CN107242993B - Spearmint enzyme mouthwash and preparation method thereof - Google Patents
Spearmint enzyme mouthwash and preparation method thereof Download PDFInfo
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- CN107242993B CN107242993B CN201710487173.4A CN201710487173A CN107242993B CN 107242993 B CN107242993 B CN 107242993B CN 201710487173 A CN201710487173 A CN 201710487173A CN 107242993 B CN107242993 B CN 107242993B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses spearmint enzyme mouthwash and a preparation method thereof. The spearmint enzyme mouthwash comprises the following components in parts by weight: 3 parts of spearmint enzyme, 8 parts of tea enzyme, 2 parts of bletilla extract, 0.3 part of thyme extract, 5 parts of liquorice extract, 2 parts of catechin, 0.5 part of pH regulator, 8 parts of cleaning agent, 5 parts of sweetening agent, 0.5 part of flavoring agent, 2 parts of coloring agent, 2 parts of solubilizer and the balance of purified water to 100 parts. According to the spearmint enzyme mouthwash, the mode that the plant enzyme and the natural plant active ingredients are used in a combined mode is adopted, oral gas is improved together, fresh air in the oral cavity is prolonged, the effects of cleaning, diminishing inflammation and preventing allergy are achieved, and the spearmint enzyme mouthwash is natural, free of stimulation and suitable for various people.
Description
Technical Field
The invention relates to the technical field of medicine and health care, and particularly relates to spearmint enzyme mouthwash and a preparation method thereof.
Background
With the development of society, people need to communicate with various languages such as social contact, negotiation, reporting work, entertainment, emotional communication and the like every day, so that the oral hygiene product becomes an indispensable cleaning and health care product in daily life of people, and is mainly used for keeping the oral cavity and teeth clean, promoting breath freshness, nursing gingiva, maintaining good oral environment and the like. The mouth wash, as a common oral cavity cleaning nursing product, gradually becomes a fashionable habit of oral cavity cleaning due to the characteristics of convenient use and strong oral cavity cleaning function.
In recent years, consumers' health care awareness is increasing, and higher requirements are put on mouth washes, which increase some taste perception requirements in addition to tooth cleaning, and also require oral care health care. However, most of the mouth washes mainly contain triclosan or metronidazole, tinidazole, hydrogen peroxide, iodine solution, alcohol and other chemical substances which are irritating or harmful to human bodies in order to achieve the purpose of bacteriostasis and anti-inflammation. For example: chinese patent with publication number CN104644505A, namely a breath freshening mouthwash, which comprises 0.02-0.5% of cortex periplocae extract, 0.5-2% of clove extract, 0.5-2% of sweet wormwood herb extract, 18-21% of sorbitol, 10-12% of edible ethanol, 0.1-0.2% of nipagin mixed ester sodium, 0.7-0.9% of hydrogenated castor oil and the balance of deionized water, wherein in order to achieve a good antibacterial effect, the ethanol content reaches 10-12%, the irritation is strong, and the physiological environment of an oral cavity is influenced after long-term use.
The plant active ingredients have the advantages of pure nature, greenness, safety and the like, and western medicines are incomparable, so the invention provides the spearmint enzyme mouthwash which mainly contains the pure nature plant active ingredients and takes the western medicines as the auxiliary ingredients, does not contain irritant and harmful chemical ingredients, can effectively remove food residues in oral cavity, dental plaque, dental calculus dirt and the like, and can refresh breath for a long time.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides the spearmint enzyme mouthwash which is green, safe and non-irritant and the preparation method thereof, and can effectively remove the peculiar smell in the oral cavity and inhibit the breeding of bacteria.
In order to achieve the purpose, the invention provides a spearmint enzyme mouthwash. Specifically, the spearmint enzyme mouthwash comprises the following components in parts by weight: 3 parts of spearmint enzyme, 8 parts of tea enzyme, 2 parts of bletilla extract, 0.3 part of thyme extract, 5 parts of liquorice extract, 2 parts of catechin, 0.5 part of pH regulator, 8 parts of cleaning agent, 5 parts of sweetening agent, 0.5 part of flavoring agent, 2 parts of coloring agent, 2 parts of solubilizer and the balance of purified water to 100 parts.
Preferably, the tea enzyme is prepared by fermenting Pu' er tea, black tea or green tea.
Preferably, the pH adjusting agent comprises citric acid.
Preferably, the cleaning agent comprises sorbitol.
Preferably, the sweetener comprises xylitol.
Preferably, the flavoring agent comprises natural mint.
Preferably, the colorant comprises Cl 42090.
Preferably, the solubilizing agent comprises a high efficiency solubilizing agent 115C.
The invention provides a preparation method of spearmint enzyme mouthwash. Specifically, the method comprises the following steps:
step one, respectively weighing 3 parts of spearmint enzyme, 8 parts of tea enzyme, 2 parts of bletilla extract, 0.3 part of thyme extract, 5 parts of liquorice extract, 2 parts of catechin, 0.5 part of pH regulator, 8 parts of detergent, 5 parts of sweetener, 0.5 part of flavoring agent, 2 parts of colorant and 2 parts of solubilizer according to the mass parts;
adding a solubilizer into the spearmint enzyme, the tea enzyme, the bletilla extract, the thyme extract, the liquorice extract, the catechin, the pH regulator, the cleaning agent, the sweetener and the colorant, adding purified water at normal temperature, and stirring until the materials are completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass portion reaches 100 parts, uniformly stirring, standing for 4 hours, adding a flavoring agent, and precipitating for 5-9 days to prepare a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing and packaging to obtain the spearmint enzyme mouthwash.
The method of the invention has the following advantages:
1. the spearmint enzyme mouthwash disclosed by the invention is prepared by combining the plant enzymes spearmint enzyme and tea enzyme with natural plant active ingredients bletilla striata extract, thyme extract and liquorice extract, does not contain irritative compounds such as tinidazole, hydrogen peroxide, iodine solution and alcohol, is good in taste and free of irritation, and can effectively remove food residues in oral cavity, dental plaque and dental calculus dirt, prevent dental allergy and refresh breath for a long time.
2. The spearmint enzyme mouthwash disclosed by the invention utilizes reasonable compatibility of various effective components to realize synergistic effect among the components, so that the mouthwash disclosed by the invention is clean and comfortable in taste and stable in property.
Detailed Description
The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
Example 1
The preparation method of the spearmint enzyme mouthwash provided by the embodiment comprises the following steps:
step one, respectively weighing 15g of spearmint enzyme, 40g of Pu' er tea enzyme, 10g of bletilla extract, 1.5g of thyme extract, 25g of liquorice extract, 10g of catechin, 2.5g of citric acid, 40g of sorbitol, 25g of xylitol, 2.5g of natural mint, Cl 4209010 g and 115C 10g of efficient solubilizer according to the mass parts;
step two, adding a high-efficiency solubilizer 115C into spearmint enzyme, tea enzyme, bletilla striata extract, thyme extract, liquorice extract, catechin, citric acid, sorbitol, xylitol and Cl42090, adding purified water at normal temperature, and stirring until the purified water is completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass reaches 500g, uniformly stirring, standing for 4h, adding natural mint, and precipitating for 7 days to obtain a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing, detecting according to QB/T2945-2012 oral cleaning care solution labels, packaging after the oral cleaning care solution is qualified, and pasting labels and anti-counterfeiting codes (production date, batch number, validity period and the like) to obtain the spearmint enzyme mouthwash.
Example 2
The preparation method of the spearmint enzyme mouthwash provided by the embodiment comprises the following steps:
step one, respectively weighing 45g of spearmint enzyme, 120g of black tea enzyme, 30g of bletilla extract, 4.5g of thyme extract, 75g of liquorice extract, 30g of catechin, 7.5g of citric acid, 120g of sorbitol, 75g of xylitol, 7.5g of natural mint, Cl 4209030 g and 115C 30g of efficient solubilizer according to the mass parts;
step two, adding a high-efficiency solubilizer 115C into spearmint enzyme, tea enzyme, bletilla striata extract, thyme extract, liquorice extract, catechin, citric acid, sorbitol, xylitol and Cl42090, adding purified water at normal temperature, and stirring until the purified water is completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass reaches 1500g, uniformly stirring, standing for 4h, adding natural mint, and precipitating for 5 days to obtain a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing, detecting according to QB/T2945-2012 oral cleaning care solution labels, packaging after the oral cleaning care solution is qualified, and pasting labels and anti-counterfeiting codes (production date, batch number, validity period and the like) to obtain the spearmint enzyme mouthwash.
Example 3
The preparation method of the spearmint enzyme mouthwash provided by the embodiment comprises the following steps:
step one, respectively weighing 18g of spearmint enzyme, 48g of green tea enzyme, 12g of bletilla extract, 1.8g of thyme extract, 30g of liquorice extract, 12g of catechin, 3g of citric acid, 48g of sorbitol, 30g of xylitol, 3g of natural mint, Cl 4209012 g and 115C 12g of efficient solubilizer according to the mass parts;
step two, adding a high-efficiency solubilizer 115C into spearmint enzyme, tea enzyme, bletilla striata extract, thyme extract, liquorice extract, catechin, citric acid, sorbitol, xylitol and Cl42090, adding purified water at normal temperature, and stirring until the purified water is completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass reaches 600g, uniformly stirring, standing for 4h, adding natural mint, and precipitating for 8 days to obtain a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing, detecting according to QB/T2945-2012 oral cleaning care solution labels, packaging after the oral cleaning care solution is qualified, and pasting labels and anti-counterfeiting codes (production date, batch number, validity period and the like) to obtain the spearmint enzyme mouthwash.
Example 4
The preparation method of the spearmint enzyme mouthwash provided by the embodiment comprises the following steps:
step one, respectively weighing 30g of spearmint enzyme, 80g of Pu' er tea enzyme, 20g of bletilla extract, 3g of thyme extract, 50g of liquorice extract, 20g of catechin, 5g of citric acid, 80g of sorbitol, 50g of xylitol, 5g of natural mint, Cl 4209020 g and 115C 20g of efficient solubilizer according to the mass parts;
step two, adding a high-efficiency solubilizer 115C into spearmint enzyme, tea enzyme, bletilla striata extract, thyme extract, liquorice extract, catechin, citric acid, sorbitol, xylitol and Cl42090, adding purified water at normal temperature, and stirring until the purified water is completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass reaches 1000g, uniformly stirring, standing for 4h, adding natural mint, and precipitating for 9 days to obtain a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing, detecting according to QB/T2945-2012 oral cleaning care solution labels, packaging after the oral cleaning care solution is qualified, and pasting labels and anti-counterfeiting codes (production date, batch number, validity period and the like) to obtain the spearmint enzyme mouthwash.
Example 5
The preparation method of the spearmint enzyme mouthwash provided by the embodiment comprises the following steps:
step one, respectively weighing 24g of spearmint enzyme, 64g of green tea enzyme, 16g of bletilla extract, 2.4g of thyme extract, 40g of liquorice extract, 16g of catechin, 4g of citric acid, 64g of sorbitol, 40g of xylitol, 4g of natural mint, Cl 4209016 g and 115C 16g of efficient solubilizer according to the mass parts;
step two, adding a high-efficiency solubilizer 115C into spearmint enzyme, tea enzyme, bletilla striata extract, thyme extract, liquorice extract, catechin, citric acid, sorbitol, xylitol and Cl42090, adding purified water at normal temperature, and stirring until the purified water is completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass reaches 800g, uniformly stirring, standing for 4h, adding natural mint, and precipitating for 6 days to obtain a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing, detecting according to QB/T2945-2012 oral cleaning care solution labels, packaging after the oral cleaning care solution is qualified, and pasting labels and anti-counterfeiting codes (production date, batch number, validity period and the like) to obtain the spearmint enzyme mouthwash.
Example 6
The preparation method of the spearmint enzyme mouthwash provided by the embodiment comprises the following steps:
weighing 36g of spearmint enzyme, 96g of Pu' er tea enzyme, 24g of bletilla extract, 3.6g of thyme extract, 60g of liquorice extract, 24g of catechin, 6g of citric acid, 96g of sorbitol, 60g of xylitol, 6g of natural mint, Cl 4209024 g and 115C 24g of efficient solubilizer according to mass parts;
step two, adding a high-efficiency solubilizer 115C into spearmint enzyme, tea enzyme, bletilla striata extract, thyme extract, liquorice extract, catechin, citric acid, sorbitol, xylitol and Cl42090, adding purified water at normal temperature, and stirring until the purified water is completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass reaches 1200g, uniformly stirring, standing for 4h, adding natural mint, and precipitating for 7 days to obtain a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing, detecting according to QB/T2945-2012 oral cleaning care solution labels, packaging after the oral cleaning care solution is qualified, and pasting labels and anti-counterfeiting codes (production date, batch number, validity period and the like) to obtain the spearmint enzyme mouthwash.
Wherein the spearmint enzyme is spearmint enzyme powder produced by Van Wateli Biotech limited; the tea enzyme is produced by Van Watelis Biotech limited; the bletilla striata extract is produced by Nanjing Dow Biotech limited; the thyme extract is produced by Nanjing Dow Biotech limited; the licorice extract is produced by Xian Chang Yue biological technology company Limited; cl42090 is blue 1 lake pigment; the efficient solubilizer 115C is produced by Auphtalein technology Limited of Shenzhen.
The using method comprises the steps of rinsing the mouth, slits between the teeth and the gum with 15-20 m L of spearmint enzyme mouthwash once in the morning and at night each time, then raising the head, rinsing the mouth for thirty seconds, spitting out the mouth, and not swallowing the mouth.
Treatment course, one bottle (500m L) is used for one treatment course, and two to three treatment courses are recommended.
The invention selects five bacteria of porphyromonas gingivalis, prevotella intermedia, actinomyces viscosus, escherichia coli and staphylococcus aureus and refers to GB 15979 appendix C3 of 2002 for antibacterial experiment, wherein the antibacterial rate is (the number of live bacteria in a control group-the number of live bacteria in the experiment group)/the number of live bacteria in the control group.
Table 1 shows the bacteriostatic test results of the spearmint enzyme mouthwash prepared in examples 1-6
It can be seen from table 1 that the spearmint enzyme mouthwash prepared in embodiments 1 to 6 of the present application has a strong inhibition effect on porphyromonas gingivalis, prevotella intermedia, actinomyces viscosus, escherichia coli and staphylococcus aureus, and especially has a strongest inhibition effect on staphylococcus aureus, so that the oral cavity bacteria breeding can be effectively inhibited, and the breath can be refreshed for a long time.
Although the invention has been described in detail above with reference to a general description and specific examples, it will be apparent to one skilled in the art that modifications or improvements may be made thereto based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.
Claims (7)
1. A spearmint enzyme mouthwash is characterized in that: the spearmint enzyme mouthwash comprises the following components in parts by weight: 3 parts of spearmint enzyme, 8 parts of tea enzyme, 2 parts of bletilla extract, 0.3 part of thyme extract, 5 parts of liquorice extract, 2 parts of catechin, 0.5 part of pH regulator, 8 parts of cleaning agent, 5 parts of sweetening agent, 0.5 part of flavoring agent, 2 parts of coloring agent, 2 parts of solubilizer and purified water for supplementing 100 parts; the cleaning agent comprises sorbitol; the solubilizing agent includes a high efficiency solubilizing agent 115C.
2. The spearmint enzyme mouthwash according to claim 1, wherein: the tea enzyme is prepared by fermenting Pu' er tea, black tea or green tea.
3. The spearmint enzyme mouthwash according to claim 1, wherein: the pH regulator comprises citric acid.
4. The spearmint enzyme mouthwash according to claim 1, wherein: the sweetener comprises xylitol.
5. The spearmint enzyme mouthwash according to claim 1, wherein: the flavoring agent comprises natural mint.
6. The spearmint enzyme mouthwash according to claim 1, wherein: the colorant comprises Cl 42090.
7. A method for preparing the spearmint enzyme mouthwash of claim 1, wherein the method comprises the following steps: the preparation method comprises the following steps:
step one, respectively weighing 3 parts of spearmint enzyme, 8 parts of tea enzyme, 2 parts of bletilla extract, 0.3 part of thyme extract, 5 parts of liquorice extract, 2 parts of catechin, 0.5 part of pH regulator, 8 parts of detergent, 5 parts of sweetener, 0.5 part of flavoring agent, 2 parts of colorant and 2 parts of solubilizer according to the mass parts;
adding a solubilizer into the spearmint enzyme, the tea enzyme, the bletilla extract, the thyme extract, the liquorice extract, the catechin, the pH regulator, the cleaning agent, the sweetener and the colorant, adding purified water at normal temperature, and stirring until the materials are completely dissolved to prepare a prepared solution;
adding purified water into the prepared solution until the total mass portion reaches 100 parts, uniformly stirring, standing for 4 hours, adding a flavoring agent, and precipitating for 5-9 days to prepare a precipitation solution;
and step four, sieving the precipitated solution with a 800-mesh sieve, sterilizing and packaging to obtain the spearmint enzyme mouthwash.
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107714569A (en) * | 2017-12-07 | 2018-02-23 | 威海职业学院 | A kind of preparation method of fragrant plant mouthwash |
| CN108852961A (en) * | 2018-07-04 | 2018-11-23 | 山东博华高效生态农业科技有限公司 | A kind of ferment product with oral cleaning |
| CN115590900B (en) * | 2022-10-10 | 2023-12-08 | 湖南循力源口腔疾病研究院有限公司 | Application of traditional Chinese medicine volatile oil in preparation of halitosis preventing and treating substances |
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