparation method thereof |
| CN114767577B (en) * | 2022-04-02 | 2023-08-04 | 湖北科技学院 | Lasting fragrance-retaining osmanthus essential oil shampoo and preparation method thereof |
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| CN107375033B (en) | 2020-06-09 |
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